#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/17/2231757.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231757_Fobs loop_ _publ_author_name 'Asiri, Abdullah M.' 'Al-Youbi, Abdulrahman O.' 'Faidallah, Hassan M.' 'Alamry, Khalid A.' 'Ng, Seik Weng' _publ_section_title ; 4-(5,3'-Dimethyl-5'-oxo-2-phenyl-2',5'-dihydro-2H-[3,4']bipyrazol-1'-yl)benzenesulfonamide monohydrate ; _journal_coeditor_code XU5305 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2474 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.142 _cell_angle_gamma 90.000 _cell_length_a 11.1570 _cell_length_b 12.3305 _cell_length_c 14.9228 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file xu5305Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 253.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16888.82 17695.34 151.77 o 3 0 0 15595.93 17087.06 184.55 o 4 0 0 1091.87 1049.95 53.45 o 5 0 0 1361.57 1551.15 72.99 o 6 0 0 322.46 446.74 44.04 o 7 0 0 88.96 158.21 29.73 o 8 0 0 791.39 856.62 70.76 o 9 0 0 3784.12 3830.85 159.63 o 10 0 0 228.50 275.06 46.13 o 11 0 0 254.55 313.03 53.75 o 12 0 0 621.48 606.84 77.07 o 13 0 0 22.57 20.70 18.99 o 1 1 0 5706.79 5661.88 65.80 o 2 1 0 9342.54 9035.95 59.74 o 3 1 0 468.43 446.04 22.24 o 4 1 0 981.26 914.14 41.39 o 5 1 0 654.63 789.14 37.82 o 6 1 0 934.98 1000.97 41.46 o 7 1 0 619.62 646.63 33.28 o 8 1 0 999.07 934.87 57.71 o 9 1 0 126.24 99.46 22.11 o 10 1 0 454.54 471.70 42.06 o 11 1 0 4864.97 5013.30 146.11 o 12 1 0 59.38 65.74 19.62 o 13 1 0 201.02 194.99 33.33 o 0 2 0 24817.35 23308.82 135.67 o 1 2 0 3106.09 3239.28 43.32 o 2 2 0 1558.64 1429.31 46.41 o 3 2 0 5107.62 5125.58 55.16 o 4 2 0 264.24 293.93 21.58 o 5 2 0 275.11 315.55 20.65 o 6 2 0 0.78 3.99 3.21 o 7 2 0 121.28 136.24 18.93 o 8 2 0 485.86 519.53 39.18 o 9 2 0 77.14 73.93 16.63 o 10 2 0 142.43 147.05 18.01 o 11 2 0 302.78 307.94 36.71 o 12 2 0 50.65 29.50 13.03 o 13 2 0 18.97 28.98 15.65 o 1 3 0 1163.50 1314.96 24.50 o 2 3 0 1328.92 1282.21 29.23 o 3 3 0 1371.42 1545.17 28.11 o 4 3 0 151.93 162.34 16.68 o 5 3 0 65.98 64.17 8.47 o 6 3 0 295.95 345.78 26.51 o 7 3 0 28.95 39.02 12.11 o 8 3 0 213.00 33.29 110.22 o 9 3 0 711.01 690.71 48.78 o 10 3 0 44.13 47.42 10.81 o 11 3 0 731.27 728.35 56.76 o 12 3 0 32.96 