#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:27:06 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181238 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/16/2231653.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231653_Fobs loop_ _publ_author_name 'Brito, Iv\'an' 'Vallejos, Javier' 'C\'ardenas, Alejandro' 'L\'opez-Rodr\'iguez, Mat\'ias' _publ_section_title ; Propane-1,3-diaminium bis(pyridine-4-carboxylate) monohydrate ; _journal_coeditor_code OM2459 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2423 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 122.669 _cell_angle_gamma 90.000 _cell_length_a 15.3600 _cell_length_b 12.5080 _cell_length_c 10.5930 _exptl_crystal_F_000 720.00 _reflns_d_resolution_high 0.7445 _cod_data_source_file om2459Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kk in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 79.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 365.91 301.86 5.04 o 8 0 0 1658.81 1835.52 28.68 o 10 0 0 874.53 909.96 15.17 o 12 0 0 295.78 287.64 5.40 o 14 0 0 13.14 16.76 1.87 o 16 0 0 141.85 123.64 4.21 o 3 1 0 2520.72 2228.34 34.63 o 5 1 0 648.32 602.53 7.03 o 7 1 0 1266.63 1321.56 14.82 o 9 1 0 583.01 561.70 6.55 o 11 1 0 512.98 515.95 6.63 o 13 1 0 136.90 132.58 2.58 o 15 1 0 24.89 27.21 1.79 o 17 1 0 19.72 18.07 1.75 o 4 2 0 3886.68 3750.41 67.24 o 6 2 0 719.05 789.13 10.49 o 8 2 0 6.10 11.04 0.52 o 10 2 0 0.89 1.27 0.56 o 12 2 0 142.71 139.85 2.66 o 14 2 0 30.55 29.31 1.83 o 16 2 0 273.79 276.20 6.24 o 1 3 0 47.71 97.67 1.83 o 3 3 0 4867.88 4489.49 97.43 o 7 3 0 469.77 418.08 5.80 o 9 3 0 124.57 106.88 1.83 o 11 3 0 176.92 177.58 2.90 o 13 3 0 23.83 24.51 1.47 o 15 3 0 0.01 1.27 1.51 o 17 3 0 3.25 4.09 2.03 o 0 4 0 2473.76 2550.70 56.28 o 2 4 0 375.57 362.79 6.04 o 4 4 0 4.11 1.83 0.60 o 6 4 0 180.20 149.98 2.58 o 8 4 0 988.53 961.47 12.75 o 10 4 0 274.13 276.44 4.17 o 12 4 0 0.33 -0.32 1.23 o 14 4 0 2.05 2.03 1.27 o 16 4 0 75.39 68.20 2.66 o 1 5 0 101.63 89.88 1.91 o 3 5 0 641.01 638.24 10.33 o 5 5 0 296.36 298.84 5.16 o 7 5 0 164.64 162.13 2.82 o 9 5 0 174.53 190.97 2.98 o 11 5 0 3.50 2.98 0.71 o 13 5 0 29.89 34.56 1.63 o 15 5 0 11.38 10.25 1.55 o 2 6 0 2898.02 3288.36 50.88 o 4 6 0 1593.06 1662.11 26.57 o 6 6 0 106.17 98.66 2.34 o 8 6 0 15.47 12.91 0.75 o 10 6 0 53.23 53.50 1.43 o 12 6 0 120.07 119.67 3.10 o 14 6 0 10.09 8.14 1.35 o 16 6 0 23.32 26.69 2.46 o 1 7 0 46.86 