#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:27:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181239 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/17/2231743.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231743_Fobs loop_ _publ_author_name 'Asiri, Abdullah M.' 'Faidallah, Hassan M.' 'Al-Youbi, Abdulrahman O.' 'Alamry, Khalid A.' 'Ng, Seik Weng' _publ_section_title ; 2-Oxo-4-phenyl-1,2,5,6-tetrahydrobenzo[h]quinoline-3-carbonitrile ; _journal_coeditor_code XU5290 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2468 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 77.001 _cell_angle_beta 74.348 _cell_angle_gamma 81.674 _cell_length_a 7.4075 _cell_length_b 9.7204 _cell_length_c 10.7358 _exptl_crystal_F_000 312.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file xu5290Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 69.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1150.89 1065.83 4.40 o 2 0 0 4.68 2.22 0.20 o 3 0 0 826.96 810.34 12.60 o 4 0 0 136.35 150.09 6.48 o 5 0 0 615.82 566.22 7.75 o 6 0 0 142.20 135.12 3.03 o 7 0 0 17.72 20.92 1.53 o 8 0 0 61.86 70.86 1.45 o -8 1 0 73.95 80.50 1.86 o -7 1 0 179.80 185.66 3.49 o -6 1 0 192.33 202.42 5.65 o -5 1 0 37.55 34.07 1.37 o -4 1 0 4.11 24.60 1.38 o -3 1 0 23.10 20.09 0.80 o -2 1 0 737.13 698.31 3.83 o -1 1 0 44.31 40.44 0.97 o 0 1 0 1259.29 1038.43 8.33 o 2 1 0 419.84 361.40 1.94 o 3 1 0 381.76 412.81 2.40 o 4 1 0 3.39 2.44 0.33 o 5 1 0 309.62 298.84 5.62 o 6 1 0 790.18 772.29 11.65 o 7 1 0 284.18 282.46 4.45 o 8 1 0 41.91 45.23 1.55 o -8 2 0 30.16 31.53 1.07 o -7 2 0 48.82 54.10 2.87 o -6 2 0 0.47 0.18 0.19 o -5 2 0 1.09 0.81 0.27 o -4 2 0 93.49 98.48 3.06 o -3 2 0 2975.04 3035.79 14.69 o -2 2 0 1124.37 1117.61 7.61 o -1 2 0 101.59 101.12 2.32 o 0 2 0 163.71 174.65 1.53 o 1 2 0 1106.15 961.92 4.28 o 2 2 0 242.80 208.35 3.87 o 3 2 0 27.03 26.50 0.90 o 4 2 0 21.03 29.09 1.11 o 5 2 0 0.34 0.72 0.53 o 6 2 0 1259.38 1192.54 13.23 o 7 2 0 143.24 142.25 3.29 o 8 2 0 28.11 29.72 1.24 o -8 3 0 34.08 41.31 1.79 o -7 3 0 18.00 18.99 1.05 o -6 3 0 1.84 1.37 0.56 o -5 3 0 0.18 0.26 0.17 o -4 3 0 161.51 