#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/16/2231619.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231619_Fobs loop_ _publ_author_name 'A. Alhadi, Abeer' 'Khaledi, Hamid' 'Mohd Ali, Hapipah' _publ_section_title ; 3,4,5-Trihydroxybenzohydrazidium perchlorate--3,4,5-trihydroxybenzohydrazide--water (1/1/1) ; _journal_coeditor_code LX2194 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2229 _journal_page_last o2230 _journal_volume 67 _journal_year 2011 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 20.1213 _cell_length_b 12.9178 _cell_length_c 7.0122 _exptl_crystal_F_000 1008.00 _reflns_d_resolution_high 0.8256 _[local]_cod_data_source_file lx2194Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 369.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -8 1652.85 1510.62 131.43 o 2 0 -8 329.49 349.48 61.57 o 4 0 -8 546.30 545.52 82.24 o 6 0 -8 488.76 501.47 105.30 o 8 0 -8 203.12 224.30 217.70 o 1 1 -8 277.52 353.08 40.21 o 2 1 -8 300.67 431.55 54.13 o 3 1 -8 181.65 195.70 48.54 o 4 1 -8 735.62 693.41 60.55 o 5 1 -8 131.46 181.95 55.45 o 6 1 -8 510.77 591.58 74.11 o 7 1 -8 255.68 270.31 69.11 o 8 1 -8 343.25 359.57 74.98 o 0 2 -8 585.33 564.66 67.52 o 1 2 -8 28.40 70.97 36.52 o 2 2 -8 194.39 128.06 49.36 o 3 2 -8 89.55 64.58 44.17 o 4 2 -8 25.61 8.85 44.03 o 5 2 -8 280.81 398.79 61.24 o 6 2 -8 115.24 63.15 52.19 o 7 2 -8 175.60 135.79 58.96 o 1 3 -8 435.03 348.42 43.82 o 2 3 -8 508.37 525.54 69.08 o 3 3 -8 741.61 684.29 66.68 o 4 3 -8 810.13 682.49 76.93 o 5 3 -8 385.67 386.41 59.78 o 6 3 -8 496.35 536.52 60.04 o 0 4 -8 1225.82 1201.53 85.47 o 1 4 -8 190.57 204.70 47.32 o 2 4 -8 84.47 73.34 77.61 o 3 4 -8 737.57 626.64 86.91 o 4 4 -8 417.38 368.91 68.87 o 5 4 -8 444.03 532.27 83.34 o 1 5 -8 79.52 133.24 52.03 o 2 5 -8 874.22 906.82 83.16 o 2 0 -7 1120.07 1124.66 60.80 o 4 0 -7 330.62 332.52 90.12 o 6 0 -7 1013.97 929.46 162.62 o 8 0 -7 83.25 14.32 81.04 o 10 0 -7 617.58 696.72 117.50 o 12 0 -7 952.29 912.39 130.71 o 0 1 -7 1400.31 1266.12 63.08 o 1 1 -7 222.49 261.55 33.02 o 2 1 -7 288.84 344.99 34.63 o 3 1 -7 229.63 240.95 36.87 o 4 1 -7 2121.60 2081.50 77.23 o 5 1 -7 122.04 90.99 48.59 o 6 1 -7 194.18 260.25 53.88 o 7 1 -7 698.09 582.48 78.37 o 8 1 -7 456.00 616.44 76.36 o 9 1 -7 228.38 207.68 65.27 o 10 1 -7 81.79 28.07 64.32 o 11 1 -7 327.83 425.18 75.93 o 12 1 -7 118.37 251.14 69.92 o 13 1 -7 169.83 56.25 68.12 o 1 2 -7 204.92 166.01 32.26 o 2 2 -7 228.63 220.15 32.46 o 3 2 -7 169.47 209.70 36.77 o 4 2 -7 452.80 449.02 50.85 o 5 2 -7 403.22 304.30 48.28 o 6 2 -7 117.64 107.97 49.59 o 7 2 -7 507.54 531.88 62.84 o 8 2 -7 49.70 91.84 50.91 o 9 2 -7 274.35 334.95 59.88 o 10 2 -7 384.73 395.43 75.28 o 11 2 -7 79.39 176.56 70.07 o 12 2 -7 114.11 85.71 64.41 o 13 2 -7 171.94 306.99 76.52 o 0 3 -7 333.58 294.48 92.46 o 1 3 -7 549.22 542.02 64.75 o 2 3 -7 122.37 183.52 42.23 o 3 3 -7 107.11 85.49 37.00 o 4 3 -7 646.32 743.93 82.73 o 5 3 -7 76.39 78.41 64.16 o 6 3 -7 50.33 35.91 47.25 o 7 3 -7 245.35 321.57 65.48 o 8 3 -7 641.02 755.68 104.87 o 9 3 -7 711.24 705.62 80.23 o 10 3 -7 993.22 1074.54 80.67 o 11 3 -7 211.74 201.86 60.12 o 12 3 -7 197.63 211.66 70.58 o 1 4 -7 387.12 400.60 57.56 o 2 4 -7 885.70 892.37 67.09 o 3 4 -7 34.78 84.44 43.48 o 4 4 -7 351.22 365.58 56.13 o 5 4 -7 407.90 420.47 59.53 o 6 4 -7 352.63 352.47 59.52 o 7 4 -7 221.84 199.25 54.84 o 8 4 -7 356.72 