#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:27:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181239 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/17/2231755.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231755_Fobs loop_ _publ_author_name 'Zhu, Xin' 'Lu, Ping' 'Ng, Seik Weng' _publ_section_title ; 2-(Tritylsulfanyl)ethyl 2-iodobenzoate ; _journal_coeditor_code XU5302 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2475 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.618 _cell_angle_gamma 90.000 _cell_length_a 28.4378 _cell_length_b 9.6154 _cell_length_c 18.3808 _exptl_crystal_F_000 2208.00 _reflns_d_resolution_high 0.7646 _cod_data_source_file xu5302Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 746.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 0 0 22422.72 22378.48 250.22 o 10 0 0 11202.44 11077.16 137.20 o 12 0 0 2923.62 1991.28 59.47 o 14 0 0 12208.88 12585.48 161.25 o 16 0 0 28584.39 28406.18 266.28 o 18 0 0 3798.44 3389.53 55.10 o 20 0 0 5785.36 5302.20 76.18 o 22 0 0 17011.63 16444.08 327.80 o 24 0 0 886.50 829.66 66.72 o 26 0 0 14413.38 14610.71 314.46 o 28 0 0 1556.56 1502.09 91.09 o 30 0 0 1748.40 1748.09 98.05 o 32 0 0 621.16 514.62 64.40 o 3 1 0 12230.87 15305.49 156.67 o 5 1 0 51262.07 52811.40 634.48 o 7 1 0 13587.67 13494.97 168.19 o 9 1 0 138891.83 145744.42 2014.74 o 11 1 0 377.55 229.21 11.15 o 13 1 0 99404.37 104441.38 783.37 o 15 1 0 3128.90 3339.41 46.08 o 17 1 0 39184.16 37771.42 305.46 o 19 1 0 15369.67 15485.84 145.13 o 21 1 0 8594.69 8185.25 93.05 o 23 1 0 7952.89 7681.13 91.65 o 25 1 0 934.00 877.94 31.96 o 27 1 0 1506.79 1476.53 49.85 o 29 1 0 141.60 134.67 31.18 o 31 1 0 391.20 420.62 42.87 o 33 1 0 290.11 277.33 57.44 o 35 1 0 782.01 724.07 78.90 o 0 2 0 137412.22 130635.73 1431.70 o 2 2 0 9289.88 9703.42 96.57 o 4 2 0 201350.83 196269.08 4709.50 o 6 2 0 19317.15 21411.89 163.13 o 8 2 0 51554.77 52003.20 395.26 o 10 2 0 6959.32 6691.90 62.55 o 12 2 0 3079.14 2561.44 35.36 o 14 2 0 11960.76 11880.11 103.83 o 16 2 0 31.61 8.85 9.53 o 18 2 0 7785.81 7506.10 78.63 o 20 2 0 4372.57 4302.90 61.51 o 22 2 0 4394.99 4584.60 66.48 o 24 2 0 472.60 501.86 27.38 o 26 2 0 8116.95 8200.73 101.68 o 28 2 0 1859.00 1722.72 54.52 o 30 2 0 1996.61 2157.74 86.71 o 32 2 0 1961.30 1868.97 73.60 o 34 2 0 644.08 751.56 52.70 o 1 3 0 8611.73 8779.17 92.78 o 3 3 0 16718.60 17305.32 167.69 o 5 3 0 