78.25 1.71 o 3 7 0 1655.66 1669.70 23.43 o 5 7 0 359.41 395.72 6.79 o 7 7 0 355.72 347.86 5.40 o 9 7 0 746.76 656.43 9.85 o 11 7 0 39.44 35.63 1.83 o 13 7 0 0.07 -0.95 1.39 o 15 7 0 13.62 15.57 1.91 o 0 8 0 646.39 740.36 17.56 o 2 8 0 1257.84 1370.10 21.73 o 4 8 0 0.00 2.62 0.79 o 6 8 0 86.87 69.91 2.14 o 8 8 0 353.46 315.96 8.26 o 10 8 0 315.70 345.55 7.15 o 12 8 0 87.15 83.21 2.50 o 14 8 0 22.95 17.56 2.07 o 1 9 0 397.08 417.25 7.19 o 3 9 0 68.10 70.02 1.87 o 5 9 0 658.95 590.26 11.80 o 7 9 0 766.62 806.41 18.99 o 9 9 0 85.73 108.51 3.69 o 11 9 0 84.70 78.88 2.66 o 13 9 0 4.99 5.76 1.67 o 0 10 0 0.70 4.93 2.90 o 2 10 0 737.06 629.74 15.17 o 4 10 0 195.44 184.10 5.32 o 6 10 0 339.58 299.04 7.82 o 8 10 0 135.78 132.62 4.25 o 10 10 0 10.34 15.01 2.18 o 12 10 0 31.65 36.78 2.58 o 1 11 0 302.89 276.20 7.47 o 3 11 0 743.33 701.35 16.36 o 5 11 0 58.72 72.69 3.34 o 7 11 0 110.37 108.00 4.21 o 9 11 0 414.88 440.96 11.52 o 11 11 0 97.40 101.16 3.93 o 13 11 0 26.85 27.25 2.62 o 0 12 0 497.52 453.03 16.24 o 2 12 0 142.17 125.95 4.21 o 4 12 0 96.39 90.36 3.81 o 6 12 0 108.66 119.12 4.69 o 8 12 0 26.03 30.70 2.98 o 10 12 0 8.13 10.01 2.03 o 12 12 0 38.02 38.73 2.90 o 1 13 0 172.78 172.18 5.24 o 3 13 0 186.93 191.05 6.08 o 5 13 0 176.64 170.95 5.44 o 7 13 0 0.01 1.55 2.11 o 9 13 0 17.19 24.59 2.74 o 11 13 0 132.28 143.46 8.10 o 0 14 0 10.73 15.01 3.10 o 2 14 0 1.64 8.02 2.14 o 4 14 0 0.45 0.00 1.83 o 6 14 0 1.95 4.01 2.38 o 8 14 0 9.51 11.28 1.87 o 1 15 0 78.54 94.73 4.53 o 3 15 0 144.39 154.51 5.52 o 5 15 0 12.95 14.58 2.62 o 7 15 0 41.99 41.31 3.10 o 0 16 0 1.07 -3.18 3.18 o 2 16 0 0.69 0.00 2.90 o 4 16 0 30.55 33.44 3.42 o -17 1 1 3.27 4.05 1.27 o -15 1 1 133.58 133.42 2.90 o -13 1 1 8.09 9.49 0.68 o -11 1 1 213.71 219.49 3.14 o -9 1 1 1739.68 1772.77 19.82 o -7 1 1 1061.86 1099.34 11.76 o -5 1 1 586.04 567.82 6.20 o 5 1 1 0.74 2.42 0.36 o 7 1 1 0.07 0.28 0.40 o 9 1 1 893.56 954.60 11.64 o 11 1 1 248.22 225.60 3.85 o 13 1 1 23.96 18.15 1.51 o 15 1 1 47.31 45.95 2.50 o -16 2 1 159.35 159.35 4.05 o -14 2 1 15.26 16.80 1.43 o -12 2 1 46.23 47.19 1.03 o -10 2 1 179.95 154.15 2.14 o -8 2 1 246.36 261.75 3.22 o -6 2 1 4199.94 4152.48 57.59 o -4 2 1 5801.45 5468.44 166.78 o 0 2 1 888.00 819.16 26.69 o 4 2 1 555.60 564.48 7.51 o 6 2 1 228.57 244.47 3.85 o 8 2 1 1515.82 1526.67 19.70 o 10 2 1 55.87 59.66 1.35 o 12 2 1 62.94 62.00 1.71 o 14 2 1 154.03 151.29 4.09 o 16 2 1 4.65 8.70 2.38 o -17 3 