#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/14/2231487.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231487_Fobs loop_ _publ_author_name 'Khan, Muneeb Hayat' 'Khan, Islam Ullah' 'Akkurt, Mehmet' _publ_section_title ; 4-Amino-2-chlorobenzoic acid ; _journal_coeditor_code HB6334 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2247 _journal_volume 67 _journal_year 2011 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.257 _cell_angle_gamma 90.000 _cell_length_a 3.9595 _cell_length_b 22.6656 _cell_length_c 8.0285 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.7486 _[local]_cod_data_source_file hb6334Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NEW in P 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 109.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -14 0 64.95 62.60 1.73 o 1 -13 0 183.49 170.27 3.84 o 1 -12 0 710.08 718.35 14.64 o 1 -11 0 769.03 822.13 16.53 o 3 -11 0 17.46 15.13 1.09 o 4 -11 0 4.70 5.15 0.79 o 1 -10 0 5.56 5.57 0.44 o 3 -10 0 42.52 39.81 1.59 o 4 -10 0 2.50 2.42 0.79 o 1 -9 0 1132.04 1137.19 22.44 o 2 -9 0 65.40 69.30 1.61 o 3 -9 0 77.72 79.36 1.99 o 4 -9 0 15.54 14.50 1.25 o 0 -8 0 7678.89 7289.73 220.95 o 1 -8 0 702.91 804.01 39.18 o 2 -8 0 344.46 375.41 7.69 o 3 -8 0 118.18 115.23 2.72 o 4 -8 0 17.06 16.49 1.26 o 1 -7 0 61.09 64.86 1.63 o 2 -7 0 709.62 768.14 14.72 o 3 -7 0 55.96 53.73 1.50 o 4 -7 0 20.73 21.43 1.38 o 0 -6 0 3227.58 3113.32 74.47 o 1 -6 0 18.96 19.65 0.51 o 2 -6 0 1270.22 1284.02 25.23 o 3 -6 0 30.60 30.88 1.02 o 4 -6 0 24.96 24.37 1.39 o 5 -6 0 11.22 9.03 1.05 o 1 -5 0 437.57 489.07 7.14 o 2 -5 0 200.29 206.76 4.68 o 3 -5 0 33.04 31.14 1.04 o 4 -5 0 18.99 19.17 1.73 o 5 -5 0 6.78 5.67 0.95 o 0 -4 0 2440.29 1895.20 56.79 o 1 -4 0 11935.23 10383.82 246.40 o 2 -4 0 45.12 48.98 2.02 o 3 -4 0 26.64 25.68 0.92 o 4 -4 0 5.44 5.51 0.59 o 5 -4 0 32.99 31.20 1.61 o 1 -3 0 11416.87 9762.49 233.62 o 2 -3 0 84.46 85.69 1.47 o 3 -3 0 182.33 181.18 2.94 o 4 -3 0 17.02 15.70 1.14 o 5 -3 0 25.99 25.00 1.49 o 1 -2 0 234.52 257.64 4.06 o 2 -2 0 136.33 134.00 2.16 o 3 -2 0 92.15 88.97 1.79 o 4 -2 0 6.47 6.25 1.12 o 5 -2 0 12.85 14.71 1.27 o 1 -1 0 683.45 756.12 11.29 o 2 -1 0 106.32 104.52 1.78 o 3 -1 0 37.17 