#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/19/2231911.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231911_Fobs loop_ _publ_author_name 'Moreno-Fuquen, Rodolfo' 'Quintero, David E.' 'Zuluaga, Fabio' 'Kennedy, Alan R.' 'De Almeida Santos, Regina H.' _publ_section_title ; 2-Bromo-N-(4-chlorophenyl)-2-methylpropanamide ; _journal_coeditor_code HG5088 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2580 _journal_volume 67 _journal_year 2011 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7449 _cell_length_b 10.1063 _cell_length_c 22.8803 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file hg5088Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' roddec2010d in P b c a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 271.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 27985.10 28230.10 185.28 o 4 0 0 32506.39 32717.50 410.32 o 6 0 0 31915.66 31362.98 359.04 o 8 0 0 237.37 211.47 43.20 o 10 0 0 651.64 628.26 78.62 o 12 0 0 642.74 606.47 87.20 o 2 1 0 3137.09 3111.44 36.86 o 4 1 0 2279.37 2305.62 36.93 o 6 1 0 1937.37 1957.26 45.36 o 8 1 0 4204.48 4040.80 107.54 o 10 1 0 402.68 382.41 45.96 o 12 1 0 1071.41 1002.11 77.41 o 2 2 0 11809.88 12616.93 60.05 o 4 2 0 7904.15 7770.38 195.33 o 6 2 0 35910.85 36342.62 268.60 o 8 2 0 534.81 590.36 44.37 o 10 2 0 1056.63 1164.40 105.85 o 12 2 0 1076.41 1140.15 119.81 o 2 3 0 15819.26 16517.67 165.22 o 4 3 0 17.55 16.45 11.18 o 6 3 0 13268.11 13330.46 160.50 o 8 3 0 5010.99 5162.38 120.13 o 10 3 0 2892.91 2861.32 240.78 o 12 3 0 4007.40 3684.76 216.21 o 0 4 0 22403.22 23712.47 155.90 o 2 4 0 1814.19 1633.74 37.40 o 4 4 0 2254.60 2102.30 36.25 o 6 4 0 9297.69 9447.66 110.53 o 8 4 0 148.68 126.66 24.96 o 10 4 0 1078.29 1162.50 116.37 o 12 4 0 232.17 234.69 76.63 o 2 5 0 14896.04 15494.97 86.43 o 4 5 0 91.62 103.64 12.94 o 6 5 0 9025.79 8877.38 141.90 o 8 5 0 3001.15 3021.26 163.62 o 10 5 0 1337.33 1170.80 121.76 o 0 6 0 1573.64 1784.86 53.92 o 2 6 0 2084.41 2128.72 40.13 o 4 6 0 1033.97 1013.75 35.83 o 6 6 0 38.93 87.26 50.25 o 8 6 0 590.57 578.05 89.34 o 10 6 0 114.48 200.90 72.69 o 2 7 0 5629.92 5642.80 70.40 o 4 7 0 1979.81 1864.93 58.37 o 6 7 0 6014.38 5701.72 152.25 o 8 7 0 5337.56 5548.48 167.94 o 10 7 0 655.64 662.53 69.39 o 0 8 0 14165.95 13551.57 263.21 o 2 8 0 416.74 407.99 37.78 o 4 8 0 494.09 477.36 35.37 o 6 8 0 1397.22 1295.95 79.23 o 8 8 0 250.84 206.04 44.39 o 2 9 0 1516.81 1509.36 69.67 o 4 9 0 146.01 151.25 25.47 o 6 9 0 4459.72 4027.32 142.80 o 8 9 0 1280.92 1245.92 91.34 o 0 10 0 13301.99 13813.90 303.13 o 2 10 0 2476.69 2663.32 96.85 o 4 10 0 106.47 162.93 59.69 o 6 10 0 3068.84 3198.23 133.46 o 8 10 0 13.27 105.63 64.88 o 2 11 0 138.89 136.50 33.86 o 4 11 0 281.79 219.58 64.75 o 6 11 0 107.46 108.67 65.37 o 0 12 0 5004.47 5361.82 213.48 o 2 12 0 566.19 588.01 85.03 o 4 12 0 127.77 148.15 64.08 o 2 13 0 66.12 -48.48 54.66 o 1 1 1 3314.37 3367.96 33.72 o 2 1 1 850.61 934.39 12.56 o 3 1 1 4812.75 4885.87 37.61 o 4 1 1 3352.15 3356.72 46.64 o 5 1 1 14108.54 14057.29 91.47 