156.44 4.22 o -3 3 0 31.93 27.22 1.57 o -2 3 0 1293.47 1358.68 9.46 o -1 3 0 464.45 441.27 2.15 o 0 3 0 16.40 12.63 0.80 o 1 3 0 413.78 388.06 3.31 o 2 3 0 780.56 749.93 7.02 o 3 3 0 236.81 254.62 3.35 o 4 3 0 477.39 507.24 4.75 o 5 3 0 133.29 130.51 2.29 o 6 3 0 10.46 7.73 0.93 o 7 3 0 13.03 11.32 0.96 o 8 3 0 112.24 110.77 2.87 o -7 4 0 25.85 29.62 1.24 o -6 4 0 213.40 185.55 5.35 o -5 4 0 59.58 50.84 1.60 o -4 4 0 2.82 2.29 0.47 o -3 4 0 1.55 2.02 0.51 o -2 4 0 81.98 91.53 2.73 o -1 4 0 45.56 41.60 1.58 o 0 4 0 19.19 20.59 0.78 o 1 4 0 153.94 151.40 2.33 o 2 4 0 47.21 58.91 1.53 o 3 4 0 54.92 60.94 1.56 o 4 4 0 303.72 346.06 6.11 o 5 4 0 0.25 0.15 0.18 o 6 4 0 0.89 0.63 0.28 o 7 4 0 79.16 72.00 2.30 o 8 4 0 28.31 22.36 1.02 o -7 5 0 3.62 2.22 0.32 o -6 5 0 18.35 17.40 1.51 o -5 5 0 126.26 92.80 3.51 o -4 5 0 94.97 86.82 2.37 o -3 5 0 28.87 33.68 2.08 o -2 5 0 101.65 96.25 3.10 o -1 5 0 32.20 30.13 1.50 o 0 5 0 253.01 265.67 3.69 o 1 5 0 716.96 679.03 32.20 o 2 5 0 77.21 81.14 3.05 o 3 5 0 283.62 278.65 5.74 o 4 5 0 527.81 525.87 5.82 o 5 5 0 2.01 1.30 0.28 o 6 5 0 0.44 0.35 0.25 o 7 5 0 0.42 0.27 0.24 o 8 5 0 92.35 101.49 2.65 o -7 6 0 0.13 0.91 0.25 o -6 6 0 12.49 14.68 1.16 o -5 6 0 0.04 0.44 0.24 o -4 6 0 0.10 -0.26 0.26 o -3 6 0 12.30 12.92 0.81 o -2 6 0 269.57 258.75 4.10 o -1 6 0 205.32 189.99 4.12 o 1 6 0 1384.18 1475.55 15.26 o 2 6 0 1.17 0.44 0.39 o 3 6 0 4.94 3.35 0.51 o 4 6 0 47.22 45.11 1.83 o 5 6 0 76.25 74.36 2.35 o 6 6 0 35.73 32.04 1.53 o 7 6 0 40.84 40.66 2.14 o -6 7 0 86.94 74.68 2.57 o -5 7 0 40.28 40.28 2.66 o -4 7 0 106.00 102.88 5.34 o -3 7 0 454.80 447.00 6.28 o -2 7 0 84.11 80.80 1.97 o -1 7 0 14.85 16.21 0.76 o 0 7 0 2.24 1.55 0.59 o 1 7 0 77.42 86.01 2.48 o 2 7 0 92.68 82.32 2.00 o 3 7 0 9.56 9.14 0.67 o 4 7 0 0.29 0.05 0.40 o 5 7 0 28.51 29.18 2.17 o 6 7 0 43.03 45.35 2.49 o 7 7 0 65.40 65.74 2.36 o -4 8 0 77.87 83.13 2.65 o -3 8 0 0.20 0.12 0.32 o -2 8 0 715.14 726.67 7.82 o -1 8 0 48.96 54.77 2.03 o 0 8 0 35.73 31.03 1.66 o 1 8 0 85.00 82.90 2.62 o 2 8 0 0.45 2.03 0.42 o 3 8 0 18.99 22.55 1.27 o 4 8 0 93.63 93.84 3.91 o 5 8 0 25.38 26.82 1.96 o 6 8 0 23.16 