33.75 0.84 o 4 -1 0 12.83 13.02 0.91 o 5 -1 0 3.51 4.41 0.84 o 1 0 0 218.31 225.71 3.36 o 2 0 0 429.82 384.38 5.97 o 3 0 0 76.00 70.88 1.65 o 4 0 0 20.19 21.59 0.98 o 5 0 0 39.17 41.81 1.83 o 1 1 0 683.43 751.75 11.19 o 2 1 0 106.33 104.55 1.88 o 3 1 0 37.17 34.19 1.08 o 4 1 0 12.83 13.29 0.82 o 5 1 0 3.51 4.94 0.84 o 1 2 0 234.57 257.34 4.19 o 2 2 0 136.35 132.23 2.23 o 3 2 0 92.15 89.19 1.72 o 4 2 0 6.47 6.20 0.75 o 5 2 0 12.85 14.60 1.27 o 1 3 0 11416.58 9755.80 273.22 o 2 3 0 84.46 87.01 1.65 o 3 3 0 182.34 180.05 3.04 o 4 3 0 17.02 15.60 0.90 o 5 3 0 25.99 26.73 1.33 o 0 4 0 2440.29 2356.47 64.27 o 1 4 0 11935.26 10133.63 316.02 o 2 4 0 45.12 46.39 1.00 o 3 4 0 26.63 23.85 0.77 o 4 4 0 5.45 5.72 0.67 o 5 4 0 32.98 30.15 1.85 o 1 5 0 437.80 484.02 7.91 o 2 5 0 200.28 204.30 3.76 o 3 5 0 33.04 31.07 0.96 o 4 5 0 19.00 17.07 0.98 o 5 5 0 6.78 5.99 0.67 o 0 6 0 3227.59 3021.83 72.69 o 1 6 0 18.96 18.81 1.00 o 2 6 0 1270.20 1269.66 20.48 o 3 6 0 30.62 30.95 0.90 o 4 6 0 24.97 25.63 1.18 o 5 6 0 11.22 9.61 0.77 o 1 7 0 61.10 63.07 1.19 o 2 7 0 709.57 756.00 12.14 o 3 7 0 55.96 53.16 1.18 o 4 7 0 20.72 20.53 1.03 o 0 8 0 7678.88 7045.36 206.82 o 1 8 0 702.83 766.94 13.32 o 2 8 0 344.59 375.52 7.07 o 3 8 0 118.17 112.58 2.72 o 4 8 0 17.05 15.07 0.96 o 1 9 0 1132.07 1129.00 15.94 o 2 9 0 65.38 69.93 1.61 o 3 9 0 77.72 76.25 1.97 o 4 9 0 15.55 14.65 0.92 o 0 10 0 605.84 611.21 12.83 o 1 10 0 5.57 7.83 1.42 o 2 10 0 194.01 185.22 3.43 o 3 10 0 42.51 40.71 1.24 o 4 10 0 2.50 2.42 0.57 o 1 11 0 768.97 815.34 14.73 o 2 11 0 325.94 328.96 5.63 o 3 11 0 17.48 14.74 1.29 o 4 11 0 4.70 5.36 0.90 o 0 12 0 2463.80 2591.60 43.35 o 1 12 0 710.11 714.20 10.39 o 2 12 0 126.85 124.63 2.55 o 3 12 0 30.76 27.25 1.78 o 4 12 0 24.64 22.01 1.07 o 1 13 0 183.51 169.40 3.21 o 2 13 0 9.52 11.11 1.73 o 3 13 0 103.82 97.30 3.31 o 4 13 0 14.72 13.34 1.35 o 0 14 0 237.88 236.49 5.51 o 1 14 0 64.94 64.44 1.63 o 2 14 0 187.01 173.21 3.51 o 3 14 0 20.55 19.02 0.82 o 4 14 0 8.88 9.24 0.78 o 1 15 0 697.20 739.66 12.08 o 2 15 0 95.10 89.24 2.28 o 3 15 0 29.29 25.43 0.92 o 4 15 0 1.46 1.21 0.53 o 0 16 0 596.64 562.58 11.82 o 1 16 0 64.13 79.15 2.68 o 2 16 0 36.27 35.48 1.39 o 3 16 0 77.35 72.32 2.20 o 4 16 0 4.70 2.94 