#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/16/2231646.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231646_Fobs loop_ _publ_author_name 'Rivera, Augusto' 'Quiroga, Diego' 'R\'ios-Motta, Jaime' 'Fejfarov\'a, Karla' 'Du\RS,7aRS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl]bis(methylene)}diphenol ; _journal_coeditor_code NR2009 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2298 _journal_page_last o2299 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90 _cell_angle_beta 109.579(3) _cell_angle_gamma 90 _cell_length_a 12.7693(3) _cell_length_b 10.4365(2) _cell_length_c 16.3229(4) _exptl_crystal_F_000 856 _reflns_d_resolution_high 0.8677 _[local]_cod_data_source_file nr2009Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 194.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7141.03 7204.90 60.48 o 4 0 0 1028.12 1201.47 27.59 o 6 0 0 1163.27 1309.06 18.83 o 8 0 0 116.77 151.73 7.27 o 10 0 0 691.02 702.41 13.93 o 12 0 0 68.22 69.91 5.68 o 1 1 0 1258.12 1339.57 8.71 o 2 1 0 15580.40 16316.90 41.45 o 3 1 0 5598.58 5865.25 23.66 o 4 1 0 244.52 269.79 6.28 o 5 1 0 740.65 725.63 18.92 o 6 1 0 20.81 33.83 3.12 o 7 1 0 132.39 114.35 3.51 o 8 1 0 76.60 89.50 3.67 o 9 1 0 162.39 152.25 5.26 o 10 1 0 134.80 123.70 5.32 o 11 1 0 4.72 6.52 3.29 < 12 1 0 486.52 558.31 8.22 o 13 1 0 8.75 10.44 2.32 o 0 2 0 35311.00 37841.70 117.64 o 1 2 0 5254.41 5675.04 26.45 o 2 2 0 16661.80 17728.90 50.60 o 3 2 0 1083.30 1180.70 13.88 o 4 2 0 1825.65 1885.74 20.40 o 5 2 0 63.04 97.46 7.57 o 6 2 0 5232.53 5409.11 22.05 o 7 2 0 114.07 105.66 3.88 o 8 2 0 0.80 0.69 2.39 < 9 2 0 214.11 188.46 5.64 o 10 2 0 40.39 46.76 4.42 o 11 2 0 233.73 214.12 5.83 o 12 2 0 0.63 -0.42 3.07 < 13 2 0 26.15 25.15 2.51 o 1 3 0 4896.54 5327.80 30.25 o 2 3 0 75.53 77.78 5.10 o 3 3 0 85.29 97.56 4.97 o 4 3 0 53.44 53.61 4.87 o 5 3 0 1344.52 1350.80 11.19 o 6 3 0 905.30 887.54 8.27 o 7 3 0 1.32 2.60 1.98 < 8 3 0 153.73 148.57 4.46 o 9 3 0 775.44 825.03 11.09 o 10 3 0 108.88 125.20 5.91 o 11 3 0 5.38 1.34 3.41 < 12 3 0 2.02 3.41 2.62 < 13 3 0 6.25 5.28 1.97 < 0 4 0 16.66 22.07 6.54 o 1 4 0 3518.22 3831.54 32.48 o 2 4 0 3199.08 3511.14 30.89 o 3 4 0 278.43 274.68 8.32 o 4 4 0 23.46 41.76 2.52 o 5 4 0 13.43 13.32 2.10 o 6 4 0 1050.33 1019.29 10.11 o 7 4 0 1.20 1.51 2.51 < 8 4 0 388.31 395.01 7.80 o 9 4 0 9.35 6.50 3.30 < 10 4 