23.56 1.59 o 7 8 0 198.50 182.10 3.06 o -5 9 0 0.23 -0.07 0.18 o -4 9 0 0.04 0.25 0.28 o -3 9 0 61.34 63.93 2.73 o -2 9 0 54.90 61.03 2.16 o -1 9 0 478.74 488.52 5.93 o 0 9 0 0.05 0.06 0.29 o 1 9 0 3.10 3.08 0.55 o 2 9 0 24.08 26.35 1.43 o 3 9 0 143.05 154.44 3.63 o 4 9 0 25.44 24.96 1.87 o 5 9 0 135.31 138.62 3.87 o 6 9 0 47.73 48.22 1.79 o -3 10 0 0.13 1.01 0.38 o -2 10 0 125.89 137.15 4.24 o -1 10 0 229.39 259.01 6.07 o 0 10 0 4.91 5.24 0.91 o 1 10 0 56.88 49.23 1.84 o 2 10 0 7.34 8.72 0.75 o 3 10 0 4.54 3.44 0.42 o 4 10 0 223.03 218.05 4.58 o 5 10 0 263.23 264.40 4.08 o -2 11 0 4.80 5.15 0.62 o -1 11 0 4.18 5.47 0.73 o 0 11 0 2.63 3.12 0.58 o 1 11 0 22.89 21.79 1.37 o 2 11 0 5.45 2.63 0.44 o 3 11 0 46.70 48.81 1.80 o -1 -11 1 2.33 2.23 0.41 o 0 -11 1 95.65 97.00 2.67 o 1 -11 1 34.81 34.61 1.60 o 2 -11 1 20.73 23.19 1.17 o -4 -10 1 75.30 81.31 2.55 o -3 -10 1 51.50 51.41 2.34 o -2 -10 1 159.63 149.76 2.76 o -1 -10 1 0.50 0.47 0.24 o 0 -10 1 4.31 4.84 0.82 o 1 -10 1 3.55 4.63 0.82 o 2 -10 1 47.77 51.37 2.47 o 3 -10 1 6.29 5.01 0.71 o -5 -9 1 19.65 18.55 1.30 o -4 -9 1 4.82 5.10 0.84 o -3 -9 1 234.66 235.16 5.94 o -2 -9 1 269.79 277.57 4.82 o -1 -9 1 4.54 3.60 0.57 o 0 -9 1 48.31 45.93 1.98 o 1 -9 1 359.88 369.94 7.70 o 2 -9 1 66.32 67.88 2.20 o 3 -9 1 28.47 31.96 2.21 o 4 -9 1 61.44 61.88 2.69 o 5 -9 1 130.20 127.66 2.45 o -6 -8 1 3.00 1.78 0.45 o -5 -8 1 13.65 12.42 1.28 o -4 -8 1 11.27 10.85 1.32 o -3 -8 1 55.67 54.01 3.01 o -2 -8 1 0.42 1.00 0.65 o -1 -8 1 0.76 0.31 0.37 o 0 -8 1 64.89 66.69 2.41 o 1 -8 1 9.79 8.31 1.20 o 2 -8 1 6.99 7.72 0.99 o 3 -8 1 827.02 824.02 8.31 o 4 -8 1 1.98 2.02 0.46 o 5 -8 1 4.54 5.40 0.78 o 6 -8 1 25.47 22.00 1.02 o -7 -7 1 26.58 22.42 1.17 o -6 -7 1 24.04 23.66 1.66 o -5 -7 1 55.33 53.45 2.85 o -4 -7 1 405.75 409.31 8.16 o -3 -7 1 369.76 357.42 5.41 o -2 -7 1 228.58 226.16 3.32 o -1 -7 1 28.88 32.67 1.52 o 0 -7 1 52.05 60.97 2.15 o 1 -7 1 6.97 6.37 0.56 o 2 -7 1 689.78 694.76 7.19 o 3 -7 1 236.14 243.12 4.54 o 4 -7 1 86.53 87.40 2.83 o 5 -7 1 2.33 2.23 0.61 o 6 -7 1 0.54 0.82 0.35 o -7 -6 1 74.00 68.48 2.45 o -6 -6 1 17.53 17.82 1.32 o -5 -6 1 15.46 16.93 