o 6 1 1 14300.74 14761.85 80.56 o 7 1 1 3963.12 3725.55 47.59 o 8 1 1 4269.00 4288.64 79.42 o 9 1 1 922.92 894.25 41.62 o 10 1 1 2557.16 2823.66 74.78 o 11 1 1 2019.72 2041.47 69.58 o 12 1 1 3517.66 3512.84 95.22 o 0 2 1 456.83 384.98 9.99 o 1 2 1 7014.05 7303.00 33.62 o 2 2 1 7138.45 7153.53 33.09 o 3 2 1 458.65 549.07 11.94 o 4 2 1 248.52 221.49 14.06 o 5 2 1 89.06 81.74 9.37 o 6 2 1 3995.57 3955.60 56.27 o 7 2 1 609.04 544.50 28.29 o 8 2 1 44.52 29.32 16.42 o 9 2 1 167.45 128.37 42.60 o 10 2 1 311.96 342.14 30.60 o 11 2 1 117.52 144.82 36.42 o 12 2 1 94.26 93.82 47.01 o 1 3 1 22358.66 22538.83 57.71 o 2 3 1 524.02 516.49 12.30 o 3 3 1 4093.97 4313.01 28.26 o 4 3 1 6441.16 6718.01 57.84 o 5 3 1 7515.64 7453.06 73.93 o 6 3 1 5756.63 5930.45 69.47 o 7 3 1 757.04 736.07 31.49 o 8 3 1 4660.77 4613.31 80.59 o 9 3 1 752.94 709.12 42.87 o 10 3 1 665.78 763.87 41.25 o 11 3 1 448.05 562.39 115.92 o 12 3 1 1930.97 2097.67 117.92 o 0 4 1 31966.09 31578.67 120.64 o 1 4 1 2267.67 2162.51 21.02 o 2 4 1 8702.60 8124.10 54.22 o 3 4 1 46.29 84.48 5.69 o 4 4 1 9800.97 9472.38 50.52 o 5 4 1 30.16 64.57 7.95 o 6 4 1 5716.82 5556.06 65.54 o 7 4 1 6187.31 6058.86 82.10 o 8 4 1 144.40 147.26 18.95 o 9 4 1 342.97 338.75 37.16 o 10 4 1 330.20 419.81 90.03 o 11 4 1 1070.81 1003.33 84.26 o 12 4 1 8.30 58.69 45.81 o 1 5 1 3081.20 3159.33 31.60 o 2 5 1 1118.81 1167.61 18.77 o 3 5 1 2795.72 3030.55 36.27 o 4 5 1 12.34 23.29 4.49 o 5 5 1 531.65 539.76 13.76 o 6 5 1 2026.66 2055.11 43.17 o 7 5 1 1924.05 1960.95 45.38 o 8 5 1 326.37 349.04 84.67 o 9 5 1 12.27 36.53 35.56 o 10 5 1 912.94 1020.18 82.01 o 11 5 1 13.71 13.87 125.32 o 0 6 1 10430.19 9772.87 101.49 o 1 6 1 5079.77 4917.71 53.65 o 2 6 1 11720.35 11455.86 64.18 o 3 6 1 64.15 93.60 10.94 o 4 6 1 5344.21 5010.30 56.68 o 5 6 1 311.06 331.74 20.11 o 6 6 1 7641.69 7376.37 90.39 o 7 6 1 7215.81 7042.38 173.39 o 8 6 1 443.46 402.18 75.75 o 9 6 1 1226.39 1243.75 86.72 o 10 6 1 262.46 296.48 39.56 o 11 6 1 1734.49 1861.87 112.40 o 1 7 1 317.38 341.45 16.91 o 2 7 1 522.71 530.70 16.77 o 3 7 1 0.28 15.64 8.45 o 4 7 1 9.86 13.63 11.05 o 5 7 1 46.96 52.53 12.71 o 6 7 1 38.90 45.94 25.06 o 7 7 1 482.25 525.67 45.60 o 8 7 1 258.20 247.21 38.44 o 9 7 1 50.32 61.79 34.08 o 10 7 1 52.38 59.71 34.01 o 0 8 1 12699.26 12378.51 177.96 o 1 8 1 1063.57 1048.07 38.21 o 2 8 1 3810.97 3794.34 63.86 o 3 8 1 659.67 641.84 29.30 o 4 8 1 5207.80 5094.56 95.72 o 5 8 1 13.51 13.53 18.95 o 6 8 1 2877.25 2876.68 99.85 o 7 8 1 2632.64 2709.26 83.95 o 8 8 1 397.16 402.33 38.36 o 9 8 1 505.77 555.19 46.83 o 1 9 1 718.70 740.51 36.41 o 2 9 1 403.36 434.83 29.36 o 3 9 1 55.17 107.73 18.90 o 4 9 1 23.91 36.92 17.96 o 5 9 1 997.97 1169.13 55.14 o 6 9 1 515.08 578.47 44.04 o 7 9 1 58.56 163.89 32.65 o 8 9 1 49.08 68.03 28.51 o 9 9 1 43.02 79.25 48.82 o 0 10 1 8496.09 8218.89 166.28 o 1 10 1 3.11 -0.38 18.15 o 2 10 1 1287.05 1313.48 49.83 o 3 10 1 428.65 418.97 38.63 o 4 10 1 3083.38 3042.89 98.55 o 5 10 1 84.74 127.18 34.16 o 6 10 1 412.04 445.84 49.45 o 7 10 1 592.05 644.26 