3075.76 2507.98 41.26 o 7 3 0 452.73 421.07 31.45 o 9 3 0 13063.96 12904.82 120.08 o 11 3 0 36.48 28.44 17.86 o 13 3 0 62727.67 65293.34 463.83 o 15 3 0 7603.47 8414.56 82.86 o 17 3 0 13036.91 13121.71 118.48 o 19 3 0 8593.99 8518.92 96.22 o 21 3 0 2103.21 2068.56 43.86 o 23 3 0 6112.67 5886.30 80.14 o 25 3 0 649.02 588.05 28.00 o 27 3 0 412.93 533.50 47.38 o 29 3 0 14.59 -18.04 21.89 o 31 3 0 2.75 9.94 22.58 o 33 3 0 202.55 243.92 30.83 o 0 4 0 83927.99 89722.88 978.04 o 2 4 0 4897.30 5167.80 66.06 o 4 4 0 30168.92 31925.81 300.21 o 6 4 0 11825.05 11227.14 122.08 o 8 4 0 1272.31 1460.13 30.40 o 10 4 0 159.76 275.01 32.49 o 12 4 0 85.29 142.28 19.74 o 14 4 0 29.83 49.40 12.90 o 16 4 0 103.51 64.04 18.20 o 18 4 0 1161.50 1242.76 42.54 o 20 4 0 1500.43 1468.32 62.81 o 22 4 0 194.86 246.28 20.40 o 24 4 0 10.09 -15.55 15.55 o 26 4 0 2348.90 2557.28 62.59 o 28 4 0 432.14 415.23 31.89 o 30 4 0 765.35 817.61 44.00 o 32 4 0 515.56 550.70 37.72 o 1 5 0 1208.05 1451.90 42.71 o 3 5 0 2675.90 3646.95 56.59 o 5 5 0 50.31 72.19 12.28 o 7 5 0 2970.30 2813.15 53.98 o 9 5 0 380.94 343.71 40.40 o 11 5 0 1131.14 1133.42 54.43 o 13 5 0 9652.51 9916.42 106.35 o 15 5 0 852.08 743.03 49.80 o 17 5 0 3669.73 4015.88 70.15 o 19 5 0 952.89 1141.90 41.02 o 21 5 0 692.70 667.41 29.33 o 23 5 0 15.67 -16.27 16.27 o 25 5 0 1248.87 1199.08 45.89 o 27 5 0 127.92 62.01 22.01 o 29 5 0 115.22 115.71 24.92 o 31 5 0 77.46 81.66 26.56 o 0 6 0 1712.82 1836.04 51.20 o 2 6 0 991.86 999.10 28.05 o 4 6 0 752.33 713.23 28.89 o 6 6 0 457.82 474.72 25.74 o 8 6 0 1185.95 1209.42 40.04 o 10 6 0 719.48 719.71 35.54 o 12 6 0 3495.88 3395.81 69.98 o 14 6 0 527.08 533.29 34.92 o 16 6 0 6876.41 6515.80 141.72 o 18 6 0 2321.62 2163.17 52.57 o 20 6 0 661.63 693.55 40.75 o 22 6 0 450.50 433.20 35.52 o 24 6 0 5.20 0.43 23.92 o 26 6 0 396.43 452.21 58.31 o 28 6 0 1.48 -25.31 25.31 o 30 6 0 34.56 44.17 23.55 o 1 7 0 12114.55 12950.43 170.52 o 3 7 0 2226.71 2292.18 50.41 o 5 7 0 4194.34 4103.09 70.65 o 7 7 0 669.47 664.59 49.61 o 9 7 0 1829.31 1847.25 52.37 o 11 7 0 384.52 343.01 28.83 o 13 7 0 1715.55 1708.84 54.90 o 15 7 0 1992.65 1966.07 71.98 o 17 7 0 1572.31 1700.51 96.31 o 19 7 0 91.80 68.81 17.12 o 21 7 0 415.83 446.17 33.96 o 23 7 0 669.93 590.04 40.02 o 25 7 0 585.88 626.05 70.49 o 27 7 0 326.21 300.46 34.79 o 29 7 0 180.81 173.33 33.84 o 0 8 0 2037.61 2044.43 65.00 o 2 8 0 35.85 42.45 17.73 o 4 8 0 1558.44 