0 159.48 175.63 6.37 o 11 4 0 113.58 112.16 5.18 o 12 4 0 130.25 138.67 4.36 o 13 4 0 162.34 180.99 12.14 o 1 5 0 1877.39 2062.59 13.80 o 2 5 0 1270.80 1283.43 8.73 o 3 5 0 19.10 14.37 1.82 o 4 5 0 1250.27 1216.59 9.05 o 5 5 0 60.61 55.09 2.90 o 6 5 0 329.24 352.67 6.50 o 7 5 0 106.55 108.64 4.23 o 8 5 0 121.29 131.06 4.73 o 9 5 0 128.31 133.15 4.77 o 10 5 0 167.22 188.40 5.76 o 11 5 0 21.87 18.38 2.93 o 12 5 0 0.02 0.68 2.21 < 0 6 0 234.20 231.56 5.61 o 1 6 0 91.24 77.02 2.85 o 2 6 0 385.67 400.95 5.70 o 3 6 0 289.68 293.33 4.56 o 4 6 0 0.25 1.71 2.07 < 5 6 0 367.50 378.77 6.21 o 6 6 0 596.53 605.11 8.85 o 7 6 0 92.40 97.72 4.54 o 8 6 0 62.34 64.54 4.18 o 9 6 0 129.86 132.84 5.17 o 10 6 0 96.11 99.81 4.49 o 11 6 0 11.43 6.92 2.36 < 1 7 0 130.95 99.46 3.58 o 2 7 0 54.12 45.77 2.92 o 3 7 0 2.53 3.13 2.34 < 4 7 0 16.06 20.45 2.70 o 5 7 0 0.52 -1.98 2.75 < 6 7 0 3.82 4.84 2.80 < 7 7 0 1589.04 1699.16 14.41 o 8 7 0 516.14 523.05 9.21 o 9 7 0 136.74 143.52 5.08 o 10 7 0 43.42 30.71 3.12 o 11 7 0 136.04 174.13 6.22 o 0 8 0 553.36 593.70 15.80 o 1 8 0 1.06 1.17 3.18 < 2 8 0 132.77 130.10 5.33 o 3 8 0 501.89 486.20 8.28 o 4 8 0 218.17 204.55 5.96 o 5 8 0 101.18 85.89 5.13 o 6 8 0 36.26 35.43 4.52 o 7 8 0 0.63 -3.05 3.67 < 8 8 0 3.56 2.34 3.09 < 9 8 0 18.15 11.93 2.73 o 10 8 0 30.09 36.55 3.92 o 1 9 0 207.31 215.46 7.30 o 2 9 0 179.24 175.31 6.26 o 3 9 0 38.88 34.73 3.89 o 4 9 0 282.74 288.08 8.44 o 5 9 0 6.85 4.90 3.37 < 6 9 0 135.51 136.56 5.54 o 7 9 0 49.76 48.10 3.93 o 8 9 0 2.15 0.14 2.87 < 9 9 0 118.44 109.02 6.37 o 0 10 0 235.49 253.26 12.14 o 1 10 0 142.70 137.80 6.22 o 2 10 0 114.08 99.77 5.39 o 3 10 0 1088.74 1129.56 15.05 o 4 10 0 97.65 97.76 6.27 o 5 10 0 250.94 270.83 9.07 o 6 10 0 45.36 43.20 4.98 o 7 10 0 120.66 115.16 6.38 o 1 11 0 0.66 0.23 3.29 < 2 11 0 16.39 15.06 3.29 o 3 11 0 244.99 245.15 7.24 o 4 11 0 327.60 314.85 7.74 o 5 11 0 359.52 357.52 14.64 o -13 0 1 0.73 1.20 3.10 < -11 0 1 1087.13 999.65 16.83 o -9 0 1 28.44 30.50 3.90 o -7 0 1 722.34 683.46 14.40 o -5 0 1 80.73 153.37 12.83 o -3 0 1 960.90 1022.49 26.98 o -1 0 1 951.47 935.94 13.92 o 1 0 1 1204.89 1226.61 13.96 o 3 0 1 1341.91 1271.50 24.00 o 5 0 1 2405.38 2784.47 62.83 o 7 0 1 321.64 341.33 9.45 o 9 0 1 126.03 152.08 9.45 o 11 0 1 157.01 147.63 8.41 o 13 0 1 4.30 3.62 2.92 < -13 1 1 2.17 2.30 2.23 < -12 1 1 31.60 33.13 3.24 o -11 