#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:27:59 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181240 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/18/2231863.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231863_Fobs loop_ _publ_author_name 'Abdel-Aziz, Hatem A.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 2-(1H-1,3-Benzodiazol-2-ylsulfanyl)-1-(4-chlorophenyl)ethanone ; _journal_coeditor_code EZ2258 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2639 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.087 _cell_angle_gamma 90.000 _cell_length_a 27.3765 _cell_length_b 9.2784 _cell_length_c 10.3630 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.8011 _cod_data_source_file ez2258Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 289.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3871.60 3460.07 23.55 o 4 0 0 2911.56 2844.59 30.24 o 6 0 0 61094.82 45478.37 150.11 o 8 0 0 6957.06 7087.01 69.88 o 10 0 0 477.11 554.20 22.75 o 12 0 0 22538.28 23378.95 165.29 o 14 0 0 2104.55 1620.30 45.41 o 16 0 0 69.52 45.36 9.64 o 18 0 0 18809.21 19903.69 187.56 o 20 0 0 51.93 63.07 8.07 o 22 0 0 9114.84 9300.26 106.22 o 24 0 0 12660.15 12656.82 325.70 o 26 0 0 38.06 60.27 18.37 o 28 0 0 86.23 125.53 22.47 o 30 0 0 12.86 23.64 11.85 o 32 0 0 6272.13 6239.75 106.26 o 34 0 0 369.25 308.65 18.23 o 1 1 0 15044.54 12613.36 118.30 o 3 1 0 490.14 473.12 8.08 o 5 1 0 656.42 595.75 9.16 o 7 1 0 10852.37 10350.15 31.08 o 9 1 0 6022.44 5858.90 29.54 o 11 1 0 656.43 680.14 11.09 o 13 1 0 1859.80 2284.53 117.41 o 15 1 0 3714.92 3905.24 53.94 o 17 1 0 7263.54 7319.94 78.04 o 19 1 0 86.03 85.08 10.04 o 21 1 0 41.34 46.93 8.32 o 23 1 0 12809.19 12993.90 83.87 o 25 1 0 40.91 71.91 12.20 o 27 1 0 32.37 59.52 9.72 o 29 1 0 159.25 170.91 16.90 o 31 1 0 208.31 280.20 17.93 o 33 1 0 605.90 640.51 21.07 o 0 2 0 4892.45 4679.16 39.11 o 2 2 0 17432.59 15426.89 58.93 o 4 2 0 7358.07 6897.64 38.90 o 6 2 0 2579.98 2540.67 29.15 o 8 2 0 666.38 632.24 12.88 o 10 2 0 6691.75 6219.35 53.60 o 12 2 0 91.45 153.97 10.04 o 14 2 0 1601.15 1615.40 33.72 o 16 2 0 35559.66 36127.21 642.31 o 18 2 0 1696.08 1796.78 57.94 o 20 2 0 1652.43 1661.07 25.96 o 22 2 0 1716.29 1805.86 28.34 o 24 2 0 2354.76 2378.61 49.63 o 26 2 0 1590.76 1704.93 41.63 o 28 2 0 4819.31 5051.52 67.22 o 30 2 0 2512.05 2483.85 50.90 o 32 2 0 70.33 66.24 6.36 o 1 3 0 42.10 57.70 3.83 o 3 3 0 513.80 413.70 10.45 o 5 3 0 10072.40 9962.39 56.10 o 7 3 0 6512.28 6439.61 65.52 o 9 3 0 27.46 45.51 5.57 o 11 3 0 2266.20 2050.16 39.99 o 13 3 0 1871.59 2320.83 40.15 o 15 3 0 5146.79 5567.17 156.94 o 17 3 0 196.83 