1 1.15 2.26 1.43 o -15 3 1 6.88 7.27 1.19 o -13 3 1 223.88 231.28 4.41 o -11 3 1 50.48 45.60 0.99 o -9 3 1 751.79 809.63 10.13 o -7 3 1 3851.46 3973.94 61.29 o -5 3 1 4914.37 5270.52 165.63 o -3 3 1 2035.69 1964.13 30.70 o 3 3 1 285.62 263.45 4.65 o 5 3 1 4612.75 4846.01 148.51 o 7 3 1 1350.65 1381.38 17.87 o 9 3 1 17.96 21.05 0.91 o 11 3 1 254.06 236.64 4.45 o 13 3 1 38.53 36.30 1.87 o 15 3 1 0.48 2.18 1.83 o -16 4 1 16.93 19.26 1.67 o -14 4 1 2.36 2.90 1.19 o -12 4 1 11.15 10.76 0.87 o -10 4 1 0.03 0.44 0.60 o -8 4 1 344.48 344.28 4.85 o -6 4 1 450.86 430.31 6.55 o -4 4 1 2.53 -0.44 0.64 o -2 4 1 946.73 1124.28 15.85 o 0 4 1 2537.63 2348.09 36.46 o 2 4 1 65.62 66.09 1.51 o 4 4 1 247.94 216.27 3.77 o 6 4 1 1454.11 1478.69 19.50 o 8 4 1 75.71 63.99 1.35 o 10 4 1 191.89 186.88 4.25 o 12 4 1 9.20 8.46 1.35 o 14 4 1 48.18 49.81 2.30 o 16 4 1 0.27 4.69 1.87 o -17 5 1 140.57 121.30 4.29 o -15 5 1 7.51 9.18 1.23 o -13 5 1 38.75 41.07 1.87 o -11 5 1 57.01 53.26 1.39 o -9 5 1 108.45 117.65 1.99 o -7 5 1 41.38 27.21 0.91 o -5 5 1 54.11 70.86 1.55 o -3 5 1 774.30 839.42 13.46 o -1 5 1 484.37 505.78 8.22 o 1 5 1 1639.35 1813.64 28.20 o 3 5 1 635.10 734.04 12.11 o 5 5 1 79.44 74.63 1.79 o 7 5 1 42.08 48.14 1.15 o 9 5 1 1026.27 1036.70 17.00 o 11 5 1 92.78 90.84 2.66 o 13 5 1 24.88 23.83 1.63 o 15 5 1 15.80 18.19 2.14 o -16 6 1 2.07 3.89 1.15 o -14 6 1 3.03 4.41 1.11 o -12 6 1 115.98 107.88 2.90 o -10 6 1 265.70 240.30 3.61 o -8 6 1 1090.47 1104.18 16.05 o -6 6 1 37.53 47.03 1.27 o -4 6 1 38.42 38.61 1.19 o -2 6 1 45.99 56.88 1.35 o 0 6 1 625.09 669.22 10.76 o 2 6 1 56.94 61.64 1.47 o 4 6 1 37.30 18.39 1.03 o 6 6 1 931.92 918.81 15.01 o 8 6 1 202.14 216.23 3.61 o 10 6 1 150.56 143.66 2.98 o 12 6 1 528.10 560.63 13.70 o 14 6 1 0.01 3.77 1.43 o -15 7 1 27.58 34.83 2.42 o -13 7 1 1.96 0.12 1.27 o -11 7 1 90.86 98.46 2.66 o -9 7 1 326.18 310.40 6.36 o -7 7 1 1009.84 923.42 13.58 o -5 7 1 222.39 196.05 3.61 o -3 7 1 0.05 -0.60 0.60 o -1 7 1 114.88 209.44 3.97 o 1 7 1 874.28 896.29 14.70 o 3 7 1 617.70 612.46 9.89 o 5 7 1 92.75 99.42 2.34 o 7 7 1 330.77 314.93 5.60 o 9 7 1 857.74 931.76 18.19 o 11 7 1 0.26 1.35 1.03 o 13 7 1 6.53 0.16 3.02 o -16 8 1 39.58 52.07 3.89 o -14 8 1 21.41 21.89 1.55 o -12 8 1 3.92 5.80 1.19 o -10 8 1 5.24 8.78 1.15 o -8 8 1 771.80 785.20 14.82 o -6 8 1 257.73 232.35 4.25 o -4 8 1 0.94 0.28 0.83 o -2 8 1 1625.44 1655.12 26.17 o 0 8 1 863.46 829.37 13.46 o 2 8 1 71.30 