1475.15 46.98 o 6 8 0 125.25 131.96 21.54 o 8 8 0 7010.11 6869.38 130.41 o 10 8 0 381.89 351.84 35.47 o 12 8 0 1901.24 1908.03 68.91 o 14 8 0 1401.03 1442.33 93.99 o 16 8 0 1329.74 1447.55 98.05 o 18 8 0 1564.07 1531.68 103.85 o 20 8 0 0.43 7.54 44.67 o 22 8 0 1289.89 1427.83 105.59 o 24 8 0 104.18 125.90 55.12 o 26 8 0 1.37 17.41 47.57 o 1 9 0 1884.01 2010.28 68.91 o 3 9 0 574.97 687.57 44.72 o 5 9 0 4173.47 4050.61 80.82 o 7 9 0 90.76 32.97 20.46 o 9 9 0 2275.37 2238.86 74.65 o 11 9 0 91.39 63.82 41.77 o 13 9 0 347.75 419.47 60.34 o 15 9 0 459.00 395.10 61.50 o 17 9 0 323.47 436.88 69.04 o 19 9 0 112.96 110.81 51.64 o 21 9 0 591.14 581.92 77.16 o 23 9 0 208.47 246.58 63.24 o 0 10 0 504.24 579.02 63.82 o 2 10 0 0.20 -6.31 26.03 o 4 10 0 2271.04 2303.54 79.79 o 6 10 0 56.00 40.10 37.42 o 8 10 0 1944.99 1842.08 107.33 o 10 10 0 353.57 378.28 59.76 o 12 10 0 1748.87 1894.87 113.72 o 14 10 0 1587.56 1586.22 105.01 o 16 10 0 770.32 919.01 91.09 o 18 10 0 1176.99 1131.35 100.37 o 20 10 0 23.17 -13.34 43.51 o 1 11 0 1023.07 1067.41 67.30 o 3 11 0 171.43 89.24 33.84 o 5 11 0 2170.61 2505.22 125.32 o 7 11 0 159.85 176.96 53.96 o 9 11 0 694.10 768.74 80.07 o 11 11 0 5.65 24.95 46.99 o 13 11 0 27.76 99.21 49.90 o 15 11 0 29.86 6.96 46.41 o 17 11 0 339.50 353.33 70.78 o 0 12 0 89.75 53.38 48.74 o 2 12 0 22.31 -21.47 44.67 o 4 12 0 924.40 1065.21 96.89 o 6 12 0 54.99 10.44 47.57 o 8 12 0 217.47 239.03 61.50 o 10 12 0 139.74 58.60 50.48 o -35 1 1 19.36 -39.45 39.45 o -33 1 1 246.50 305.73 41.84 o -31 1 1 203.32 203.38 35.85 o -29 1 1 218.29 173.19 32.81 o -27 1 1 318.79 345.38 44.90 o -25 1 1 180.83 220.09 23.07 o -23 1 1 47.47 43.69 19.98 o -21 1 1 2116.56 2086.90 62.30 o -19 1 1 236.50 157.85 20.03 o -17 1 1 3435.02 3731.55 52.77 o -15 1 1 2759.04 2403.77 38.45 o -13 1 1 619.52 515.93 25.88 o -11 1 1 1062.33 989.24 21.13 o -9 1 1 4621.50 5160.28 80.81 o -7 1 1 5640.87 5253.11 120.10 o -5 1 1 33584.74 34887.63 332.16 o -3 1 1 413.27 351.90 14.28 o -1 1 1 1699.51 1757.37 39.45 o 3 1 1 18227.92 19802.25 200.97 o 5 1 1 20091.19 20556.10 332.73 o 7 1 1 45427.16 49659.54 514.47 o 9 1 1 35.52 23.89 7.34 o 11 1 1 4626.17 4756.93 52.59 o 13 1 1 3988.29 4209.64 51.01 o 15 1 1 10339.36 10640.09 117.37 o 17 1 1 632.24 679.51 25.21 o 19 1 1 37.25 40.66 11.95 o 21 1 1 507.93 483.57 22.95 o 23 1 1 2458.47 2374.62 46.77 o 25 1 1 1006.08 1067.37 35.39 o 27 1 1 4.28 -14.09 14.09 o 29 