#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/16/2231638.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231638_Fobs loop_ _publ_author_name 'Deng, Yi-Fang' _publ_section_title ; Poly[[[\m~3~-5-(pyridine-4-carboxamido)isophthalato]{\m~3~-5-[(pyridin-1-ium-4-yl)carbonylamino]isophthalato}neodymium(III)] dihydrate] ; _journal_coeditor_code NG5214 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1298 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.813 _cell_angle_gamma 90.000 _cell_length_a 13.4421 _cell_length_b 13.7754 _cell_length_c 16.2418 _exptl_crystal_F_000 1492.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file ng5214Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 325.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 31991.86 37080.04 344.16 o 2 0 0 2709.65 2302.77 36.89 o 3 0 0 71785.16 71172.77 3427.37 o 4 0 0 26952.16 25280.00 1238.99 o 5 0 0 55170.94 55978.23 2864.34 o 6 0 0 26091.59 25651.48 2232.63 o 7 0 0 4824.31 5008.59 300.20 o 8 0 0 4432.95 4082.73 188.29 o 9 0 0 26010.20 26477.11 548.89 o 10 0 0 13717.13 14673.83 429.43 o 11 0 0 13699.12 13904.24 443.19 o 12 0 0 3189.42 2897.64 213.60 o 13 0 0 311.73 434.31 99.92 o 14 0 0 6173.45 6292.66 339.72 o 1 1 0 470.10 434.26 19.42 o 2 1 0 152.77 153.15 11.50 o 3 1 0 2801.79 2765.05 104.96 o 4 1 0 195.21 145.11 12.84 o 5 1 0 220.10 180.47 15.70 o 6 1 0 4120.55 4429.00 148.17 o 7 1 0 386.65 398.08 28.23 o 8 1 0 146.70 167.22 29.10 o 9 1 0 365.24 462.26 60.44 o 10 1 0 51.85 75.99 33.87 o 11 1 0 10.73 17.73 27.30 o 12 1 0 1524.77 1252.11 101.27 o 13 1 0 323.20 291.97 58.25 o 14 1 0 230.56 260.86 57.73 o 0 2 0 27807.53 29329.11 1374.84 o 1 2 0 39326.30 38114.45 1979.00 o 2 2 0 8498.01 9283.46 595.47 o 3 2 0 9000.89 9208.82 464.39 o 4 2 0 16457.18 16148.15 829.37 o 5 2 0 39605.05 41558.78 1933.57 o 6 2 0 36090.98 37426.88 1226.29 o 7 2 0 1591.72 1436.40 42.28 o 8 2 0 1124.43 1063.73 102.44 o 9 2 0 13012.66 12937.76 796.38 o 10 2 0 13006.59 13274.83 370.37 o 11 2 0 6478.88 6991.60 222.34 o 12 2 0 606.20 586.40 80.54 o 13 2 0 509.52 610.82 81.76 o 14 2 0 5921.15 6222.43 240.22 o 1 3 0 8658.27 8060.75 276.86 o 2 3 0 2858.66 2436.61 115.65 o 3 3 0 2411.81 2468.96 137.87 o 4 3 0 13.57 28.12 11.79 o 5 3 0 1746.24 1775.56 92.84 o 6 3 0 578.36 465.16 24.38 o 7 3 0 706.32 694.58 41.32 o 8 3 0 3148.19 2665.71 92.43 o 9 3 0 8.52 29.11 19.42 o 10 3 0 102.53 132.49 