1 1 115.90 113.60 5.02 o -10 1 1 62.50 55.33 3.96 o -9 1 1 54.03 53.42 3.73 o -8 1 1 48.41 33.13 2.60 o -7 1 1 419.44 446.97 5.85 o -6 1 1 2466.20 2506.79 17.39 o -5 1 1 4127.30 4202.13 37.34 o -4 1 1 6871.48 6687.11 39.64 o -3 1 1 9131.35 9414.42 35.41 o -2 1 1 2037.29 1971.07 15.55 o -1 1 1 2338.40 2167.38 15.71 o 0 1 1 102.47 89.09 3.18 o 1 1 1 42.82 45.38 2.54 o 2 1 1 322.58 308.73 6.37 o 3 1 1 1388.09 1426.37 14.06 o 4 1 1 25.73 35.75 3.53 o 5 1 1 2488.73 2669.86 25.72 o 6 1 1 34.63 32.71 2.90 o 7 1 1 727.46 804.41 9.50 o 8 1 1 564.74 547.76 8.61 o 9 1 1 321.36 321.38 8.32 o 10 1 1 1232.93 1259.42 16.29 o 11 1 1 33.87 40.84 3.76 o 12 1 1 24.82 32.68 2.89 o 13 1 1 62.05 71.47 3.39 o -13 2 1 0.79 11.50 2.38 o -12 2 1 174.37 161.70 5.63 o -11 2 1 92.42 80.19 4.58 o -10 2 1 167.19 188.05 5.93 o -9 2 1 196.76 184.07 5.30 o -8 2 1 1347.26 1290.23 12.22 o -7 2 1 144.35 126.38 3.73 o -6 2 1 1606.61 1523.77 11.92 o -5 2 1 339.95 355.31 10.49 o -4 2 1 20.22 19.07 3.25 o -3 2 1 6425.83 6704.86 32.15 o -2 2 1 8225.95 8324.97 33.79 o -1 2 1 8368.51 8658.75 31.77 o 0 2 1 3388.07 3645.93 21.45 o 1 2 1 4454.17 4796.82 22.41 o 2 2 1 380.72 451.45 7.57 o 3 2 1 0.03 1.92 2.31 < 4 2 1 197.51 194.23 6.40 o 5 2 1 3734.10 3622.03 22.54 o 6 2 1 331.11 346.53 6.18 o 7 2 1 59.08 60.30 2.89 o 8 2 1 50.68 50.19 3.37 o 9 2 1 23.45 20.72 3.59 o 10 2 1 67.14 66.38 4.71 o 11 2 1 259.55 249.94 6.51 o 12 2 1 17.04 14.16 2.87 o 13 2 1 83.22 95.11 3.63 o -13 3 1 198.76 215.43 4.75 o -12 3 1 356.04 408.75 7.62 o -11 3 1 395.14 400.49 8.57 o -10 3 1 540.50 561.43 10.98 o -9 3 1 75.67 73.03 4.08 o -8 3 1 36.32 34.18 2.70 o -7 3 1 483.31 417.21 5.75 o -6 3 1 5417.48 5180.19 17.62 o -5 3 1 1151.14 1191.81 11.78 o -4 3 1 962.76 1031.63 18.08 o -3 3 1 1670.51 1635.46 18.94 o -2 3 1 1.65 2.05 2.67 < -1 3 1 6550.09 7102.75 38.72 o 0 3 1 93.51 107.53 5.69 o 1 3 1 0.20 0.37 2.14 < 2 3 1 0.53 -0.22 2.35 < 3 3 1 2410.48 2448.69 23.16 o 4 3 1 137.42 98.48 6.31 o 5 3 1 227.05 227.19 4.88 o 6 3 1 2169.18 2182.47 12.42 o 7 3 1 1243.35 1230.86 11.14 o 8 3 1 26.16 29.13 3.05 o 9 3 1 1443.51 1553.93 15.06 o 10 3 1 358.45 375.12 8.27 o 11 3 1 58.23 53.04 4.38 o 12 3 1 30.17 33.37 3.16 o 13 3 1 2.23 0.06 2.31 < -13 4 1 166.38 181.74 4.99 o -12 4 1 131.56 135.25 4.76 o -11 4 1 2.70 2.60 2.89 < -10 4 1 365.15 373.66 8.75 o -9 4 1 63.56 67.00 4.29 o -8 4 1 833.40 