#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/16/2231665.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231665_Fobs loop_ _publ_author_name 'Zhang, Jinfang' _publ_section_title ; catena-Poly[[tetrakis(hexamethylphosphoramide-\kO)bis(nitrato-\k^2^O,O')yttrium(III)] [silver(I)-di-\m-sulfido-molybdenum(VI)-di-\m-sulfido]] ; _journal_coeditor_code PV2435 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1206 _journal_page_last m1207 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.900 _cell_angle_gamma 90.000 _cell_length_a 15.7770 _cell_length_b 29.6500 _cell_length_c 11.3390 _exptl_crystal_F_000 2583.30 _reflns_d_resolution_high 0.8100 _[local]_cod_data_source_file pv2435Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s in P1 New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 425.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 15987.98 15826.86 211.75 o 5 0 0 14418.12 11611.99 173.44 o 6 0 0 76114.00 71158.85 572.91 o 7 0 0 59152.33 53845.04 796.59 o 8 0 0 6654.54 7152.44 207.59 o 9 0 0 32575.72 34643.31 414.85 o 10 0 0 3020.54 3314.76 301.69 o 11 0 0 13319.79 14358.53 646.49 o 12 0 0 25183.41 26783.30 578.99 o 13 0 0 3202.26 2977.39 555.89 o 14 0 0 683.88 768.37 189.35 o 15 0 0 4279.16 4344.27 298.01 o 16 0 0 13810.76 14370.55 899.63 o 17 0 0 7436.33 8267.38 355.49 o 18 0 0 2113.83 1640.87 520.61 o 19 0 0 8461.68 9185.59 495.98 o 3 1 0 16449.43 17166.18 161.94 o 4 1 0 70415.78 68418.96 372.33 o 5 1 0 3691.51 3807.55 81.07 o 6 1 0 43877.77 42908.12 300.71 o 7 1 0 1198.35 1439.72 80.05 o 8 1 0 98697.84 99333.82 493.16 o 9 1 0 23886.11 24618.27 230.54 o 10 1 0 65507.09 66304.61 417.17 o 11 1 0 9945.46 9652.94 163.38 o 12 1 0 4263.00 4338.26 156.26 o 13 1 0 18294.48 18382.78 333.58 o 14 1 0 10284.19 9658.54 299.07 o 15 1 0 8677.20 8850.86 427.70 o 16 1 0 491.13 431.64 167.16 o 17 1 0 9916.52 10824.43 294.60 o 18 1 0 103.18 71.40 54.01 o 19 1 0 1635.51 1423.51 322.69 o 4 2 0 15196.76 13072.73 132.45 o 5 2 0 125208.89 124237.27 660.46 o 6 2 0 937.50 1038.60 105.67 o 7 2 0 164081.56 162343.56 828.28 o 8 2 0 1668.43 1414.86 110.58 o 9 2 0 94075.17 94653.29 1007.18 o 10 2 0 17738.63 17370.70 267.33 o 11 2 0 20384.68 20887.76 331.80 o 12 2 0 5821.97 5952.41 149.86 o 13 2 0 5022.68 5228.23 217.23 o 14 2 0 12398.35 12220.33 207.87 o 15 2 0 168.55 171.38 44.26 o 16 2 0 10285.08 10753.20 724.91 o 17 2 0 245.32 226.09 72.38 o 18 2 