13.38 25.81 o 13 3 0 188.56 199.65 33.14 o 0 4 0 95.90 101.44 9.29 o 1 4 0 666.93 690.32 17.36 o 2 4 0 4383.64 4750.30 57.94 o 3 4 0 203.78 230.05 15.18 o 4 4 0 1905.02 2175.03 38.35 o 5 4 0 2596.69 2854.52 77.25 o 6 4 0 631.44 637.52 44.25 o 7 4 0 11.38 0.76 14.72 o 8 4 0 252.13 207.76 37.65 o 9 4 0 15.07 13.07 12.15 o 10 4 0 71.58 81.97 18.44 o 11 4 0 301.66 312.04 38.15 o 12 4 0 2.00 -6.12 9.71 o 13 4 0 20.94 45.70 25.78 o 1 5 0 690.99 795.52 20.49 o 2 5 0 625.70 659.80 23.20 o 3 5 0 1224.61 1336.42 36.39 o 4 5 0 185.65 213.45 12.74 o 5 5 0 1.53 1.70 6.54 o 6 5 0 878.91 893.00 39.06 o 7 5 0 75.16 57.55 19.31 o 8 5 0 84.69 74.09 22.81 o 9 5 0 2.20 -2.29 9.48 o 10 5 0 7.77 25.81 20.09 o 11 5 0 42.10 77.89 19.74 o 12 5 0 98.67 123.68 25.78 o 0 6 0 131.88 311.46 33.17 o 1 6 0 489.97 503.65 17.74 o 2 6 0 1725.36 1757.85 36.30 o 3 6 0 192.27 190.52 14.75 o 4 6 0 595.10 646.12 29.18 o 5 6 0 296.09 350.06 17.95 o 6 6 0 24.14 18.19 9.60 o 7 6 0 21.38 32.75 16.65 o 8 6 0 69.08 84.83 26.01 o 9 6 0 104.58 57.12 22.12 o 10 6 0 53.12 56.66 23.35 o 11 6 0 3.02 -23.94 18.13 o 12 6 0 41.17 38.42 17.33 o 1 7 0 78.07 110.05 9.16 o 2 7 0 2863.28 2975.23 56.16 o 3 7 0 579.16 633.43 93.61 o 4 7 0 22.05 2.05 9.43 o 5 7 0 42.14 55.27 8.02 o 6 7 0 1097.64 1127.67 46.72 o 7 7 0 127.80 204.76 38.73 o 8 7 0 496.62 591.03 67.59 o 9 7 0 566.79 606.45 73.18 o 10 7 0 0.82 -27.97 18.65 o 11 7 0 723.54 744.29 88.60 o 0 8 0 1269.69 1446.18 48.68 o 1 8 0 142.61 121.90 10.19 o 2 8 0 176.63 41.66 47.31 o 3 8 0 2216.10 2384.36 85.43 o 4 8 0 1148.49 1086.72 51.68 o 5 8 0 1404.10 1476.33 39.00 o 6 8 0 2285.94 2172.05 55.00 o 7 8 0 147.01 186.66 35.44 o 8 8 0 183.15 166.30 38.07 o 9 8 0 883.38 843.13 87.88 o 10 8 0 206.34 191.48 44.66 o 11 8 0 141.94 138.88 38.48 o 1 9 0 1513.36 1531.91 54.04 o 2 9 0 1377.25 1545.65 92.57 o 3 9 0 1108.15 1152.41 71.22 o 4 9 0 303.96 301.42 22.83 o 5 9 0 8.59 20.76 6.62 o 6 9 0 384.90 337.50 22.60 o 7 9 0 46.54 62.21 21.69 o 8 9 0 403.04 421.24 56.30 o 9 9 0 93.04 136.21 33.69 o 10 9 0 0.50 -11.10 23.75 o 11 9 0 166.09 157.91 40.32 o 0 10 0 1758.86 1700.53 85.54 o 1 10 0 331.93 346.50 27.42 o 2 10 0 904.20 901.38 63.85 o 3 10 0 88.58 67.42 12.75 o 4 10 0 62.45 85.16 16.25 o 5 10 0 12.60 21.13 9.99 o 6 10 0 