866.43 10.45 o -7 4 1 421.83 418.42 6.75 o -6 4 1 1.04 -0.39 2.05 < -5 4 1 143.32 161.34 3.88 o -4 4 1 137.24 134.41 4.01 o -3 4 1 142.83 190.95 8.84 o -2 4 1 177.14 227.51 8.63 o -1 4 1 922.63 1040.46 17.00 o 0 4 1 860.98 904.32 15.26 o 1 4 1 1735.87 1832.35 19.49 o 2 4 1 0.56 0.00 3.11 < 3 4 1 139.13 143.90 5.09 o 4 4 1 63.02 58.63 2.96 o 5 4 1 329.88 353.97 6.14 o 6 4 1 100.17 95.43 3.70 o 7 4 1 19.59 21.21 2.86 o 8 4 1 5.52 7.74 2.90 < 9 4 1 837.27 863.46 11.66 o 10 4 1 62.86 66.05 4.40 o 11 4 1 0.26 -0.70 3.08 < 12 4 1 57.85 60.33 3.23 o -12 5 1 116.09 120.82 4.49 o -11 5 1 751.73 807.33 10.61 o -10 5 1 2526.91 2713.53 20.38 o -9 5 1 5.46 6.43 3.20 < -8 5 1 10.56 6.55 2.83 < -7 5 1 2989.31 2999.41 17.70 o -6 5 1 153.77 137.35 4.08 o -5 5 1 747.13 661.15 7.44 o -4 5 1 856.73 864.87 8.67 o -3 5 1 296.00 328.23 5.23 o -2 5 1 3.41 2.44 1.99 < -1 5 1 299.12 320.58 7.60 o 0 5 1 878.60 926.71 11.35 o 1 5 1 102.43 107.47 3.47 o 2 5 1 404.13 376.19 5.63 o 3 5 1 1121.55 1143.26 9.42 o 4 5 1 1232.06 1309.92 9.09 o 5 5 1 1055.42 1051.33 9.80 o 6 5 1 40.90 38.96 3.09 o 7 5 1 12.86 8.71 2.79 o 8 5 1 164.39 169.75 5.31 o 9 5 1 95.78 88.37 4.21 o 10 5 1 127.38 135.36 5.30 o 11 5 1 16.95 20.63 2.85 o 12 5 1 20.12 23.88 2.88 o -12 6 1 115.47 119.07 4.54 o -11 6 1 338.08 375.94 7.20 o -10 6 1 191.80 194.23 5.94 o -9 6 1 103.32 113.41 5.34 o -8 6 1 767.82 800.76 11.30 o -7 6 1 576.92 614.07 9.79 o -6 6 1 33.14 24.97 3.09 o -5 6 1 1342.85 1381.65 11.15 o -4 6 1 5.88 6.94 1.89 o -3 6 1 938.53 938.70 8.42 o -2 6 1 495.33 454.80 5.93 o -1 6 1 1.15 2.63 1.65 < 0 6 1 0.00 3.24 1.65 < 1 6 1 7.15 5.55 2.33 < 2 6 1 1294.40 1336.92 9.53 o 3 6 1 1513.65 1541.68 10.38 o 4 6 1 91.68 88.64 3.27 o 5 6 1 125.64 126.52 4.76 o 6 6 1 1994.17 2040.39 16.83 o 7 6 1 472.55 491.17 8.01 o 8 6 1 0.54 -1.89 3.19 < 9 6 1 0.04 -1.18 2.86 < 10 6 1 163.65 169.08 5.69 o 11 6 1 29.35 31.28 3.24 o -11 7 1 0.01 -0.20 2.49 < -10 7 1 158.60 152.68 4.45 o -9 7 1 71.68 59.77 3.62 o -8 7 1 1517.68 1591.20 14.57 o -7 7 1 1206.23 1296.44 13.18 o -6 7 1 1.72 1.20 2.77 < -5 7 1 39.94 42.91 3.31 o -4 7 1 593.76 601.92 8.14 o -3 7 1 406.77 428.06 6.72 o -2 7 1 8.69 6.69 2.22 o -1 7 1 538.20 531.42 7.18 o 0 7 1 26.75 25.14 2.40 o 1 7 1 10.99 9.23 2.25 o 2 7 1 304.06 277.20 5.59 o 3 7 1 0.35 0.44 2.26 < 4 7 1 358.86 362.81 6.45 o 5 7 1 28.16 23.30 3.18 o 6 7 1 90.77 