0.60 o 1 17 0 62.70 54.63 1.60 o 2 17 0 19.67 19.12 1.45 o 3 17 0 48.95 46.83 1.39 o 4 17 0 7.04 5.93 0.66 o 0 18 0 97.94 101.47 2.93 o 1 18 0 0.47 0.63 0.43 o 2 18 0 17.17 18.91 1.44 o 3 18 0 10.77 10.26 0.65 o 4 18 0 0.84 1.31 0.67 o 1 19 0 88.15 94.74 3.01 o 2 19 0 144.32 140.44 3.95 o 3 19 0 7.35 5.72 0.97 o 0 20 0 28.94 27.52 1.35 o 1 20 0 25.75 23.84 1.57 o 2 20 0 31.75 34.56 1.88 o 3 20 0 1.21 0.21 0.48 o 1 21 0 11.37 8.93 1.08 o 2 21 0 4.35 4.83 1.05 o 3 21 0 10.69 10.08 1.64 o 0 22 0 80.94 79.09 2.51 o 1 22 0 22.05 18.17 1.31 o 2 22 0 38.98 37.29 1.93 o 3 22 0 2.24 2.31 0.53 o 1 23 0 24.87 25.10 1.52 o 2 23 0 2.58 2.63 0.90 o 3 23 0 11.45 12.92 0.86 o 0 24 0 175.74 163.96 4.22 o 1 24 0 4.33 5.04 0.92 o 2 24 0 22.84 22.79 1.53 o 3 24 0 29.66 31.83 1.81 o 1 25 0 73.91 71.64 2.52 o 2 25 0 10.55 10.71 1.28 o 0 26 0 17.58 12.92 1.12 o 1 26 0 0.25 1.58 0.78 o 2 26 0 0.64 0.53 0.74 o 1 27 0 74.90 74.68 2.63 o 2 27 0 16.17 19.54 1.59 o 0 28 0 53.52 57.25 2.08 o 1 28 0 14.73 17.44 1.38 o 1 29 0 10.06 9.66 1.16 o 0 30 0 34.65 35.50 1.62 o 0 -17 1 140.62 144.43 4.56 o 0 -16 1 585.52 613.74 15.64 o 0 -15 1 19.16 22.58 1.30 o -1 -14 1 213.94 211.55 4.54 o 0 -14 1 40.53 39.60 1.76 o 2 -14 1 110.50 105.88 2.63 o -1 -13 1 278.79 293.90 6.11 o 0 -13 1 235.12 242.22 6.56 o 2 -13 1 43.36 44.85 1.39 o 3 -13 1 16.56 13.86 0.96 o 4 -13 1 26.54 29.41 1.40 o -1 -12 1 36.03 48.74 1.33 o 0 -12 1 1.28 1.79 0.44 o 1 -12 1 198.58 207.76 5.94 o 2 -12 1 177.72 177.83 3.91 o 3 -12 1 140.56 140.54 3.29 o 4 -12 1 17.74 19.64 1.19 o -1 -11 1 36.33 26.33 0.61 o 0 -11 1 252.98 275.41 7.26 o 1 -11 1 137.91 140.17 3.48 o 2 -11 1 206.69 199.89 4.36 o 3 -11 1 325.23 320.10 6.44 o 4 -11 1 3.30 4.20 0.77 o -1 -10 1 1666.60 1804.10 28.19 o 0 -10 1 96.48 119.22 3.37 o 1 -10 1 389.92 406.08 8.93 o 2 -10 1 171.67 166.17 3.59 o 3 -10 1 75.07 75.00 3.34 o 4 -10 1 27.27 31.72 1.43 o -1 -9 1 41.78 34.89 0.68 o 0 -9 1 88.97 95.45 1.73 o 1 -9 1 461.41 439.13 9.46 o 2 -9 1 42.94 44.01 1.36 o 3 -9 1 50.78 48.37 2.15 o 4 -9 1 34.08 34.14 1.56 o -4 -8 1 27.69 28.89 1.50 o -3 -8 1 318.98 310.49 6.28 o 0 -8 1 1170.44 1224.49 20.26 o 1 -8 1 308.76 310.28 6.81 o 2 -8 1 68.89 63.97 1.74 o 3 -8 1 303.51 298.73 6.20 o 4 -8 1 202.21 