39.61 o 11 3 0 1061.22 958.87 92.64 o 12 3 0 1495.57 1280.76 102.20 o 13 3 0 105.53 188.71 42.14 o 14 3 0 155.06 193.28 44.05 o 0 4 0 932.14 973.06 34.27 o 1 4 0 15049.98 13752.33 425.96 o 2 4 0 129.01 90.79 9.97 o 3 4 0 1569.26 1400.92 107.56 o 4 4 0 13780.92 14266.68 781.67 o 5 4 0 24991.03 24081.85 1663.34 o 6 4 0 5102.30 5028.05 302.12 o 7 4 0 1309.98 1293.15 78.08 o 8 4 0 1987.81 2048.95 72.63 o 9 4 0 4636.18 4697.59 403.80 o 10 4 0 6040.76 6066.75 387.67 o 11 4 0 4537.54 4395.46 180.33 o 12 4 0 6.97 33.01 28.80 o 13 4 0 992.42 1110.97 96.06 o 14 4 0 4501.24 4600.97 205.98 o 1 5 0 4747.72 4038.40 90.59 o 2 5 0 12092.29 12488.75 464.09 o 3 5 0 4638.48 4485.27 181.18 o 4 5 0 1979.51 1843.28 124.54 o 5 5 0 44.78 34.09 14.67 o 6 5 0 2906.13 2862.95 172.74 o 7 5 0 4784.66 4417.71 282.80 o 8 5 0 4206.75 4110.99 207.81 o 9 5 0 2094.68 1884.15 75.98 o 10 5 0 180.04 161.79 37.51 o 11 5 0 1510.97 1549.00 110.63 o 12 5 0 1462.87 1493.48 113.59 o 13 5 0 587.54 713.55 93.54 o 14 5 0 230.68 315.75 61.51 o 0 6 0 32718.36 30414.85 1661.67 o 1 6 0 20967.81 20093.54 633.10 o 2 6 0 2434.27 2293.37 69.61 o 3 6 0 7820.50 7703.02 304.00 o 4 6 0 7033.81 7514.10 334.55 o 5 6 0 11042.35 10075.15 652.32 o 6 6 0 6372.17 6636.31 342.09 o 7 6 0 5.84 11.72 16.01 o 8 6 0 2630.88 2339.93 184.67 o 9 6 0 7060.20 6423.15 305.23 o 10 6 0 12416.49 12217.12 755.11 o 11 6 0 4148.71 3613.59 222.30 o 12 6 0 156.58 272.42 61.06 o 13 6 0 640.90 877.39 100.59 o 1 7 0 4562.49 4126.83 111.52 o 2 7 0 21441.95 20750.86 614.29 o 3 7 0 10986.52 11409.09 395.91 o 4 7 0 1587.25 1356.30 76.39 o 5 7 0 221.75 146.49 25.53 o 6 7 0 895.55 1081.85 108.07 o 7 7 0 1530.02 1382.05 90.19 o 8 7 0 1530.71 1845.18 125.95 o 9 7 0 7356.73 6431.27 345.81 o 10 7 0 1317.56 1141.27 67.98 o 11 7 0 2565.21 2331.13 111.20 o 12 7 0 2917.60 2919.17 158.32 o 13 7 0 3408.29 3349.97 176.07 o 0 8 0 12315.10 11571.91 505.88 o 1 8 0 5986.68 5485.47 153.65 o 2 8 0 6943.41 6418.03 287.90 o 3 8 0 716.14 791.24 42.91 o 4 8 0 14062.27 13386.75 826.22 o 5 8 0 12719.08 12144.34 1131.39 o 6 8 0 6673.88 6326.67 389.14 o 7 8 0 1302.87 1082.85 66.41 o 8 8 0 7532.06 6798.26 385.23 o 9 8 0 9877.35 9757.21 331.39 o 10 8 0 682.12 784.38 62.71 o 11 8 0 2110.33 2227.58 111.66 o 12 8 0 103.86 126.74 49.19 o 13 8 0 419.92 593.74 135.89 o 1 9 0 13334.63 12626.24 397.17 o 2 9 0 8995.55 8117.93 183.44 o 3 9 0 7407.13 7780.48 266.83 o 4 9 0 6634.95 