1.10 o -4 -6 1 18.75 18.15 1.20 o -3 -6 1 47.45 45.68 1.85 o -2 -6 1 5.45 4.60 0.91 o -1 -6 1 131.92 147.39 5.04 o 1 -6 1 60.32 67.16 2.38 o 2 -6 1 216.59 222.30 3.00 o 3 -6 1 9.86 10.99 0.75 o 4 -6 1 10.34 10.90 1.00 o 5 -6 1 62.83 48.67 2.12 o 6 -6 1 3.36 4.53 0.49 o 7 -6 1 5.48 6.56 0.65 o -7 -5 1 76.38 73.31 2.02 o -6 -5 1 7.27 7.07 0.75 o -5 -5 1 69.09 61.19 2.56 o -4 -5 1 221.03 221.39 3.09 o -3 -5 1 73.12 74.21 3.15 o -2 -5 1 0.86 0.61 0.38 o -1 -5 1 0.36 4.51 0.82 o 0 -5 1 9.85 9.93 0.70 o 1 -5 1 39.98 52.21 1.95 o 2 -5 1 154.04 150.69 3.86 o 3 -5 1 32.51 35.37 1.49 o 4 -5 1 33.06 34.60 1.10 o 5 -5 1 24.81 24.21 1.13 o 6 -5 1 15.97 13.40 1.32 o 7 -5 1 25.83 26.34 1.07 o -8 -4 1 57.74 53.84 1.32 o -7 -4 1 0.64 0.68 0.30 o -6 -4 1 0.18 0.67 0.25 o -5 -4 1 10.49 9.41 0.58 o -4 -4 1 92.92 99.38 3.50 o -3 -4 1 107.85 122.34 3.62 o -2 -4 1 47.55 49.26 2.23 o -1 -4 1 10.73 12.42 0.64 o 0 -4 1 29.83 27.70 1.36 o 1 -4 1 32.55 34.31 0.88 o 2 -4 1 170.61 182.61 3.89 o 3 -4 1 13.49 10.67 1.08 o 4 -4 1 6.59 5.17 0.59 o 5 -4 1 40.38 35.32 1.33 o 6 -4 1 88.50 66.80 3.17 o 7 -4 1 32.05 26.04 1.22 o -8 -3 1 13.99 15.94 0.79 o -7 -3 1 19.35 16.95 1.09 o -6 -3 1 23.77 26.66 1.19 o -5 -3 1 0.01 -0.01 0.17 o -4 -3 1 233.89 242.17 5.09 o -3 -3 1 52.05 58.95 2.27 o -2 -3 1 377.00 365.03 3.27 o -1 -3 1 29.30 24.55 0.51 o 0 -3 1 158.24 156.33 2.03 o 1 -3 1 411.68 421.76 3.64 o 2 -3 1 14.67 11.29 0.52 o 3 -3 1 211.84 220.61 4.46 o 4 -3 1 109.12 106.03 3.46 o 5 -3 1 0.88 0.75 0.29 o 6 -3 1 45.82 31.87 2.30 o 7 -3 1 167.65 143.68 3.05 o 8 -3 1 3.86 3.95 0.60 o -8 -2 1 1.10 0.64 0.22 o -7 -2 1 5.30 5.35 0.64 o -6 -2 1 0.08 0.59 0.35 o -5 -2 1 133.47 127.48 4.71 o -4 -2 1 8.63 9.09 0.61 o -3 -2 1 136.61 139.76 4.11 o -2 -2 1 887.96 896.27 11.85 o -1 -2 1 64.63 66.60 0.85 o 0 -2 1 15.50 16.16 0.56 o 1 -2 1 83.76 100.10 1.70 o 3 -2 1 261.48 288.90 4.63 o 4 -2 1 161.24 161.61 3.95 o 5 -2 1 217.28 225.75 7.41 o 6 -2 1 98.61 96.10 2.69 o 7 -2 1 5.59 6.49 0.68 o 8 -2 1 0.01 0.18 0.31 o -8 -1 1 1.04 1.49 0.28 o -7 -1 1 277.66 270.91 3.43 o -6 -1 1 1343.52 1320.07 13.17 o -5 -1 1 5.63 4.21 0.55 o -4 -1 1 36.79 32.84 1.70 