#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/19/2231984.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231984_Fobs loop_ _publ_author_name 'Wu, Huilu' 'Kou, Fan' 'Jia, Fei' 'Liu, Bin' 'Yuan, Jingkun' _publ_section_title ; Bis[1,3-bis(1-propyl-1H-benzimidazol-2-yl)-2-oxapropane]cadmium(II) dipicrate dimethylformamide monosolvate ; _journal_coeditor_code LH5332 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1461 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.207 _cell_angle_beta 112.449 _cell_angle_gamma 97.986 _cell_length_a 14.2110 _cell_length_b 14.9970 _cell_length_c 16.1900 _exptl_crystal_F_000 1412.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file lh5332Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P1 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 274.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1100.90 1370.71 22.99 o 3 0 0 12627.93 12455.84 102.99 o 4 0 0 1605.60 1597.93 65.55 o 5 0 0 13448.56 13614.65 183.01 o 6 0 0 3330.24 3405.32 39.81 o 7 0 0 762.79 710.15 17.81 o 8 0 0 697.08 795.65 20.20 o 9 0 0 1049.65 969.28 23.56 o 10 0 0 1017.26 937.08 39.50 o 11 0 0 300.23 249.22 26.69 o 12 0 0 487.11 505.92 35.70 o 13 0 0 120.34 112.36 25.41 o 14 0 0 396.35 378.30 35.14 o 15 0 0 71.13 80.41 25.58 o -15 1 0 79.88 74.63 24.66 o -14 1 0 9.47 7.44 19.15 o -13 1 0 564.07 636.18 40.41 o -12 1 0 27.92 17.92 17.15 o -11 1 0 285.00 205.31 24.92 o -10 1 0 808.11 889.04 24.66 o -9 1 0 1659.59 1604.28 38.02 o -8 1 0 1214.77 1250.29 25.87 o -7 1 0 2894.65 3251.57 78.14 o -6 1 0 14774.18 14161.38 118.61 o -5 1 0 4527.74 4878.35 49.27 o -4 1 0 8985.71 9308.26 78.50 o -3 1 0 43123.61 44957.02 342.59 o -2 1 0 8234.01 8508.64 55.61 o 1 1 0 9200.15 9110.64 103.67 o 2 1 0 867.12 646.06 15.74 o 3 1 0 3504.05 3145.84 50.33 o 4 1 0 18.89 47.33 7.68 o 5 1 0 382.73 338.30 13.44 o 6 1 0 746.80 621.14 15.37 o 7 1 0 655.71 758.11 18.08 o 8 1 0 1502.41 1443.16 54.87 o 9 1 0 264.99 264.95 13.88 o 10 1 0 411.51 354.03 27.88 o 11 1 0 1216.11 1169.40 46.67 o 12 1 0 23.21 24.06 17.35 o 13 1 0 353.03 346.35 35.38 o 14 1 0 0.33 -5.88 20.14 o 15 1 0 151.06 223.55 33.82 o -15 2 0 133.46 56.48 23.44 o -14 2 0 513.91 488.30 38.59 o -13 2 0 19.22 13.51 17.11 o -12 2 0 292.19 293.97 27.90 o -11 2 0 17.14 -13.84 12.57 o -10 2 0 460.24 524.19 25.38 o -9 2 0 355.41 374.20 16.98 o -8 2 0 2237.49 2201.43 48.84 o -7 2 0 11373.56 12073.82 107.82 o -6 2 0 647.17 905.84 19.61 o -5 2 0 4381.69 4328.04 45.98 o -4 2 0 8089.25 8815.32 76.03 o -3 2 0 21074.76 20928.81 150.63 o -2 2 0 1778.81 2115.84 23.03 o -1 2 0 1585.83 1810.54 19.89 o 0 2 0 11842.59 12307.56 96.52 o 1 2 0 35.62 28.59 4.28 o 2 2 0 2026.53 2182.12 