424.40 71.84 o 9 4 -7 380.84 372.00 72.50 o 10 4 -7 914.48 841.84 97.29 o 11 4 -7 127.31 -31.91 61.01 o 12 4 -7 18.20 67.58 65.22 o 0 5 -7 1112.71 1073.29 167.21 o 1 5 -7 5.57 37.65 46.71 o 2 5 -7 25.43 141.35 46.63 o 3 5 -7 7.73 -46.69 46.69 o 4 5 -7 521.64 658.54 71.60 o 5 5 -7 24.89 -3.77 78.74 o 6 5 -7 53.57 94.84 57.03 o 7 5 -7 170.46 260.03 63.62 o 8 5 -7 49.29 119.27 59.01 o 9 5 -7 138.83 218.41 69.44 o 10 5 -7 232.29 154.41 99.00 o 11 5 -7 118.52 234.70 75.14 o 1 6 -7 736.03 730.94 69.52 o 2 6 -7 38.52 40.45 49.99 o 3 6 -7 885.14 1010.78 72.38 o 4 6 -7 113.10 112.22 59.43 o 5 6 -7 172.51 192.33 62.63 o 6 6 -7 59.27 124.59 60.86 o 7 6 -7 268.60 192.20 62.46 o 8 6 -7 243.44 283.70 67.27 o 9 6 -7 331.21 382.28 71.40 o 10 6 -7 143.80 95.20 68.90 o 0 7 -7 878.06 952.13 215.73 o 1 7 -7 42.30 41.16 50.19 o 2 7 -7 262.54 244.43 59.26 o 3 7 -7 12.59 58.34 52.00 o 4 7 -7 155.86 227.84 63.90 o 5 7 -7 53.90 118.89 61.57 o 6 7 -7 49.78 -39.44 54.74 o 7 7 -7 278.02 319.25 117.93 o 8 7 -7 334.78 324.02 70.96 o 1 8 -7 163.87 146.97 57.20 o 2 8 -7 699.28 645.06 72.88 o 3 8 -7 78.91 44.40 53.30 o 4 8 -7 460.17 691.46 80.84 o 5 8 -7 516.67 551.18 77.48 o 0 0 -6 4699.75 4667.82 132.92 o 2 0 -6 571.45 640.60 62.84 o 4 0 -6 501.18 521.93 70.60 o 6 0 -6 585.16 622.76 103.82 o 8 0 -6 1235.04 1340.36 90.62 o 10 0 -6 311.15 468.68 101.45 o 12 0 -6 554.14 650.84 115.50 o 14 0 -6 82.47 20.35 90.43 o 16 0 -6 154.90 179.37 101.73 o 1 1 -6 49.61 24.46 24.72 o 2 1 -6 522.36 545.99 35.46 o 3 1 -6 580.10 530.10 38.81 o 4 1 -6 24.66 44.44 29.39 o 5 1 -6 550.85 592.90 39.04 o 6 1 -6 782.74 823.36 53.81 o 7 1 -6 606.40 660.78 64.11 o 8 1 -6 75.73 73.56 45.27 o 9 1 -6 1697.60 1647.84 83.90 o 10 1 -6 678.17 668.85 64.45 o 11 1 -6 93.13 92.69 49.97 o 12 1 -6 28.92 -23.04 57.98 o 13 1 -6 178.75 184.29 67.33 o 14 1 -6 852.33 737.11 89.63 o 15 1 -6 54.65 159.14 68.95 o 16 1 -6 479.71 528.72 85.91 o 17 1 -6 881.64 977.44 102.26 o 0 2 -6 138.39 97.21 42.80 o 1 2 -6 45.80 52.21 31.59 o 2 2 -6 770.63 835.18 44.87 o 3 2 -6 2068.10 2201.79 61.78 o 4 2 -6 223.64 283.35 50.25 o 5 2 -6 83.05 118.97 35.86 o 6 2 -6 470.29 489.15 63.22 o 7 2 -6 838.97 837.96 72.95 o 8 2 -6 587.58 520.15 65.93 o 9 2 -6 62.05 84.91 60.76 o 10 2 -6 182.12 233.50 64.74 o 11 2 -6 570.15 610.88 64.92 o 12 2 -6 777.05 801.54 71.30 o 13 2 -6 1057.35 1022.58 78.02 o 14 2 -6 242.13 171.24 70.85 o 15 2 -6 97.61 80.63 75.90 o 16 2 -6 49.88 110.49 70.35 o 1 3 -6 3973.26 3927.65 90.53 o 2 3 -6 381.17 427.65 41.38 o 3 3 -6 2929.77 2966.75 78.09 o 4 3 -6 1771.04 1778.74 69.11 o 5 3 -6 394.58 424.23 49.66 o 6 3 -6 711.51 708.77 69.07 o 7 3 -6 20.72 76.15 52.56 o 8 3 -6 25.69 58.70 53.07 o 9 3 -6 1515.49 1504.14 93.93 o 10 3 -6 78.73 107.13 58.09 o 11 3 -6 74.45 106.70 59.96 o 12 3 -6 122.90 108.73 98.43 o 13 3 -6 347.25 276.06 68.49 o 14 3 -6 252.74 339.00 72.36 o 15 3 -6 48.18 86.17 56.32 o 16 3 -6 22.95 47.65 99.94 o 0 4 -6 85.80 106.66 51.48 o 1 4 -6 229.70 331.56 45.98 o 2 4 -6 228.04 229.74 51.96 o 3 4 -6 1805.72 1733.79 69.82 o 4 4 -6 31.66 -7.92 35.72 o 5 4 -6 73.75 103.29 38.99 o 6 4 -6 298.24 346.96 60.91 o 7 4 -6 237.05 314.45 60.53 o 8 4 -6 634.18 756.11 76.82 o 9 4 -6 80.18 28.84 56.38 o 10 4 -6 35.46 47.84 58.30 o 11 4 -6 1513.26 1523.62 110.81 o 12 4 -6 329.53 433.06 75.65 o 13 4 -6 90.37 96.60 61.53 o 14 4 -6 256.06 204.25 69.34 o 15 4 -6 288.33 334.02 74.99 o 16 