o -3 -1 1 968.09 990.92 5.08 o -2 -1 1 131.68 135.30 2.36 o -1 -1 1 826.90 810.15 2.01 o 0 -1 1 282.13 242.15 2.82 o 1 -1 1 32.81 37.31 0.96 o 2 -1 1 834.57 816.89 6.12 o 3 -1 1 368.21 390.74 3.55 o 4 -1 1 85.06 99.91 2.48 o 5 -1 1 215.66 210.23 4.53 o 6 -1 1 0.62 0.83 0.39 o 7 -1 1 10.48 10.08 1.28 o 8 -1 1 0.03 0.07 0.28 o -8 0 1 40.94 43.57 1.84 o -7 0 1 13.49 13.98 0.79 o -6 0 1 936.69 920.15 11.54 o -5 0 1 411.11 406.14 4.08 o -4 0 1 3.37 3.62 0.48 o -3 0 1 164.21 155.52 2.69 o -2 0 1 3.24 8.70 0.38 o -1 0 1 861.43 775.44 3.72 o 0 0 1 668.30 556.60 8.04 o 1 0 1 20.76 20.61 0.68 o 2 0 1 579.10 527.67 4.74 o 3 0 1 105.83 121.85 2.88 o 4 0 1 0.27 1.43 0.26 o 5 0 1 246.28 235.44 5.82 o 6 0 1 169.06 161.50 2.66 o 7 0 1 40.73 44.07 1.76 o 8 0 1 22.15 18.93 0.98 o -8 1 1 128.90 131.16 3.28 o -7 1 1 28.38 29.15 1.38 o -6 1 1 486.50 501.51 8.88 o -5 1 1 27.49 25.45 1.84 o -4 1 1 36.70 46.79 1.95 o -3 1 1 438.71 431.45 5.14 o -2 1 1 0.25 0.24 0.13 o 0 1 1 199.02 190.67 1.78 o 1 1 1 25.52 20.82 1.36 o 2 1 1 0.09 0.36 0.21 o 3 1 1 161.29 154.06 3.30 o 4 1 1 92.30 100.00 1.47 o 5 1 1 52.37 50.61 1.69 o 6 1 1 95.99 93.25 2.02 o 7 1 1 152.84 155.75 3.34 o 8 1 1 0.50 0.89 0.23 o -8 2 1 115.98 146.09 3.37 o -7 2 1 27.73 27.07 1.99 o -6 2 1 81.54 84.52 3.71 o -5 2 1 181.64 173.17 3.32 o -4 2 1 24.66 21.89 1.49 o -3 2 1 57.50 72.14 2.33 o -2 2 1 646.22 666.55 6.00 o -1 2 1 817.17 750.39 5.24 o 0 2 1 1550.66 1379.14 5.72 o 1 2 1 427.63 435.11 2.68 o 2 2 1 1487.66 1345.91 8.03 o 3 2 1 157.00 161.45 1.38 o 4 2 1 320.86 314.87 10.20 o 5 2 1 0.21 0.29 0.24 o 6 2 1 90.02 86.58 2.03 o 7 2 1 116.08 115.03 4.27 o 8 2 1 75.08 84.97 2.22 o -8 3 1 13.14 17.75 1.08 o -7 3 1 6.82 6.72 1.02 o -6 3 1 5.86 4.63 0.94 o -5 3 1 4.28 4.78 0.59 o -4 3 1 53.49 59.70 2.66 o -3 3 1 4.01 5.56 0.74 o -2 3 1 1005.57 1096.24 8.69 o -1 3 1 373.59 355.32 4.19 o 0 3 1 329.32 306.15 3.21 o 1 3 1 429.53 439.70 2.91 o 2 3 1 12.37 14.04 0.68 o 3 3 1 116.21 126.78 2.18 o 4 3 1 627.83 655.22 5.59 o 5 3 1 5.81 4.03 0.43 o 6 3 1 2.72 3.86 0.55 o 7 3 1 456.02 464.94 9.02 o 8 3 1 243.45 251.51 3.80 o -7 4 1 9.95 9.64 1.06 o -6 4 1 0.05 0.22 0.35 