253.97 16.15 o 19 3 0 3226.76 3193.42 42.64 o 21 3 0 10.96 3.27 7.39 o 23 3 0 2430.22 2380.46 41.67 o 25 3 0 4733.60 4928.49 59.23 o 27 3 0 2701.20 2751.73 47.96 o 29 3 0 2676.28 2609.53 36.29 o 31 3 0 348.95 400.15 13.20 o 0 4 0 22668.57 19837.53 77.39 o 2 4 0 840.74 809.37 16.14 o 4 4 0 85.28 104.32 6.43 o 6 4 0 6536.07 6769.43 98.45 o 8 4 0 9551.41 9667.92 94.44 o 10 4 0 7.67 31.46 4.40 o 12 4 0 4676.16 4435.73 51.34 o 14 4 0 1967.17 2042.79 40.31 o 16 4 0 786.61 720.46 22.04 o 18 4 0 11513.59 11139.73 103.76 o 20 4 0 4026.95 4074.48 98.09 o 22 4 0 49.73 56.20 11.55 o 24 4 0 2138.17 2099.19 43.93 o 26 4 0 2832.24 2897.91 47.58 o 28 4 0 32.28 32.42 7.88 o 30 4 0 1567.75 1457.73 41.45 o 1 5 0 2286.68 2121.23 35.21 o 3 5 0 5495.96 5400.78 73.31 o 5 5 0 6108.15 5977.59 63.64 o 7 5 0 2011.10 2312.45 41.03 o 9 5 0 6907.89 6676.48 100.64 o 11 5 0 10.45 16.27 5.30 o 13 5 0 73.12 101.36 13.24 o 15 5 0 2202.46 2117.05 38.78 o 17 5 0 3497.37 3148.20 62.52 o 19 5 0 3714.96 3696.73 71.50 o 21 5 0 795.53 908.86 36.05 o 23 5 0 4751.29 4801.74 66.48 o 25 5 0 359.45 418.39 19.12 o 27 5 0 668.77 737.49 26.32 o 29 5 0 248.19 253.31 20.45 o 0 6 0 8290.61 7879.18 132.07 o 2 6 0 14496.87 14844.26 158.25 o 4 6 0 5.31 15.39 5.37 o 6 6 0 5456.61 5823.25 68.86 o 8 6 0 3444.51 3260.81 50.65 o 10 6 0 1094.88 1108.33 23.46 o 12 6 0 184.70 225.05 10.94 o 14 6 0 10.12 21.25 7.39 o 16 6 0 702.21 734.71 31.62 o 18 6 0 1461.14 1350.92 43.11 o 20 6 0 3.64 48.18 27.25 o 22 6 0 1540.86 1611.15 36.62 o 24 6 0 3256.12 3312.09 48.23 o 26 6 0 934.61 951.75 41.39 o 28 6 0 270.78 194.26 15.74 o 1 7 0 5309.74 5326.54 55.44 o 3 7 0 948.16 904.46 23.12 o 5 7 0 331.10 276.02 13.13 o 7 7 0 4383.45 4461.06 73.50 o 9 7 0 869.96 928.53 27.89 o 11 7 0 4946.70 4992.08 65.62 o 13 7 0 289.54 333.87 38.05 o 15 7 0 3744.28 3949.87 71.77 o 17 7 0 473.34 521.36 26.27 o 19 7 0 4606.26 4578.55 73.40 o 21 7 0 2474.25 2380.80 40.34 o 23 7 0 1382.87 1435.22 36.32 o 25 7 0 1916.28 1972.05 49.19 o 0 8 0 514.29 514.52 35.65 o 2 8 0 2478.42 2511.69 54.38 o 4 8 0 2120.56 2257.04 51.57 o 6 8 0 337.60 361.66 21.28 o 8 8 0 433.16 432.39 23.76 o 10 8 0 1398.36 1449.76 35.31 o 12 8 0 49.69 42.73 10.95 o 14 8 0 8.55 40.65 30.24 o 16 8 0 1023.75 1082.59 34.55 o 18 8 0 2479.25 2634.46 53.60 o 20 8 0 1014.52 990.38 28.11 o 22 8 0 3166.04 2998.49 41.70 o 1 9 0 8.87 19.36 7.57 o 3 9 0 504.29 499.60 24.17 o 5 9 0 7450.42 7388.18 96.21 o 7 9 0 1628.59 1664.86 42.87 o 9 9 0 1089.88 1048.25 44.65 o 11 9 0 436.32 417.67 32.10 o 13 9 0 47.09 50.42 13.73 o 15 9 0 354.95 377.43 19.59 o 17 9 0 3486.47 3299.02 70.26 o 19 9 0 578.66 491.66 24.02 o 0 10 0 4756.25 