4 -6 99.85 216.30 94.29 o 1 5 -6 166.74 220.64 49.49 o 2 5 -6 2061.72 2111.40 90.34 o 3 5 -6 268.71 256.99 46.21 o 4 5 -6 580.03 551.73 51.13 o 5 5 -6 1025.89 1081.34 63.14 o 6 5 -6 2.66 47.67 45.43 o 7 5 -6 139.50 161.46 59.05 o 8 5 -6 277.90 306.65 65.67 o 9 5 -6 260.07 171.72 61.50 o 10 5 -6 144.60 9.83 61.74 o 11 5 -6 86.66 74.22 62.34 o 12 5 -6 1057.34 1104.52 97.12 o 13 5 -6 258.91 345.15 72.40 o 14 5 -6 70.27 41.95 64.42 o 15 5 -6 203.18 268.68 75.70 o 0 6 -6 79.99 72.02 63.39 o 1 6 -6 200.06 182.20 49.65 o 2 6 -6 29.87 79.75 56.03 o 3 6 -6 1179.72 1123.12 75.04 o 4 6 -6 9.87 105.49 44.76 o 5 6 -6 35.76 14.10 42.60 o 6 6 -6 690.30 728.69 68.53 o 7 6 -6 552.89 580.92 64.48 o 8 6 -6 229.16 258.82 56.80 o 9 6 -6 87.89 112.41 64.93 o 10 6 -6 398.18 401.18 99.57 o 11 6 -6 638.18 683.91 94.65 o 12 6 -6 156.67 124.74 71.10 o 13 6 -6 488.58 387.55 83.67 o 14 6 -6 134.27 151.11 69.89 o 1 7 -6 803.57 846.45 69.64 o 2 7 -6 1127.75 1076.59 75.10 o 3 7 -6 530.93 491.76 61.96 o 4 7 -6 181.53 85.54 50.65 o 5 7 -6 385.18 379.04 56.17 o 6 7 -6 79.58 50.09 60.76 o 7 7 -6 169.52 227.57 62.26 o 8 7 -6 500.24 537.27 72.71 o 9 7 -6 132.52 68.02 55.57 o 10 7 -6 629.56 612.80 97.34 o 11 7 -6 361.84 473.83 129.28 o 12 7 -6 157.30 196.54 73.72 o 13 7 -6 390.15 244.00 101.25 o 0 8 -6 299.95 325.25 142.95 o 1 8 -6 256.27 267.43 57.46 o 2 8 -6 5.67 17.86 47.86 o 3 8 -6 1249.83 1173.19 82.77 o 4 8 -6 379.08 414.30 62.16 o 5 8 -6 448.15 475.88 60.04 o 6 8 -6 79.25 89.39 57.60 o 7 8 -6 160.35 227.76 81.96 o 8 8 -6 108.44 177.61 64.72 o 9 8 -6 35.73 75.90 85.37 o 10 8 -6 27.19 13.03 55.72 o 11 8 -6 73.25 42.54 57.44 o 1 9 -6 72.89 75.98 53.24 o 2 9 -6 206.00 128.80 58.41 o 3 9 -6 240.24 193.77 58.24 o 4 9 -6 465.74 473.69 65.97 o 5 9 -6 30.47 57.25 57.40 o 6 9 -6 368.92 380.17 107.14 o 7 9 -6 63.39 49.60 72.50 o 8 9 -6 52.94 104.03 59.72 o 9 9 -6 748.74 845.67 102.54 o 10 9 -6 51.85 50.65 60.66 o 0 10 -6 227.35 181.12 83.83 o 1 10 -6 412.69 337.27 64.93 o 2 10 -6 119.24 181.56 57.82 o 3 10 -6 601.38 584.73 71.19 o 4 10 -6 196.83 142.57 68.64 o 5 10 -6 170.54 239.41 121.90 o 6 10 -6 280.63 259.28 69.65 o 7 10 -6 35.12 6.75 59.12 o 1 11 -6 119.46 78.92 59.41 o 2 11 -6 926.21 792.24 95.86 o 2 0 -5 490.76 536.13 49.77 o 4 0 -5 1242.49 1323.29 64.78 o 6 0 -5 2279.15 2305.45 92.37 o 8 0 -5 742.14 804.85 73.92 o 10 0 -5 2828.00 2837.33 128.42 o 12 0 -5 688.66 769.68 77.30 o 14 0 -5 3864.11 3902.82 197.68 o 16 0 -5 480.44 408.40 432.12 o 18 0 -5 89.26 106.41 97.18 o 0 1 -5 1421.96 1321.45 64.27 o 1 1 -5 737.72 792.96 40.92 o 2 1 -5 317.13 361.49 33.69 o 3 1 -5 331.14 308.15 32.40 o 4 1 -5 2689.58 2675.79 61.60 o 5 1 -5 43.53 55.47 27.79 o 6 1 -5 62.36 65.87 27.38 o 7 1 -5 796.00 785.34 41.70 o 8 1 -5 135.89 178.53 42.99 o 9 1 -5 2871.11 2877.07 80.32 o 10 1 -5 50.81 72.53 38.09 o 11 1 -5 926.24 1029.48 68.57 o 12 1 -5 241.19 212.52 51.54 o 13 1 -5 63.97 100.28 48.38 o 14 1 -5 753.01 724.02 80.44 o 15 1 -5 424.27 535.75 78.08 o 16 1 -5 282.99 232.27 71.55 o 17 1 -5 347.07 409.06 71.58 o 18 1 -5 1169.20 1206.68 135.06 o 19 1 -5 243.09 136.15 65.78 o 1 2 -5 644.57 628.25 38.74 o 2 2 -5 824.27 811.46 41.97 o 3 2 -5 1525.15 1582.72 56.35 o 4 2 -5 185.38 220.45 33.95 o 5 2 -5 3129.11 3006.80 93.30 o 6 2 -5 523.55 507.71 40.44 o 7 2 -5 929.85 978.09 42.80 o 8 2 -5 918.05 872.01 72.72 o 9 2 -5 2699.72 2639.11 105.08 o 10 2 -5 132.72 177.80 