o -5 4 1 2.00 3.15 0.51 o -4 4 1 53.89 63.62 1.67 o -3 4 1 191.02 212.65 4.90 o -2 4 1 17.73 19.50 1.30 o -1 4 1 208.80 204.00 3.61 o 0 4 1 79.58 75.47 1.84 o 1 4 1 652.67 684.86 6.60 o 2 4 1 136.74 136.35 2.45 o 3 4 1 71.14 77.00 1.89 o 4 4 1 0.06 0.81 0.46 o 5 4 1 0.02 0.21 0.20 o 6 4 1 247.82 222.87 4.26 o 7 4 1 139.94 133.84 3.23 o 8 4 1 44.73 50.93 2.30 o -7 5 1 4.18 3.71 0.58 o -6 5 1 47.06 39.01 2.28 o -5 5 1 461.57 378.37 5.48 o -4 5 1 4.00 3.85 0.45 o -3 5 1 12.54 11.68 1.25 o -2 5 1 22.67 24.23 1.59 o -1 5 1 1.43 1.20 0.36 o 0 5 1 982.76 973.87 7.41 o 1 5 1 184.43 221.31 2.55 o 2 5 1 23.29 19.71 1.27 o 3 5 1 0.13 0.24 0.21 o 4 5 1 0.57 0.27 0.31 o 5 5 1 181.67 185.63 3.07 o 6 5 1 3.46 3.63 0.58 o 7 5 1 6.60 11.06 0.92 o 8 5 1 25.53 20.50 1.37 o -6 6 1 91.24 77.91 2.69 o -5 6 1 68.96 59.83 2.10 o -4 6 1 14.49 10.73 1.00 o -3 6 1 51.98 51.78 2.28 o -2 6 1 442.61 433.61 5.23 o -1 6 1 9.13 10.51 1.01 o 0 6 1 47.84 48.20 1.81 o 1 6 1 12.48 10.99 1.13 o 2 6 1 49.62 55.88 2.61 o 3 6 1 244.71 242.34 5.40 o 4 6 1 67.47 58.24 1.69 o 5 6 1 0.40 1.55 1.10 o 6 6 1 3.07 3.47 0.55 o 7 6 1 27.76 29.20 1.95 o 8 6 1 2.94 3.28 0.51 o -6 7 1 1.47 0.98 0.33 o -5 7 1 2.70 2.74 0.74 o -4 7 1 17.73 15.99 1.77 o -3 7 1 215.46 213.50 4.45 o -2 7 1 163.93 159.68 2.46 o -1 7 1 31.86 30.16 1.13 o 0 7 1 64.77 77.78 3.29 o 1 7 1 152.36 169.17 4.66 o 2 7 1 2.25 1.88 0.31 o 3 7 1 19.37 18.02 1.16 o 4 7 1 31.95 29.42 2.19 o 5 7 1 224.95 237.77 6.20 o 6 7 1 42.32 38.26 2.37 o 7 7 1 9.62 12.54 1.14 o -4 8 1 0.40 0.69 0.44 o -3 8 1 4.76 4.82 0.90 o -2 8 1 33.95 32.26 1.71 o -1 8 1 577.59 566.13 5.41 o 0 8 1 17.57 20.36 1.03 o 1 8 1 225.28 215.20 4.25 o 2 8 1 115.39 113.37 2.99 o 3 8 1 16.68 16.71 1.13 o 4 8 1 0.02 0.17 0.22 o 5 8 1 0.27 0.44 0.40 o 6 8 1 24.25 26.57 1.78 o 7 8 1 12.81 16.27 1.07 o -5 9 1 43.56 45.87 1.60 o -4 9 1 11.89 16.23 1.46 o -3 9 1 158.00 158.88 4.00 o -2 9 1 144.36 146.66 3.47 o -1 9 1 164.16 165.59 3.61 o 0 9 1 7.01 8.03 0.87 o 1 9 1 28.64 28.16 1.56 o 2 9 1 27.01 32.21 1.61 o 3 9 1 215.69 219.13 3.99 o 4 9 1 23.34 21.35 1.78 o 5 9 1 20.38 20.18 1.56 o 6 9 1 3.93 4.31 0.61 o -3 10 1 4.57 