19.79 18.87 6.70 o 7 10 0 426.15 369.63 50.98 o 8 10 0 11.04 -8.52 10.48 o 9 10 0 1096.97 1059.88 94.27 o 10 10 0 120.01 95.94 32.19 o 1 11 0 277.21 289.55 18.51 o 2 11 0 1144.96 1200.37 44.38 o 3 11 0 763.74 718.51 43.58 o 4 11 0 153.46 149.34 21.65 o 5 11 0 0.12 -6.77 8.80 o 6 11 0 161.64 158.21 18.42 o 7 11 0 66.11 58.55 16.31 o 8 11 0 106.57 117.34 32.52 o 9 11 0 78.14 84.81 30.38 o 10 11 0 12.48 -10.57 13.94 o 0 12 0 1008.09 915.22 68.18 o 1 12 0 0.04 6.90 7.80 o 2 12 0 384.37 383.96 32.22 o 3 12 0 502.40 499.97 38.03 o 4 12 0 28.50 13.60 8.77 o 5 12 0 0.37 -4.06 8.54 o 6 12 0 61.22 87.41 18.91 o 7 12 0 3.89 -1.22 9.63 o 8 12 0 173.71 196.42 39.13 o 9 12 0 57.87 56.13 25.07 o 1 13 0 182.16 176.99 22.60 o 2 13 0 2.80 13.05 7.61 o 3 13 0 253.66 219.31 26.91 o 4 13 0 13.70 2.57 9.62 o 5 13 0 7.12 5.32 10.85 o 6 13 0 45.53 44.46 15.70 o 7 13 0 28.46 37.88 20.11 o 8 13 0 9.93 0.72 17.24 o 0 14 0 63.98 97.10 24.32 o 1 14 0 73.85 70.85 15.98 o 2 14 0 5.19 16.10 21.67 o 3 14 0 13.84 22.65 10.00 o 4 14 0 72.94 55.55 15.37 o 5 14 0 60.25 28.09 29.22 o 6 14 0 107.54 95.43 27.14 o 1 15 0 120.58 150.26 22.53 o 2 15 0 7.34 -6.93 17.92 o 3 15 0 41.33 30.85 21.62 o 4 15 0 11.43 31.10 23.42 o -13 1 1 11.03 15.98 15.00 o -12 1 1 48.81 64.58 19.04 o -11 1 1 3.45 -2.89 9.27 o -10 1 1 700.36 768.78 66.03 o -9 1 1 525.98 504.97 41.11 o -8 1 1 655.93 659.48 43.55 o -7 1 1 531.49 558.06 30.46 o -6 1 1 6631.17 6895.20 120.82 o -5 1 1 6.26 11.39 6.14 o -4 1 1 3817.81 4353.40 124.61 o -3 1 1 2244.96 2390.41 49.77 o -2 1 1 70.62 83.14 8.23 o -1 1 1 16.37 6.37 1.99 o 1 1 1 348.58 342.32 12.78 o 2 1 1 1523.76 1375.82 31.60 o 3 1 1 12735.74 13107.92 215.52 o 4 1 1 718.98 772.32 31.07 o 5 1 1 3248.00 3506.02 79.07 o 6 1 1 2.76 2.33 5.47 o 7 1 1 0.10 4.91 5.53 o 8 1 1 0.79 4.99 7.79 o 9 1 1 655.88 617.32 35.28 o 10 1 1 324.78 286.50 33.86 o 11 1 1 225.75 254.46 33.62 o 12 1 1 193.03 201.15 31.90 o 13 1 1 33.23 -9.81 34.68 o -13 2 1 2.40 2.44 8.77 o -12 2 1 348.50 318.62 39.35 o -11 2 1 27.60 19.59 10.83 o -10 2 1 0.24 3.16 9.79 o -9 2 1 58.83 94.34 18.56 o -8 2 1 256.69 224.50 29.87 o -7 2 1 224.18 206.90 23.77 o -6 2 1 319.86 280.34 25.61 o -5 2 1 554.24 645.23 36.16 o -4 2 1 2945.81 2883.75 77.41 o -3 2 1 3400.61 3317.02 64.12 o -2 2 1 2901.74 2942.34 48.76 o -1 2 1 594.74 530.61 17.41 o 0 2 1 7743.55 7727.04 62.56 o 1 2 1 1348.89 1536.03 28.48 o 2 2 1 5642.67 5733.91 132.09 o 3 2 1 909.22 899.55 25.35 o 4 2 1 3720.90 3872.23 101.67 o 5 2 1 625.97 590.71 25.67 o 6 2 1 127.45 126.10 12.94 o 7 2 1 1113.12 1001.55 42.27 o 8 2 1 171.26 187.72 24.18 o 9 2 1 4.81 5.09 5.79 o 10 2 1 122.36 112.42 21.13 o 11 2 1 334.40 368.60 40.12 o 12 2 1 17.70 29.90 13.75 o 13 2 1 7.07 0.98 19.84 o -13 3 1 614.80 695.78 61.57 o -12 3 1 72.11 48.81 15.50 o -11 3 1 190.24 172.81 33.25 o -10 3 1 229.88 259.67 31.68 o -9 3 1 340.18 75.80 188.64 o -8 3 1 969.37 925.09 43.57 o -7 3 1 584.01 576.26 24.51 o -6 3 1 719.68 684.07 33.57 o -5 3 1 159.26 110.53 10.14 o -4 3 1 369.01 360.58 49.66 o -3 3 1 570.42 710.32 18.33 o -2 3 1 609.87 591.00 24.12 o -1 3 1 2132.08 2031.22 62.91 o 0 3 1 0.37 3.02 2.74 o 1 3 1 2633.69 2352.54 32.75 o 2 3 1 689.57 696.81 21.92 o 3 3 1 2232.92 2215.10 76.67 o 4 3 1 1260.77 1297.81 58.65 o 5 3 1 1280.98 1300.40 38.30 o 6 3 1 1274.90 1214.74 40.81 o 7 3 1 677.71 748.96 37.45 o 8 3 1 1067.13 1091.66 58.09 o 9 3 1 35.89 35.21 10.22 o 10 3 1 1246.19 1174.82 51.46 o 11 3 1 312.77 342.94 58.98 o 12 3 1 78.06 70.43 20.04 o 13 3 1 32.99 62.88 27.47 o -13 4 1 15.76 25.16 12.49 o -12 4 1 499.76 547.11 64.50 o -11 4 1 16.30 24.96 13.28 o -10 4 1 184.41 184.28 38.61 o -9 4 1 118.56 24.38 52.52 o -8 4 1 32.47 19.66 13.30 o -7 4 1 85.88 84.71 14.82 o -6 4 1 1605.29 1723.46 57.41 o -5 4 1 5795.46 6454.46 113.40 o -4 4 1 993.04 1008.60 29.56 o -3 4 1 1163.90 1137.49 28.27 o -2 4 1 8.04 17.93 3.65 o -1 4 1 4853.02 4527.74 69.96 o 0 4 1 335.33 215.51 9.21 o 1 4 1 1471.82 1423.20 25.29 o 2 4 1 798.65 928.99 33.51 o 3 4 1 932.89 935.95 24.46 o 4 4 1 692.83 846.09 28.81 o 5 4 1 845.61 759.45 40.57 o 6 4 1 1132.02 1219.62 55.62 o 7 4 1 54.53 78.18 21.46 o 8 4 1 66.58 60.08 20.64 o 9 4 1 4.12 5.02 11.86 o 10 4 1 395.88 426.39 42.25 o 11 4 1 1.64 -7.43 18.12 o 12 4 1 339.60 477.45 50.03 o 13 4 1 219.44 218.01 48.97 o -13 5 1 122.72 126.34 39.27 o -12 5 1 72.76 63.77 18.68 o -11 5 1 10.90 21.09 17.91 o -10 5 1 460.13 399.95 57.65 o -9 5 1 827.02 872.69 82.29 o -8 5 1 1795.50 1762.62 108.06 o -7 5 1 6.01 14.11 10.78 o -6 5 1 156.13 176.49 15.37 o -5 5 1 