4631.04 88.05 o 2 10 0 130.70 127.26 16.22 o 4 10 0 233.21 229.43 20.86 o 6 10 0 5778.16 5846.57 106.64 o 8 10 0 181.35 164.23 19.27 o 10 10 0 856.04 874.02 38.91 o 12 10 0 1020.30 975.45 33.00 o 14 10 0 133.52 105.32 8.36 o 1 11 0 552.81 468.35 24.63 o 3 11 0 568.28 524.29 25.65 o 5 11 0 1543.21 1398.64 39.66 o 7 11 0 1982.99 1868.42 43.70 o 9 11 0 15.01 11.70 5.10 o -33 1 1 264.05 276.63 14.14 o -31 1 1 1207.12 1155.88 34.65 o -29 1 1 5.93 23.11 9.34 o -27 1 1 11.73 11.41 7.29 o -25 1 1 457.43 526.32 24.40 o -23 1 1 7573.51 7357.66 57.86 o -21 1 1 14445.41 14615.63 106.03 o -19 1 1 3151.33 3002.88 53.12 o -17 1 1 6586.93 6982.69 103.54 o -15 1 1 1953.72 2258.08 52.89 o -13 1 1 562.03 574.06 15.17 o -11 1 1 7127.88 8040.12 60.35 o -9 1 1 24721.49 23745.36 79.86 o -7 1 1 6897.27 6888.34 41.35 o -5 1 1 5962.85 5332.70 46.82 o -3 1 1 11550.76 10533.45 178.34 o -1 1 1 4.98 6.12 1.52 o 1 1 1 8334.14 7955.95 27.30 o 3 1 1 11015.56 10288.54 84.83 o 5 1 1 14925.64 14471.65 57.02 o 7 1 1 17265.06 16061.13 156.17 o 9 1 1 5281.57 5190.21 46.07 o 11 1 1 21429.45 22609.84 87.73 o 13 1 1 71.43 128.98 9.65 o 15 1 1 527.78 699.99 23.38 o 17 1 1 420.20 547.19 22.50 o 19 1 1 5691.74 6105.32 80.02 o 21 1 1 3861.12 3978.92 45.93 o 23 1 1 2801.05 3063.69 62.48 o 25 1 1 10847.66 10964.91 108.29 o 27 1 1 9445.33 9753.08 148.81 o 29 1 1 1605.35 1621.18 49.05 o 31 1 1 17.89 13.95 7.08 o 33 1 1 1.39 7.75 6.05 o -32 2 1 25.10 21.18 4.10 o -30 2 1 757.58 737.20 27.96 o -28 2 1 2.55 3.56 5.83 o -26 2 1 12.19 17.74 7.34 o -24 2 1 318.46 397.80 18.17 o -22 2 1 2419.00 2357.44 32.16 o -20 2 1 1.63 7.40 3.75 o -18 2 1 2114.93 2175.48 51.77 o -16 2 1 1607.50 2076.98 40.00 o -14 2 1 4361.34 4637.14 79.42 o -12 2 1 1205.65 1222.79 20.45 o -10 2 1 1.54 10.66 3.84 o -8 2 1 263.66 210.84 8.25 o -6 2 1 2414.42 2165.25 22.13 o -4 2 1 2672.92 2566.74 28.59 o -2 2 1 274.76 321.76 5.68 o 0 2 1 169.97 158.05 5.32 o 4 2 1 4309.74 4333.04 37.68 o 6 2 1 926.42 958.97 14.62 o 8 2 1 2972.25 3166.75 34.89 o 10 2 1 1391.84 1468.43 34.94 o 12 2 1 477.45 726.88 20.92 o 14 2 1 742.99 795.83 32.48 o 16 2 1 327.18 325.30 17.14 o 18 2 1 1188.52 1275.16 35.59 o 20 2 1 1.08 48.53 23.18 o 22 2 1 401.75 401.03 13.79 o 24 2 1 1183.47 1220.85 44.60 o 26 2 1 1806.81 1867.33 43.75 o 28 2 1 787.18 760.06 31.79 o 30 2 1 126.02 124.87 12.61 o 32 2 1 153.47 141.58 8.55 o -31 3 1 291.70 320.96 15.41 o -29 3 1 322.52 341.60 13.17 o -27 3 1 35.57 38.42 7.77 o -25 3 1 3652.36 3729.38 51.38 o -23 3 1 3863.35 3974.20 53.65 o -21 3 1 601.47 619.36 20.14 o -19 3 1 614.72 603.65 23.08 o -17 3 1 1905.61 2001.18 61.19 o -15 3 1 1308.85 1537.88 50.33 o -13 3 1 1933.71 1984.04 29.52 o -11 3 1 571.13 593.12 22.75 o -9 3 1 2038.15 2279.86 26.82 o -7 3 1 17821.70 17029.54 76.10 o -5 3 1 3941.36 3635.68 122.91 o -3 3 1 621.68 576.25 11.12 o -1 3 1 7779.83 7376.92 28.11 o 1 3 1 88.25 86.19 4.41 o 3 3 1 2079.18 2078.70 27.34 o 5 3 1 48.52 92.68 5.82 o 7 3 1 3596.85 3529.27 56.97 o 9 3 1 7282.12 7746.87 60.71 o 11 3 1 10875.16 11125.53 80.12 o 13 3 1 96.98 81.34 8.38 o 15 3 1 136.78 92.00 13.60 o 17 3 1 3924.78 3917.06 77.48 o 19 3 1 4727.04 4542.31 63.10 o 21 3 1 4634.21 4277.03 48.37 o 23 3 1 157.76 146.61 11.14 o 25 3 1 3400.72 3384.05 55.89 o 27 3 1 124.87 114.40 20.49 o 29 3 1 75.08 82.14 8.42 o 31 3 1 741.16 771.51 17.84 o -30 4 1 795.14 858.36 38.36 o -28 4 1 1348.93 1388.05 57.58 o -26 4 1 438.61 501.75 17.60 o -24 4 1 4412.13 4479.71 54.40 o -22 4 1 457.28 449.93 38.71 o -20 4 1 369.90 339.64 21.48 o -18 4 1 317.90 324.69 20.08 o -16 4 1 3371.05 3187.45 57.65 o -14 4 1 8314.13 8877.72 159.80 o -12 4 1 6578.14 7096.48 70.45 o -10 4 1 1711.31 2176.00 30.08 o -8 4 1 68.11 91.18 7.32 o -6 4 1 0.54 10.59 2.76 o -4 4 1 9962.54 9644.34 96.25 o -2 4 1 10995.53 10702.26 75.60 o 0 4 1 48.74 67.63 4.30 o 2 4 1 9032.20 8587.34 47.16 o 4 4 1 36.76 66.21 4.79 o 6 4 1 700.86 838.95 16.92 o 8 4 1 2770.94 2672.15 32.04 o 10 4 1 7429.31 7791.30 67.62 o 12 4 1 918.26 1151.83 31.62 o 14 4 1 248.19 212.58 13.65 o 16 4 1 7724.23 7755.30 93.75 o 18 4 1 2649.77 2888.50 46.41 o 20 4 1 989.29 982.83 25.17 o 22 4 1 2163.88 1935.60 55.22 o 24 4 1 6.83 13.16 6.65 o 26 4 1 121.64 118.84 10.63 o 28 4 1 10.35 18.77 7.21 o 30 4 1 2999.67 2780.40 61.05 o -29 5 1 1073.61 1149.35 42.67 o -27 5 1 1049.12 1125.63 49.72 o -25 5 1 969.22 1004.43 36.93 o -23 5 1 4190.78 4209.27 112.72 o -21 5 1 78.37 97.58 12.68 o -19 5 1 739.14 681.28 46.06 o -17 5 1 4405.63 4227.95 71.05 o -15 5 1 3615.76 3630.81 67.05 o -13 5 1 866.40 936.21 22.16 o -11 5 1 1265.52 1475.94 36.26 o -9 5 1 6645.74 6934.74 76.36 o -7 5 1 124.91 121.75 9.67 o -5 5 1 244.09 197.65 12.07 o -3 5 1 178.73 267.51 14.08 o -1 5 1 4199.72 4407.29 55.23 o 1 5 1 3006.00 3025.91 27.91 o 3 5 1 3802.78 3666.64 36.03 o 5 5 1 3139.09 3101.79 41.11 o 7 5 1 4298.62 4755.87 44.99 o 9 5 1 9525.04 9671.36 84.59 o 11 5 1 901.27 963.65 26.14 o 13 5 1 704.80 728.87 18.37 o 15 5 1 1158.61 1199.19 26.54 o 17 5 1 324.74 291.65 13.77 o 19 5 1 1685.95 1652.88 48.97 o 21 5 1 1042.60 1082.68 32.65 o 23 5 1 2843.57 2707.71 50.09 o 25 5 1 267.55 260.35 18.54 o 27 5 1 162.08 167.90 13.59 o 29 5 1 1066.05 953.48 33.06 o -28 6 1 349.44 368.87 22.21 o -26 6 1 624.41 642.20 24.96 o -24 6 1 273.13 295.03 19.59 o -22 6 1 1.90 3.41 11.76 