1 1 22.84 -11.02 33.65 o 31 1 1 189.78 175.79 48.16 o 33 1 1 172.24 156.65 52.22 o -34 2 1 407.56 354.35 78.03 o -32 2 1 171.07 202.93 54.25 o -30 2 1 307.71 297.42 30.31 o -28 2 1 866.59 890.73 35.79 o -26 2 1 909.87 931.47 34.22 o -24 2 1 4118.55 3892.19 63.04 o -22 2 1 26.08 -13.17 13.73 o -20 2 1 2899.73 2614.68 43.22 o -18 2 1 32.13 35.41 12.24 o -16 2 1 4478.34 4130.38 56.40 o -14 2 1 5296.93 5042.19 55.49 o -12 2 1 53091.34 58149.53 548.82 o -10 2 1 1364.86 1048.93 22.96 o -8 2 1 3228.31 3404.15 41.59 o -6 2 1 193.63 120.56 13.98 o -4 2 1 64.99 64.10 9.50 o -2 2 1 27873.31 28586.07 261.38 o 0 2 1 27117.67 29740.67 270.98 o 2 2 1 107544.32 113806.86 1021.71 o 4 2 1 12115.86 13085.19 134.31 o 6 2 1 276.23 209.02 16.52 o 8 2 1 3725.60 4282.95 45.38 o 10 2 1 10585.09 9600.41 83.03 o 12 2 1 15613.62 16841.51 134.89 o 14 2 1 13797.56 13498.40 115.39 o 16 2 1 20195.93 21213.01 170.65 o 18 2 1 846.84 785.97 47.73 o 20 2 1 993.61 899.88 31.91 o 22 2 1 410.90 394.66 22.17 o 24 2 1 3452.31 3409.32 58.30 o 26 2 1 76.57 50.52 19.25 o 28 2 1 630.68 588.09 44.26 o 30 2 1 235.67 208.43 29.71 o 32 2 1 604.76 588.22 47.81 o 34 2 1 131.33 121.23 33.53 o -33 3 1 1009.33 1136.09 62.28 o -31 3 1 1.82 16.33 22.72 o -29 3 1 2661.77 2450.14 63.10 o -27 3 1 295.89 341.10 34.25 o -25 3 1 1645.94 1642.37 43.02 o -23 3 1 4924.34 4857.52 71.91 o -21 3 1 4688.30 4707.98 68.06 o -19 3 1 3130.78 2981.98 46.41 o -17 3 1 2303.35 2270.37 38.73 o -15 3 1 2418.80 1884.90 32.82 o -13 3 1 2486.82 2611.84 37.84 o -11 3 1 50848.77 50672.52 578.74 o -9 3 1 4706.08 4587.50 54.31 o -7 3 1 108699.73 112250.50 889.67 o -5 3 1 2798.21 2529.76 39.63 o -3 3 1 62222.53 64617.49 578.04 o -1 3 1 16212.38 16498.25 161.11 o 1 3 1 9306.83 9213.28 118.70 o 3 3 1 45220.04 46907.71 519.76 o 5 3 1 18836.25 18968.19 174.77 o 7 3 1 35927.52 37727.52 306.50 o 9 3 1 17472.66 17769.79 163.03 o 11 3 1 42473.04 43760.27 295.10 o 13 3 1 3504.69 3159.68 42.52 o 15 3 1 12454.03 11805.50 106.89 o 17 3 1 637.33 652.46 24.95 o 19 3 1 6108.91 5708.62 73.92 o 21 3 1 322.24 295.57 20.43 o 23 3 1 2195.96 2088.82 45.99 o 25 3 1 931.72 809.71 37.40 o 27 3 1 1065.77 1131.23 43.95 o 29 3 1 528.86 507.68 33.91 o 31 3 1 37.52 7.27 20.58 o 33 3 1 568.59 570.46 38.13 o -34 4 1 222.32 284.29 64.98 o -32 4 1 490.40 614.58 47.49 o -30 4 1 521.25 568.29 36.58 o -28 4 1 2987.38 2963.36 71.47 o -26 4 1 193.23 156.10 24.05 o -24 4 1 4380.52 