56.78 o 8 10 1 38.98 40.65 67.98 o 1 11 1 645.25 746.67 40.30 o 2 11 1 2.79 40.13 26.29 o 3 11 1 84.69 179.27 45.05 o 4 11 1 805.67 883.27 104.12 o 5 11 1 1355.97 1369.56 91.06 o 6 11 1 1358.61 1463.98 97.02 o 7 11 1 358.40 563.06 101.43 o 0 12 1 162.96 125.12 49.09 o 1 12 1 3.52 -1.44 25.04 o 2 12 1 195.28 166.63 42.15 o 3 12 1 0.79 7.14 79.91 o 4 12 1 112.33 61.98 41.55 o 5 12 1 31.84 40.75 41.61 o 1 13 1 1211.63 1332.75 87.71 o 2 13 1 145.14 190.62 45.96 o 2 0 2 8300.68 8713.04 63.19 o 3 0 2 15665.65 16474.29 183.13 o 4 0 2 4927.31 4901.78 65.78 o 5 0 2 1183.76 1006.11 43.08 o 6 0 2 1793.15 1818.88 47.95 o 7 0 2 13482.98 13527.54 219.76 o 8 0 2 7869.10 7911.39 153.02 o 9 0 2 11662.48 11800.81 200.43 o 10 0 2 66.18 39.23 29.54 o 11 0 2 6471.41 6626.53 350.16 o 12 0 2 841.76 782.89 90.95 o 1 1 2 338.56 403.38 9.82 o 2 1 2 2.68 32.58 3.85 o 3 1 2 450.36 406.96 11.87 o 4 1 2 4217.21 4447.02 37.55 o 5 1 2 3909.78 3895.48 39.77 o 6 1 2 43.59 39.61 8.24 o 7 1 2 591.98 550.03 21.12 o 8 1 2 43.74 45.59 22.12 o 9 1 2 918.25 941.05 42.17 o 10 1 2 5.01 2.72 21.27 o 11 1 2 7.45 -3.30 22.55 o 12 1 2 0.87 100.03 27.23 o 0 2 2 1597.32 1684.94 23.10 o 1 2 2 137.74 220.59 7.78 o 2 2 2 8691.27 9131.18 51.23 o 3 2 2 2320.50 2288.90 24.04 o 4 2 2 447.23 394.84 12.26 o 5 2 2 6928.01 6834.85 66.35 o 6 2 2 1377.59 1389.22 38.40 o 7 2 2 9759.31 9871.20 109.80 o 8 2 2 5152.98 5125.32 85.95 o 9 2 2 11164.84 11285.00 137.50 o 10 2 2 4.55 9.70 19.79 o 11 2 2 6073.74 6193.04 117.35 o 12 2 2 241.81 200.33 139.87 o 1 3 2 16045.89 15441.98 63.38 o 2 3 2 3489.78 3441.67 35.00 o 3 3 2 22081.75 21980.27 85.02 o 4 3 2 3120.91 3009.02 37.60 o 5 3 2 5788.97 5574.11 55.17 o 6 3 2 17.65 20.74 9.96 o 7 3 2 8454.81 8197.95 101.85 o 8 3 2 389.46 418.60 27.40 o 9 3 2 857.81 871.54 40.64 o 10 3 2 972.06 976.73 55.02 o 11 3 2 87.68 -7.80 38.11 o 12 3 2 2.58 70.39 82.40 o 0 4 2 407.39 480.18 13.49 o 1 4 2 208.31 269.06 8.78 o 2 4 2 3245.03 3459.11 33.33 o 3 4 2 225.93 206.90 9.73 o 4 4 2 201.87 194.87 9.31 o 5 4 2 3039.99 3115.16 70.46 o 6 4 2 205.12 195.27 13.92 o 7 4 2 2786.82 2869.57 56.98 o 8 4 2 848.56 872.78 35.76 o 9 4 2 4725.11 4898.62 109.62 o 10 4 2 28.25 26.04 40.69 o 11 4 2 1911.02 1884.66 134.66 o 12 4 2 107.49 65.20 38.44 o 1 5 2 23688.60 22846.85 83.63 o 2 5 2 2678.64 2476.34 54.64 o 3 5 2 30929.21 31226.81 121.51 o 4 5 2 2011.97 1803.74 27.22 o 5 5 2 7896.15 7535.78 65.99 o 6 5 2 3.27 10.08 11.26 o 7 5 2 7645.34 7581.69 87.69 o 8 5 2 4.11 37.03 28.47 o 9 5 2 1139.88 1157.67 80.11 o 10 5 2 2381.66 2345.46 92.52 o 11 5 2 24.78 37.17 32.31 o 0 6 2 287.95 325.68 17.29 o 1 6 2 385.01 401.12 14.17 o 2 6 2 4.51 7.93 5.01 o 3 6 2 89.53 86.14 12.15 o 4 6 2 64.52 71.06 10.87 o 5 6 2 70.13 88.98 10.72 o 6 6 2 298.28 321.01 22.64 o 7 6 2 248.58 252.78 34.13 o 8 6 2 50.94 -10.13 26.87 o 9 6 2 38.03 136.09 38.43 o 10 6 2 4.12 -0.54 29.96 o 11 6 2 5.18 23.36 35.64 o 1 7 2 7997.58 7697.78 72.77 o 2 7 2 99.14 104.48 8.88 o 3 7 2 13246.63 13347.84 90.74 o 4 7 2 3190.15 3046.52 64.55 o 5 7 2 8019.72 8236.68 