4.77 0.50 o -2 10 1 259.02 261.47 3.98 o -1 10 1 90.05 97.07 2.44 o 0 10 1 27.69 26.92 2.05 o 1 10 1 66.50 72.33 2.28 o 2 10 1 0.13 0.02 0.22 o 3 10 1 6.77 6.70 0.66 o 4 10 1 66.65 72.85 2.76 o 5 10 1 68.22 70.91 2.29 o -2 11 1 0.32 0.75 0.27 o -1 11 1 83.58 89.70 2.98 o 0 11 1 64.90 61.54 2.57 o 1 11 1 15.49 13.75 1.20 o 2 11 1 5.50 8.26 0.86 o 3 11 1 216.18 210.52 6.17 o 4 11 1 98.67 90.82 2.11 o 0 -11 2 1.99 1.93 0.33 o 1 -11 2 49.45 50.12 1.60 o -4 -10 2 7.96 7.55 0.67 o -3 -10 2 0.64 0.88 0.34 o -2 -10 2 137.09 142.39 3.88 o -1 -10 2 133.21 129.24 2.52 o 0 -10 2 37.60 33.08 1.83 o 1 -10 2 23.14 23.67 1.59 o 2 -10 2 2.67 2.55 0.54 o 3 -10 2 56.65 60.50 2.21 o -5 -9 2 31.78 32.79 1.47 o -4 -9 2 89.93 95.21 3.12 o -3 -9 2 30.34 29.72 1.98 o -2 -9 2 41.29 45.51 2.64 o -1 -9 2 15.05 12.76 0.96 o 0 -9 2 1.00 0.21 0.23 o 1 -9 2 6.78 6.01 0.97 o 2 -9 2 40.53 40.94 2.45 o 3 -9 2 38.55 37.33 2.26 o 4 -9 2 1.50 1.21 0.24 o -6 -8 2 39.01 35.10 1.40 o -5 -8 2 23.92 24.34 1.58 o -4 -8 2 485.33 503.15 8.25 o -3 -8 2 694.23 700.57 10.45 o -2 -8 2 42.62 45.53 2.81 o -1 -8 2 5.43 6.34 0.71 o 0 -8 2 0.79 1.62 0.40 o 1 -8 2 19.66 22.72 1.89 o 2 -8 2 0.78 0.79 0.31 o 3 -8 2 29.52 29.84 2.26 o 4 -8 2 0.79 0.74 0.46 o 5 -8 2 2.39 1.75 0.32 o -6 -7 2 79.24 85.15 2.74 o -5 -7 2 38.46 42.18 2.35 o -4 -7 2 529.45 528.47 8.97 o -3 -7 2 78.60 78.89 3.56 o -2 -7 2 184.06 191.57 4.09 o -1 -7 2 27.59 25.62 1.34 o 0 -7 2 54.25 53.41 2.01 o 1 -7 2 180.48 179.47 3.87 o 2 -7 2 1236.58 1243.01 9.61 o 3 -7 2 183.29 191.61 3.98 o 4 -7 2 7.59 8.52 1.27 o 5 -7 2 4.27 4.92 0.96 o 6 -7 2 0.47 0.07 0.26 o -7 -6 2 0.70 0.38 0.25 o -6 -6 2 342.42 316.39 4.00 o -5 -6 2 3.54 3.87 0.80 o -4 -6 2 0.09 0.62 0.39 o -3 -6 2 112.97 116.64 3.01 o -2 -6 2 9.87 9.69 0.88 o -1 -6 2 44.11 46.94 1.93 o 1 -6 2 118.23 115.23 2.81 o 2 -6 2 14.69 16.10 0.81 o 3 -6 2 1620.92 1625.28 8.91 o 4 -6 2 82.47 78.36 2.61 o 5 -6 2 115.69 106.09 4.37 o 6 -6 2 3.51 3.46 0.71 o 7 -6 2 6.82 7.66 0.72 o -7 -5 2 40.92 34.25 1.19 o -6 -5 2 163.13 161.67 2.62 o -5 -5 2 23.49 20.17 0.98 o -4 -5 2 27.50 29.74 1.19 o -3 -5 2 5.32 5.65 0.64 o 