56.30 o 11 2 -5 179.32 150.72 55.70 o 12 2 -5 53.74 12.86 48.64 o 13 2 -5 1215.61 1213.92 87.61 o 14 2 -5 152.08 80.24 61.71 o 15 2 -5 272.56 301.24 72.70 o 16 2 -5 302.76 166.77 97.86 o 17 2 -5 4.51 -7.57 57.17 o 18 2 -5 72.40 58.67 68.58 o 19 2 -5 211.80 161.58 86.13 o 0 3 -5 1421.55 1480.03 93.18 o 1 3 -5 1194.76 1286.55 49.21 o 2 3 -5 127.58 106.11 29.02 o 3 3 -5 1029.23 1010.81 42.81 o 4 3 -5 443.41 460.87 38.27 o 5 3 -5 196.34 148.31 39.16 o 6 3 -5 411.49 402.16 46.50 o 7 3 -5 403.91 365.99 45.84 o 8 3 -5 672.01 622.88 95.40 o 9 3 -5 463.69 449.03 66.19 o 10 3 -5 575.31 742.08 87.21 o 11 3 -5 438.53 497.40 69.52 o 12 3 -5 334.50 383.07 63.83 o 13 3 -5 37.39 90.54 59.12 o 14 3 -5 1139.35 1097.36 106.38 o 15 3 -5 251.09 270.01 88.08 o 16 3 -5 345.66 159.31 167.08 o 17 3 -5 59.62 67.46 68.27 o 18 3 -5 49.32 157.12 71.31 o 19 3 -5 420.11 427.50 83.93 o 1 4 -5 364.50 384.37 40.81 o 2 4 -5 491.83 467.79 36.31 o 3 4 -5 558.57 617.08 49.66 o 4 4 -5 233.57 153.60 38.04 o 5 4 -5 996.57 986.84 60.85 o 6 4 -5 262.16 268.26 45.58 o 7 4 -5 74.77 45.80 41.38 o 8 4 -5 84.38 39.26 64.00 o 9 4 -5 496.85 492.88 67.35 o 10 4 -5 1813.16 1926.54 100.16 o 11 4 -5 125.76 222.51 61.59 o 12 4 -5 63.19 4.00 54.29 o 13 4 -5 27.19 48.26 56.30 o 14 4 -5 1185.66 1251.42 95.38 o 15 4 -5 416.44 510.94 78.14 o 16 4 -5 605.11 287.03 79.17 o 17 4 -5 67.12 19.98 68.28 o 18 4 -5 81.66 91.88 83.85 o 0 5 -5 642.88 562.51 63.35 o 1 5 -5 293.47 353.34 41.64 o 2 5 -5 114.59 71.88 40.79 o 3 5 -5 937.67 870.86 57.79 o 4 5 -5 1102.00 993.60 63.82 o 5 5 -5 13.99 -15.96 36.55 o 6 5 -5 0.25 24.41 44.90 o 7 5 -5 1547.06 1503.44 72.62 o 8 5 -5 0.99 18.94 56.43 o 9 5 -5 1532.76 1375.43 101.19 o 10 5 -5 143.37 148.40 58.32 o 11 5 -5 204.65 194.29 63.34 o 12 5 -5 854.79 791.94 82.04 o 13 5 -5 334.80 311.05 68.06 o 14 5 -5 325.97 301.71 76.66 o 15 5 -5 1600.30 1493.25 105.64 o 16 5 -5 151.22 98.46 77.87 o 17 5 -5 69.64 -37.02 96.99 o 18 5 -5 103.26 102.70 91.58 o 1 6 -5 867.05 745.88 77.14 o 2 6 -5 188.15 224.22 44.62 o 3 6 -5 485.20 486.33 51.80 o 4 6 -5 643.71 651.35 56.41 o 5 6 -5 1556.75 1613.77 69.23 o 6 6 -5 345.77 341.79 46.46 o 7 6 -5 493.38 447.46 54.59 o 8 6 -5 358.27 406.61 88.78 o 9 6 -5 723.47 629.47 73.73 o 10 6 -5 118.76 38.30 63.79 o 11 6 -5 55.90 51.71 60.17 o 12 6 -5 159.85 137.19 63.52 o 13 6 -5 357.01 435.24 120.58 o 14 6 -5 818.04 788.38 85.81 o 15 6 -5 68.52 81.74 63.70 o 16 6 -5 79.13 35.41 119.62 o 0 7 -5 68.91 138.86 64.44 o 1 7 -5 28.98 21.97 47.89 o 2 7 -5 372.52 292.89 52.56 o 3 7 -5 94.25 111.27 47.69 o 4 7 -5 1025.06 1016.68 71.06 o 5 7 -5 569.48 609.33 56.11 o 6 7 -5 322.77 319.17 48.79 o 7 7 -5 21.03 26.16 49.22 o 8 7 -5 97.13 127.65 58.18 o 9 7 -5 271.78 307.64 66.38 o 10 7 -5 276.13 309.64 72.88 o 11 7 -5 129.72 -23.43 63.41 o 12 7 -5 843.07 817.27 89.69 o 13 7 -5 114.81 25.47 65.12 o 14 7 -5 192.17 115.15 79.50 o 15 7 -5 958.11 928.06 160.65 o 16 7 -5 480.75 475.98 106.72 o 1 8 -5 53.32 73.57 47.30 o 2 8 -5 396.22 413.57 57.00 o 3 8 -5 771.30 717.21 66.12 o 4 8 -5 889.44 892.82 71.00 o 5 8 -5 718.43 707.38 66.79 o 6 8 -5 475.65 489.10 67.01 o 7 8 -5 120.80 126.52 56.55 o 8 8 -5 563.00 617.13 74.46 o 9 8 -5 350.00 238.48 62.10 o 10 8 -5 196.63 352.42 71.76 o 11 8 -5 33.87 28.08 74.54 o 12 8 -5 200.03 251.05 74.60 o 13 8 -5 335.22 406.66 85.25 o 14 8 -5 567.82 580.54 132.09 o 15 8 -5 116.47 215.48 79.32 o 0 9 -5 