23.75 o 3 2 0 639.86 841.47 20.43 o 4 2 0 693.13 727.67 13.81 o 5 2 0 881.16 741.35 15.32 o 6 2 0 244.70 249.95 10.97 o 7 2 0 2206.34 1990.50 48.44 o 8 2 0 208.10 221.18 12.45 o 9 2 0 1629.35 1595.47 49.27 o 10 2 0 771.46 732.69 37.01 o 11 2 0 452.79 426.90 32.43 o 12 2 0 663.81 732.63 42.20 o 13 2 0 276.12 254.80 31.52 o 14 2 0 305.39 308.33 35.12 o -15 3 0 61.83 36.90 22.14 o -14 3 0 186.48 217.13 29.49 o -13 3 0 446.55 417.70 33.07 o -12 3 0 0.10 -8.02 14.43 o -11 3 0 441.52 540.59 22.05 o -10 3 0 508.36 499.75 19.42 o -9 3 0 1120.18 1062.08 26.03 o -8 3 0 1731.95 1731.83 31.86 o -7 3 0 1711.41 1897.74 39.57 o -6 3 0 12840.45 13370.38 115.30 o -5 3 0 2504.24 2291.46 36.39 o -4 3 0 12798.94 13252.06 87.57 o -3 3 0 1403.58 1602.51 16.60 o -2 3 0 23028.17 22987.62 444.35 o -1 3 0 849.76 753.30 12.89 o 0 3 0 135.09 55.47 4.47 o 1 3 0 28214.70 30574.04 228.02 o 2 3 0 4156.92 4281.04 64.28 o 3 3 0 2718.68 2586.79 37.89 o 4 3 0 2937.50 3145.90 35.14 o 5 3 0 59.48 43.17 9.98 o 6 3 0 166.21 219.21 12.65 o 7 3 0 638.91 714.23 18.19 o 8 3 0 961.11 944.17 21.98 o 9 3 0 5.53 12.43 13.81 o 10 3 0 634.60 617.51 35.23 o 11 3 0 334.21 345.29 32.31 o 12 3 0 82.83 66.76 22.16 o 13 3 0 723.37 682.99 42.81 o 14 3 0 0.11 -21.14 19.65 o -15 4 0 173.40 244.15 31.70 o -14 4 0 126.73 79.74 23.73 o -13 4 0 7.31 -0.28 16.67 o -12 4 0 870.47 913.64 42.52 o -11 4 0 2.95 -4.77 11.58 o -10 4 0 277.10 255.33 16.25 o -9 4 0 210.15 202.94 14.44 o -8 4 0 2743.21 2692.08 73.79 o -7 4 0 7332.17 7821.01 79.71 o -6 4 0 3539.12 3655.75 45.53 o -5 4 0 7061.12 6787.33 52.57 o -4 4 0 11798.36 11741.47 79.48 o -3 4 0 10846.05 10198.09 69.28 o -2 4 0 12294.59 13869.48 90.25 o -1 4 0 17386.09 16133.97 200.66 o 0 4 0 13542.28 15031.48 241.46 o 1 4 0 4878.53 5775.56 55.07 o 2 4 0 667.96 657.45 19.18 o 3 4 0 1164.20 1220.55 20.11 o 4 4 0 2247.21 2032.75 27.64 o 5 4 0 16.00 2.83 11.24 o 6 4 0 1673.89 1655.07 27.08 o 7 4 0 2894.46 2570.29 48.22 o 8 4 0 0.86 -4.58 11.28 o 9 4 0 1483.97 1485.07 50.27 o 10 4 0 474.40 458.48 31.65 o 11 4 0 415.17 497.63 35.56 o 12 4 0 341.96 359.28 33.08 o 13 4 0 36.46 16.39 20.83 o 14 4 0 392.44 404.71 41.54 o -15 5 0 46.40 30.08 22.49 o -14 5 0 275.95 337.08 34.15 o -13 5 0 184.22 229.42 30.23 o -12 5 0 5.75 -15.11 20.64 o -11 5 0 1534.29 1438.31 35.49 o -10 5 0 35.68 11.15 9.22 o -9 5 0 868.41 896.74 25.27 o -8 5 0 1190.82 1278.98 28.53 o -7 5 0 5542.25 5651.75 64.72 o -6 5 0 7902.05 7417.86 59.01 o -5 5 0 1432.98 1333.99 18.14 o -4 5 0 647.22 663.30 11.47 o -3 5 0 340.15 413.30 24.98 o -2 5 0 35.72 61.09 4.36 o -1 5 0 891.34 901.09 17.96 o 0 5 0 4712.35 4521.72 76.51 o 1 5 0 1099.01 1176.04 42.38 o 2 5 0 1463.48 1226.16 21.39 o 3 5 0 