#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/19/2231907.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231907_Fobs loop_ _publ_author_name 'Pansuriya, Pramod' 'Naidu, Hariska' 'Friedrich, Holger B.' 'Maguire, Glenn E. M.' _publ_section_title ; 1,1'-(Propane-1,3-diyl)bis(3-phenylurea) ; _journal_coeditor_code HG5067 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2552 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.957 _cell_angle_gamma 90.000 _cell_length_a 33.8111 _cell_length_b 4.5980 _cell_length_c 9.8909 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7443 _[local]_cod_data_source_file hg5067Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' twin4s in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 217.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 7476.62 6927.28 121.72 o 6 0 0 203.64 175.11 2.58 o 8 0 0 4000.29 3935.65 49.03 o 10 0 0 1504.80 1351.64 17.22 o 12 0 0 13.83 9.10 0.99 o 14 0 0 2512.05 2418.42 30.55 o 16 0 0 3.04 5.35 1.08 o 18 0 0 192.85 233.34 3.89 o 20 0 0 209.66 162.49 3.10 o 22 0 0 45.30 50.39 1.88 o 24 0 0 876.62 810.54 11.31 o 26 0 0 337.96 309.73 5.30 o 28 0 0 492.05 455.99 7.23 o 30 0 0 0.62 5.82 1.92 o 32 0 0 1990.44 1909.08 25.38 o 34 0 0 29.87 31.39 2.39 o 36 0 0 876.68 834.70 12.43 o 38 0 0 2371.38 2429.82 32.24 o 40 0 0 60.33 65.60 3.52 o 42 0 0 65.67 61.89 3.61 o 44 0 0 30.13 41.62 3.43 o 1 1 0 6708.11 6620.45 57.39 o 3 1 0 2145.70 2155.89 17.97 o 5 1 0 251.78 306.92 2.58 o 7 1 0 145.20 188.39 1.74 o 9 1 0 504.16 510.56 4.13 o 11 1 0 96.79 100.55 1.36 o 13 1 0 3972.06 4088.01 33.64 o 15 1 0 217.88 208.66 2.16 o 17 1 0 2842.38 2918.33 23.04 o 19 1 0 1244.79 1238.75 10.14 o 21 1 0 1492.70 1436.71 11.73 o 23 1 0 51.50 51.00 1.13 o 25 1 0 2603.05 2418.28 22.10 o 27 1 0 291.15 259.53 3.38 o 29 1 0 46.03 40.92 1.60 o 31 1 0 617.77 567.95 6.24 o 33 1 0 439.20 418.03 5.07 o 35 1 0 213.15 215.51 3.61 o 37 1 0 162.44 153.81 3.05 o 39 1 0 134.39 143.58 3.10 o 41 1 0 2.21 4.60 1.97 o 43 1 0 10.33 8.21 2.11 o 0 2 0 9037.82 10711.94 117.59 o 2 2 0 196.14 254.74 2.44 o 4 2 0 1636.12 1741.90 13.84 o 6 2 0 130.13 161.69 1.69 o 8 2 0 1562.49 1711.16 12.01 o 10 2 0 4.94 3.94 0.66 o 12 2 0 1891.37 2020.61 16.24 o 14 2 0 897.51 1025.72 8.54 o 