123.13 2.30 o 4 8 1 64.90 56.00 1.75 o 6 8 1 309.52 295.11 7.90 o 8 8 1 1105.72 1114.95 25.22 o 10 8 1 176.48 184.33 4.37 o 12 8 1 52.52 60.53 3.34 o 14 8 1 0.24 1.83 1.75 o -15 9 1 31.55 27.96 2.03 o -13 9 1 58.03 55.25 2.22 o -11 9 1 62.22 62.56 2.30 o -9 9 1 294.76 293.16 7.55 o -5 9 1 1360.08 1315.21 24.82 o -3 9 1 56.78 68.08 1.87 o -1 9 1 48.78 49.25 1.51 o 1 9 1 0.99 -0.79 1.27 o 3 9 1 440.93 464.95 11.08 o 5 9 1 96.52 96.95 3.73 o 7 9 1 94.52 93.18 3.46 o 9 9 1 5.26 7.27 1.03 o 11 9 1 96.44 100.81 4.25 o 13 9 1 0.49 4.61 2.46 o -14 10 1 112.49 98.07 3.73 o -12 10 1 0.33 5.52 1.43 o -10 10 1 35.19 35.11 2.34 o -8 10 1 136.99 130.48 4.09 o -6 10 1 19.22 18.75 2.38 o -4 10 1 6.20 6.63 2.14 o -2 10 1 20.26 9.65 1.79 o 0 10 1 8.15 6.95 1.75 o 2 10 1 23.69 10.57 1.63 o 4 10 1 75.89 74.59 3.06 o 6 10 1 942.20 916.31 21.09 o 8 10 1 213.66 213.97 6.63 o 10 10 1 2.50 6.95 1.03 o 12 10 1 21.81 20.69 2.74 o -13 11 1 55.43 64.74 3.34 o -11 11 1 12.43 8.82 2.18 o -9 11 1 15.93 16.64 2.26 o -7 11 1 85.31 83.81 3.57 o -5 11 1 418.75 404.73 10.45 o -3 11 1 26.30 34.08 2.30 o -1 11 1 58.39 57.99 2.50 o 1 11 1 16.28 17.87 1.87 o 3 11 1 0.04 -0.32 1.35 o 5 11 1 0.05 0.32 1.87 o 7 11 1 16.06 13.03 2.07 o 9 11 1 346.23 340.87 9.49 o 11 11 1 8.28 9.37 2.18 o -12 12 1 132.63 168.69 6.51 o -10 12 1 172.13 177.82 5.80 o -8 12 1 106.11 107.96 4.29 o -6 12 1 1.59 5.72 2.30 o -4 12 1 0.15 -0.48 1.51 o -2 12 1 224.57 195.46 5.52 o 0 12 1 255.99 260.56 7.15 o 2 12 1 227.12 223.10 6.24 o 4 12 1 7.85 8.10 1.75 o 6 12 1 104.80 101.72 4.01 o 8 12 1 54.75 48.62 3.10 o 10 12 1 1.44 5.56 2.30 o -11 13 1 16.00 8.02 2.18 o -9 13 1 11.41 13.50 1.79 o -7 13 1 11.53 8.62 2.14 o -5 13 1 2.76 3.34 1.75 o -3 13 1 272.70 262.66 7.39 o -1 13 1 2.90 0.71 2.03 o 1 13 1 1.10 4.29 1.79 o 3 13 1 339.82 326.25 9.29 o 5 13 1 0.96 2.34 2.66 o 7 13 1 97.73 105.93 4.13 o 9 13 1 2.18 -0.68 2.62 o -10 14 1 7.30 2.70 1.99 o -8 14 1 0.21 3.06 2.26 o -6 14 1 69.17 82.46 3.77 o -4 14 1 2.36 4.29 2.74 o -2 14 1 390.94 389.44 10.29 o 0 14 1 88.23 85.99 3.69 o 2 14 1 2.60 4.33 2.34 o 4 14 1 591.74 596.62 14.78 o 6 14 1 144.11 184.22 6.24 o 8 14 1 4.58 0.75 2.11 o -7 15 1 103.36 132.46 5.04 o -5 15 1 28.26 36.06 3.06 o -3 15 1 92.22 76.38 3.42 o -1 15 1 25.03 23.31 2.74 o 1 15 1 0.01 3.97 2.03 o 3 15 1 19.32 23.00 2.54 o 5 15 1 2.30 -0.36 2.11 o -4 16 1 4.01 7.35 2.58 o -2 16 1 3.58 0.24 2.07 o 0 16 1 121.19 133.73 5.32 o 2 16 1 