2824.21 2673.04 34.57 o 4 5 0 1881.81 1798.34 34.80 o 5 5 0 22.45 48.55 7.45 o 6 5 0 1769.03 1836.70 32.84 o 7 5 0 12.04 6.21 8.76 o 8 5 0 203.96 178.67 21.96 o 9 5 0 206.42 208.96 25.07 o 10 5 0 1313.25 1315.92 51.90 o 11 5 0 260.89 239.38 29.89 o 12 5 0 295.02 248.84 31.53 o 13 5 0 44.48 22.74 20.90 o -15 6 0 119.87 149.74 29.08 o -14 6 0 35.05 41.71 21.80 o -13 6 0 360.20 360.16 31.51 o -12 6 0 635.32 605.49 39.11 o -11 6 0 6.64 1.08 10.75 o -10 6 0 1268.18 1185.27 36.97 o -9 6 0 29.16 25.89 9.54 o -8 6 0 1867.14 1824.86 34.93 o -7 6 0 46.92 64.97 9.60 o -6 6 0 3808.22 4023.10 38.57 o -5 6 0 144.69 200.01 8.13 o -4 6 0 20.13 18.44 8.00 o -3 6 0 5744.18 6049.88 47.57 o -2 6 0 714.13 759.47 12.79 o 0 6 0 7685.80 7475.87 73.05 o 1 6 0 1.33 -6.73 7.49 o 2 6 0 1340.50 1242.69 35.57 o 3 6 0 25.27 8.79 5.27 o 4 6 0 737.84 632.43 17.39 o 5 6 0 2403.54 2316.90 48.25 o 6 6 0 373.11 339.87 14.02 o 7 6 0 1515.39 1633.00 30.08 o 8 6 0 16.68 17.13 15.24 o 9 6 0 373.60 356.02 30.06 o 10 6 0 8.02 -10.96 15.98 o 11 6 0 395.47 407.42 34.29 o 12 6 0 11.10 10.08 20.04 o 13 6 0 84.72 67.94 25.24 o -14 7 0 282.73 345.04 34.01 o -13 7 0 71.56 66.07 14.50 o -12 7 0 100.26 62.48 14.69 o -11 7 0 1663.87 1668.93 39.79 o -10 7 0 95.20 89.38 18.39 o -9 7 0 1115.28 1179.51 30.29 o -8 7 0 86.73 90.14 11.19 o -7 7 0 677.27 586.30 14.67 o -6 7 0 330.45 339.06 10.88 o -5 7 0 3357.01 3424.13 33.63 o -4 7 0 1618.28 1542.01 19.66 o -3 7 0 674.58 712.48 13.11 o -2 7 0 2477.97 2263.39 25.50 o -1 7 0 1654.64 1788.38 32.39 o 0 7 0 1308.25 1384.94 26.62 o 1 7 0 782.58 663.53 18.60 o 2 7 0 263.18 260.49 19.69 o 3 7 0 805.27 688.06 19.10 o 4 7 0 137.76 143.32 10.87 o 5 7 0 2067.39 1937.65 41.39 o 6 7 0 416.31 442.83 30.55 o 7 7 0 554.40 596.01 33.76 o 8 7 0 1424.24 1391.61 51.43 o 9 7 0 252.08 292.60 30.24 o 10 7 0 304.13 210.92 29.26 o 11 7 0 10.59 -24.42 17.08 o 12 7 0 219.47 181.19 29.82 o 13 7 0 96.58 94.81 29.52 o -13 8 0 291.83 309.42 22.94 o -12 8 0 283.79 351.95 22.55 o -11 8 0 622.48 626.41 26.96 o -10 8 0 857.58 757.02 27.62 o -9 8 0 332.29 296.92 23.08 o -8 8 0 445.01 454.13 21.44 o -7 8 0 101.83 117.12 12.37 o -6 8 0 1093.79 1135.45 27.71 o -5 8 0 1186.81 1175.71 18.10 o -4 8 0 340.58 351.89 11.25 o -3 8 0 322.72 365.41 10.66 o -2 8 0 16.58 20.99 6.55 o -1 8 0 169.51 155.74 11.90 o 0 8 0 369.93 337.89 14.98 o 1 8 0 441.02 358.78 30.29 o 2 8 0 890.89 900.15 34.73 o 3 8 0 551.33 631.09 19.81 o 4 8 0 2352.57 2510.70 39.94 o 5 8 0 146.15 184.13 16.62 o 6 8 0 1390.06 1513.77 30.86 o 7 8 0 1072.81 1086.73 45.57 o 8 8 0 655.08 559.00 36.39 o 9 8 0 182.06 168.13 25.77 o 10 8 0 21.09 -5.91 19.72 o 11 8 0 266.27 285.09 35.47 o 12 8 0 4.26 -26.08 20.30 o -13 