0 5727.95 6210.76 322.27 o 19 2 0 1871.08 1393.88 335.79 o 2 3 0 45882.50 47143.58 365.10 o 4 3 0 4084.28 3951.78 78.48 o 6 3 0 47613.42 47468.07 287.83 o 7 3 0 8618.86 9333.53 166.87 o 8 3 0 58233.29 56028.39 311.90 o 9 3 0 186.70 327.06 43.39 o 10 3 0 7082.75 6863.01 139.01 o 11 3 0 6241.98 6229.54 141.89 o 12 3 0 1222.22 1056.81 102.78 o 13 3 0 573.58 547.48 70.08 o 14 3 0 8704.13 9248.63 336.25 o 15 3 0 3394.47 3409.03 283.10 o 16 3 0 2862.87 2957.02 288.81 o 17 3 0 6405.17 7065.11 317.96 o 18 3 0 12060.88 12876.13 409.59 o 19 3 0 1292.13 752.97 225.53 o 1 4 0 1461.48 1600.90 54.14 o 2 4 0 153514.23 125479.04 1306.78 o 3 4 0 9342.49 9426.01 176.57 o 4 4 0 140.02 177.34 24.36 o 5 4 0 17115.10 16372.58 165.16 o 6 4 0 35.31 67.62 12.41 o 7 4 0 20293.63 20488.12 252.27 o 8 4 0 21226.48 22146.21 304.41 o 9 4 0 46870.73 45641.96 426.38 o 10 4 0 25986.53 26332.60 258.06 o 11 4 0 6918.17 6853.93 159.41 o 12 4 0 6211.19 6136.28 175.94 o 13 4 0 8472.95 8506.95 214.54 o 14 4 0 9191.39 10061.79 378.68 o 15 4 0 686.31 683.95 106.94 o 16 4 0 3744.22 4150.09 280.96 o 17 4 0 138.04 209.71 68.02 o 18 4 0 2230.12 2547.36 431.29 o 19 4 0 82.47 74.93 71.12 o 1 5 0 180974.95 181581.83 396.03 o 2 5 0 5399.63 5092.79 65.95 o 3 5 0 22804.32 22109.60 196.69 o 4 5 0 31866.07 31720.64 270.05 o 5 5 0 39292.08 40243.21 337.52 o 6 5 0 20757.15 19595.29 224.04 o 7 5 0 669.60 799.40 78.78 o 8 5 0 37120.77 35936.40 238.20 o 9 5 0 73.72 89.86 48.92 o 10 5 0 12230.20 12891.25 136.91 o 11 5 0 25612.18 26999.85 337.08 o 12 5 0 13358.84 14535.42 205.85 o 13 5 0 2984.21 2904.08 197.23 o 14 5 0 1738.28 1655.27 188.96 o 15 5 0 9678.11 9561.34 369.43 o 16 5 0 808.70 603.49 89.92 o 17 5 0 1892.06 1857.13 284.39 o 18 5 0 143.13 172.77 63.73 o 19 5 0 1003.81 611.32 204.48 o 0 6 0 96346.17 94436.22 985.16 o 1 6 0 19350.68 19521.13 179.58 o 2 6 0 53638.04 51878.39 741.85 o 3 6 0 3569.69 2781.93 60.60 o 4 6 0 574.63 562.74 48.03 o 5 6 0 21972.77 20865.72 292.14 o 6 6 0 36195.54 34810.48 239.97 o 7 6 0 4167.45 4227.06 99.95 o 8 6 0 3016.55 2858.88 119.36 o 9 6 0 3616.13 3797.93 96.00 o 10 6 0 7376.63 7611.83 146.63 o 11 6 0 3283.14 3062.17 82.73 o 12 6 0 1522.30 1319.36 149.43 o 13 6 0 3200.12 3237.30 365.63 o 14 6 0 10.49 59.47 29.70 o 15 6 0 717.94 564.85 98.17 o 16 6 0 1056.29 831.75 236.41 o 17 6 0 3853.29 4311.37 145.35 o 18 6 0 1332.35 1307.24 234.61 o 19 6 0 1442.72 1077.02 289.38 o 1 7 0 