85.19 o 6 7 2 18.81 29.40 18.94 o 7 7 2 3421.15 3653.67 145.84 o 8 7 2 123.23 65.22 28.75 o 9 7 2 2899.51 3034.73 108.62 o 10 7 2 770.93 827.14 65.82 o 0 8 2 304.71 327.33 35.70 o 1 8 2 331.59 291.41 22.81 o 2 8 2 698.68 666.45 28.51 o 3 8 2 1326.29 1375.91 40.45 o 4 8 2 127.78 133.35 15.03 o 5 8 2 12.15 -13.49 19.69 o 6 8 2 756.92 760.67 45.88 o 7 8 2 1681.31 1649.09 66.86 o 8 8 2 552.90 552.27 45.63 o 9 8 2 482.24 542.34 47.96 o 1 9 2 797.34 735.20 35.92 o 2 9 2 81.21 73.70 14.89 o 3 9 2 6140.33 6466.28 90.64 o 4 9 2 133.26 120.66 21.41 o 5 9 2 1272.07 1338.73 66.50 o 6 9 2 10.39 27.96 25.37 o 7 9 2 2396.81 2317.39 80.88 o 8 9 2 11.30 26.84 36.22 o 9 9 2 798.79 950.05 90.74 o 0 10 2 231.11 265.29 40.36 o 1 10 2 165.06 151.02 20.68 o 2 10 2 776.31 847.58 40.84 o 3 10 2 4.81 10.31 23.62 o 4 10 2 3.24 48.15 44.29 o 5 10 2 452.04 540.99 48.92 o 6 10 2 29.64 32.20 30.71 o 7 10 2 329.03 391.38 49.18 o 8 10 2 1142.82 1618.77 158.46 o 1 11 2 289.17 245.85 28.03 o 2 11 2 39.63 48.89 35.38 o 3 11 2 1262.00 1057.09 76.05 o 4 11 2 110.55 107.90 41.52 o 5 11 2 383.90 470.08 50.06 o 6 11 2 31.50 47.67 33.32 o 7 11 2 73.14 18.80 65.60 o 0 12 2 35.92 21.99 30.44 o 1 12 2 14.69 27.52 25.41 o 2 12 2 257.25 300.32 72.41 o 3 12 2 6.22 15.03 39.90 o 4 12 2 9.94 -15.20 51.40 o 5 12 2 447.90 578.90 69.13 o 1 13 2 15.22 27.06 54.63 o 2 13 2 142.35 146.78 44.30 o 1 1 3 35249.05 35339.34 205.86 o 2 1 3 4114.97 4261.10 29.81 o 3 1 3 68463.48 69462.63 464.26 o 4 1 3 4231.40 4481.65 51.32 o 5 1 3 979.57 777.39 20.45 o 6 1 3 2771.37 2758.02 42.69 o 7 1 3 11064.33 10555.36 164.97 o 8 1 3 1189.29 1167.21 43.74 o 9 1 3 6960.93 6906.79 108.94 o 10 1 3 1664.18 1708.90 59.91 o 11 1 3 279.30 265.46 31.14 o 12 1 3 552.93 571.19 66.36 o 0 2 3 6365.40 6548.78 56.82 o 1 2 3 70.32 76.64 6.46 o 2 2 3 10569.86 10949.65 64.03 o 3 2 3 20.23 45.65 4.68 o 4 2 3 1410.66 1357.16 19.44 o 5 2 3 7400.32 7224.06 111.77 o 6 2 3 41.35 35.82 9.61 o 7 2 3 200.47 180.62 21.56 o 8 2 3 215.86 257.29 23.99 o 9 2 3 5764.55 5774.95 98.99 o 10 2 3 105.82 120.87 22.91 o 11 2 3 1282.33 1248.85 66.22 o 12 2 3 8.09 24.24 36.28 o 1 3 3 7529.15 7547.52 43.93 o 2 3 3 986.44 1016.78 17.94 o 3 3 3 21810.22 21445.71 113.56 o 4 3 3 824.36 882.13 15.61 o 5 3 3 5003.88 5034.45 75.74 o 6 3 3 91.43 78.88 9.40 o 7 3 3 4948.85 4956.84 77.11 o 8 3 3 100.86 82.55 17.18 o 9 3 3 6327.90 6325.89 102.46 o 10 3 3 275.06 276.08 34.21 o 11 3 3 326.77 265.37 49.90 o 12 3 3 331.59 233.74 43.63 o 0 4 3 58.17 42.68 6.53 o 1 4 3 7686.29 7967.32 40.42 o 2 4 3 164.76 107.60 10.27 o 3 4 3 6650.72 6718.78 56.92 o 4 4 3 2923.94 2622.21 99.48 o 5 4 3 6583.46 6408.94 53.32 o 6 4 3 494.61 536.03 24.61 o 7 4 3 462.75 428.47 24.24 o 8 4 3 106.67 78.83 15.48 o 9 4 3 9378.12 9306.27 151.90 o 10 4 3 1108.00 1102.54 63.08 o 11 4 3 2282.13 2286.05 93.69 o 12 4 3 171.88 205.63 39.49 o 1 5 3 3102.29 3090.80 34.34 o 2 5 3 1712.59 1851.19 37.52 o 3 5 3 8201.67 8431.10 74.41 o 4 5 3 609.77 617.76 17.80 o 5 5 3 197.44 192.68 11.67 o 6 5 3 677.81 693.96 20.05 o 7 5 3 2176.05 