42.42 93.95 16.42 o -4 5 1 126.41 112.13 11.26 o -3 5 1 305.82 226.89 13.11 o -2 5 1 784.52 886.48 23.47 o -1 5 1 695.09 610.81 17.56 o 0 5 1 2346.75 2557.09 37.90 o 1 5 1 480.12 455.65 15.70 o 2 5 1 2980.28 3201.20 51.64 o 3 5 1 461.82 538.06 23.72 o 4 5 1 3615.40 3580.82 93.54 o 5 5 1 581.84 603.03 26.92 o 6 5 1 1648.22 1661.00 79.99 o 7 5 1 123.07 110.93 28.37 o 8 5 1 504.26 434.95 55.91 o 9 5 1 280.38 256.03 45.41 o 10 5 1 19.29 7.36 12.21 o 11 5 1 328.20 304.00 69.58 o 12 5 1 10.01 17.61 9.40 o -12 6 1 140.55 122.68 37.26 o -11 6 1 13.03 5.21 13.02 o -10 6 1 54.54 29.15 20.13 o -9 6 1 588.08 675.34 72.77 o -8 6 1 89.03 96.51 26.38 o -7 6 1 670.06 643.76 63.59 o -6 6 1 17.01 14.13 6.77 o -5 6 1 1415.85 1571.69 35.22 o -4 6 1 87.50 139.66 15.89 o -3 6 1 4311.06 4716.49 86.27 o -2 6 1 9.00 5.41 2.97 o -1 6 1 31.80 25.17 5.67 o 0 6 1 440.83 422.85 15.89 o 1 6 1 1043.42 1341.96 29.12 o 2 6 1 426.44 467.37 21.03 o 3 6 1 2303.67 2520.43 63.94 o 4 6 1 0.03 2.51 3.68 o 5 6 1 816.44 795.36 28.56 o 6 6 1 217.77 241.85 26.47 o 7 6 1 156.84 128.94 30.91 o 8 6 1 4.64 10.88 13.72 o 9 6 1 15.54 5.20 9.65 o 10 6 1 40.57 45.54 22.82 o 11 6 1 83.65 99.53 31.88 o 12 6 1 182.58 207.13 32.98 o -12 7 1 10.58 16.88 19.04 o -11 7 1 741.07 845.57 93.03 o -10 7 1 388.01 391.77 60.60 o -9 7 1 224.50 224.11 43.92 o -8 7 1 384.15 452.77 58.57 o -7 7 1 85.18 40.08 13.10 o -6 7 1 10.60 6.45 8.49 o -5 7 1 44.58 42.76 6.73 o -4 7 1 1.07 0.58 2.85 o -3 7 1 2134.63 2371.26 63.84 o -2 7 1 4.97 1.24 3.11 o -1 7 1 2434.52 2633.05 43.23 o 0 7 1 923.37 1005.00 26.68 o 1 7 1 1775.59 2003.94 38.24 o 2 7 1 549.43 581.33 37.32 o 3 7 1 584.86 530.66 26.34 o 4 7 1 246.40 200.43 21.42 o 5 7 1 690.20 669.08 29.80 o 6 7 1 324.67 316.60 19.51 o 7 7 1 55.44 41.18 19.22 o 8 7 1 1595.62 1430.80 106.94 o 9 7 1 8.30 8.97 12.88 o 10 7 1 245.30 159.05 40.86 o 11 7 1 12.28 -2.26 11.51 o 12 7 1 70.48 38.13 22.04 o -11 8 1 0.32 -12.41 14.84 o -10 8 1 141.78 171.78 42.53 o -9 8 1 497.01 561.97 70.78 o -8 8 1 125.02 167.97 38.19 o -7 8 1 1004.43 917.70 45.13 o -6 8 1 1161.89 1059.73 35.55 o -5 8 1 116.24 120.51 12.23 o -4 8 1 947.48 1026.35 41.14 o -3 8 1 4755.59 4855.58 105.85 o -2 8 1 0.23 3.84 4.92 o -1 8 1 19.04 16.67 4.45 o 0 8 1 179.04 191.22 14.26 o 1 