6489.67 356.89 o 5 9 0 2572.77 2007.02 91.91 o 6 9 0 1900.69 1818.26 110.63 o 7 9 0 6856.75 6991.60 360.23 o 8 9 0 15316.54 13340.35 941.53 o 9 9 0 1402.76 1456.88 76.65 o 10 9 0 2.14 31.10 23.15 o 11 9 0 1088.45 1263.36 117.48 o 12 9 0 1299.15 1519.86 126.95 o 0 10 0 2628.14 2652.24 108.69 o 1 10 0 2485.43 2439.37 60.42 o 2 10 0 541.38 557.78 37.42 o 3 10 0 659.89 738.14 42.18 o 4 10 0 5600.36 4977.04 196.75 o 5 10 0 9026.63 8538.92 529.96 o 6 10 0 1026.54 930.50 71.01 o 7 10 0 8.34 13.98 19.35 o 8 10 0 60.20 19.09 21.00 o 9 10 0 430.91 674.70 79.52 o 10 10 0 1556.43 1429.15 130.23 o 11 10 0 2089.94 2082.01 143.65 o 12 10 0 22.01 57.73 45.22 o 1 11 0 3612.62 3716.79 164.83 o 2 11 0 6788.03 6758.58 290.47 o 3 11 0 13970.77 14044.80 467.11 o 4 11 0 3901.09 3658.17 121.53 o 5 11 0 552.72 312.95 41.39 o 6 11 0 5902.54 5232.61 162.04 o 7 11 0 10922.40 10983.12 506.31 o 8 11 0 10440.75 9249.40 562.83 o 9 11 0 537.74 768.75 79.57 o 10 11 0 126.57 157.68 48.47 o 11 11 0 1455.24 1650.19 182.30 o 0 12 0 4108.92 4086.21 222.04 o 1 12 0 726.20 783.84 47.36 o 2 12 0 759.42 712.56 46.65 o 3 12 0 354.23 283.66 34.92 o 4 12 0 422.65 494.00 58.07 o 5 12 0 1184.14 1092.72 79.98 o 6 12 0 1318.84 1288.98 123.99 o 7 12 0 9.54 25.37 29.95 o 8 12 0 232.56 329.05 58.53 o 9 12 0 708.12 695.29 78.91 o 10 12 0 965.72 1149.81 98.86 o 1 13 0 2067.91 2348.54 167.84 o 2 13 0 4604.63 5160.90 306.00 o 3 13 0 8310.95 8665.87 540.11 o 4 13 0 791.41 975.64 78.83 o 5 13 0 166.78 135.53 37.37 o 6 13 0 3646.85 3939.06 250.99 o 7 13 0 4384.33 4491.63 362.00 o 8 13 0 2179.36 2954.34 157.18 o 9 13 0 676.00 691.83 81.01 o 0 14 0 1044.78 1042.26 138.11 o 1 14 0 3.02 4.61 28.21 o 2 14 0 666.09 659.44 80.67 o 3 14 0 184.43 195.52 45.45 o 4 14 0 8.72 58.15 33.35 o 5 14 0 886.34 873.55 80.13 o 6 14 0 50.50 95.99 35.25 o 7 14 0 111.58 61.95 39.74 o 8 14 0 355.74 328.05 63.03 o 1 15 0 192.66 423.75 71.86 o 2 15 0 4267.25 4478.13 278.00 o 3 15 0 4305.24 4182.37 271.78 o 4 15 0 2030.42 2023.40 136.42 o 5 15 0 26.58 11.34 30.55 o 6 15 0 1074.07 1353.82 118.14 o 7 15 0 4040.18 4268.88 213.96 o 0 16 0 56.71 117.68 60.40 o 1 16 0 22.63 67.20 32.62 o 2 16 0 1256.13 1071.13 151.88 o 3 16 0 2.60 59.51 37.75 o 4 16 0 48.28 86.15 54.18 o 5 16 0 27.56 30.80 29.89 o -15 1 1 4553.08 4601.71 210.15 o -14 1 1 6056.09 6560.76 304.64 o -13 1 1 3718.65 3902.47 179.50 o -12 1 1 28.51 52.60 33.41 o -11 1 1 1751.58 