202.09 4.66 o -5 -7 1 6.86 6.09 0.84 o -4 -7 1 5.01 3.57 0.70 o -3 -7 1 178.41 178.14 3.94 o -2 -7 1 1894.87 2029.01 50.19 o 0 -7 1 1289.76 1323.49 26.10 o 1 -7 1 134.87 133.19 3.07 o 2 -7 1 324.28 322.47 6.72 o 3 -7 1 292.75 278.93 5.87 o 4 -7 1 75.99 82.24 2.45 o -5 -6 1 3.63 5.25 0.84 o -4 -6 1 59.99 60.40 2.09 o -3 -6 1 7.06 7.09 1.12 o -2 -6 1 1526.91 1542.12 23.17 o 0 -6 1 386.89 368.32 5.36 o 1 -6 1 139.08 142.01 3.24 o 2 -6 1 205.35 201.46 6.10 o 3 -6 1 17.29 16.70 1.07 o 4 -6 1 10.27 12.29 1.14 o -5 -5 1 4.06 3.57 0.84 o -4 -5 1 15.87 16.39 1.18 o -3 -5 1 122.91 123.26 2.90 o -2 -5 1 2042.48 2148.12 34.30 o -1 -5 1 1449.25 1502.57 30.16 o 0 -5 1 239.64 247.06 3.83 o 1 -5 1 1202.93 1272.74 25.42 o 2 -5 1 46.46 41.17 1.10 o 3 -5 1 67.24 66.96 1.80 o 4 -5 1 66.89 73.47 3.68 o -5 -4 1 1.05 -0.11 0.74 o -4 -4 1 17.84 19.38 0.89 o -3 -4 1 73.77 83.92 1.99 o -2 -4 1 193.16 199.60 3.15 o -1 -4 1 5184.35 4943.55 117.27 o 0 -4 1 1112.00 1114.89 16.36 o 1 -4 1 1988.01 1961.79 43.36 o 2 -4 1 99.99 100.86 2.57 o 3 -4 1 53.95 53.83 1.53 o 4 -4 1 394.58 390.95 9.44 o -5 -3 1 6.83 6.20 0.95 o -4 -3 1 34.72 36.19 1.23 o -3 -3 1 469.63 473.22 6.85 o -2 -3 1 1608.76 1702.04 23.26 o -1 -3 1 78.43 71.33 1.54 o 1 -3 1 667.61 652.09 13.84 o 2 -3 1 141.57 146.31 3.42 o 3 -3 1 27.79 26.78 0.97 o 4 -3 1 12.50 15.07 0.89 o -5 -2 1 4.54 4.20 0.84 o -4 -2 1 20.14 22.32 0.95 o -3 -2 1 10.06 10.87 0.58 o -2 -2 1 687.60 686.25 9.81 o -1 -2 1 2205.38 2202.31 38.44 o 1 -2 1 324.14 307.60 4.55 o 2 -2 1 342.03 351.09 5.35 o 3 -2 1 46.42 46.74 1.01 o 4 -2 1 34.58 36.55 1.31 o -5 -1 1 0.89 1.16 0.74 o -4 -1 1 12.34 11.40 1.72 o -3 -1 1 341.24 359.51 5.94 o -2 -1 1 412.60 419.57 6.74 o -1 -1 1 4875.68 4627.86 107.01 o 2 -1 1 289.52 291.67 4.50 o 3 -1 1 154.98 152.73 2.56 o 4 -1 1 17.50 19.59 0.95 o -5 0 1 5.75 5.99 0.84 o -4 0 1 94.71 97.42 2.50 o -3 0 1 135.15 138.92 2.79 o -2 0 1 1383.28 1278.17 19.09 o -1 0 1 57.82 60.02 0.96 o 1 0 1 167.57 172.79 3.69 o 2 0 1 8.28 7.08 0.40 o 3 0 1 273.47 275.11 5.39 o 4 0 1 2.82 3.15 0.54 o -5 1 1 0.89 0.84 0.63 o -4 1 1 12.34 11.24 0.77 o -3 1 1 341.23 358.77 6.19 o -2 1 1 412.60 420.94 6.47 o -1 1 1 4875.57 4621.55 81.23 o 0 1 1 748.21 720.45 15.63 o 1 1 1 214.10 216.17 