16 2 0 552.56 549.27 4.93 o 18 2 0 3549.67 3808.59 30.22 o 20 2 0 290.68 291.58 3.10 o 22 2 0 44.69 42.56 1.22 o 24 2 0 0.00 0.33 0.94 o 26 2 0 126.62 128.47 2.11 o 28 2 0 15.36 11.78 1.22 o 30 2 0 5.01 7.84 1.22 o 32 2 0 118.78 101.87 2.72 o 34 2 0 3.02 6.33 1.64 o 36 2 0 159.96 153.34 3.47 o 38 2 0 81.51 85.45 2.82 o 40 2 0 60.32 58.93 2.63 o 42 2 0 30.69 36.36 2.63 o 1 3 0 9.93 7.04 0.70 o 3 3 0 0.97 2.25 0.66 o 5 3 0 56.01 70.20 1.17 o 7 3 0 163.35 163.01 1.92 o 9 3 0 153.70 167.00 2.16 o 11 3 0 24.71 25.71 1.13 o 13 3 0 2224.60 2215.72 18.68 o 15 3 0 69.02 71.79 1.55 o 17 3 0 3422.16 3431.29 28.58 o 19 3 0 1623.93 1541.54 13.42 o 21 3 0 1467.91 1443.89 12.67 o 23 3 0 0.74 -0.28 1.22 o 25 3 0 142.46 151.00 2.77 o 27 3 0 11.56 13.19 1.41 o 29 3 0 12.32 11.82 1.64 o 31 3 0 92.57 79.58 2.53 o 33 3 0 5.77 5.96 1.74 o 35 3 0 0.10 2.16 1.78 o 37 3 0 47.41 62.92 2.91 o 39 3 0 104.18 121.95 3.71 o 0 4 0 0.45 2.58 1.83 o 2 4 0 485.84 474.43 6.01 o 4 4 0 3.04 4.18 1.36 o 6 4 0 49.81 42.46 1.74 o 8 4 0 100.45 98.58 2.35 o 10 4 0 1.10 0.52 1.41 o 12 4 0 547.83 577.75 7.09 o 14 4 0 1048.89 1075.69 12.01 o 16 4 0 27.91 31.86 1.78 o 18 4 0 2658.30 2675.98 27.73 o 20 4 0 143.66 145.69 3.05 o 22 4 0 0.43 2.16 1.60 o 24 4 0 33.31 38.05 2.06 o 26 4 0 117.25 119.46 2.96 o 28 4 0 0.74 0.19 1.60 o 30 4 0 57.53 64.57 2.86 o 32 4 0 36.93 33.03 2.44 o 34 4 0 1.50 3.47 2.06 o 1 5 0 1112.45 1036.23 11.92 o 3 5 0 78.60 78.59 2.39 o 5 5 0 14.75 9.01 1.60 o 7 5 0 393.93 390.86 6.05 o 9 5 0 131.94 133.45 3.28 o 11 5 0 21.68 21.91 1.83 o 13 5 0 75.40 77.05 2.44 o 15 5 0 33.76 35.90 2.06 o 17 5 0 4.89 4.13 1.64 o 19 5 0 72.87 69.54 2.49 o 21 5 0 6.94 6.52 2.02 o 23 5 0 19.72 19.29 2.16 o 25 5 0 7.06 6.29 1.97 o 0 6 0 1380.05 1355.44 26.60 o 2 6 0 146.50 149.17 3.71 o 4 6 0 22.80 20.83 2.11 o 6 6 0 3.62 2.53 1.97 o 8 6 0 75.82 71.79 2.58 o 10 6 0 2.30 3.43 1.88 o -43 1 1 11.83 13.89 1.78 o -41 1 1 230.71 238.46 4.08 o -39 1 1 3.93 4.55 1.45 o -37 1 1 7.21 11.17 1.50 o -35 1 1 62.46 71.04 2.02 o -33 1 1 1.80 1.13 1.13 o -31 1 1 28.53 33.27 1.50 o -29 1 1 41.10 50.16 1.60 o -27 1 1 195.39 207.96 2.96 o -25 1 1 75.40 88.07 1.83 o -23 1 1 600.07 614.49 5.77 o -21 1 1 585.14 634.53 5.91 o -19 1 1 5.04 10.75 0.75 o -17 1 1 977.66 1041.77 