244.55 215.94 187.54 o 1 9 -5 2193.22 2212.72 114.08 o 2 9 -5 111.03 74.64 49.42 o 3 9 -5 942.71 899.39 74.82 o 4 9 -5 128.15 28.79 50.05 o 5 9 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370.45 58.94 o 16 8 2 398.46 429.10 61.15 o 17 8 2 113.65 199.66 56.92 o 18 8 2 335.33 490.79 88.40 o 19 8 2 197.64 304.55 61.83 o 20 8 2 595.52 444.36 67.91 o 1 9 2 592.42 581.41 47.61 o 2 9 2 284.51 364.51 41.92 o 3 9 2 1624.23 1568.68 63.38 o 4 9 2 106.27 135.40 60.69 o 5 9 2 798.06 804.35 52.92 o 6 9 2 11.29 -3.07 35.78 o 7 9 2 147.11 91.41 39.11 o 8 9 2 533.72 612.35 51.79 o 9 9 2 2285.79 2334.38 100.98 o 10 9 2 1078.85 1042.77 60.76 o 11 9 2 518.84 541.60 52.23 o 12 9 2 24.10 98.73 41.44 o 13 9 2 716.88 754.43 66.13 o 14 9 2 804.13 773.64 69.77 o 15 9 2 36.42 -0.88 83.22 o 16 9 2 245.69 298.65 74.20 o 17 9 2 1022.78 1172.36 83.10 o 18 9 2 351.63 353.94 74.37 o 19 9 2 122.01 201.07 72.37 o 0 10 2 363.73 475.89 72.68 o 1 10 2 1747.67 1790.60 88.41 o 2 10 2 667.04 647.72 51.41 o 3 10 2 2286.61 2252.60 75.12 o 4 10 2 795.33 809.18 54.62 o 5 10 2 1659.70 1492.78 84.49 o 6 10 2 772.58 781.02 54.44 o 7 10 2 2544.18 2515.57 81.49 o 8 10 2 213.58 193.48 43.37 o 9 10 2 301.05 284.52 53.12 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6 2 3 880.23 955.78 33.19 o 7 2 3 344.58 330.80 24.62 o 8 2 3 1504.43 1437.41 40.41 o 9 2 3 714.39 655.40 33.72 o 10 2 3 897.62 869.12 35.24 o 11 2 3 228.38 292.72 43.64 o 12 2 3 257.60 225.86 43.83 o 13 2 3 3126.74 3215.23 78.06 o 14 2 3 441.25 373.67 42.49 o 15 2 3 3235.37 3157.21 81.69 o 16 2 3 723.35 793.67 86.79 o 17 2 3 36.21 3.65 35.59 o 18 2 3 132.62 106.85 52.01 o 19 2 3 1120.98 1107.27 77.06 o 20 2 3 270.71 283.10 60.34 o 21 2 3 547.30 475.84 64.37 o 22 2 3 41.92 86.00 73.44 o 0 3 3 352.62 310.30 35.23 o 1 3 3 1995.13 2027.15 41.25 o 2 3 3 229.12 309.89 27.37 o 3 3 3 156.40 119.06 23.44 o 4 3 3 3895.37 3746.69 61.84 o 5 3 3 584.59 679.22 33.92 o 6 3 3 6366.56 6648.22 82.95 o 7 3 3 431.63 560.35 27.43 o 8 3 3 1714.41 1739.58 44.77 o 9 3 3 1220.87 1170.92 49.29 o 10 3 3 775.31 724.55 53.27 o 11 3 3 1371.66 1448.04 55.33 o 12 3 3 1048.48 974.94 62.87 o 13 3 3 113.19 110.33 35.12 o 14 3 3 1403.50 1435.76 61.45 o 15 3 3 873.96 909.61 67.82 o 16 3 3 251.01 283.21 54.28 o 17 3 3 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3907.25 86.37 o 8 5 3 886.09 1034.24 50.92 o 9 5 3 1373.63 1421.61 56.68 o 10 5 3 6.93 33.88 31.31 o 11 5 3 136.62 147.76 41.48 o 12 5 3 239.77 261.71 53.27 o 13 5 3 1272.76 1349.51 82.34 o 14 5 3 1640.37 1732.47 84.78 o 15 5 3 1146.09 1189.22 77.17 o 16 5 3 1055.12 1006.04 73.34 o 17 5 3 443.66 409.07 60.46 o 18 5 3 560.70 648.49 91.43 o 19 5 3 188.03 230.92 57.97 o 20 5 3 278.75 329.43 62.57 o 21 5 3 55.46 97.30 65.49 o 1 6 3 132.05 145.91 22.21 o 2 6 3 72.86 58.96 27.51 o 3 6 3 3249.17 3198.70 68.62 o 4 6 3 977.43 936.38 51.41 o 5 6 3 3225.35 3058.88 65.37 o 6 6 3 387.04 439.00 36.29 o 7 6 3 554.40 613.29 41.23 o 8 6 3 21.12 10.22 33.22 o 9 6 3 668.28 675.84 55.39 o 10 6 3 29.32 28.76 34.44 o 11 6 3 894.26 926.44 54.48 o 12 6 3 153.71 176.05 50.16 o 13 6 3 226.69 246.69 59.06 o 14 6 3 924.67 909.27 84.04 o 15 6 3 1114.23 1013.51 73.82 o 16 6 3 73.72 123.28 51.20 o 17 6 3 93.70 162.35 54.83 o 18 6 3 26.62 77.58 51.89 o 19 6 3 68.21 92.73 55.12 o 20 6 3 36.20 89.96 103.35 o 0 7 3 38.64 47.58 33.40 o 1 7 3 374.77 414.46 27.88 o 2 7 3 956.59 910.63 