2232.67 58.77 o 8 5 3 302.88 324.34 29.67 o 9 5 3 77.48 127.28 32.37 o 10 5 3 346.11 467.15 48.82 o 11 5 3 47.62 33.75 30.89 o 0 6 3 3075.82 2843.29 46.17 o 1 6 3 510.89 506.71 16.68 o 2 6 3 2335.66 2128.86 44.88 o 3 6 3 2491.54 2358.21 43.57 o 4 6 3 1524.38 1505.28 34.52 o 5 6 3 10473.55 10413.46 82.69 o 6 6 3 930.08 906.13 36.91 o 7 6 3 148.27 136.18 28.33 o 8 6 3 68.42 23.42 26.16 o 9 6 3 8455.88 8429.07 185.02 o 10 6 3 517.66 599.21 56.15 o 11 6 3 3864.87 3985.59 131.44 o 1 7 3 150.14 149.16 11.86 o 2 7 3 52.17 60.61 7.69 o 3 7 3 95.05 106.73 17.09 o 4 7 3 100.89 106.38 13.98 o 5 7 3 162.34 168.66 17.05 o 6 7 3 476.63 516.35 33.45 o 7 7 3 264.25 297.66 38.28 o 8 7 3 780.86 734.91 55.33 o 9 7 3 92.49 128.36 37.55 o 10 7 3 132.29 129.17 43.91 o 0 8 3 10328.60 10280.62 162.65 o 1 8 3 1755.89 1736.05 43.06 o 2 8 3 4457.49 4498.72 68.94 o 3 8 3 2592.53 2539.84 53.35 o 4 8 3 1482.52 1472.59 46.92 o 5 8 3 3224.71 3214.02 87.35 o 6 8 3 523.96 579.02 38.72 o 7 8 3 384.67 432.65 45.55 o 8 8 3 8.62 -8.98 29.67 o 9 8 3 5198.55 5336.14 148.48 o 1 9 3 1497.82 1612.22 51.27 o 2 9 3 128.30 125.10 17.12 o 3 9 3 2957.03 3227.43 64.91 o 4 9 3 162.09 180.35 25.28 o 5 9 3 11.88 37.60 21.37 o 6 9 3 30.34 72.82 30.79 o 7 9 3 573.27 663.50 53.94 o 8 9 3 49.83 89.51 28.79 o 9 9 3 451.09 506.70 71.53 o 0 10 3 4224.95 4111.01 118.22 o 1 10 3 1134.27 1130.23 45.83 o 2 10 3 753.63 733.96 39.58 o 3 10 3 1132.74 1036.45 48.40 o 4 10 3 251.63 298.53 33.14 o 5 10 3 288.54 202.41 34.96 o 6 10 3 487.37 490.62 49.76 o 7 10 3 413.25 367.21 45.86 o 8 10 3 65.36 36.11 68.53 o 1 11 3 2126.32 2350.12 68.29 o 2 11 3 251.24 229.82 32.84 o 3 11 3 2549.47 2948.86 95.00 o 4 11 3 189.46 255.68 39.60 o 5 11 3 211.77 373.74 46.20 o 6 11 3 51.93 86.27 36.77 o 7 11 3 454.75 557.77 101.31 o 0 12 3 368.61 354.78 72.47 o 1 12 3 33.64 0.42 30.90 o 2 12 3 16.20 43.65 43.20 o 3 12 3 18.24 63.84 54.08 o 4 12 3 7.09 58.35 40.70 o 5 12 3 147.35 126.00 48.48 o 1 13 3 675.76 630.80 93.24 o 2 13 3 408.85 365.05 59.60 o 0 0 4 30709.47 31626.92 209.08 o 1 0 4 31624.70 33018.59 206.11 o 2 0 4 54740.46 56015.73 186.99 o 3 0 4 2084.38 2179.69 39.25 o 4 0 4 68933.38 72578.11 250.02 o 5 0 4 3630.33 4066.15 55.18 o 6 0 4 2127.73 2156.22 50.10 o 7 0 4 3826.59 3951.88 71.52 o 8 0 4 11943.42 11920.81 189.33 o 9 0 4 1463.58 1434.57 153.41 o 10 0 4 482.45 478.86 49.24 o 11 0 4 1939.35 2025.11 99.42 o 12 0 4 66.72 61.39 90.36 o 1 1 4 1677.15 1817.76 17.80 o 2 1 4 392.18 367.50 8.46 o 3 1 4 299.68 315.16 8.07 o 4 1 4 2798.81 2840.09 43.41 o 5 1 4 379.50 385.39 20.06 o 6 1 4 7.16 -0.38 10.74 o 7 1 4 176.36 195.74 20.99 o 8 1 4 1019.37 1035.79 41.59 o 9 1 4 72.38 72.15 18.78 o 10 1 4 425.31 394.81 33.27 o 11 1 4 21.74 14.09 26.95 o 12 1 4 152.80 134.16 34.02 o 0 2 4 20413.12 20904.96 529.84 o 1 2 4 1608.43 1631.63 28.18 o 2 2 4 73597.85 73553.18 484.58 o 3 2 4 388.20 338.38 14.78 o 4 2 4 25578.33 26095.41 84.22 o 5 2 4 6890.62 7528.40 64.25 o 6 2 4 1690.25 1566.11 33.81 o 7 2 4 1549.09 1486.47 34.51 o 8 2 4 5177.18 5079.94 87.08 o 9 2 4 