8.49 o -15 1 1 372.65 420.75 3.71 o -13 1 1 223.66 226.02 2.21 o -11 1 1 43.36 44.53 0.84 o -9 1 1 615.85 608.86 4.79 o -7 1 1 74.52 60.06 0.89 o -5 1 1 1008.65 1021.73 8.63 o -3 1 1 21405.24 22053.01 242.73 o -1 1 1 1289.40 1340.57 16.56 o 1 1 1 644.81 684.46 7.23 o 3 1 1 701.76 773.14 8.07 o 5 1 1 1011.72 1021.69 9.20 o 7 1 1 57.73 52.79 0.89 o 9 1 1 289.06 307.34 2.77 o 11 1 1 1881.93 1953.09 15.48 o 13 1 1 1516.35 1516.76 12.15 o 15 1 1 4159.69 4404.31 32.94 o 17 1 1 34.01 27.50 0.80 o 19 1 1 17.49 21.91 0.84 o 21 1 1 175.99 166.90 2.02 o 23 1 1 170.43 148.46 2.06 o 25 1 1 145.59 136.64 2.25 o 27 1 1 0.15 0.70 0.99 o 29 1 1 731.69 731.80 7.60 o 31 1 1 225.49 211.43 3.43 o 33 1 1 174.14 169.15 3.10 o 35 1 1 194.17 207.35 3.52 o 37 1 1 2.02 1.27 1.55 o 39 1 1 9.84 15.63 1.88 o 41 1 1 34.86 55.88 9.57 o 43 1 1 68.84 89.06 3.43 o -42 2 1 14.56 21.54 2.25 o -40 2 1 146.22 154.14 3.94 o -38 2 1 8.68 6.29 1.83 o -36 2 1 13.89 12.39 1.83 o -34 2 1 259.26 222.83 3.71 o -32 2 1 19.47 17.36 1.50 o -30 2 1 74.99 70.66 2.06 o -28 2 1 837.07 745.27 8.31 o -26 2 1 20.31 21.68 1.13 o -24 2 1 9.49 9.53 0.94 o -22 2 1 110.50 102.85 1.69 o -20 2 1 123.31 125.00 1.69 o -18 2 1 147.22 145.13 1.78 o -16 2 1 45.59 45.84 1.03 o -14 2 1 295.95 287.63 2.72 o -12 2 1 0.28 0.14 0.56 o -10 2 1 242.96 239.87 2.30 o -8 2 1 157.16 171.08 1.88 o -6 2 1 3.39 4.32 0.61 o -4 2 1 160.45 153.58 1.78 o -2 2 1 1425.80 1659.69 16.00 o 0 2 1 12.09 16.09 0.80 o 2 2 1 22.72 26.51 0.89 o 4 2 1 64.34 80.99 1.31 o 6 2 1 136.05 137.53 1.78 o 8 2 1 97.17 106.28 1.50 o 10 2 1 218.56 233.25 2.39 o 12 2 1 261.49 264.78 2.53 o 14 2 1 9.35 7.84 0.66 o 16 2 1 34.96 35.47 0.94 o 18 2 1 39.00 39.46 1.03 o 20 2 1 50.37 46.73 1.27 o 22 2 1 206.12 199.23 2.58 o 24 2 1 3.08 2.72 0.99 o 26 2 1 1.46 5.11 1.13 o 28 2 1 65.61 57.48 1.88 o 30 2 1 152.57 138.28 3.00 o 32 2 1 38.82 34.53 1.97 o 34 2 1 12.41 11.26 1.69 o 36 2 1 15.04 20.51 8.77 o 38 2 1 112.05 128.24 7.98 o 40 2 1 21.34 24.87 6.71 o -39 3 1 1.52 4.69 2.21 o -37 3 1 16.69 15.91 2.39 o -35 3 1 72.75 66.16 3.19 o -33 3 1 0.91 -1.41 1.83 o -31 3 1 0.58 3.33 1.64 o -29 3 1 4.00 5.11 1.50 o -27 3 1 2.09 -1.17 1.17 o -25 3 1 5.17 4.50 1.27 o -23 3 1 8.67 9.15 1.22 o -21 3 1 88.49 86.15 1.78 o -19 3 1 97.73 