49.39 o 3 7 3 600.83 561.75 42.32 o 4 7 3 2418.66 2310.27 66.69 o 5 7 3 1044.67 1058.29 52.49 o 6 7 3 15.26 25.83 30.02 o 7 7 3 965.78 969.32 49.72 o 8 7 3 565.73 571.51 47.52 o 9 7 3 18.50 3.23 36.28 o 10 7 3 1004.24 1049.21 58.33 o 11 7 3 332.59 228.75 68.10 o 12 7 3 3095.53 3206.87 101.07 o 13 7 3 33.61 48.39 47.76 o 14 7 3 498.00 614.53 64.74 o 15 7 3 1138.42 1198.87 80.57 o 16 7 3 216.70 161.64 57.21 o 17 7 3 51.21 144.23 55.13 o 18 7 3 60.78 66.94 53.61 o 19 7 3 53.88 69.00 52.42 o 20 7 3 404.97 508.84 70.00 o 1 8 3 478.32 538.76 41.21 o 2 8 3 3158.31 2981.50 74.29 o 3 8 3 886.91 868.29 49.43 o 4 8 3 785.07 769.61 49.69 o 5 8 3 141.90 104.57 41.87 o 6 8 3 1028.41 1063.86 90.26 o 7 8 3 143.75 84.97 34.79 o 8 8 3 40.26 62.56 35.11 o 9 8 3 998.93 1029.32 59.47 o 10 8 3 692.35 673.68 52.86 o 11 8 3 129.71 152.22 40.70 o 12 8 3 595.55 603.95 63.63 o 13 8 3 171.21 227.22 54.49 o 14 8 3 212.43 216.32 54.72 o 15 8 3 514.74 664.71 89.53 o 16 8 3 131.36 146.20 56.10 o 17 8 3 191.62 180.12 92.37 o 18 8 3 122.25 277.61 61.27 o 19 8 3 42.02 90.53 55.68 o 0 9 3 1314.39 1246.12 109.50 o 1 9 3 2143.85 2217.68 84.03 o 2 9 3 457.69 476.43 51.72 o 3 9 3 1236.00 1219.72 58.62 o 4 9 3 1701.15 1630.58 83.04 o 5 9 3 72.70 18.34 36.82 o 6 9 3 407.51 394.84 49.96 o 7 9 3 1280.66 1267.10 66.86 o 8 9 3 13.58 15.34 36.52 o 9 9 3 256.70 222.81 43.59 o 10 9 3 114.70 92.04 40.55 o 11 9 3 310.56 297.16 47.71 o 12 9 3 219.44 231.59 53.80 o 13 9 3 1357.06 1234.37 82.70 o 14 9 3 337.97 367.49 63.03 o 15 9 3 201.38 313.14 63.51 o 16 9 3 369.91 324.13 63.23 o 17 9 3 167.59 160.00 59.63 o 1 10 3 488.30 475.44 53.23 o 2 10 3 49.40 16.46 39.13 o 3 10 3 727.94 809.87 60.79 o 4 10 3 3226.10 3096.14 96.21 o 5 10 3 1275.63 1344.84 65.37 o 6 10 3 244.77 182.44 42.11 o 7 10 3 554.16 574.31 51.09 o 8 10 3 2.31 46.91 39.55 o 9 10 3 331.46 435.62 66.25 o 10 10 3 420.54 450.37 58.10 o 11 10 3 1190.90 1275.00 122.91 o 12 10 3 39.50 -25.52 53.20 o 13 10 3 1331.06 1453.91 88.91 o 14 10 3 380.31 557.52 70.23 o 15 10 3 62.33 110.78 55.15 o 16 10 3 541.73 669.61 74.94 o 0 11 3 462.69 508.77 81.59 o 1 11 3 26.01 116.12 45.05 o 2 11 3 134.41 137.98 45.29 o 3 11 3 361.40 333.43 53.21 o 4 11 3 1726.58 1717.57 93.51 o 5 11 3 101.57 128.95 59.63 o 6 11 3 156.83 107.55 46.70 o 7 11 3 239.73 222.74 49.25 o 8 11 3 329.74 424.45 52.58 o 9 11 3 66.87 63.04 65.68 o 10 11 3 862.11 838.50 69.79 o 11 11 3 384.62 421.61 59.91 o 12 11 3 830.91 852.46 87.63 o 13 11 3 160.30 190.97 69.61 o 14 11 3 144.93 153.54 62.28 o 15 11 3 131.92 141.93 59.97 o 1 12 3 300.00 348.31 66.48 o 2 12 3 756.38 839.61 66.95 o 3 12 3 982.17 901.71 69.53 o 4 12 3 204.04 183.41 49.75 o 5 12 3 225.89 256.43 51.55 o 6 12 3 813.20 962.05 87.86 o 7 12 3 392.59 521.44 60.88 o 8 12 3 490.70 577.50 64.03 o 9 12 3 273.59 315.48 66.36 o 10 12 3 329.90 242.72 65.56 o 11 12 3 218.74 327.32 65.59 o 12 12 3 22.06 151.95 67.86 o 13 12 3 467.50 605.87 85.33 o 0 13 3 1743.02 1797.51 223.60 o 1 13 3 479.80 456.62 76.09 o 2 13 3 873.22 808.05 100.89 o 3 13 3 214.14 208.78 54.09 o 4 13 3 112.19 124.84 68.07 o 5 13 3 31.74 27.91 48.10 o 6 13 3 430.18 450.46 60.78 o 7 13 3 324.82 407.60 60.86 o 8 13 3 417.24 455.80 61.42 o 9 13 3 441.71 414.39 72.18 o 10 13 3 31.54 21.29 59.80 o 1 14 3 156.27 138.91 54.53 o 2 14 3 420.34 495.55 64.25 o 3 14 3 13.08 5.98 50.05 o 4 14 3 154.98 119.99 53.82 o 5 14 3 286.27 261.10 