4330.11 74.84 o -22 4 1 495.08 454.15 24.60 o -20 4 1 18392.00 18358.00 174.62 o -18 4 1 1002.87 1084.12 28.91 o -16 4 1 23722.69 23118.03 203.06 o -14 4 1 1238.38 1070.74 27.99 o -12 4 1 28366.92 29544.61 254.44 o -10 4 1 7838.37 7183.08 77.61 o -8 4 1 9547.98 9715.74 106.26 o -6 4 1 14431.48 13426.36 142.80 o -4 4 1 3260.28 3005.04 47.66 o -2 4 1 41820.77 41512.19 383.43 o 0 4 1 15.06 -6.09 6.09 o 2 4 1 31766.32 31720.58 296.49 o 4 4 1 4660.72 5130.57 64.72 o 6 4 1 68865.77 69000.73 650.21 o 8 4 1 8313.69 9293.73 91.95 o 10 4 1 14697.08 14326.27 134.97 o 12 4 1 17425.29 17231.20 141.51 o 14 4 1 3457.56 3093.43 69.92 o 16 4 1 11718.96 11575.34 116.98 o 18 4 1 843.28 825.72 29.20 o 20 4 1 9232.16 9361.62 106.05 o 22 4 1 238.08 292.43 25.09 o 24 4 1 2448.80 2494.43 60.31 o 26 4 1 91.53 105.06 25.29 o 28 4 1 3128.80 3135.14 74.35 o 30 4 1 146.66 37.09 21.51 o 32 4 1 887.04 1046.42 48.55 o -33 5 1 741.77 910.88 92.83 o -31 5 1 17.08 53.40 23.36 o -29 5 1 2221.64 2211.25 97.54 o -27 5 1 316.33 427.88 32.48 o -25 5 1 1927.35 1999.49 55.69 o -23 5 1 1323.39 1417.26 40.51 o -21 5 1 2327.46 2102.05 46.26 o -19 5 1 1517.95 1389.54 58.94 o -17 5 1 787.69 772.12 60.74 o -15 5 1 16339.72 16118.25 157.81 o -13 5 1 2476.47 2558.28 43.97 o -11 5 1 29191.01 28482.92 244.89 o -9 5 1 4.26 8.64 13.01 o -7 5 1 18631.00 17160.41 181.63 o -5 5 1 5454.40 5707.28 82.86 o -3 5 1 42498.58 42870.44 401.40 o -1 5 1 71838.41 78344.95 611.58 o 1 5 1 15095.82 14318.57 132.03 o 3 5 1 25569.76 25121.61 244.97 o 5 5 1 24601.32 25816.04 256.61 o 7 5 1 31803.69 30790.30 313.75 o 9 5 1 1348.98 1444.09 40.58 o 11 5 1 30319.81 30048.30 300.21 o 13 5 1 4732.97 4777.26 64.43 o 15 5 1 17147.04 17412.10 169.22 o 17 5 1 431.60 397.37 25.44 o 19 5 1 8891.15 8810.17 152.30 o 21 5 1 1783.13 1661.15 47.42 o 23 5 1 785.24 786.97 36.85 o 25 5 1 2272.52 2264.38 76.84 o 27 5 1 827.31 1029.67 44.62 o 29 5 1 528.26 576.50 36.88 o 31 5 1 132.47 188.69 38.87 o -30 6 1 701.58 696.72 74.51 o -28 6 1 1090.37 1307.82 61.86 o -26 6 1 593.11 632.57 77.16 o -24 6 1 2619.48 3010.59 81.82 o -22 6 1 113.04 115.27 26.93 o -20 6 1 4274.16 3998.86 73.96 o -18 6 1 4.87 7.67 20.48 o -16 6 1 12373.21 12305.17 144.07 o -14 6 1 4891.33 5067.03 89.40 o -12 6 1 10580.55 10438.70 139.88 o -10 6 1 10618.79 10825.29 175.53 o -8 6 1 12537.27 12478.12 146.39 o -6 6 1 15556.74 14712.28 164.10 o -4 6 1 7335.48 7684.36 100.24 o -2 6 1 