96.38 1.78 o -17 3 1 41.62 41.06 1.27 o -15 3 1 3.19 3.05 0.84 o -13 3 1 0.03 0.61 0.75 o -11 3 1 506.51 526.47 5.02 o -9 3 1 162.60 148.13 1.97 o -7 3 1 186.28 192.76 2.67 o -5 3 1 52.95 78.17 1.50 o -3 3 1 2099.25 2607.52 23.18 o -1 3 1 474.92 500.00 5.07 o 1 3 1 650.79 760.56 7.32 o 3 3 1 46.59 44.44 1.22 o 5 3 1 417.91 463.50 4.79 o 7 3 1 6.76 8.82 0.94 o 9 3 1 87.16 95.91 1.74 o 11 3 1 77.89 70.38 1.45 o 13 3 1 2.71 2.86 0.80 o 15 3 1 60.13 54.62 1.41 o 17 3 1 40.37 44.01 1.36 o 19 3 1 14.81 14.08 1.17 o 21 3 1 53.66 59.40 1.69 o 23 3 1 36.96 38.29 1.50 o 25 3 1 20.83 20.41 1.36 o 27 3 1 14.63 19.80 6.62 o 29 3 1 475.02 439.76 15.72 o 31 3 1 32.49 30.12 6.62 o 33 3 1 97.74 84.79 7.55 o 35 3 1 13.85 24.96 6.52 o 37 3 1 3.59 4.79 5.16 o -34 4 1 59.40 71.93 9.43 o -32 4 1 23.10 32.99 7.98 o -30 4 1 70.58 92.48 8.87 o -28 4 1 123.53 122.70 9.43 o -26 4 1 8.02 10.79 7.32 o -24 4 1 410.22 430.65 6.71 o -22 4 1 140.70 137.29 3.38 o -20 4 1 542.27 532.47 6.85 o -18 4 1 129.43 137.81 2.96 o -16 4 1 1148.24 1171.23 13.00 o -14 4 1 5.84 6.62 1.41 o -12 4 1 3.77 5.54 1.31 o -10 4 1 49.54 50.91 1.88 o -8 4 1 1.86 0.47 1.31 o -6 4 1 164.07 148.56 3.14 o -4 4 1 655.19 562.74 7.51 o -2 4 1 246.33 199.65 3.28 o 0 4 1 0.82 1.22 1.13 o 2 4 1 6.62 1.45 1.13 o 4 4 1 372.34 375.85 5.02 o 6 4 1 166.87 161.98 2.91 o 8 4 1 411.14 412.54 5.40 o 10 4 1 155.96 154.05 2.72 o 12 4 1 15.49 17.88 1.31 o 14 4 1 1120.70 1123.13 12.43 o 16 4 1 419.37 420.33 5.63 o 18 4 1 131.01 133.02 2.63 o 20 4 1 55.46 59.87 1.97 o 22 4 1 475.23 472.84 5.82 o 24 4 1 1.43 3.14 1.45 o 26 4 1 0.97 1.41 1.45 o 28 4 1 33.76 39.51 2.11 o 30 4 1 1.46 -0.75 1.69 o 32 4 1 71.58 80.47 3.05 o -25 5 1 6.94 6.38 6.38 o -23 5 1 51.81 50.39 7.55 o -21 5 1 88.20 72.54 7.74 o -19 5 1 0.28 1.45 1.60 o -17 5 1 111.25 124.53 3.10 o -15 5 1 180.42 178.12 3.61 o -13 5 1 67.43 74.23 2.53 o -11 5 1 415.77 423.43 5.96 o -9 5 1 12.07 14.97 1.69 o -7 5 1 8.23 8.68 1.69 o -5 5 1 0.14 3.38 1.64 o -3 5 1 13.89 13.65 1.78 o -1 5 1 16.32 18.30 1.83 o 1 5 1 70.66 73.71 2.67 o 3 5 1 258.53 256.15 4.13 o 5 5 1 157.55 149.64 3.05 o 7 5 1 17.13 14.69 1.50 o 9 5 1 240.31 228.18 3.89 o 11 5 1 483.90 478.75 6.43 o 13 5 1 105.82 112.47 2.72 o 15 5 1 572.86 598.54 7.70 o 17 5 1 187.15 