8 1 219.52 258.68 16.86 o 2 8 1 3.06 14.19 4.78 o 3 8 1 324.12 357.59 28.23 o 4 8 1 113.96 107.50 16.02 o 5 8 1 0.22 -0.57 4.48 o 6 8 1 1426.77 1379.89 53.63 o 7 8 1 30.22 56.12 20.71 o 8 8 1 11.05 9.31 7.28 o 9 8 1 110.52 63.08 26.37 o 10 8 1 31.52 26.89 19.06 o 11 8 1 29.96 5.26 12.90 o -11 9 1 51.07 46.84 24.80 o -10 9 1 79.76 51.41 27.62 o -9 9 1 437.28 460.26 59.76 o -8 9 1 49.11 34.63 17.76 o -7 9 1 11.00 3.79 7.96 o -6 9 1 126.86 129.95 13.71 o -5 9 1 96.09 90.48 11.40 o -4 9 1 223.69 187.12 22.69 o -3 9 1 653.92 585.62 31.20 o -2 9 1 434.94 400.30 30.74 o -1 9 1 0.78 -3.30 3.02 o 0 9 1 370.80 364.93 20.98 o 1 9 1 42.78 5.09 9.21 o 2 9 1 36.62 29.41 10.23 o 3 9 1 15.65 9.61 8.88 o 4 9 1 2.28 5.93 6.11 o 5 9 1 230.25 221.62 16.53 o 6 9 1 37.24 46.62 11.11 o 7 9 1 152.01 164.91 34.70 o 8 9 1 70.43 28.89 16.48 o 9 9 1 0.02 0.71 9.88 o 10 9 1 83.25 78.35 28.78 o 11 9 1 218.35 143.33 38.75 o -11 10 1 103.37 146.20 38.78 o -10 10 1 109.09 101.81 30.72 o -9 10 1 482.06 470.96 61.98 o -8 10 1 549.71 615.22 66.42 o -7 10 1 469.95 511.99 42.97 o -6 10 1 8.01 10.57 9.25 o -5 10 1 155.37 149.13 26.72 o -4 10 1 1233.37 1200.17 55.60 o -3 10 1 13.64 19.08 8.98 o -2 10 1 856.82 890.88 46.38 o -1 10 1 30.51 37.07 8.01 o 0 10 1 193.45 209.48 17.51 o 1 10 1 1049.15 1060.90 39.56 o 2 10 1 946.68 949.77 50.21 o 3 10 1 30.11 4.51 6.91 o 4 10 1 71.20 62.22 11.70 o 5 10 1 131.43 125.74 15.25 o 6 10 1 513.92 481.07 33.83 o 7 10 1 732.41 799.85 77.09 o 8 10 1 7.06 0.52 10.39 o 9 10 1 113.51 165.08 40.08 o 10 10 1 29.98 33.25 22.89 o -10 11 1 99.72 25.21 18.63 o -9 11 1 7.83 -9.97 13.08 o -8 11 1 86.06 107.49 29.62 o -7 11 1 0.39 -13.20 10.03 o -6 11 1 1459.95 1457.68 46.80 o -5 11 1 2.97 3.47 9.06 o -4 11 1 757.83 796.23 48.94 o -3 11 1 329.28 280.57 27.86 o -2 11 1 1260.71 1204.25 79.59 o -1 11 1 12.13 6.23 4.40 o 0 11 1 93.50 98.47 12.96 o 1 11 1 702.91 687.24 33.49 o 2 11 1 1818.50 1761.42 53.65 o 3 11 1 982.90 940.49 40.92 o 4 11 1 499.52 448.20 36.96 o 5 11 1 59.98 38.28 28.35 o 6 11 1 5.93 -8.44 9.56 o 7 11 1 255.96 242.39 43.30 o 8 11 1 118.59 131.24 33.70 o 9 11 1 21.50 21.28 16.74 o -9 12 1 180.67 174.82 38.09 o -8 12 1 376.69 536.35 65.10 o -7 12 1 322.31 319.58 35.47 o -6 12 1 34.44 19.17 16.68 o -5 12 1 0.17 -2.79 9.50 o -4 12 1 475.24 382.16 33.97 o -3 12 1 8.67 12.09 21.43 o -2 12 1 294.02 285.46 27.72 o -1 12 1 0.04 -13.21 9.82 o 0 12 1 238.25 212.65 18.67 o 1 12 1 807.14 721.65 36.59 o 2 12 1 878.02 840.61 68.33 o 3 12 1 484.04 426.24 54.29 o 4 12 1 154.62 160.30 23.32 o 5 12 1 91.83 91.86 18.74 o 6 12 1 74.23 63.47 16.81 o 7 12 1 87.85 109.97 30.96 o 8 12 1 228.99 265.40 49.36 o -8 13 1 6.21 10.46 12.48 o -7 13 1 150.34 161.43 26.50 o -6 13 1 560.78 521.03 70.78 o -5 13 1 15.16 21.67 11.49 o -4 13 1 191.47 217.17 26.91 o -3 13 1 75.29 98.06 17.72 o -2 13 1 83.42 104.94 17.70 o -1 13 1 344.52 372.94 32.69 o 0 13 1 83.35 115.71 18.69 o 1 13 1 315.84 358.32 32.23 o 2 13 1 357.52 348.01 32.29 o 3 13 1 24.52 28.77 11.87 o 4 13 1 224.79 225.89 30.77 o 5 13 1 103.91 116.48 24.35 o 6 13 1 25.62 22.81 11.97 o 7 13 1 18.37 55.14 23.41 o -6 14 1 3.60 -20.67 20.93 o -5 14 1 88.73 82.99 18.89 o -4 14 1 63.62 74.61 17.17 o -3 14 1 49.40 38.31 12.55 o -2 14 1 0.04 -1.48 17.25 o -1 14 1 0.64 -0.94 9.55 o 0 14 1 112.04 159.79 22.40 o 1 14 1 49.23 50.73 16.83 o 2 14 1 52.83 86.76 17.56 o 3 14 1 122.88 118.47 20.81 o 4 14 1 488.97 541.28 45.22 o 5 14 1 299.17 251.17 31.46 o 6 14 1 196.34 216.05 42.46 o -5 15 1 65.42 52.18 21.33 o -4 15 1 16.41 36.56 22.33 o -3 15 1 232.49 259.95 45.97 o -2 15 1 355.00 355.21 51.32 o -1 15 1 752.44 838.64 76.96 o 0 15 1 68.05 54.24 19.56 o 1 15 1 1.56 31.25 17.81 o 2 15 1 96.24 193.96 38.06 o 3 15 1 106.83 99.03 26.42 o 4 15 1 539.85 650.41 70.59 o -13 0 2 176.36 169.56 42.80 o -12 0 2 2398.15 2544.71 153.27 o -11 0 2 57.65 70.26 25.56 o -10 0 2 2751.78 2769.60 141.84 o -9 0 2 117.08 125.32 28.46 o -8 0 2 130.36 114.17 19.51 o -7 0 2 1104.85 1325.59 56.82 o -6 0 2 4189.67 4148.61 92.27 o -5 0 2 65.87 58.17 16.34 o -4 0 2 8256.24 8224.04 148.14 o -3 0 2 64066.14 65524.53 357.36 o -2 0 2 29809.19 28510.16 187.28 o -1 0 2 2001.25 2002.01 37.45 o 0 0 2 116.31 97.90 6.35 o 1 0 2 6028.74 6331.59 65.88 o 2 0 2 1.02 0.42 2.88 o 3 0 2 284.34 240.31 23.29 o 4 0 2 3202.57 3397.65 99.51 o 5 0 2 1168.65 1015.48 60.45 o 6 0 2 1.86 0.78 7.88 o 7 0 2 74.56 99.73 24.08 o 8 0 2 87.59 79.08 22.21 o 9 0 2 52.17 38.03 18.22 o 10 0 2 963.79 836.64 81.32 o 11 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