91.62 4.38 o 7 7 1 968.67 1061.42 12.74 o 8 7 1 106.66 107.18 4.59 o 9 7 1 0.28 0.57 2.99 < 10 7 1 2.17 4.20 2.57 < -10 8 1 6.68 6.87 2.37 < -9 8 1 1.76 0.87 2.73 < -8 8 1 94.72 82.66 4.56 o -7 8 1 412.16 401.64 9.78 o -6 8 1 224.73 230.31 7.30 o -5 8 1 33.66 31.98 4.03 o -4 8 1 102.36 96.42 4.47 o -3 8 1 14.75 16.11 3.05 o -2 8 1 153.98 145.39 5.51 o -1 8 1 73.06 72.00 4.43 o 0 8 1 53.99 52.33 3.81 o 1 8 1 0.92 0.69 2.76 < 2 8 1 293.52 289.41 6.09 o 3 8 1 29.33 29.66 3.05 o 4 8 1 1237.11 1266.14 13.52 o 5 8 1 587.05 614.16 10.33 o 6 8 1 66.74 63.85 4.40 o 7 8 1 3.79 3.82 3.51 < 8 8 1 79.48 67.34 4.50 o 9 8 1 46.75 43.67 3.44 o -9 9 1 527.16 530.88 10.37 o -8 9 1 14.53 21.71 3.45 o -7 9 1 0.06 2.85 3.42 < -6 9 1 46.64 49.01 4.36 o -5 9 1 314.69 332.13 10.97 o -4 9 1 90.88 89.42 5.50 o -3 9 1 245.10 259.80 8.13 o -2 9 1 523.61 541.54 10.96 o -1 9 1 238.96 244.02 8.50 o 0 9 1 6.39 5.54 4.05 < 1 9 1 96.89 98.10 5.15 o 2 9 1 19.53 11.74 3.55 o 3 9 1 310.32 337.53 8.31 o 4 9 1 0.08 -3.06 3.61 < 5 9 1 118.54 118.21 5.48 o 6 9 1 48.31 53.56 4.09 o 7 9 1 42.97 39.87 3.76 o 8 9 1 131.19 128.74 4.84 o -7 10 1 15.35 29.73 4.19 o -6 10 1 12.57 11.41 3.46 o -5 10 1 12.29 9.42 3.91 < -4 10 1 250.70 242.03 9.04 o -3 10 1 62.44 57.85 4.46 o -2 10 1 29.94 33.74 4.28 o -1 10 1 67.00 64.73 5.43 o 0 10 1 24.44 23.24 4.48 o 1 10 1 9.62 3.39 3.76 < 2 10 1 948.93 942.15 13.79 o 3 10 1 420.37 439.30 8.78 o 4 10 1 24.84 21.62 3.70 o 5 10 1 1.03 1.67 3.38 < 6 10 1 41.32 41.05 4.84 o 7 10 1 0.03 -0.86 3.61 < -5 11 1 86.97 77.75 5.24 o -4 11 1 16.44 10.95 2.84 o -3 11 1 6.04 2.16 2.89 < -2 11 1 27.08 17.32 3.32 o -1 11 1 0.12 -5.06 3.28 < 0 11 1 11.66 7.11 3.26 < 1 11 1 81.27 76.79 4.92 o 2 11 1 122.29 107.55 4.88 o 3 11 1 47.87 52.71 4.53 o 4 11 1 24.22 17.72 2.84 o -14 0 2 56.30 70.71 4.80 o -12 0 2 135.12 149.90 6.25 o -10 0 2 162.85 163.46 6.90 o -8 0 2 601.46 559.76 9.92 o -6 0 2 3839.91 3754.90 68.31 o -4 0 2 1589.39 1587.70 33.74 o -2 0 2 1526.86 1473.63 24.75 o 0 0 2 1319.44 1384.59 19.51 o 2 0 2 4003.74 3728.34 33.30 o 4 0 2 415.06 427.58 15.23 o 6 0 2 4650.98 4805.19 46.59 o 8 0 2 319.41 296.58 10.24 o 10 0 2 195.79 214.51 8.25 o 12 0 2 7.63 5.95 3.96 < -14 1 2 28.34 41.60 3.33 o -13 1 2 53.73 46.74 3.08 o -12 1 2 59.06 58.11 3.53 o -11 1 2 16.90 16.97 3.19 o -10 1 2 477.70 456.15 7.49 o -9 1 2 81.80 72.29 3.59 o -8 1 2 1.91 