155.41 7.51 o 19 5 1 0.30 -0.47 1.45 o 21 5 1 44.91 49.55 5.58 o 23 5 1 9.72 9.85 5.11 o 25 5 1 37.43 41.06 2.30 o -10 6 1 142.18 128.47 8.82 o -8 6 1 54.39 57.25 2.49 o -6 6 1 1.93 5.44 1.88 o -4 6 1 1.28 1.83 1.97 o -2 6 1 14.51 8.59 2.25 o 0 6 1 8.12 4.79 2.16 o 2 6 1 6.99 9.76 2.25 o 4 6 1 5.61 5.96 2.16 o 6 6 1 10.09 14.59 2.82 o 8 6 1 61.62 68.65 3.47 o -44 0 2 626.11 672.63 11.07 o -42 0 2 50.83 49.27 3.10 o -40 0 2 76.44 77.89 3.33 o -38 0 2 119.56 116.46 3.71 o -36 0 2 109.92 107.97 3.47 o -34 0 2 288.48 283.08 5.54 o -32 0 2 1468.04 1399.36 19.10 o -30 0 2 2525.64 2344.38 30.59 o -28 0 2 2389.66 2236.13 29.14 o -26 0 2 171.19 166.90 3.57 o -24 0 2 465.09 405.92 6.33 o -22 0 2 487.10 469.13 6.99 o -20 0 2 962.67 894.67 12.11 o -18 0 2 1007.13 1041.35 13.84 o -16 0 2 605.23 638.99 8.77 o -14 0 2 1272.41 1133.17 14.73 o -12 0 2 6041.27 5489.39 68.32 o -10 0 2 5378.10 5059.16 62.92 o -8 0 2 24588.90 23318.04 289.93 o -6 0 2 47444.37 46922.25 1152.08 o -4 0 2 5657.64 5539.13 79.44 o -2 0 2 4425.30 4178.52 73.48 o 0 0 2 3355.91 3523.77 87.93 o 2 0 2 6304.16 6404.89 158.08 o 4 0 2 35652.42 34950.68 859.05 o 6 0 2 17774.77 17471.85 219.46 o 8 0 2 4126.75 4115.27 46.31 o 10 0 2 4742.71 4551.79 51.24 o 12 0 2 1207.31 1135.89 13.33 o 14 0 2 468.89 533.41 6.76 o 16 0 2 722.19 807.06 9.85 o 18 0 2 864.32 820.15 10.14 o 20 0 2 480.60 472.51 5.82 o 22 0 2 615.35 552.13 8.12 o 24 0 2 240.00 232.27 4.32 o 26 0 2 3320.73 3176.73 40.63 o 28 0 2 3529.75 3408.62 43.64 o 30 0 2 1989.14 1970.74 26.09 o 32 0 2 295.62 302.41 5.68 o 34 0 2 98.84 108.53 4.04 o 36 0 2 151.59 161.41 4.93 o 38 0 2 55.03 62.17 3.61 o 40 0 2 69.40 71.79 3.94 o 42 0 2 478.50 560.02 13.98 o -43 1 2 303.21 322.22 5.07 o -41 1 2 25.85 32.00 2.16 o -39 1 2 3.78 2.63 1.64 o -37 1 2 45.69 35.75 1.88 o -35 1 2 79.45 70.24 2.11 o -33 1 2 154.53 141.28 2.67 o -31 1 2 926.21 817.71 8.45 o -29 1 2 391.56 353.00 4.32 o -27 1 2 634.60 579.30 6.19 o -25 1 2 120.16 115.62 2.11 o -23 1 2 112.91 110.41 1.78 o -21 1 2 681.88 666.72 6.15 o -19 1 2 1151.53 1164.19 10.14 o -17 1 2 140.93 155.22 1.97 o -15 1 2 2510.12 2687.85 20.97 o -13 1 2 3313.83 3441.75 28.43 o -11 1 2 514.99 568.23 5.07 o -9 1 2 453.90 423.61 3.85 o -7 1 2 1647.97 1681.84 15.81 o -5 1 2 