75.75 o 6 14 3 141.34 133.02 53.11 o 0 0 4 4043.94 4045.96 90.00 o 2 0 4 2545.63 2421.65 99.00 o 4 0 4 67.08 49.02 29.39 o 6 0 4 4229.27 4201.54 100.50 o 8 0 4 5722.30 5250.99 117.01 o 10 0 4 867.96 887.94 64.27 o 12 0 4 4.68 15.43 43.79 o 14 0 4 577.01 519.17 62.35 o 16 0 4 763.18 789.58 80.70 o 18 0 4 326.76 436.71 137.70 o 20 0 4 314.76 445.89 144.26 o 1 1 4 2002.03 1919.59 38.81 o 2 1 4 1468.84 1547.40 50.43 o 3 1 4 2129.13 2121.19 47.69 o 4 1 4 680.98 687.87 32.20 o 5 1 4 296.96 296.10 26.18 o 6 1 4 293.67 306.91 30.52 o 7 1 4 100.49 94.62 26.27 o 8 1 4 600.18 663.14 39.19 o 9 1 4 1218.58 1280.39 49.60 o 10 1 4 1262.99 1277.33 50.38 o 11 1 4 811.39 849.54 48.29 o 12 1 4 756.10 770.17 46.53 o 13 1 4 315.10 403.60 43.45 o 14 1 4 1495.25 1531.58 65.79 o 15 1 4 244.46 274.47 42.60 o 16 1 4 2353.33 2273.59 97.11 o 17 1 4 1499.18 1450.77 84.61 o 18 1 4 281.34 230.60 56.24 o 19 1 4 80.57 88.48 52.56 o 20 1 4 523.36 551.50 118.22 o 21 1 4 46.12 240.64 96.43 o 0 2 4 5815.69 6015.61 123.32 o 1 2 4 4068.26 4195.14 62.53 o 2 2 4 3743.11 3823.82 93.25 o 3 2 4 5224.61 5060.50 74.09 o 4 2 4 78.04 97.35 23.61 o 5 2 4 122.97 215.55 42.23 o 6 2 4 67.37 24.37 22.63 o 7 2 4 1131.56 1093.14 40.20 o 8 2 4 1147.93 1111.16 40.63 o 9 2 4 27.53 0.32 28.49 o 10 2 4 277.20 303.49 36.46 o 11 2 4 211.90 306.20 46.88 o 12 2 4 303.44 264.73 39.75 o 13 2 4 123.53 107.48 45.24 o 14 2 4 136.94 115.69 72.69 o 15 2 4 567.25 638.20 61.35 o 16 2 4 199.00 147.51 51.52 o 17 2 4 196.30 217.00 54.40 o 18 2 4 465.60 426.77 62.58 o 19 2 4 347.71 399.73 69.85 o 20 2 4 137.63 201.22 63.03 o 21 2 4 234.11 277.20 61.61 o 1 3 4 3337.87 3389.36 59.55 o 2 3 4 3325.89 3160.35 61.61 o 3 3 4 1233.42 1329.17 47.08 o 4 3 4 716.98 804.11 39.54 o 5 3 4 152.21 153.69 24.74 o 6 3 4 1545.41 1577.20 48.87 o 7 3 4 395.03 450.30 30.15 o 8 3 4 883.14 957.93 49.16 o 9 3 4 561.35 554.43 32.45 o 10 3 4 685.38 624.60 58.11 o 11 3 4 1042.23 962.21 66.47 o 12 3 4 182.21 144.99 47.04 o 13 3 4 148.24 146.83 48.07 o 14 3 4 1283.06 1363.21 117.55 o 15 3 4 35.33 46.72 47.31 o 16 3 4 174.33 117.66 50.92 o 17 3 4 742.15 759.55 84.04 o 18 3 4 332.67 401.42 61.99 o 19 3 4 54.90 79.20 54.32 o 20 3 4 582.79 610.53 78.55 o 0 4 4 1618.05 1398.37 62.12 o 1 4 4 1451.82 1553.10 48.87 o 2 4 4 593.50 624.61 39.81 o 3 4 4 1313.94 1394.70 52.00 o 4 4 4 612.97 610.52 38.71 o 5 4 4 24.88 10.14 26.66 o 6 4 4 447.23 454.76 39.09 o 7 4 4 115.15 94.08 31.26 o 8 4 4 2897.60 2914.00 71.64 o 9 4 4 194.51 152.88 45.43 o 10 4 4 9.53 -35.13 42.01 o 11 4 4 1132.57 1130.84 71.75 o 12 4 4 1018.46 1016.58 69.29 o 13 4 4 1095.53 1091.02 97.48 o 14 4 4 821.99 811.18 68.25 o 15 4 4 364.33 426.94 58.82 o 16 4 4 656.42 652.32 67.34 o 17 4 4 17.64 11.04 50.83 o 18 4 4 639.85 755.67 118.12 o 19 4 4 18.91 84.30 55.10 o 20 4 4 9.34 23.42 52.96 o 1 5 4 2617.69 2528.84 55.95 o 2 5 4 1418.27 1358.58 53.45 o 3 5 4 611.85 502.96 39.76 o 4 5 4 96.19 152.87 30.55 o 5 5 4 1984.87 1856.66 56.93 o 6 5 4 68.64 22.44 30.20 o 7 5 4 156.82 157.16 35.99 o 8 5 4 6.10 14.22 37.13 o 9 5 4 2269.62 2259.33 70.74 o 10 5 4 45.94 -24.82 44.22 o 11 5 4 150.74 135.00 48.75 o 12 5 4 1281.83 1403.82 79.42 o 13 5 4 418.52 465.97 57.92 o 14 5 4 212.94 203.33 52.91 o 15 5 4 33.12 44.43 50.42 o 16 5 4 254.81 233.51 78.74 o 17 5 4 176.75 223.33 58.31 o 18 5 4 1330.63 1267.91 86.16 o 19 5 4 146.98 99.43 57.67 o 20 5 4 330.85 365.06 71.41 