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51.07 2.45 o 0 0 10 330.49 334.02 6.67 o 1 0 10 209.53 217.96 5.74 o 2 0 10 3.92 3.04 0.77 o 3 0 10 0.02 0.45 0.49 o 4 0 10 0.85 0.66 0.50 o 5 0 10 0.57 0.73 0.29 o 6 0 10 6.36 6.43 0.83 o 7 0 10 15.10 16.28 0.80 o -3 1 10 14.36 12.76 0.98 o -2 1 10 131.69 140.12 3.94 o -1 1 10 156.82 160.61 4.64 o 0 1 10 36.57 38.38 2.39 o 1 1 10 1422.03 1374.98 14.98 o 2 1 10 33.63 31.77 2.42 o 3 1 10 23.39 24.96 2.29 o 4 1 10 2.16 2.46 0.50 o 5 1 10 82.02 84.37 2.60 o 6 1 10 0.16 0.21 0.25 o 7 1 10 134.66 134.07 5.46 o -3 2 10 5.72 5.75 0.73 o -2 2 10 6.50 6.35 0.91 o -1 2 10 80.06 80.23 3.40 o 0 2 10 1.00 1.53 0.54 o 1 2 10 61.56 59.31 3.18 o 2 2 10 119.77 122.83 4.77 o 3 2 10 0.07 0.76 0.59 o 4 2 10 124.27 118.18 3.20 o 5 2 10 0.65 0.71 0.35 o 6 2 10 108.05 117.75 2.94 o 7 2 10 382.42 381.70 6.94 o -3 3 10 133.38 134.50 3.46 o -2 3 10 201.82 192.85 4.91 o -1 3 10 107.82 111.65 4.04 o 0 3 10 1.28 0.97 0.49 o 1 3 10 39.95 39.89 2.60 o 2 3 10 146.59 149.85 5.23 o 3 3 10 0.02 0.19 0.27 o 4 3 10 0.00 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6.40 0.85 o 3 1 12 45.92 46.88 2.26 o 4 1 12 4.30 4.73 0.73 o 5 1 12 22.90 19.36 1.28 o -1 2 12 61.60 53.21 1.79 o 0 2 12 53.36 53.34 2.16 o 1 2 12 0.44 0.67 0.36 o 2 2 12 78.56 78.70 3.00 o 3 2 12 44.97 40.65 2.21 o 4 2 12 83.92 81.42 3.03 o 5 2 12 51.52 49.02 2.14 o 6 2 12 41.32 38.66 1.48 o -1 3 12 103.34 95.64 2.51 o 0 3 12 265.89 251.09 4.77 o 1 3 12 0.02 -0.05 0.29 o 2 3 12 334.59 354.37 6.42 o 3 3 12 133.36 138.17 4.06 o 4 3 12 35.15 35.79 2.01 o 5 3 12 42.33 39.37 1.89 o 6 3 12 43.72 37.76 1.43 o -1 4 12 14.07 12.96 0.90 o 0 4 12 15.13 14.19 1.12 o 1 4 12 8.97 7.59 0.89 o 2 4 12 549.87 564.64 7.87 o 3 4 12 56.67 58.80 2.53 o 4 4 12 1.28 1.24 0.39 o 5 4 12 0.32 0.68 0.30 o -1 5 12 17.52 16.21 0.89 o 0 5 12 127.88 123.99 3.03 o 1 5 12 0.18 0.50 0.31 o 2 5 12 6.23 7.15 0.84 o 3 5 12 73.10 73.42 2.57 o 4 5 12 11.74 10.14 0.90 o 5 5 12 65.23 59.63 1.74 o 0 6 12 0.32 0.94 0.26 o 1 6 12 3.35 3.63 0.50 o 2 6 12 20.70 18.86 1.14 o 3 6 12 1.17 0.31 0.22 o 2 1 13 0.01 0.21 0.14 o 3 1 13 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