5448.95 4915.23 63.41 o 0 6 1 369.23 278.50 16.58 o 2 6 1 24839.34 24332.64 212.77 o 4 6 1 10.20 15.21 12.00 o 6 6 1 21084.19 20292.55 261.60 o 8 6 1 2478.43 2336.75 53.57 o 10 6 1 6941.63 6716.56 101.78 o 12 6 1 9240.29 9034.04 127.34 o 14 6 1 1100.09 1085.48 42.13 o 16 6 1 20607.48 20458.88 243.40 o 18 6 1 426.19 590.51 47.57 o 20 6 1 6846.53 6643.15 170.57 o 22 6 1 1183.77 1370.90 55.69 o 24 6 1 1397.28 1435.69 84.71 o 26 6 1 56.50 51.90 32.78 o 28 6 1 854.44 939.48 55.34 o 30 6 1 1.82 21.83 23.32 o -29 7 1 701.66 774.76 53.67 o -27 7 1 226.43 254.06 34.25 o -25 7 1 365.35 420.77 45.83 o -23 7 1 398.38 520.83 38.04 o -21 7 1 330.16 363.70 28.35 o -19 7 1 2436.65 2407.75 117.20 o -17 7 1 3605.28 3478.09 97.01 o -15 7 1 4196.95 4245.54 103.99 o -13 7 1 1621.58 1445.25 59.86 o -11 7 1 5887.97 6029.84 124.42 o -9 7 1 167.57 111.11 28.65 o -7 7 1 19956.53 19572.70 213.88 o -5 7 1 11585.94 11913.57 144.88 o -3 7 1 10501.43 10616.41 114.05 o -1 7 1 2186.79 2111.51 42.96 o 1 7 1 11131.37 11348.39 119.07 o 3 7 1 8300.33 8079.99 110.37 o 5 7 1 2906.23 3100.81 62.94 o 7 7 1 9075.47 9397.33 153.17 o 9 7 1 5622.26 5206.12 104.55 o 11 7 1 6462.37 6086.42 100.75 o 13 7 1 335.85 368.42 51.64 o 15 7 1 3932.08 3774.08 139.24 o 17 7 1 27.27 29.01 37.13 o 19 7 1 607.25 742.08 33.86 o 21 7 1 399.06 443.87 48.16 o 23 7 1 788.96 961.68 87.61 o 25 7 1 837.96 794.05 47.23 o 27 7 1 22.01 72.86 29.69 o 29 7 1 1018.09 1053.03 100.95 o -26 8 1 376.75 399.74 70.78 o -24 8 1 1023.14 1126.71 96.31 o -22 8 1 0.56 69.04 48.16 o -20 8 1 1855.71 1890.81 111.39 o -18 8 1 1085.89 1143.54 92.25 o -16 8 1 3896.25 3950.45 152.59 o -14 8 1 853.59 951.35 57.83 o -12 8 1 4024.43 3941.15 99.45 o -10 8 1 284.57 228.94 32.16 o -8 8 1 3093.89 2917.25 112.27 o -6 8 1 1214.69 1117.88 51.61 o -4 8 1 1410.10 1286.73 44.62 o -2 8 1 2317.28 2178.33 53.85 o 0 8 1 416.30 399.41 27.65 o 2 8 1 4767.59 4554.67 80.26 o 4 8 1 100.01 55.82 19.36 o 6 8 1 3231.14 3133.05 67.32 o 8 8 1 137.81 167.89 29.72 o 10 8 1 4299.21 4301.46 146.79 o 12 8 1 1106.93 1077.98 78.90 o 14 8 1 131.42 143.30 48.16 o 16 8 1 1189.91 1247.39 89.35 o 18 8 1 137.48 30.17 41.19 o 20 8 1 3164.23 3369.69 148.53 o 22 8 1 45.34 87.61 47.57 o 24 8 1 778.01 1016.48 96.31 o 26 8 1 52.42 81.23 52.80 o -25 9 1 52.31 73.10 53.96 o -23 9 1 0.75 41.77 51.06 o -21 9 1 25.59 -15.08 41.19 o -19 9 1 38.83 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