598.47 610.84 36.17 o 10 2 4 253.93 328.47 30.86 o 11 2 4 970.82 987.22 49.80 o 12 2 4 2.26 3.33 28.37 o 1 3 4 1997.46 1881.63 23.08 o 2 3 4 3261.65 3532.69 46.14 o 3 3 4 7376.70 7531.75 85.28 o 4 3 4 7093.02 7087.08 103.73 o 5 3 4 1443.02 1446.89 33.65 o 6 3 4 3249.27 3185.39 41.35 o 7 3 4 260.10 210.89 19.31 o 8 3 4 3290.01 3226.48 68.87 o 9 3 4 36.53 35.48 18.18 o 10 3 4 5829.48 5723.74 109.86 o 11 3 4 325.52 277.89 38.84 o 12 3 4 186.59 147.14 34.75 o 0 4 4 7399.42 8148.89 127.98 o 1 4 4 34.46 29.98 5.15 o 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2159.96 2020.97 74.61 o 10 2 11 112.88 138.72 44.15 o 11 2 11 315.83 466.43 64.56 o 1 3 11 5431.13 5424.66 74.41 o 2 3 11 99.99 113.42 12.44 o 3 3 11 22854.52 22702.29 137.43 o 4 3 11 10.83 19.34 10.98 o 5 3 11 575.12 586.56 26.70 o 6 3 11 13.11 15.23 11.49 o 7 3 11 2109.09 2050.09 58.74 o 8 3 11 618.48 714.23 47.47 o 9 3 11 3660.18 3682.02 100.94 o 10 3 11 217.25 177.26 35.53 o 11 3 11 87.83 112.33 39.60 o 0 4 11 7329.46 7043.51 139.67 o 1 4 11 3031.22 2917.69 53.99 o 2 4 11 1496.83 1481.21 37.34 o 3 4 11 2018.13 2024.59 61.96 o 4 4 11 1507.57 1386.11 40.04 o 5 4 11 2243.62 2131.55 58.71 o 6 4 11 1575.00 1599.74 47.00 o 7 4 11 513.96 520.90 35.86 o 8 4 11 484.17 509.38 43.14 o 9 4 11 5672.37 5523.55 125.93 o 10 4 11 1081.55 1082.99 62.17 o 11 4 11 1323.76 1310.81 89.12 o 1 5 11 1717.58 1687.33 43.82 o 2 5 11 413.15 388.50 18.16 o 3 5 11 4790.37 4783.19 68.22 o 4 5 11 793.71 764.52 42.95 o 5 5 11 157.98 151.67 28.04 o 6 5 11 106.05 120.61 18.38 o 7 5 11 261.02 264.82 28.44 o 8 5 11 7.99 -4.19 23.60 o 9 5 11 236.75 263.84 37.10 o 10 5 11 253.30 315.53 56.26 o 0 6 11 2045.63 1931.02 68.44 o 1 6 11 926.31 968.12 34.40 o 2 6 11 2548.82 2510.85 42.40 o 3 6 11 1094.27 1064.47 50.19 o 4 6 11 161.50 173.85 28.18 o 5 6 11 4159.47 4110.69 102.52 o 6 6 11 1834.66 1837.14 61.18 o 7 6 11 601.78 619.40 38.10 o 8 6 11 644.63 601.23 51.72 o 9 6 11 5439.09 5417.22 173.05 o 10 6 11 558.13 663.99 70.77 o 1 7 11 0.17 26.17 13.86 o 2 7 11 147.53 130.31 16.24 o 3 7 11 69.55 73.52 25.34 o 4 7 11 55.48 55.60 30.27 o 5 7 11 347.03 330.12 36.10 o 6 7 11 160.18 160.18 30.77 o 7 7 11 36.32 14.23 27.44 o 8 7 11 88.92 100.55 40.07 o 9 7 11 64.00 69.79 39.40 o 0 8 11 3263.02 3093.55 92.71 o 1 8 11 135.93 112.90 19.95 o 2 8 11 209.17 218.30 29.96 o 3 8 11 1942.03 1781.71 69.84 o 4 8 11 558.29 568.24 44.27 o 5 8 11 4133.40 4044.89 130.15 o 6 8 11 705.70 758.12 52.95 o 7 8 11 604.20 617.74 51.11 o 8 8 11 616.53 689.09 73.45 o 9 8 11 2161.37 2325.58 191.56 o 1 9 11 448.51 469.41 52.93 o 2 9 11 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o 10 0 12 422.18 440.12 83.54 o 11 0 12 3261.44 3050.19 194.06 o 1 1 12 486.32 511.15 21.94 o 2 1 12 569.61 585.86 19.38 o 3 1 12 15.75 31.88 9.32 o 4 1 12 30.41 39.28 8.89 o 5 1 12 618.87 617.17 23.27 o 6 1 12 0.26 5.39 11.03 o 7 1 12 137.76 117.68 18.23 o 8 1 12 15.46 30.25 19.74 o 9 1 12 666.33 578.47 58.08 o 10 1 12 483.31 529.13 61.00 o 11 1 12 13.23 53.86 45.13 o 0 2 12 91.27 83.00 23.49 o 1 2 