836.05 756.50 33.90 o 2 7 0 6225.84 6283.96 94.37 o 3 7 0 6202.67 7407.32 114.82 o 4 7 0 11498.17 10388.61 214.78 o 5 7 0 1253.25 1724.01 101.78 o 6 7 0 14065.22 12882.38 157.75 o 7 7 0 24.02 61.49 19.92 o 8 7 0 26043.88 25876.08 276.98 o 9 7 0 3926.41 3912.99 83.74 o 10 7 0 7507.04 7722.22 135.28 o 11 7 0 26.53 64.59 18.52 o 12 7 0 153.21 228.33 37.46 o 13 7 0 2597.82 2855.60 156.92 o 14 7 0 752.76 662.80 114.12 o 15 7 0 3042.41 2515.87 215.05 o 16 7 0 44.35 79.31 34.02 o 17 7 0 142.67 183.49 78.12 o 18 7 0 13.56 46.28 102.64 o 19 7 0 557.64 431.02 94.21 o 0 8 0 757.82 722.79 54.66 o 1 8 0 6931.26 6528.01 98.68 o 2 8 0 15537.33 15155.51 147.85 o 3 8 0 3521.49 3031.33 64.31 o 4 8 0 8321.46 7904.42 119.69 o 5 8 0 6603.24 6934.60 133.13 o 6 8 0 1083.00 1074.52 85.32 o 7 8 0 13539.58 13728.68 169.85 o 8 8 0 287.44 383.21 40.02 o 9 8 0 1203.55 1302.51 85.45 o 10 8 0 6502.51 6257.72 117.24 o 11 8 0 1076.22 1163.44 120.37 o 12 8 0 2115.77 1812.07 122.62 o 13 8 0 1923.49 2058.30 217.68 o 14 8 0 3456.57 3106.56 188.02 o 15 8 0 400.73 263.91 52.80 o 16 8 0 1448.35 1496.30 226.73 o 17 8 0 710.59 691.07 128.37 o 18 8 0 2.99 53.20 47.89 o 19 8 0 41.52 138.40 59.12 o 1 9 0 931.88 994.00 70.88 o 2 9 0 133.22 183.30 22.12 o 3 9 0 6113.47 5522.76 89.54 o 4 9 0 13856.08 14667.79 150.32 o 5 9 0 7657.81 7283.64 149.89 o 6 9 0 2943.77 2599.98 93.24 o 7 9 0 6978.34 7174.56 134.98 o 8 9 0 21072.32 21707.14 201.35 o 9 9 0 560.00 557.13 50.89 o 10 9 0 342.90 303.10 46.30 o 11 9 0 1332.30 1379.99 120.55 o 12 9 0 63.43 109.99 26.46 o 13 9 0 1142.56 1378.25 186.99 o 14 9 0 347.44 283.13 65.04 o 15 9 0 818.18 710.40 115.16 o 16 9 0 308.92 235.10 74.95 o 17 9 0 52.63 97.70 52.15 o 18 9 0 556.00 382.05 123.92 o 0 10 0 18321.98 18996.38 656.72 o 1 10 0 99.30 155.61 18.80 o 2 10 0 1149.55 845.76 72.70 o 3 10 0 17117.24 17783.92 177.56 o 4 10 0 794.18 1005.01 49.92 o 5 10 0 3761.70 3793.38 89.58 o 6 10 0 7086.91 7136.75 187.79 o 7 10 0 6706.85 6773.04 126.55 o 8 10 0 148.79 309.77 38.70 o 9 10 0 2987.18 2843.85 82.53 o 10 10 0 8203.76 8430.16 162.25 o 11 10 0 401.53 427.82 62.21 o 12 10 0 74.64 60.59 22.64 o 13 10 0 3804.25 3886.21 141.52 o 14 10 0 3163.84 2998.67 154.89 o 15 10 0 129.48 105.12 31.61 o 16 10 0 54.50 26.08 46.38 o 17 10 0 159.69 160.27 80.77 o 18 10 0 148.07 218.18 100.27 o 1 11 0 277.72 438.30 41.18 o 2 11 0 615.10 595.29 127.33 o 3 11 0 374.61 391.27 63.67 o 4 11 0 9658.44 