76.28 67.52 3.42 o 4 16 1 29.32 29.83 3.93 o -18 0 2 75.81 79.68 5.32 o -16 0 2 20.53 25.78 1.95 o -14 0 2 574.11 552.69 10.88 o -12 0 2 835.74 868.73 14.70 o -10 0 2 396.63 377.53 6.47 o -8 0 2 1344.36 1383.33 22.08 o -6 0 2 264.69 163.76 2.54 o -4 0 2 1565.12 1682.92 37.14 o 0 0 2 19.90 14.54 0.71 o 2 0 2 0.46 0.56 0.40 o 4 0 2 166.09 187.27 3.85 o 6 0 2 580.80 633.91 10.45 o 8 0 2 684.65 710.65 11.80 o 10 0 2 343.04 309.93 6.47 o 12 0 2 620.55 605.16 21.21 o 14 0 2 6.44 7.23 2.46 o -17 1 2 63.69 61.72 2.03 o -15 1 2 837.35 835.56 13.98 o -13 1 2 143.14 134.61 2.14 o -11 1 2 393.70 390.36 5.00 o -9 1 2 620.40 643.01 7.15 o -7 1 2 1118.75 1253.96 13.31 o -5 1 2 1021.24 1005.52 12.03 o -3 1 2 1553.45 1467.01 22.84 o 3 1 2 4259.84 4447.87 98.15 o 5 1 2 771.32 792.95 10.60 o 7 1 2 224.05 208.36 3.14 o 9 1 2 60.02 57.67 1.55 o 11 1 2 91.68 96.60 2.78 o 13 1 2 46.88 49.33 2.26 o 15 1 2 6.43 4.61 2.03 o -18 2 2 25.81 20.97 2.94 o -16 2 2 0.67 0.40 0.87 o -14 2 2 62.23 57.39 1.35 o -12 2 2 24.17 28.68 0.83 o -10 2 2 50.75 62.87 1.07 o -8 2 2 84.77 98.94 1.39 o -6 2 2 6291.59 6059.30 185.65 o -4 2 2 1740.37 1354.05 19.34 o -2 2 2 58.97 109.58 1.95 o 0 2 2 70.58 72.41 1.47 o 4 2 2 71.67 91.59 1.75 o 6 2 2 1634.53 1780.39 25.78 o 8 2 2 146.11 125.31 2.38 o 10 2 2 66.37 62.64 1.71 o 12 2 2 3.35 2.74 1.15 o 14 2 2 170.64 154.11 5.68 o -17 3 2 358.02 334.51 9.10 o -15 3 2 493.46 477.22 9.81 o -13 3 2 22.11 25.82 0.87 o -11 3 2 84.07 104.78 1.75 o -9 3 2 161.85 165.39 2.30 o -7 3 2 785.84 802.48 10.60 o -5 3 2 521.26 481.15 7.03 o -3 3 2 722.97 822.22 13.07 o -1 3 2 3480.06 3172.94 49.09 o 1 3 2 2235.96 2022.52 31.66 o 3 3 2 2525.33 2677.01 41.55 o 5 3 2 968.29 1074.23 14.18 o 7 3 2 76.65 73.60 1.63 o 9 3 2 88.21 84.96 2.46 o 11 3 2 158.11 156.73 3.34 o 13 3 2 0.48 1.43 1.19 o 15 3 2 4.35 4.05 2.07 o -18 4 2 21.85 16.13 3.81 o -16 4 2 7.96 7.86 1.75 o -14 4 2 46.14 55.53 1.83 o -12 4 2 34.99 34.99 1.07 o -10 4 2 2194.79 2281.45 32.29 o -8 4 2 267.06 319.86 4.57 o -6 4 2 252.64 264.05 4.05 o -2 4 2 293.17 242.09 4.21 o 0 4 2 383.11 383.92 6.32 o 2 4 2 1780.18 1798.63 28.28 o 4 4 2 28.92 38.17 1.15 o 6 4 2 739.84 775.27 10.25 o 8 4 2 125.80 115.82 2.78 o 10 4 2 86.51 85.44 2.58 o 12 4 2 77.78 74.87 2.46 o 14 4 2 54.49 55.37 3.02 o -17 5 2 14.38 12.59 1.87 o -15 5 2 131.68 127.06 2.90 o -13 5 2 45.51 37.06 1.31 o -11 5 2 12.36 9.85 0.79 o -9 5 2 668.86 687.02 9.45 o -7 5 2 60.28 76.18 1.47 