o -20 6 1 2836.72 2809.63 91.57 o -18 6 1 4594.15 4706.07 119.13 o -16 6 1 216.04 233.62 27.91 o -14 6 1 3498.91 3536.95 54.39 o -12 6 1 6549.64 6720.45 74.69 o -10 6 1 2957.95 3239.38 52.97 o -8 6 1 4954.08 5135.21 69.41 o -6 6 1 34.66 62.16 8.74 o -4 6 1 8829.90 9168.50 87.32 o -2 6 1 199.78 208.58 13.83 o 0 6 1 9088.93 8702.78 137.58 o 2 6 1 1168.94 1249.57 53.62 o 4 6 1 2180.71 2114.57 70.45 o 6 6 1 12134.72 12144.15 169.47 o 8 6 1 28.33 57.36 13.43 o 10 6 1 319.41 338.41 16.81 o 12 6 1 108.82 131.44 15.26 o 14 6 1 9090.69 9353.37 110.00 o 16 6 1 1215.74 1345.54 60.40 o 18 6 1 2488.89 2618.25 49.59 o 20 6 1 486.58 516.05 23.72 o 22 6 1 75.37 86.85 11.42 o 24 6 1 1947.06 1923.52 36.58 o 26 6 1 4761.34 5033.85 225.99 o -25 7 1 939.87 947.91 26.36 o -23 7 1 1410.76 1432.29 37.39 o -21 7 1 543.36 509.53 36.12 o -19 7 1 1881.48 1957.80 51.81 o -17 7 1 13896.74 14585.28 205.69 o -15 7 1 1663.64 1808.80 72.63 o -13 7 1 87.05 85.41 18.10 o -11 7 1 2402.66 2461.57 58.88 o -9 7 1 2958.59 3010.23 63.43 o -7 7 1 3308.72 3301.51 80.31 o -5 7 1 53.00 59.93 6.42 o -3 7 1 45.50 50.59 7.61 o -1 7 1 524.28 464.04 19.83 o 1 7 1 1046.37 1099.91 36.72 o 3 7 1 1932.51 2061.68 48.47 o 5 7 1 1009.97 1045.58 33.70 o 7 7 1 3369.28 3367.32 62.69 o 9 7 1 145.82 148.56 33.87 o 11 7 1 152.15 164.90 15.83 o 13 7 1 1982.42 2045.34 52.28 o 15 7 1 913.64 974.69 41.20 o 17 7 1 336.79 367.58 18.48 o 19 7 1 45.70 50.78 7.48 o 21 7 1 793.44 755.55 22.66 o 23 7 1 18.45 35.18 6.30 o 25 7 1 1513.12 1371.78 52.32 o -24 8 1 2860.96 3020.50 55.19 o -22 8 1 28.15 40.84 6.75 o -20 8 1 2602.23 2580.55 47.57 o -18 8 1 137.31 171.55 15.75 o -16 8 1 7416.45 8092.46 144.41 o -14 8 1 630.83 660.38 43.24 o -12 8 1 1205.67 1338.34 60.98 o -10 8 1 2906.64 2978.14 64.65 o -8 8 1 860.78 803.69 47.94 o -6 8 1 190.11 180.88 23.82 o -4 8 1 3336.64 3479.59 95.76 o -2 8 1 2138.58 2131.15 74.31 o 0 8 1 81.35 110.14 18.82 o 2 8 1 2659.32 2926.58 309.20 o 4 8 1 684.85 730.95 29.73 o 6 8 1 73.73 94.91 12.14 o 8 8 1 1006.56 1186.13 104.73 o 10 8 1 38.58 39.05 9.09 o 12 8 1 175.43 149.10 14.73 o 14 8 1 1094.62 1128.24 37.66 o 16 8 1 3164.30 3317.61 49.59 o 18 8 1 2.73 3.94 4.80 o 20 8 1 720.94 692.04 23.31 o 22 8 1 1650.56 1567.81 42.61 o -21 9 1 4.70 12.44 5.02 o -19 9 1 925.45 889.13 33.94 o -17 9 1 836.05 830.22 26.66 o -15 9 1 632.76 691.95 38.56 o -13 9 1 23.55 23.29 11.99 o -11 9 1 11.55 21.63 11.20 o -9 9 1 387.73 407.18 25.26 o -7 9 1 2163.91 2201.57 75.04 o -5 9 1 3109.90 3214.91 90.32 o -3 9 1 408.70 414.69 33.67 o -1 9 1 5764.53 5842.40 120.21 o 1 9 1 1763.68 1764.31 65.91 o 3 9 1 76.71 89.06 17.29 o 5 9 1 2776.53 2850.44 