o 0 6 4 707.45 714.84 64.01 o 1 6 4 3423.08 3347.12 61.28 o 2 6 4 129.71 94.49 34.99 o 3 6 4 1801.28 1701.65 68.40 o 4 6 4 30.48 70.99 32.66 o 5 6 4 289.84 312.32 36.71 o 6 6 4 371.08 373.80 55.53 o 7 6 4 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4 8 4 1724.05 1796.62 85.37 o 5 8 4 1386.29 1425.53 63.41 o 6 8 4 862.77 882.29 53.92 o 7 8 4 234.82 280.86 41.74 o 8 8 4 823.96 901.91 56.51 o 9 8 4 1136.53 1135.33 61.85 o 10 8 4 502.29 533.27 60.12 o 11 8 4 281.49 269.39 54.52 o 12 8 4 30.25 -2.74 47.96 o 13 8 4 9.85 19.25 49.27 o 14 8 4 352.45 345.99 61.50 o 15 8 4 95.58 203.87 56.58 o 16 8 4 502.48 600.82 69.48 o 17 8 4 194.70 311.01 77.42 o 1 9 4 145.40 221.73 46.69 o 2 9 4 1096.70 1095.47 68.58 o 3 9 4 1097.10 1141.36 74.77 o 4 9 4 176.28 164.31 44.82 o 5 9 4 469.52 471.49 52.68 o 6 9 4 1009.53 854.80 54.62 o 7 9 4 565.68 557.49 50.17 o 8 9 4 682.32 700.97 54.18 o 9 9 4 587.45 598.81 53.69 o 10 9 4 302.56 304.31 58.68 o 11 9 4 18.94 89.57 51.00 o 12 9 4 296.22 331.66 61.57 o 13 9 4 565.97 575.37 68.99 o 14 9 4 467.63 554.31 69.71 o 15 9 4 242.89 252.00 61.73 o 16 9 4 177.45 179.04 82.15 o 0 10 4 174.29 127.18 63.39 o 1 10 4 585.61 647.83 59.82 o 2 10 4 714.58 702.23 61.43 o 3 10 4 1343.08 1529.91 81.08 o 4 10 4 206.24 197.72 47.49 o 5 10 4 399.80 425.98 53.96 o 6 10 4 266.67 263.94 50.46 o 7 10 4 280.79 366.86 54.07 o 8 10 4 68.48 63.93 57.73 o 9 10 4 253.65 165.82 69.10 o 10 10 4 182.81 190.32 62.25 o 11 10 4 226.03 171.11 66.30 o 12 10 4 152.98 259.51 59.02 o 13 10 4 7.51 57.19 53.82 o 14 10 4 340.05 429.44 66.86 o 1 11 4 260.01 253.95 50.94 o 2 11 4 1120.12 1180.88 75.55 o 3 11 4 183.20 259.26 53.47 o 4 11 4 457.47 482.24 58.09 o 5 11 4 392.32 427.49 57.36 o 6 11 4 291.59 121.34 48.23 o 7 11 4 520.76 527.77 62.13 o 8 11 4 110.88 151.29 51.64 o 9 11 4 23.56 55.76 70.95 o 10 11 4 167.45 133.92 81.04 o 11 11 4 242.52 397.51 174.42 o 12 11 4 472.33 465.74 139.67 o 0 12 4 233.12 404.66 81.97 o 1 12 4 92.01 97.47 50.33 o 2 12 4 198.68 221.43 53.57 o 3 12 4 294.94 315.60 58.01 o 4 12 4 171.69 88.11 51.68 o 5 12 4 267.92 250.77 55.14 o 6 12 4 61.78 111.12 49.82 o 7 12 4 83.20 107.75 50.23 o 8 12 4 451.49 450.97 72.31 o 9 12 4 63.03 -9.03 56.22 o 10 12 4 68.76 275.06 89.98 o 1 13 4 400.75 355.93 59.78 o 2 13 4 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7 744.91 734.43 83.67 o 2 6 7 37.40 40.18 44.85 o 3 6 7 873.80 964.15 73.05 o 4 6 7 113.11 95.51 58.06 o 5 6 7 177.18 179.34 71.33 o 6 6 7 60.51 88.25 118.68 o 7 6 7 264.61 247.16 156.72 o 8 6 7 242.05 201.64 66.34 o 9 6 7 328.71 355.54 76.67 o 10 6 7 142.34 106.05 69.25 o 0 7 7 896.51 962.29 224.91 o 1 7 7 40.70 3.13 46.24 o 2 7 7 262.47 307.76 56.43 o 3 7 7 11.70 88.23 50.79 o 4 7 7 158.64 207.91 139.57 o 5 7 7 52.88 11.50 67.68 o 6 7 7 49.55 76.70 101.64 o 7 7 7 272.77 322.95 208.52 o 8 7 7 325.02 238.05 84.00 o 1 8 7 166.21 127.84 63.98 o 2 8 7 687.04 779.08 122.87 o 3 8 7 78.60 28.14 49.34 o 4 8 7 462.05 350.19 72.26 o 5 8 7 514.75 432.17 77.12 o 4 0 8 542.65 575.72 131.14 o 6 0 8 489.83 493.10 140.32 o 8 0 8 195.85 234.75 119.34 o 1 1 8 272.24 216.39 118.03 o 2 1 8 305.37 133.77 112.78 o 3 1 8 184.26 52.46 118.03 o 4 1 8 731.95 739.44 102.21 o 5 1 8 126.82 95.48 64.05 o 6 1 8 518.28 381.46 75.96 o 7 1 8 257.33 183.48 77.31 o 8 1 8 341.05 301.40 75.80 o 0 2 8 586.23 596.70 135.08 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