2.35 2.21 < -7 1 2 1418.77 1331.22 9.82 o -6 1 2 4.25 12.48 2.74 o -5 1 2 6175.07 6308.83 59.62 o -4 1 2 9393.37 9026.71 48.44 o -3 1 2 3020.05 2894.16 24.50 o -2 1 2 2604.62 2748.56 21.56 o -1 1 2 2133.98 2304.25 18.14 o 0 1 2 1628.56 1614.51 12.24 o 1 1 2 634.43 587.66 8.19 o 2 1 2 695.62 693.60 9.29 o 3 1 2 1.23 0.25 2.28 < 4 1 2 1593.56 1685.75 18.25 o 5 1 2 1475.90 1448.01 16.29 o 6 1 2 446.94 402.01 6.98 o 7 1 2 122.16 106.72 5.11 o 8 1 2 641.22 613.80 10.11 o 9 1 2 11.00 9.59 3.56 < 10 1 2 145.24 112.33 6.25 o 11 1 2 15.97 10.84 2.86 o 12 1 2 23.57 22.92 3.03 o 13 1 2 7.71 4.58 2.29 < -14 2 2 47.32 62.28 4.74 o -13 2 2 17.59 19.49 2.39 o -12 2 2 56.48 47.21 3.96 o -11 2 2 185.72 194.70 5.83 o -10 2 2 45.23 42.07 3.51 o -9 2 2 30.08 29.07 3.25 o -8 2 2 532.09 537.01 7.53 o -7 2 2 42.20 28.24 2.22 o -6 2 2 222.06 187.36 4.37 o -5 2 2 1533.18 1425.02 20.02 o -4 2 2 3097.85 3120.30 28.89 o -3 2 2 4.51 14.15 2.94 o -2 2 2 3236.97 3297.93 25.18 o -1 2 2 17170.40 18438.90 59.71 o 0 2 2 3700.31 3723.11 26.52 o 1 2 2 0.95 5.60 2.65 < 2 2 2 1313.60 1374.56 13.55 o 3 2 2 44.01 48.46 3.57 o 4 2 2 43.87 39.53 4.31 o 5 2 2 2.24 2.26 2.60 < 6 2 2 258.82 234.24 5.25 o 7 2 2 1337.49 1307.62 12.84 o 8 2 2 229.69 235.71 6.18 o 9 2 2 133.38 123.89 5.44 o 10 2 2 89.25 67.63 4.18 o 11 2 2 5.93 -3.13 2.88 < 12 2 2 31.46 32.93 3.21 o 13 2 2 37.46 54.85 8.32 o -13 3 2 21.13 24.16 2.58 o -12 3 2 185.82 185.47 5.71 o -11 3 2 398.21 416.79 8.71 o -10 3 2 104.79 115.62 5.30 o -9 3 2 669.15 689.82 10.81 o -8 3 2 41.00 41.77 2.82 o -7 3 2 329.28 293.29 5.07 o -6 3 2 1328.84 1168.12 8.80 o -5 3 2 1353.63 1298.07 11.34 o -4 3 2 527.53 572.48 13.09 o -3 3 2 2489.69 2414.98 21.44 o -2 3 2 11115.00 11753.90 45.77 o -1 3 2 882.98 968.00 12.15 o 0 3 2 249.69 271.70 7.37 o 1 3 2 259.31 290.83 7.96 o 2 3 2 208.90 198.42 7.08 o 3 3 2 1150.83 1198.62 14.90 o 4 3 2 624.97 691.66 10.66 o 5 3 2 596.68 604.69 7.90 o 6 3 2 24.72 27.64 2.89 o 7 3 2 203.41 200.65 5.21 o 8 3 2 269.45 277.21 6.88 o 9 3 2 553.01 589.54 10.66 o 10 3 2 338.42 342.18 8.48 o 11 3 2 25.49 31.50 3.88 o 12 3 2 6.10 1.92 2.32 < -13 4 2 11.08 9.49 2.15 o -12 4 2 31.14 33.28 3.29 o -11 4 2 27.66 22.18 3.52 o -10 4 2 28.24 29.22 3.88 o -9 4 2 4.74 3.00 2.89 < -8 4 2 6.94 4.78 2.51 < -7 4 2 1127.62 1090.95 9.93 o -6 4 2 367.66 320.16 5.47 o -5 4 2 277.52 310.60 5.16 o -4 4 2 1008.76 