1593.96 106.45 o -10 1 1 13161.27 13280.55 285.28 o -9 1 1 28680.67 26306.29 1540.80 o -8 1 1 12402.34 11457.12 578.67 o -7 1 1 464.51 613.96 80.23 o -6 1 1 15316.91 13607.84 845.02 o -5 1 1 10087.84 9568.91 551.31 o -4 1 1 39493.14 37812.36 1817.45 o -3 1 1 14982.02 17294.52 686.21 o -2 1 1 1816.40 1895.46 77.62 o -1 1 1 29729.11 29883.34 911.92 o 0 1 1 44690.57 48572.02 418.77 o 1 1 1 84091.79 87899.64 3357.84 o 2 1 1 24470.56 26893.99 431.12 o 3 1 1 1.45 33.93 9.32 o 4 1 1 3423.39 3188.86 70.60 o 5 1 1 14079.21 14380.87 358.14 o 6 1 1 38939.83 40007.17 770.07 o 7 1 1 10746.02 11094.78 276.89 o 8 1 1 69.27 102.19 26.22 o 9 1 1 6724.27 7095.35 201.43 o 10 1 1 12660.79 13186.05 292.97 o 11 1 1 13581.37 14056.26 320.27 o 12 1 1 5187.39 5055.06 200.53 o 13 1 1 25.31 51.76 27.82 o 14 1 1 2391.81 2675.96 172.97 o -15 2 1 16.93 46.13 23.52 o -14 2 1 433.89 438.19 70.52 o -13 2 1 269.91 341.70 62.15 o -12 2 1 132.36 96.55 39.96 o -11 2 1 1681.05 1444.17 101.65 o -10 2 1 2425.84 2166.34 116.94 o -9 2 1 6.97 6.51 14.97 o -8 2 1 470.19 435.44 35.35 o -7 2 1 4.14 19.02 10.13 o -6 2 1 630.12 548.96 50.84 o -5 2 1 931.69 715.93 47.75 o -4 2 1 141.90 156.77 17.02 o -3 2 1 683.82 632.96 48.14 o -2 2 1 8164.46 8385.07 339.78 o -1 2 1 1017.69 1200.49 50.03 o 0 2 1 1922.37 1645.42 29.25 o 1 2 1 271.71 222.95 13.15 o 2 2 1 717.32 656.48 24.51 o 3 2 1 89.07 83.71 11.01 o 4 2 1 45.15 82.24 12.41 o 5 2 1 21697.86 24016.81 629.08 o 6 2 1 295.12 306.74 24.91 o 7 2 1 840.61 1015.55 43.12 o 8 2 1 4503.37 4229.98 281.17 o 9 2 1 300.56 290.88 39.54 o 10 2 1 456.35 397.33 63.20 o 11 2 1 221.88 171.60 48.34 o 12 2 1 311.15 323.80 62.23 o 13 2 1 383.57 433.37 71.94 o 14 2 1 971.23 978.34 103.99 o -15 3 1 2643.99 3071.51 171.08 o -14 3 1 5544.98 6339.59 240.52 o -13 3 1 4866.45 4724.27 199.24 o -12 3 1 1161.83 1088.93 95.14 o -11 3 1 789.39 893.87 88.86 o -10 3 1 8855.90 7840.41 278.85 o -9 3 1 8779.89 8885.74 306.24 o -8 3 1 6465.46 6068.84 326.64 o -7 3 1 31.60 35.11 15.66 o -6 3 1 2589.76 2411.79 147.56 o -5 3 1 34403.51 32589.60 1740.06 o -4 3 1 27876.19 26231.09 1644.05 o -3 3 1 18240.99 18547.82 836.18 o -2 3 1 95.17 112.24 10.71 o -1 3 1 11408.47 10263.32 414.71 o 0 3 1 12162.87 12110.20 275.49 o 1 3 1 22402.18 21940.76 783.14 o 2 3 1 1230.44 1134.25 54.48 o 3 3 1 371.23 296.81 22.15 o 4 3 1 13942.84 13931.48 682.26 o 5 3 1 28401.43 29953.83 935.64 o 6 3 1 23716.44 