9180.79 162.47 o 5 11 0 168.09 234.96 27.05 o 6 11 0 14689.00 15374.24 186.31 o 7 11 0 48.13 81.45 26.68 o 8 11 0 449.78 612.10 57.68 o 9 11 0 387.67 361.89 46.55 o 10 11 0 208.62 248.13 34.06 o 11 11 0 216.82 255.22 38.97 o 12 11 0 2776.24 2958.63 140.59 o 13 11 0 1975.90 1768.19 177.21 o 14 11 0 157.18 154.05 40.56 o 15 11 0 403.64 282.22 112.60 o 16 11 0 426.11 398.06 85.65 o 17 11 0 321.85 306.68 78.86 o 18 11 0 317.43 231.29 94.70 o 0 12 0 6343.15 6095.85 157.49 o 1 12 0 12602.48 12395.01 146.97 o 2 12 0 3441.58 3304.18 88.95 o 3 12 0 161.46 111.36 22.55 o 4 12 0 40259.86 42035.98 278.22 o 5 12 0 476.42 282.24 35.31 o 6 12 0 15044.19 15405.64 198.38 o 7 12 0 8570.17 9068.88 231.94 o 8 12 0 6468.08 6281.06 127.55 o 9 12 0 10622.53 10888.14 169.95 o 10 12 0 15758.31 16178.56 258.85 o 11 12 0 920.83 1266.74 114.52 o 12 12 0 134.32 245.41 49.45 o 13 12 0 5386.11 5496.83 238.68 o 14 12 0 56.24 92.84 96.77 o 15 12 0 1104.52 987.22 303.07 o 16 12 0 1945.16 2093.49 125.15 o 17 12 0 2063.73 1323.57 329.79 o 18 12 0 233.68 264.70 153.39 o 1 13 0 7018.11 7583.74 164.29 o 2 13 0 1351.49 1339.20 44.58 o 3 13 0 22.67 64.92 27.74 o 4 13 0 22731.84 23429.32 283.49 o 5 13 0 1425.41 1636.24 71.55 o 6 13 0 23.70 68.14 32.30 o 7 13 0 1418.64 1297.24 58.96 o 8 13 0 5883.71 6103.93 108.00 o 9 13 0 912.88 969.03 96.10 o 10 13 0 120.03 194.97 54.40 o 11 13 0 1931.99 1803.15 80.70 o 12 13 0 1260.20 1465.49 129.61 o 13 13 0 293.14 160.50 61.25 o 14 13 0 2156.71 2210.02 203.56 o 15 13 0 2621.95 2601.84 120.37 o 16 13 0 397.89 290.27 93.49 o 17 13 0 2165.87 2413.81 1585.46 o 18 13 0 1112.33 879.51 351.19 o 0 14 0 6915.44 6604.04 171.96 o 1 14 0 881.38 1321.62 97.35 o 2 14 0 5372.27 5233.25 99.69 o 3 14 0 8178.68 8168.14 143.17 o 4 14 0 1002.79 1105.41 81.15 o 5 14 0 2699.09 2291.31 84.46 o 6 14 0 2038.19 2078.08 121.62 o 7 14 0 314.95 379.66 41.86 o 8 14 0 9254.36 9575.71 194.71 o 9 14 0 3469.22 3525.70 158.91 o 10 14 0 456.54 398.72 52.22 o 11 14 0 621.41 672.01 120.69 o 12 14 0 2602.37 2722.44 119.27 o 13 14 0 1311.91 971.38 151.38 o 14 14 0 1197.80 1176.62 176.54 o 15 14 0 968.76 868.94 200.86 o 16 14 0 7.55 20.86 37.87 o 17 14 0 841.39 703.91 287.93 o 1 15 0 10261.12 11971.79 205.91 o 2 15 0 585.00 750.40 65.24 o 3 15 0 17890.57 17505.53 368.62 o 4 15 0 2303.77 2083.56 61.39 o 5 15 0 13649.40 14063.14 188.63 o 6 15 0 328.74 346.00 64.52 o 7 15 0 5347.89 5443.46 128.85 o 8 