55.99 o 7 9 1 830.19 825.75 34.01 o 9 9 1 2045.41 2091.17 49.36 o 11 9 1 1947.46 1956.01 95.88 o 13 9 1 92.15 69.11 7.27 o 15 9 1 400.20 395.72 14.89 o 17 9 1 1573.92 1411.95 28.88 o -16 10 1 434.18 374.94 17.93 o -14 10 1 2131.27 2126.52 100.00 o -12 10 1 47.88 50.56 11.54 o -10 10 1 11.76 24.55 10.11 o -8 10 1 43.63 31.91 10.75 o -6 10 1 13.82 20.37 10.46 o -4 10 1 703.70 683.00 37.03 o -2 10 1 53.44 54.28 12.23 o 0 10 1 505.67 516.56 32.40 o 2 10 1 119.32 118.19 16.56 o 4 10 1 72.91 94.55 10.39 o 6 10 1 547.41 526.56 21.84 o 8 10 1 4796.06 4593.76 59.59 o 10 10 1 1662.63 1543.74 73.65 o 12 10 1 1621.25 1685.22 46.70 o -9 11 1 3464.18 3381.54 56.50 o -7 11 1 538.38 514.39 24.17 o -5 11 1 953.26 900.40 33.27 o -3 11 1 1573.48 1531.81 44.15 o -1 11 1 2.89 -0.29 4.54 o 1 11 1 1927.67 1728.77 42.01 o 3 11 1 2255.86 2040.17 44.51 o 5 11 1 26.76 21.98 6.23 o -34 0 2 3470.90 3827.71 59.71 o -32 0 2 8157.10 8533.61 120.69 o -30 0 2 1682.46 1777.48 66.04 o -28 0 2 850.11 697.69 46.93 o -26 0 2 11549.90 12345.22 133.03 o -24 0 2 4925.78 4978.85 84.96 o -22 0 2 860.18 941.86 28.22 o -20 0 2 2720.56 2697.52 65.26 o -18 0 2 11202.81 11016.80 137.29 o -16 0 2 1654.39 1976.50 54.16 o -14 0 2 44809.70 43402.64 232.39 o -12 0 2 16933.54 16422.79 130.93 o -10 0 2 1.70 12.97 4.38 o -8 0 2 17023.50 15552.13 100.62 o -6 0 2 18.78 23.61 4.17 o -4 0 2 275.54 252.09 9.78 o -2 0 2 6243.85 5327.76 37.66 o 0 0 2 204.75 273.76 15.75 o 2 0 2 16050.50 15215.35 48.93 o 6 0 2 26992.47 23704.97 118.99 o 8 0 2 6481.51 5791.08 66.62 o 10 0 2 1259.29 1194.31 34.05 o 12 0 2 447.11 251.07 17.78 o 14 0 2 894.11 806.12 34.28 o 16 0 2 673.01 753.25 36.18 o 18 0 2 23054.23 22730.75 150.01 o 20 0 2 412.78 415.43 19.23 o 22 0 2 118.98 147.10 15.17 o 24 0 2 1540.04 1767.53 77.12 o 26 0 2 7508.75 7914.41 160.69 o 28 0 2 433.71 440.10 37.38 o 30 0 2 528.56 556.39 37.00 o 32 0 2 1916.46 1972.14 56.11 o -33 1 2 2159.56 2123.92 36.39 o -31 1 2 1945.99 1958.08 43.99 o -29 1 2 1562.65 1517.65 44.81 o -27 1 2 5353.69 5327.55 72.05 o -25 1 2 6498.53 6465.91 82.01 o -23 1 2 21.19 27.98 4.87 o -21 1 2 0.38 11.70 5.55 o -19 1 2 204.13 225.46 14.63 o -17 1 2 7264.33 7266.78 128.98 o -15 1 2 1889.69 1751.45 26.18 o -13 1 2 539.60 471.95 12.91 o -11 1 2 6391.32 6702.90 37.52 o -9 1 2 754.71 595.65 13.65 o -7 1 2 170.76 176.76 6.08 o -5 1 2 192.19 210.31 5.81 o -3 1 2 10493.61 9538.42 34.11 o -1 1 2 20584.29 17659.35 85.77 o 1 1 2 383.98 325.31 10.70 o 3 1 2 3638.14 3481.08 78.93 o 5 1 2 48274.48 43101.50 504.98 o 7 1 2 1320.68 1306.98 22.49 o 9 1 2 12545.73 12184.51 73.10 o 11 1 2 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