24517.14 923.08 o 7 3 1 14176.60 14847.58 966.51 o 8 3 1 850.57 865.19 56.23 o 9 3 1 2010.79 2104.45 88.21 o 10 3 1 9039.60 9217.92 247.01 o 11 3 1 5968.39 6256.89 215.02 o 12 3 1 3540.10 3424.37 165.94 o 13 3 1 46.14 60.96 33.53 o 14 3 1 2393.14 2669.69 154.59 o -14 4 1 21.47 52.64 34.46 o -13 4 1 154.67 234.02 110.80 o -12 4 1 1207.19 1193.87 100.16 o -11 4 1 12.55 35.18 34.90 o -10 4 1 1246.80 1130.55 78.71 o -9 4 1 2575.93 2303.05 89.73 o -8 4 1 509.22 446.38 38.58 o -7 4 1 2083.54 2121.33 118.85 o -6 4 1 679.84 585.66 42.50 o -5 4 1 2009.68 2076.02 99.24 o -4 4 1 62.68 69.45 15.37 o -3 4 1 8631.12 8334.38 371.27 o -2 4 1 3912.23 3626.40 134.78 o -1 4 1 5728.84 5762.06 186.09 o 0 4 1 791.95 638.87 20.45 o 1 4 1 7939.65 9406.95 275.07 o 2 4 1 118.48 157.85 17.50 o 3 4 1 11667.19 11634.96 677.90 o 4 4 1 6007.67 6086.17 246.52 o 5 4 1 519.48 350.27 23.90 o 6 4 1 2642.63 2395.57 60.78 o 7 4 1 1865.17 2190.46 124.93 o 8 4 1 1026.91 962.84 115.78 o 9 4 1 10414.68 9493.69 417.93 o 10 4 1 881.30 780.07 95.50 o 11 4 1 693.29 664.03 81.46 o 12 4 1 3298.56 2869.12 153.33 o 13 4 1 1057.35 1165.33 97.65 o 14 4 1 1652.65 1699.02 121.68 o -14 5 1 3985.71 4377.98 204.53 o -13 5 1 3066.34 3233.53 244.91 o -12 5 1 168.18 217.62 56.50 o -11 5 1 749.18 634.82 65.12 o -10 5 1 7768.30 8005.69 396.83 o -9 5 1 9830.69 9038.91 484.20 o -8 5 1 7535.32 7949.32 387.22 o -7 5 1 12.81 1.97 14.10 o -6 5 1 1999.01 2010.66 78.69 o -5 5 1 22913.86 21339.67 1222.67 o -4 5 1 28041.11 29826.83 1562.77 o -3 5 1 1624.90 1135.86 39.12 o -2 5 1 1280.54 893.82 34.17 o -1 5 1 20591.43 19963.49 523.11 o 0 5 1 6048.18 6413.85 158.22 o 1 5 1 32399.88 32269.53 974.76 o 2 5 1 2681.71 2297.26 78.82 o 3 5 1 2380.25 2452.04 154.41 o 4 5 1 15318.84 16068.73 825.32 o 5 5 1 17098.85 15758.78 777.25 o 6 5 1 14300.96 14569.87 679.63 o 7 5 1 5032.89 4258.74 190.94 o 8 5 1 1238.34 1063.53 65.58 o 9 5 1 4603.59 4094.70 212.74 o 10 5 1 20459.38 19481.83 1483.95 o 11 5 1 9002.97 8532.12 390.13 o 12 5 1 2057.64 2381.60 157.87 o 13 5 1 166.32 196.51 45.14 o -14 6 1 57.84 56.40 43.74 o -13 6 1 581.32 667.62 89.54 o -12 6 1 1225.13 1357.80 108.63 o -11 6 1 3317.34 3209.98 120.78 o -10 6 1 727.31 725.25 56.80 o -9 6 1 1834.66 1472.20 74.80 o -8 6 1 3269.89 3457.39 180.31 o -7 6 1 5010.66 4046.43 344.97 o -6 6 1 2370.94 2656.90 138.52 o -5 6 1 2931.61 2216.78 121.08 o -4 6 1 1542.55 1449.37 94.96 o -3 6 1 