15 0 8801.78 8765.82 238.34 o 9 15 0 3867.35 3867.65 248.87 o 10 15 0 3693.40 4067.18 126.05 o 11 15 0 303.09 282.55 53.03 o 12 15 0 3699.87 3435.54 271.74 o 13 15 0 253.17 180.82 34.64 o 14 15 0 3512.16 3717.29 155.67 o 15 15 0 654.77 692.50 91.91 o 16 15 0 2185.24 2287.12 630.17 o 17 15 0 1289.74 884.46 471.43 o 0 16 0 45802.82 48678.80 379.94 o 1 16 0 3447.76 3282.05 64.37 o 2 16 0 6200.40 6327.32 121.42 o 3 16 0 9285.32 9221.84 134.34 o 4 16 0 2483.25 2643.36 69.55 o 5 16 0 468.48 507.54 60.39 o 6 16 0 1443.39 1562.20 65.92 o 7 16 0 1034.85 1044.34 75.42 o 8 16 0 627.29 661.41 72.55 o 9 16 0 29.43 41.89 34.30 o 10 16 0 244.14 373.82 56.79 o 11 16 0 56.07 38.92 28.43 o 12 16 0 12.68 18.46 33.73 o 13 16 0 3670.03 3631.88 507.28 o 14 16 0 206.12 333.88 135.10 o 15 16 0 18.76 -2.14 60.62 o 16 16 0 34.44 126.76 100.85 o 17 16 0 1408.94 1048.04 379.81 o 1 17 0 7434.48 7659.12 136.01 o 2 17 0 106.31 195.23 30.99 o 3 17 0 2465.20 2581.88 76.14 o 4 17 0 82.96 149.19 22.99 o 5 17 0 384.85 377.14 38.46 o 6 17 0 2034.29 2082.72 73.80 o 7 17 0 3215.62 3123.46 75.97 o 8 17 0 2268.33 2486.84 61.82 o 9 17 0 69.21 139.40 24.12 o 10 17 0 308.00 274.94 41.51 o 11 17 0 262.99 328.81 63.38 o 12 17 0 260.99 220.27 48.97 o 13 17 0 179.43 267.22 141.95 o 14 17 0 472.68 309.48 73.66 o 15 17 0 983.15 1463.75 538.83 o 16 17 0 113.69 209.81 97.45 o 17 17 0 11.28 -51.29 139.95 o 0 18 0 8842.09 9339.48 192.50 o 1 18 0 57.49 84.52 29.75 o 2 18 0 2643.65 2549.02 100.30 o 3 18 0 215.53 282.04 36.21 o 4 18 0 8817.79 9332.06 217.25 o 5 18 0 6904.69 6791.69 118.90 o 6 18 0 657.62 733.64 79.34 o 7 18 0 8339.08 8409.63 176.88 o 8 18 0 842.35 934.62 74.72 o 9 18 0 5349.58 5704.52 166.37 o 10 18 0 1476.41 1602.17 108.36 o 11 18 0 2684.75 2794.88 90.97 o 12 18 0 49.74 47.82 18.18 o 13 18 0 3214.79 3211.43 124.38 o 14 18 0 1386.42 1355.52 74.70 o 15 18 0 1710.55 1335.30 619.00 o 1 19 0 12676.76 13500.19 142.58 o 2 19 0 7751.01 7418.67 151.62 o 3 19 0 1492.13 1681.01 100.04 o 4 19 0 661.66 709.94 70.84 o 5 19 0 4024.46 4144.55 200.63 o 6 19 0 12169.86 11711.47 217.70 o 7 19 0 36.74 25.73 19.99 o 8 19 0 4762.04 4925.32 254.97 o 9 19 0 690.36 563.80 95.62 o 10 19 0 3653.19 3417.35 111.34 o 11 19 0 239.62 276.07 43.80 o 12 19 0 15.27 37.14 27.47 o 13 19 0 133.03 212.58 50.93 o 14 19 0 412.13 648.12 146.00 o 15 19 0 262.95 279.01 99.40 o 16 19 0 855.49 832.64 516.13 o 0 20 0 18773.25 18381.90 