996.52 10.12 o -3 4 2 2663.00 2828.49 26.71 o -2 4 2 716.47 884.76 15.79 o -1 4 2 182.02 183.38 7.48 o 0 4 2 2541.17 2922.25 29.12 o 1 4 2 1228.79 1408.33 20.77 o 2 4 2 251.92 296.77 9.08 o 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390.79 425.40 10.16 o 3 0 3 1418.18 1500.60 27.02 o 5 0 3 613.14 766.65 15.89 o 7 0 3 6.25 3.57 4.37 < 9 0 3 1326.53 1178.01 23.16 o 11 0 3 339.30 328.15 12.46 o -14 1 3 3.68 11.31 2.37 o -13 1 3 77.30 72.62 3.51 o -12 1 3 116.07 110.01 4.35 o -11 1 3 514.01 533.42 7.75 o -10 1 3 271.27 268.70 5.64 o -9 1 3 1154.17 1061.83 9.81 o -8 1 3 994.79 983.26 9.16 o -7 1 3 2.93 8.17 1.94 o -6 1 3 859.28 786.82 11.98 o -5 1 3 0.84 2.52 3.62 < -4 1 3 1211.54 1278.51 21.67 o -3 1 3 3749.68 3810.00 32.56 o -2 1 3 1920.64 1987.12 19.06 o -1 1 3 1549.26 1461.07 16.35 o 0 1 3 3990.21 3995.79 20.29 o 1 1 3 5615.38 5261.76 22.64 o 2 1 3 618.07 661.83 9.61 o 3 1 3 175.31 171.96 5.77 o 4 1 3 982.27 1048.49 15.10 o 5 1 3 85.75 85.57 4.38 o 6 1 3 127.79 107.99 4.44 o 7 1 3 1.59 -0.91 3.06 < 8 1 3 144.28 157.26 5.98 o 9 1 3 130.84 141.41 7.29 o 10 1 3 3.17 8.29 3.92 < 11 1 3 420.92 431.10 8.99 o 12 1 3 14.79 13.63 2.79 o -14 2 3 45.31 44.20 3.79 o -13 2 3 5.74 8.27 2.42 o -12 2 3 94.77 98.91 4.34 o -11 2 3 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804.94 15.60 o -3 2 4 1817.40 1741.03 21.19 o -2 2 4 1890.29 1886.04 18.77 o -1 2 4 1873.11 1866.26 17.81 o 0 2 4 1994.91 2014.92 19.04 o 1 2 4 210.35 175.51 6.15 o 2 2 4 1040.25 1114.33 14.27 o 3 2 4 5.15 4.31 3.92 < 4 2 4 2340.87 2488.34 18.30 o 5 2 4 1.18 -0.92 2.07 < 6 2 4 556.99 570.59 9.70 o 7 2 4 1.10 7.61 3.82 < 8 2 4 787.64 808.09 11.94 o 9 2 4 210.94 195.24 6.91 o 10 2 4 0.70 -0.70 4.73 < 11 2 4 8.56 10.46 2.99 o 12 2 4 5.64 6.39 2.78 < -14 3 4 0.59 0.86 3.35 < -13 3 4 10.90 7.58 2.53 < -12 3 4 154.45 145.34 4.78 o -11 3 4 828.92 906.44 11.38 o -10 3 4 267.10 268.12 6.90 o -9 3 4 3.77 5.60 2.74 < -8 3 4 1.77 -1.84 2.32 < -7 3 4 30.50 27.80 2.37 o -6 3 4 2154.38 2183.11 13.03 o -5 3 4 247.53 246.21 5.89 o -4 3 4 119.54 101.72 7.47 o -3 3 4 818.36 998.00 18.43 o -2 3 4 982.44 1140.70 17.57 o -1 3 4 1355.28 1534.16 18.53 o 0 3 4 95.05 90.67 5.40 o 1 3 4 29.51 25.11 4.35 o 2 3 4 412.36 455.46 13.28 o 3 3 4 4802.17 5409.54 31.04 o 4 3 4 900.57 943.99 9.37 o 5 3 4 248.45 262.01 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