12 1463.96 1514.60 35.40 o 2 2 12 3595.65 3447.79 55.53 o 3 2 12 4434.64 4485.38 60.42 o 4 2 12 1203.90 1162.48 24.39 o 5 2 12 6574.75 6474.20 67.48 o 6 2 12 212.03 215.28 17.16 o 7 2 12 3300.39 3463.46 87.79 o 8 2 12 890.55 956.50 51.42 o 9 2 12 3925.12 3864.81 109.05 o 10 2 12 248.14 217.82 77.79 o 11 2 12 2726.85 2728.01 128.82 o 1 3 12 7309.49 6937.72 88.79 o 2 3 12 1437.04 1500.93 36.67 o 3 3 12 4476.15 4131.83 56.25 o 4 3 12 3383.67 3235.54 70.97 o 5 3 12 1081.65 1031.77 50.19 o 6 3 12 652.55 626.23 26.57 o 7 3 12 2265.22 2195.87 63.11 o 8 3 12 9.76 30.10 21.55 o 9 3 12 603.64 535.01 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76.50 65.42 o 4 6 23 2212.39 2201.99 94.23 o 5 6 23 739.80 683.33 60.20 o 6 6 23 810.29 864.84 80.15 o 1 7 23 4.96 30.97 41.39 o 2 7 23 187.25 215.14 68.29 o 3 7 23 93.55 75.08 37.20 o 4 7 23 0.61 15.03 42.97 o 0 8 23 705.11 497.85 93.33 o 0 0 24 540.67 618.82 66.36 o 1 0 24 142.29 120.94 24.05 o 2 0 24 9540.44 9841.62 138.91 o 3 0 24 72.29 61.15 23.00 o 4 0 24 5484.60 5594.17 286.26 o 5 0 24 653.88 740.72 103.52 o 6 0 24 162.99 240.72 78.17 o 7 0 24 72.80 27.70 60.17 o 1 1 24 12.04 50.17 17.71 o 2 1 24 62.64 140.31 23.17 o 3 1 24 159.46 250.88 24.07 o 4 1 24 545.75 597.44 36.33 o 5 1 24 35.84 62.17 30.93 o 6 1 24 41.15 97.49 32.49 o 7 1 24 46.07 137.68 42.16 o 0 2 24 735.33 657.25 55.02 o 1 2 24 26.10 4.91 19.60 o 2 2 24 7625.18 7816.93 108.09 o 3 2 24 524.21 508.18 38.00 o 4 2 24 3124.80 3266.97 89.16 o 5 2 24 208.88 188.63 25.69 o 6 2 24 84.67 94.49 26.53 o 7 2 24 8.52 114.56 41.60 o 1 3 24 180.75 138.26 22.75 o 2 3 24 85.55 85.44 28.66 o 3 3 24 324.68 335.77 29.68 o 4 3 24 1436.57 1313.13 55.74 o 5 3 24 6.08 16.66 22.81 o 6 3 24 288.28 329.86 39.69 o 0 4 24 1199.10 1141.46 114.59 o 1 4 24 0.07 26.56 29.69 o 2 4 24 1669.85 1462.10 84.89 o 3 4 24 261.69 228.39 58.23 o 4 4 24 863.25 853.28 43.72 o 5 4 24 45.19 44.64 24.30 o 6 4 24 10.98 17.32 32.53 o 1 5 24 165.57 204.43 35.30 o 2 5 24 15.41 38.82 28.58 o 3 5 24 329.88 302.15 38.00 o 4 5 24 925.44 856.35 47.35 o 5 5 24 4.71 7.19 26.43 o 6 5 24 480.47 533.58 54.77 o 0 6 24 372.15 365.21 86.41 o 1 6 24 4.28 -55.32 36.88 o 2 6 24 188.37 134.21 33.82 o 3 6 24 87.11 48.61 35.78 o 4 6 24 25.49 30.48 29.79 o 5 6 24 27.99 23.05 36.01 o 1 7 24 306.42 340.86 55.01 o 2 7 24 245.65 258.66 54.14 o 3 7 24 503.77 472.82 53.11 o 1 1 25 2190.57 2349.43 53.90 o 2 1 25 563.77 655.20 35.60 o 3 1 25 6487.27 6974.08 126.78 o 4 1 25 32.55 112.51 24.42 o 5 1 25 461.44 518.24 41.43 o 6 1 25 972.29 1015.68 62.42 o 7 1 25 1056.38 1311.63 137.32 o 0 2 25 68.17 2.37 37.21 o 1 2 25 874.64 880.31 40.41 o 2 2 25 282.09 376.78 31.05 o 3 2 25 377.80 414.23 36.07 o 4 2 25 371.58 417.82 34.21 o 5 2 25 203.98 265.01 34.24 o 6 2 25 16.94 -24.38 27.27 o 1 3 25 156.83 215.48 30.73 o 2 3 25 235.50 191.92 26.47 o 3 3 25 2843.20 2953.90 70.49 o 4 3 25 27.10 54.36 29.31 o 5 3 25 400.83 419.11 37.60 o 6 3 25 181.51 266.06 37.88 o 0 4 25 587.81 487.99 60.46 o 1 4 25 1004.29 905.68 55.10 o 2 4 25 74.71 103.01 31.03 o 3 4 