4.63 o 2 1 1 289.57 291.10 4.52 o 3 1 1 155.02 152.80 2.75 o 4 1 1 17.50 19.75 0.95 o -5 2 1 4.54 2.94 0.74 o -4 2 1 20.14 20.17 2.40 o -3 2 1 10.05 10.81 0.83 o -2 2 1 687.61 692.18 10.30 o -1 2 1 2205.37 2197.94 37.08 o 1 2 1 324.21 306.19 6.45 o 2 2 1 342.02 349.33 7.67 o 3 2 1 46.41 45.98 1.08 o 4 2 1 34.57 35.56 1.31 o -5 3 1 6.83 7.62 0.69 o -4 3 1 34.73 35.98 1.30 o -3 3 1 469.64 465.42 6.83 o -2 3 1 1608.70 1714.09 26.47 o -1 3 1 78.38 71.62 1.18 o 0 3 1 1153.53 1219.49 25.20 o 1 3 1 667.52 639.15 13.30 o 2 3 1 141.54 143.67 3.34 o 3 3 1 27.79 27.16 0.77 o 4 3 1 12.51 17.44 1.01 o -5 4 1 1.05 0.63 0.59 o -4 4 1 17.84 19.06 0.96 o -3 4 1 73.77 82.75 1.93 o -2 4 1 193.20 204.39 3.67 o -1 4 1 5184.39 4833.13 79.71 o 0 4 1 1111.88 1179.05 23.45 o 1 4 1 1988.10 1943.62 39.92 o 2 4 1 100.02 98.32 2.53 o 3 4 1 53.94 55.40 1.20 o 4 4 1 394.57 388.69 7.82 o -5 5 1 4.06 5.15 0.61 o -4 5 1 15.87 15.97 0.91 o -3 5 1 122.90 119.01 2.24 o -2 5 1 2042.52 2133.79 28.72 o -1 5 1 1449.27 1490.66 21.68 o 0 5 1 239.76 247.68 5.15 o 1 5 1 1202.95 1249.11 25.35 o 2 5 1 46.47 40.49 1.25 o 3 5 1 67.24 68.40 1.42 o 4 5 1 66.89 72.00 2.31 o -5 6 1 3.63 4.88 0.82 o -4 6 1 60.00 57.35 1.77 o -3 6 1 7.07 6.84 2.39 o -2 6 1 1526.90 1573.37 23.91 o -1 6 1 693.74 710.02 10.93 o 0 6 1 386.84 367.29 5.35 o 1 6 1 139.00 140.34 2.12 o 2 6 1 205.35 196.32 4.50 o 3 6 1 17.29 17.24 0.77 o 4 6 1 10.27 14.92 0.96 o -5 7 1 6.86 6.88 1.42 o -4 7 1 5.01 4.46 0.62 o -3 7 1 178.42 172.68 3.23 o -2 7 1 1894.86 1973.76 32.92 o -1 7 1 473.09 531.72 7.69 o 0 7 1 1289.79 1296.02 22.29 o 1 7 1 134.80 132.20 2.03 o 2 7 1 324.22 320.45 7.12 o 3 7 1 292.72 284.28 7.56 o 4 7 1 76.00 77.47 2.17 o -5 8 1 13.84 14.23 0.82 o -4 8 1 27.68 27.99 1.15 o -3 8 1 319.02 309.43 5.63 o -2 8 1 1149.29 1108.80 17.25 o -1 8 1 516.76 616.43 8.87 o 0 8 1 1170.50 1203.31 17.28 o 1 8 1 308.86 306.20 7.93 o 2 8 1 68.92 64.11 1.75 o 3 8 1 303.51 289.64 6.18 o 4 8 1 202.21 199.20 4.49 o -4 9 1 10.40 10.19 1.05 o -3 9 1 648.38 652.78 11.08 o -2 9 1 204.83 237.27 4.17 o -1 9 1 41.76 39.53 1.39 o 0 9 1 88.89 93.85 1.56 o 1 9 1 461.39 436.57 6.12 o 2 9 1 42.96 43.69 1.18 o 3 9 1 50.81 52.36 1.72 o 4 9 1 34.07 33.61 1.33 o -4 10 1 8.90 8.25 1.71 o -3 