470.20 o 1 20 0 2.55 49.06 20.20 o 2 20 0 20921.23 20793.10 254.32 o 3 20 0 3560.06 3562.57 138.60 o 4 20 0 13873.25 14582.10 197.53 o 5 20 0 112.46 93.91 35.62 o 6 20 0 574.54 501.78 54.34 o 7 20 0 1307.82 1384.60 107.19 o 8 20 0 794.57 855.24 88.39 o 9 20 0 1639.52 1851.88 66.32 o 10 20 0 486.44 399.35 55.68 o 11 20 0 15.72 54.76 92.87 o 12 20 0 625.07 538.71 75.50 o 13 20 0 285.89 218.00 52.57 o 14 20 0 1404.81 1356.39 463.05 o 15 20 0 281.80 235.61 104.19 o 1 21 0 2681.66 2765.52 104.17 o 2 21 0 869.68 961.07 104.65 o 3 21 0 4778.88 4842.24 94.43 o 4 21 0 4431.32 4435.72 221.14 o 5 21 0 87.08 107.00 24.42 o 6 21 0 13539.17 14220.48 285.71 o 7 21 0 175.83 197.46 44.78 o 8 21 0 1754.43 2084.41 111.95 o 9 21 0 12515.30 12393.25 272.47 o 10 21 0 9074.94 9810.91 358.21 o 11 21 0 5663.36 6166.35 370.30 o 12 21 0 2722.80 2848.04 189.71 o 13 21 0 8134.29 9426.65 347.45 o 14 21 0 4761.99 5652.73 267.71 o 15 21 0 4030.39 4513.59 326.11 o 0 22 0 21953.10 21763.90 475.61 o 1 22 0 1030.01 1199.74 107.89 o 2 22 0 5297.51 5321.58 174.49 o 3 22 0 5551.39 5699.51 135.32 o 4 22 0 10140.18 10934.10 164.86 o 5 22 0 5223.21 5269.03 190.22 o 6 22 0 2987.45 2595.29 158.40 o 7 22 0 9725.24 10412.81 338.40 o 8 22 0 68.26 7.00 19.75 o 9 22 0 1269.73 1164.72 85.33 o 10 22 0 17.22 36.33 73.58 o 11 22 0 904.42 920.74 130.97 o 12 22 0 2762.94 3410.59 606.27 o 13 22 0 126.01 -72.04 158.52 o 14 22 0 1521.38 1430.69 343.21 o 15 22 0 708.04 532.22 152.55 o 1 23 0 9951.75 10635.18 156.74 o 2 23 0 446.73 577.84 55.16 o 3 23 0 15490.55 15610.65 225.86 o 4 23 0 24308.60 23292.51 392.52 o 5 23 0 3776.88 3776.33 166.93 o 6 23 0 8070.42 8590.77 200.26 o 7 23 0 6559.49 6871.57 204.94 o 8 23 0 10061.75 10153.14 223.11 o 9 23 0 65.82 89.54 34.75 o 10 23 0 2109.98 2552.88 626.50 o 11 23 0 40.76 -71.11 165.29 o 12 23 0 439.12 330.40 99.23 o 13 23 0 1840.16 2054.04 666.40 o 14 23 0 28.79 -4.57 148.91 o 0 24 0 4526.49 4688.06 227.15 o 1 24 0 2265.59 2272.58 143.94 o 2 24 0 3090.33 3449.90 162.52 o 3 24 0 9737.46 9825.03 184.68 o 4 24 0 2506.12 2013.11 279.35 o 5 24 0 32295.34 33272.55 530.08 o 6 24 0 337.22 243.78 54.20 o 7 24 0 16279.29 16454.86 453.96 o 8 24 0 7964.38 8726.04 468.56 o 9 24 0 8737.93 9441.09 297.41 o 10 24 0 7216.94 7453.04 504.13 o 11 24 0 4674.63 5954.01 751.16 o 12 24 0 14206.15 15505.01 4266.65 o 13 24 0 3643.95 3250.69 742.72 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