25 372.03 391.11 40.38 o 4 4 25 970.48 883.87 49.37 o 5 4 25 497.81 545.10 45.05 o 6 4 25 38.26 54.66 48.83 o 1 5 25 328.53 404.36 42.91 o 2 5 25 211.00 195.72 34.91 o 3 5 25 612.04 645.31 72.17 o 4 5 25 0.58 35.59 26.01 o 5 5 25 360.50 390.12 40.28 o 0 6 25 286.15 289.74 77.02 o 1 6 25 1141.49 1204.46 90.08 o 2 6 25 446.71 363.17 41.22 o 3 6 25 555.32 546.94 49.33 o 4 6 25 412.74 350.35 50.23 o 0 0 26 4329.68 4576.75 333.13 o 1 0 26 114.31 197.98 31.60 o 2 0 26 607.55 634.24 41.45 o 3 0 26 31.45 117.58 36.38 o 4 0 26 149.72 290.15 54.59 o 5 0 26 664.24 813.51 78.49 o 6 0 26 32.97 105.68 62.00 o 1 1 26 136.82 251.16 25.24 o 2 1 26 61.40 93.71 21.62 o 3 1 26 86.28 200.42 27.56 o 4 1 26 2.97 69.16 28.67 o 5 1 26 77.75 156.11 54.14 o 6 1 26 0.15 154.74 71.09 o 0 2 26 403.60 373.02 46.93 o 1 2 26 98.62 116.57 23.80 o 2 2 26 370.74 370.89 33.41 o 3 2 26 275.15 279.31 32.10 o 4 2 26 393.80 430.16 39.02 o 5 2 26 942.95 983.96 81.69 o 6 2 26 255.32 201.57 45.51 o 1 3 26 1647.43 1643.14 65.77 o 2 3 26 796.53 873.69 45.28 o 3 3 26 944.01 998.75 49.26 o 4 3 26 301.84 280.77 30.24 o 5 3 26 918.55 905.23 46.54 o 0 4 26 80.00 88.96 43.26 o 1 4 26 1.08 3.84 27.23 o 2 4 26 484.31 415.44 37.37 o 3 4 26 208.30 197.63 36.12 o 4 4 26 143.70 135.13 31.81 o 5 4 26 186.48 163.37 32.62 o 1 5 26 2422.24 2444.86 90.07 o 2 5 26 1003.62 892.94 57.78 o 3 5 26 1588.19 1616.26 74.62 o 4 5 26 283.79 299.43 40.40 o 0 6 26 19.66 71.00 59.46 o 1 6 26 206.12 105.99 45.07 o 2 6 26 7.50 45.78 42.72 o 3 6 26 5.94 -50.70 76.32 o 1 1 27 188.04 237.86 25.27 o 2 1 27 652.40 755.99 37.85 o 3 1 27 313.25 336.88 29.45 o 4 1 27 61.73 94.92 30.98 o 5 1 27 1618.79 1721.62 106.77 o 0 2 27 833.18 973.52 58.41 o 1 2 27 89.99 127.68 23.05 o 2 2 27 6.29 45.21 27.80 o 3 2 27 3.51 4.72 24.29 o 4 2 27 228.01 257.55 30.37 o 5 2 27 12.40 84.89 35.12 o 1 3 27 569.93 651.85 42.09 o 2 3 27 298.84 314.28 32.10 o 3 3 27 234.05 215.07 37.83 o 4 3 27 12.00 24.54 24.23 o 5 3 27 755.98 770.57 61.89 o 0 4 27 1985.41 2021.69 118.30 o 1 4 27 15.17 42.18 28.81 o 2 4 27 525.00 575.52 48.75 o 3 4 27 4.78 2.15 26.49 o 4 4 27 233.97 152.65 78.46 o 1 5 27 244.41 283.61 36.96 o 2 5 27 78.81 149.14 52.53 o 3 5 27 124.23 90.78 34.04 o 0 0 28 12064.05 12831.83 679.93 o 1 0 28 23.50 39.17 29.73 o 2 0 28 2693.50 2709.88 108.46 o 3 0 28 153.15 27.79 41.16 o 4 0 28 865.42 920.80 88.67 o 1 1 28 49.19 122.00 23.01 o 2 1 28 92.93 125.77 24.84 o 3 1 28 18.45 43.57 23.34 o 4 1 28 0.69 64.14 35.66 o 0 2 28 7001.46 7087.24 148.45 o 1 2 28 132.45 116.87 30.68 o 2 2 28 804.91 811.37 48.98 o 3 2 28 4.18 4.27 24.33 o 4 2 28 689.44 803.47 57.93 o 1 3 28 4.89 -1.51 36.06 o 2 3 28 394.68 432.86 35.38 o 3 3 28 63.59 72.02 26.36 o 0 4 28 1293.34 1126.16 127.82 o 1 4 28 9.55 65.73 53.89 o 2 4 28 65.80 139.16 39.40 o 1 1 29 423.36 554.22 36.90 o 2 1 29 5.68 56.45 23.26 o 3 1 29 14.50 48.62 35.94 o 0 2 29 1315.37 1551.66 88.34 o 1 2 29 3.15 37.87 46.17 o 2 2 29 198.44 269.43 44.11 o 3 2 29 2.05 16.34 32.20 o 1 3 29 816.54 881.99 79.00 o 2 3 29 100.36 142.12 69.53 o