10 1 22.99 31.47 1.77 o -2 10 1 150.57 137.83 2.63 o -1 10 1 1666.58 1780.70 24.74 o 0 10 1 96.52 117.55 1.93 o 1 10 1 389.91 405.21 5.75 o 2 10 1 171.65 159.76 3.76 o 3 10 1 75.06 74.40 1.93 o 4 10 1 27.27 27.31 2.42 o -4 11 1 62.55 58.45 1.79 o -3 11 1 327.11 330.83 5.74 o -2 11 1 38.13 38.97 5.86 o -1 11 1 36.36 28.36 1.46 o 0 11 1 252.92 269.54 4.43 o 1 11 1 137.90 138.40 2.18 o 2 11 1 206.69 198.26 4.61 o 3 11 1 325.24 320.61 6.81 o 4 11 1 3.30 5.57 1.49 o -4 12 1 125.28 114.65 2.85 o -3 12 1 230.76 225.92 5.33 o -2 12 1 183.99 199.10 3.81 o -1 12 1 36.03 48.30 1.09 o 0 12 1 1.27 1.77 0.31 o 1 12 1 198.62 203.14 3.08 o 2 12 1 177.79 171.74 4.48 o 3 12 1 140.52 137.56 3.23 o 4 12 1 17.74 18.70 1.00 o -4 13 1 20.71 19.80 1.03 o -3 13 1 13.51 14.33 1.17 o -2 13 1 246.74 264.92 4.65 o -1 13 1 278.78 292.15 4.65 o 0 13 1 235.12 241.57 3.86 o 1 13 1 229.67 218.19 3.28 o 2 13 1 43.33 42.02 1.94 o 3 13 1 16.57 15.91 0.96 o 4 13 1 26.55 26.57 1.16 o -4 14 1 29.22 32.67 1.29 o -3 14 1 13.08 12.18 0.64 o -2 14 1 263.34 268.85 15.07 o -1 14 1 213.95 210.16 3.52 o 0 14 1 40.56 39.28 1.23 o 1 14 1 58.05 53.99 1.42 o 2 14 1 110.52 98.84 3.14 o 3 14 1 2.26 2.15 0.82 o 4 14 1 5.16 4.52 0.89 o -4 15 1 38.15 35.82 1.30 o -3 15 1 10.64 11.95 0.63 o -2 15 1 3.40 8.79 0.79 o -1 15 1 132.46 136.42 2.99 o 0 15 1 19.19 22.76 1.68 o 1 15 1 9.78 7.05 0.41 o 2 15 1 140.29 131.19 3.79 o 3 15 1 35.09 34.87 2.01 o 4 15 1 22.26 22.43 2.92 o -4 16 1 22.61 23.42 1.10 o -3 16 1 7.80 9.24 0.56 o -2 16 1 356.57 338.32 5.67 o -1 16 1 153.15 176.12 3.41 o 0 16 1 585.47 596.09 8.77 o 1 16 1 29.56 31.23 1.47 o 2 16 1 111.03 107.45 3.43 o 3 16 1 58.15 60.03 1.84 o 4 16 1 12.21 15.60 2.17 o -4 17 1 25.34 26.57 1.40 o -3 17 1 103.62 104.36 2.57 o -2 17 1 47.06 45.48 1.26 o -1 17 1 146.43 138.45 2.60 o 0 17 1 140.62 146.98 6.22 o 1 17 1 75.29 71.58 1.76 o 2 17 1 137.22 134.45 3.92 o 3 17 1 16.71 16.96 1.58 o 4 17 1 13.96 12.13 0.86 o -4 18 1 2.60 3.83 0.58 o -3 18 1 1.24 1.57 0.41 o -2 18 1 0.73 0.58 0.66 o -1 18 1 46.01 51.02 1.29 o 0 18 1 70.90 71.33 1.68 o 1 18 1 2.49 1.58 0.73 o 2 18 1 97.60 101.26 3.36 o 3 18 1 7.38 7.46 1.64 o -4 19 1 5.67 6.62 0.68 o -3 19 1 101.44 95.60 2.31 o -2 19 1 3.50 6.83 1.94 o -1 19 1 