18038.65 18158.79 181.31 o -3 1 2 7668.15 8220.22 113.88 o -1 1 2 3201.51 3120.10 52.08 o 1 1 2 9722.21 10216.58 169.91 o 3 1 2 13551.18 13557.26 187.74 o 5 1 2 1984.74 2006.21 20.51 o 7 1 2 357.33 333.43 3.14 o 9 1 2 401.21 448.30 3.89 o 11 1 2 4589.61 4762.71 37.30 o 13 1 2 3291.20 3538.65 26.60 o 15 1 2 167.90 188.06 2.11 o 17 1 2 1220.43 1231.38 10.28 o 19 1 2 580.87 573.25 5.21 o 21 1 2 80.94 79.39 1.50 o 23 1 2 108.33 107.59 1.69 o 25 1 2 460.56 446.79 4.69 o 27 1 2 322.73 313.44 4.22 o 29 1 2 796.99 751.27 8.40 o 31 1 2 215.93 200.26 3.38 o 33 1 2 80.10 73.95 2.58 o 35 1 2 33.01 31.20 2.21 o 37 1 2 3.39 -0.33 1.97 o 39 1 2 34.66 38.15 2.72 o 41 1 2 216.26 242.64 5.16 o -42 2 2 62.90 80.33 3.28 o -40 2 2 56.93 67.19 3.05 o -38 2 2 51.46 53.44 2.49 o -36 2 2 31.37 30.97 2.16 o -34 2 2 24.39 28.34 2.06 o -32 2 2 308.62 296.78 4.69 o -30 2 2 160.67 164.42 3.05 o -28 2 2 249.09 242.87 3.43 o -26 2 2 909.60 921.04 9.20 o -24 2 2 57.51 54.24 1.45 o -22 2 2 136.65 130.73 1.97 o -20 2 2 54.89 49.27 1.22 o -18 2 2 157.09 147.71 1.83 o -16 2 2 84.57 97.13 1.45 o -14 2 2 2436.86 2702.02 20.36 o -12 2 2 1434.82 1592.78 12.20 o -10 2 2 62.03 71.27 1.17 o -8 2 2 1914.55 2109.02 18.82 o -6 2 2 1528.36 1816.13 18.82 o -4 2 2 69.29 74.09 1.64 o -2 2 2 1386.71 1532.81 16.00 o 0 2 2 1389.80 1526.34 15.91 o 2 2 2 60.42 63.49 1.27 o 4 2 2 1248.19 1466.32 14.17 o 6 2 2 1499.90 1661.19 16.00 o 8 2 2 75.99 87.70 1.45 o 10 2 2 1943.24 2126.89 19.19 o 12 2 2 3224.42 3490.83 29.33 o 14 2 2 114.99 129.51 1.92 o 16 2 2 216.21 202.47 2.67 o 18 2 2 76.10 66.30 1.60 o 20 2 2 106.42 106.51 2.16 o 22 2 2 59.57 54.43 1.83 o 24 2 2 680.47 720.54 6.99 o 26 2 2 255.96 242.49 3.43 o 28 2 2 172.59 163.43 3.28 o 30 2 2 358.34 331.74 5.07 o 32 2 2 19.61 20.88 2.06 o 34 2 2 43.04 46.83 2.44 o 36 2 2 71.85 73.67 2.82 o 38 2 2 73.17 87.74 3.10 o 40 2 2 87.02 106.94 3.47 o -39 3 2 26.22 30.64 3.10 o -37 3 2 18.07 15.91 2.77 o -35 3 2 16.29 16.14 2.63 o -33 3 2 39.34 45.94 2.96 o -31 3 2 76.04 70.34 3.19 o -29 3 2 6.82 4.08 2.21 o -27 3 2 662.44 659.21 8.12 o -25 3 2 953.22 962.66 10.32 o -23 3 2 542.71 542.37 6.43 o -21 3 2 334.56 344.88 4.50 o -19 3 2 1585.07 1602.35 15.72 o -17 3 2 1118.95 1147.20 10.84 o -15 3 2 1972.60 2024.79 18.25 o -13 