13904.82 13197.69 523.44 o -2 6 1 12881.10 11698.72 359.76 o -1 6 1 1214.09 1126.63 31.77 o 0 6 1 296.65 310.59 19.13 o 1 6 1 4797.79 4549.09 142.74 o 2 6 1 10639.35 10856.46 319.75 o 3 6 1 18588.34 19033.61 970.70 o 4 6 1 1558.66 1567.55 107.04 o 5 6 1 7.96 29.45 15.81 o 6 6 1 1752.66 1743.45 73.65 o 7 6 1 8715.98 7494.14 356.64 o 8 6 1 3184.07 3356.48 225.54 o 9 6 1 463.15 437.47 52.57 o 10 6 1 23.07 42.34 27.79 o 11 6 1 31.64 65.90 31.26 o 12 6 1 2063.31 2026.54 132.65 o 13 6 1 1194.67 1241.98 110.54 o -13 7 1 4864.37 4894.64 325.51 o -12 7 1 1226.26 1107.01 106.28 o -11 7 1 29.03 69.49 29.66 o -10 7 1 20015.80 18687.10 792.89 o -9 7 1 8974.20 8480.40 364.08 o -8 7 1 10926.63 9822.28 454.33 o -7 7 1 16.19 5.08 16.96 o -6 7 1 3330.42 3317.41 154.03 o -5 7 1 10958.44 11192.38 633.51 o -4 7 1 13381.45 13327.51 662.56 o -3 7 1 5883.34 5208.76 141.15 o -2 7 1 104.11 77.98 13.56 o -1 7 1 6829.12 6570.72 173.04 o 0 7 1 19700.79 18554.89 508.52 o 1 7 1 27761.10 27662.69 942.67 o 2 7 1 10336.25 9880.03 334.83 o 3 7 1 5036.97 5125.05 224.00 o 4 7 1 14731.67 14816.54 734.04 o 5 7 1 10077.38 9929.42 687.90 o 6 7 1 12104.62 11391.14 869.17 o 7 7 1 25.44 74.59 24.40 o 8 7 1 2624.08 2332.17 120.50 o 9 7 1 6794.66 6159.76 337.28 o 10 7 1 3595.15 3535.47 131.75 o 11 7 1 7812.94 7748.63 417.79 o 12 7 1 2456.08 2449.17 185.85 o 13 7 1 167.52 179.41 78.16 o -13 8 1 1264.14 1322.55 117.02 o -12 8 1 2622.24 2769.89 172.05 o -11 8 1 3080.91 3063.67 118.39 o -10 8 1 281.34 390.53 49.55 o -9 8 1 918.20 718.47 57.64 o -8 8 1 5926.98 5560.72 268.89 o -7 8 1 5731.41 5184.40 317.28 o -6 8 1 1897.21 2141.51 130.57 o -5 8 1 982.09 916.12 50.22 o -4 8 1 16.32 16.92 13.15 o -3 8 1 1467.11 1537.34 85.66 o -2 8 1 13132.82 12414.17 402.64 o -1 8 1 17905.29 17595.22 525.99 o 0 8 1 5329.92 4862.08 133.92 o 1 8 1 167.54 140.97 17.60 o 2 8 1 15837.59 15463.49 517.18 o 3 8 1 2004.31 2099.50 68.38 o 4 8 1 10341.21 10101.10 482.59 o 5 8 1 421.05 508.31 42.21 o 6 8 1 46.01 80.12 25.11 o 7 8 1 4759.97 4368.60 293.70 o 8 8 1 5473.81 5368.27 242.93 o 9 8 1 1462.15 1500.48 118.19 o 10 8 1 95.57 106.11 34.82 o 11 8 1 124.95 113.01 49.80 o 12 8 1 739.34 1114.65 169.64 o -13 9 1 1788.88 1907.34 204.28 o -12 9 1 38.58 65.80 32.17 o -11 9 1 41.91 114.87 31.67 o -10 9 1 2162.38 2044.63 91.91 o -9 9 1 3618.83 3761.62 179.09 o -8 9 1 425.73 444.56 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