307.39 287.74 5.43 o 0 19 1 79.73 79.38 2.02 o 1 19 1 56.73 56.09 2.18 o 2 19 1 55.97 57.46 2.45 o 3 19 1 37.27 36.50 3.39 o -3 20 1 17.88 18.41 0.77 o -2 20 1 180.16 171.78 3.22 o -1 20 1 117.53 118.08 4.52 o 0 20 1 69.67 62.28 1.45 o 1 20 1 447.32 427.19 9.52 o 2 20 1 54.72 53.25 2.31 o 3 20 1 24.33 23.74 1.09 o -3 21 1 10.13 8.79 0.63 o -2 21 1 4.81 6.92 0.78 o -1 21 1 19.78 19.10 1.21 o 0 21 1 20.85 22.32 2.28 o 1 21 1 168.75 165.22 4.32 o 2 21 1 11.40 9.77 1.27 o 3 21 1 5.54 7.09 1.42 o -3 22 1 3.34 4.15 0.58 o -2 22 1 140.14 128.00 3.26 o -1 22 1 1.20 1.22 0.42 o 0 22 1 31.28 32.14 0.99 o 1 22 1 74.00 68.69 2.56 o 2 22 1 21.32 19.75 1.58 o 3 22 1 14.50 14.97 1.14 o -3 23 1 18.15 15.13 1.37 o -2 23 1 31.95 33.67 1.68 o -1 23 1 158.10 146.67 2.69 o 0 23 1 308.07 300.81 4.84 o 1 23 1 26.36 26.15 1.62 o 2 23 1 34.82 31.09 1.86 o 3 23 1 5.05 6.99 2.16 o -3 24 1 5.36 4.73 1.05 o -2 24 1 1.83 0.95 0.78 o -1 24 1 23.47 24.16 0.89 o 0 24 1 54.40 61.94 1.58 o 1 24 1 7.31 5.67 1.03 o 2 24 1 14.02 14.71 1.40 o -2 25 1 0.69 2.21 0.86 o -1 25 1 31.60 34.14 1.79 o 0 25 1 51.88 50.44 1.39 o 1 25 1 15.61 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1887.63 35.21 o 2 -5 2 85.78 87.55 2.13 o 3 -5 2 13.42 12.97 0.72 o 4 -5 2 39.06 38.60 1.29 o -5 -4 2 20.01 19.54 1.28 o -4 -4 2 13.90 12.54 0.62 o -3 -4 2 1.95 0.80 0.28 o -2 -4 2 216.99 214.49 4.91 o -1 -4 2 1077.89 1013.40 18.73 o 2 -4 2 887.89 873.07 16.08 o 3 -4 2 44.41 46.43 1.42 o 4 -4 2 5.58 5.78 0.60 o -5 -3 2 0.86 1.79 0.74 o -4 -3 2 6.04 6.23 0.58 o -3 -3 2 71.61 77.05 1.48 o -2 -3 2 18.57 18.49 0.90 o -1 -3 2 13.92 16.28 0.93 o 2 -3 2 31.39 32.46 1.03 o 3 -3 2 62.38 61.24 1.76 o 4 -3 2 15.72 15.39 0.83 o -5 -2 2 5.33 3.68 0.84 o -4 -2 2 45.05 49.62 1.26 o -3 -2 2 251.23 257.26 4.10 o -2 -2 2 275.49 274.73 4.81 o -1 -2 2 1941.04 1907.17 39.49 o 0 -2 2 984.17 994.71 21.64 o 2 -2 2 640.61 631.45 14.38 o 3 -2 2 112.54 106.46 2.69 o 4 -2 2 11.85 13.13 0.82 o -5 -1 2 2.55 2.00 0.74 o -4 -1 2 126.52 126.77 2.62 o -3 -1 2 2.90 2.91 0.35 o -2 -1 2 93.67 88.26 1.69 o -1 -1 2 721.84 721.96 10.82 o 0 -1 2 1694.88 1653.61 25.49 o 1 -1 2 600.18 597.88 12.82 o 2 -1 2 1198.22 1254.51 29.12 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