3 2 2102.37 2142.61 19.24 o -11 3 2 199.66 204.44 2.72 o -9 3 2 48.08 51.52 1.60 o -7 3 2 366.67 380.07 4.46 o -5 3 2 99.83 103.42 1.97 o -3 3 2 125.29 128.90 2.35 o -1 3 2 11.88 13.14 1.36 o 1 3 2 154.41 158.55 2.63 o 3 3 2 106.62 107.31 2.16 o 5 3 2 506.87 505.82 6.10 o 7 3 2 48.79 55.51 1.36 o 9 3 2 164.30 167.65 2.30 o 11 3 2 2796.18 2769.92 25.01 o 13 3 2 2758.14 2696.86 23.04 o 15 3 2 803.12 820.76 8.12 o 17 3 2 1256.83 1265.96 12.01 o 19 3 2 269.17 266.19 3.47 o 21 3 2 402.47 393.26 4.65 o 23 3 2 689.40 691.78 6.90 o 25 3 2 479.05 475.60 5.49 o 27 3 2 4.86 3.47 1.50 o 29 3 2 55.72 52.98 1.88 o 31 3 2 28.98 32.70 2.02 o 33 3 2 16.90 13.80 2.02 o 35 3 2 18.06 15.44 2.16 o 37 3 2 18.87 21.21 2.30 o -34 4 2 39.59 33.03 3.47 o -32 4 2 60.03 66.54 3.94 o -30 4 2 57.29 61.80 3.75 o -28 4 2 151.59 150.39 5.02 o -26 4 2 364.87 400.76 6.52 o -24 4 2 171.62 169.95 3.94 o -22 4 2 22.53 20.04 2.21 o -20 4 2 49.79 54.01 2.25 o -18 4 2 56.94 55.51 2.25 o -16 4 2 143.62 154.80 3.14 o -14 4 2 945.16 965.57 10.93 o -12 4 2 744.21 761.36 8.92 o -10 4 2 300.76 314.71 5.02 o -8 4 2 221.78 205.19 3.85 o -6 4 2 39.59 32.42 2.02 o -4 4 2 239.41 243.53 4.22 o -2 4 2 241.59 227.24 3.61 o 0 4 2 296.34 286.41 4.22 o 2 4 2 200.48 206.04 3.43 o 4 4 2 44.76 41.20 1.83 o 6 4 2 158.71 143.44 2.86 o 8 4 2 415.07 422.63 5.63 o 10 4 2 1044.01 1063.82 11.92 o 12 4 2 1325.90 1327.57 14.36 o 14 4 2 182.24 198.01 3.10 o 16 4 2 45.32 45.47 1.64 o 18 4 2 35.56 35.10 1.64 o 20 4 2 16.33 17.55 1.50 o 22 4 2 126.62 118.90 2.44 o 24 4 2 263.06 281.25 4.22 o 26 4 2 138.03 133.54 2.63 o 28 4 2 43.99 51.15 2.06 o 30 4 2 74.70 83.62 2.53 o 32 4 2 46.21 37.82 2.39 o -25 5 2 18.84 23.70 2.53 o -23 5 2 15.08 17.50 2.39 o -21 5 2 70.74 70.90 3.00 o -19 5 2 32.71 34.21 2.35 o -17 5 2 78.26 83.85 2.82 o -15 5 2 72.39 76.44 2.67 o -13 5 2 162.95 171.27 3.61 o -11 5 2 103.79 105.62 2.96 o -9 5 2 231.67 224.85 4.46 o -7 5 2 606.34 564.24 8.07 o -5 5 2 412.24 403.34 7.18 o -3 5 2 83.71 77.80 3.24 o -1 5 2 98.86 90.56 3.43 o 1 5 2 75.36 69.49 3.14 o 3 5 2 321.88 302.84 6.01 o 5 5 2 433.14 401.70 7.18 o 7 5 2 171.95 170.98 4.41 o 9 5 2 83.28 75.73 3.28 o 11 5 2 119.42 124.81 4.50 o 13 5 2 101.10 101.45 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