o -5 5 2 6.80 5.56 0.60 o -3 5 2 5655.07 5654.60 172.42 o -1 5 2 4796.63 4660.36 83.17 o 1 5 2 436.57 599.00 9.97 o 3 5 2 1147.62 1285.58 21.09 o 5 5 2 465.18 445.88 7.67 o 7 5 2 336.82 349.41 5.60 o 9 5 2 387.20 359.14 7.43 o 11 5 2 7.85 6.00 2.11 o 13 5 2 30.70 35.07 2.62 o -16 6 2 0.58 5.16 2.03 o -14 6 2 270.82 264.37 5.56 o -12 6 2 11.16 7.15 0.79 o -10 6 2 67.56 81.38 1.67 o -8 6 2 1.30 0.71 0.71 o -6 6 2 16.69 12.07 0.83 o -4 6 2 304.95 333.88 5.64 o -2 6 2 514.91 510.66 8.46 o 0 6 2 227.40 254.40 4.29 o 2 6 2 419.21 483.22 8.26 o 4 6 2 401.48 374.43 6.51 o 6 6 2 100.79 86.90 2.14 o 8 6 2 73.53 76.22 2.11 o 10 6 2 258.80 250.67 6.71 o 12 6 2 3.02 3.10 1.91 o 14 6 2 0.01 7.27 2.07 o -17 7 2 4.87 3.02 2.26 o -15 7 2 31.17 36.54 1.91 o -13 7 2 95.02 86.98 2.54 o -11 7 2 290.59 264.41 4.93 o -9 7 2 265.99 261.23 4.61 o -7 7 2 23.81 25.82 0.99 o -5 7 2 15.60 10.80 0.91 o -3 7 2 13.67 12.35 0.83 o -1 7 2 1349.74 1664.85 26.49 o 3 7 2 45.71 70.38 1.91 o 5 7 2 23.91 23.51 1.51 o 7 7 2 0.38 0.91 0.75 o 9 7 2 40.06 34.20 1.27 o 11 7 2 287.63 303.97 8.70 o 13 7 2 34.96 35.91 3.18 o -16 8 2 2.95 6.67 2.22 o -14 8 2 21.97 26.29 1.59 o -12 8 2 42.96 39.04 1.75 o -10 8 2 27.60 21.45 1.31 o -8 8 2 139.32 116.61 2.50 o -6 8 2 748.06 679.95 10.01 o -4 8 2 34.52 21.29 1.07 o -2 8 2 454.74 456.65 6.95 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178.46 161.26 3.85 o -7 11 2 0.00 -1.59 2.03 o -5 11 2 369.09 356.00 9.10 o -3 11 2 83.50 87.74 3.46 o -1 11 2 453.44 409.26 10.09 o 1 11 2 176.09 133.69 4.37 o 3 11 2 473.66 429.80 10.88 o 5 11 2 102.99 103.67 3.81 o 7 11 2 43.32 50.13 3.06 o 9 11 2 304.24 326.17 9.10 o 11 11 2 0.27 0.64 2.86 o -12 12 2 203.08 211.18 6.24 o -10 12 2 206.78 208.72 5.96 o -8 12 2 212.55 212.81 6.28 o -6 12 2 109.60 98.26 3.69 o -4 12 2 52.95 57.39 3.14 o -2 12 2 361.22 356.12 9.18 o 0 12 2 4.62 7.98 1.91 o 2 12 2 74.69 67.24 3.30 o 4 12 2 25.07 32.05 2.46 o 6 12 2 2.57 2.62 2.22 o 8 12 2 28.28 36.10 3.06 o 10 12 2 7.25 1.07 2.22 o -11 13 2 31.59 32.97 2.62 o -9 13 2 111.13 98.62 3.73 o -7 13 2 110.65 112.64 4.05 o -5 13 2 4.42 0.68 1.71 o -3 13 2 54.44 48.58 2.90 o -1 13 2 174.14 145.05 4.61 o 1 13 2 38.62 38.45 2.46 o 3 13 2 2.22 2.66 2.22 o 5 13 2 5.27 7.35 2.74 o 7 13 2 81.15 90.32 3.81 o 9 13 2 16.64 18.83 2.42 o -10 14 2 43.22 37.49 2.82 o -8 14 2 17.39 17.28 2.18 o -6 14 2 0.23 3.18 2.18 o -4 14 2 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