9 0 1.08 -0.77 18.15 o -12 9 0 631.78 663.98 42.93 o -11 9 0 26.98 20.09 12.39 o -10 9 0 736.82 664.24 27.19 o -9 9 0 116.90 121.26 15.05 o -8 9 0 1.75 -11.97 7.98 o -7 9 0 361.59 355.68 18.24 o -6 9 0 1607.15 1655.90 34.59 o -5 9 0 1259.88 1256.81 29.51 o -4 9 0 177.83 168.83 13.18 o -3 9 0 50.33 51.89 6.08 o -2 9 0 1774.38 1588.93 23.38 o -1 9 0 631.89 586.79 19.92 o 0 9 0 151.65 139.04 21.14 o 1 9 0 1650.48 1783.72 34.82 o 2 9 0 855.10 845.69 35.08 o 3 9 0 2240.91 2260.61 47.65 o 4 9 0 50.26 63.45 13.83 o 5 9 0 4330.89 4317.91 74.70 o 6 9 0 28.02 27.78 16.00 o 7 9 0 483.12 465.68 34.56 o 8 9 0 613.35 620.85 39.39 o 9 9 0 1.01 -12.00 17.72 o 10 9 0 84.85 101.73 25.73 o 11 9 0 28.38 -17.18 19.18 o -14 10 0 30.10 48.61 23.26 o -13 10 0 162.68 171.60 30.08 o -12 10 0 1.51 -12.83 17.83 o -11 10 0 374.11 446.78 36.55 o -10 10 0 425.50 472.37 24.56 o -9 10 0 3.05 -21.96 14.64 o -8 10 0 768.55 767.01 26.80 o -7 10 0 416.92 391.22 19.74 o -6 10 0 1115.02 1054.59 28.70 o -5 10 0 918.96 917.32 26.60 o -4 10 0 1496.54 1654.22 35.05 o -3 10 0 394.30 376.35 18.16 o -2 10 0 50.36 58.66 7.62 o -1 10 0 3175.06 3376.17 71.10 o 0 10 0 14.06 6.87 8.61 o 1 10 0 3052.58 3173.33 51.44 o 2 10 0 2050.64 1972.62 56.24 o 3 10 0 550.76 585.83 22.48 o 4 10 0 1370.79 1315.57 31.56 o 5 10 0 6.40 -8.16 10.65 o 6 10 0 159.41 131.16 22.88 o 7 10 0 64.31 78.36 21.89 o 8 10 0 365.04 353.78 34.18 o 9 10 0 260.67 244.27 32.28 o 10 10 0 169.21 163.56 29.93 o 11 10 0 132.93 119.70 29.99 o -13 11 0 8.54 0.68 19.85 o -12 11 0 32.88 63.33 24.54 o -11 11 0 104.68 99.18 24.77 o -10 11 0 793.92 749.40 45.06 o -9 11 0 413.56 339.83 32.76 o -8 11 0 116.44 100.16 15.02 o -7 11 0 151.91 181.21 16.95 o -6 11 0 2.51 -5.97 8.91 o -5 11 0 639.24 673.88 24.64 o -4 11 0 306.21 342.93 30.00 o -3 11 0 2165.86 2081.70 41.18 o -2 11 0 1472.50 1454.23 40.66 o -1 11 0 14.61 2.54 8.49 o 0 11 0 1699.08 1755.40 37.89 o 1 11 0 699.24 743.34 25.57 o 2 11 0 1140.91 1053.95 43.16 o 3 11 0 341.40 326.41 18.22 o 4 11 0 204.57 189.97 16.00 o 6 11 0 12.10 1.12 15.71 o 7 11 0 516.86 513.61 38.32 o 8 11 0 65.92 108.50 26.00 o 9 11 0 391.28 365.49 37.95 o 10 11 0 221.92 278.39 38.14 o -13 12 0 87.94 89.09 26.79 o -12 12 0 0.26 16.61 20.39 o -11 12 0 416.78 490.43 39.65 o -10 12 0 4.55 4.73 18.95 o -9 12 0 618.22 655.34 43.75 o -8 12 0 428.74 407.30 34.67 o -7 12 0 80.71 45.96 13.78 o -6 12 0 1667.37 1668.75 39.91 o -5 12 0 662.51 690.80 35.76 o -4 12 0 1022.71 1015.63 30.53 o -3 12 0 746.24 747.60 26.76 o -2 12 0 19.56 8.03 12.59 o -1 12 0 1560.11 1527.72 36.74 o 0 12 0 457.11 440.34 23.47 o 1 12 0 1634.76 1556.68 37.32 o 2 12 0 58.17 49.93 11.51 o 3 12 0 710.17 738.17 26.84 o 4 12 0 130.13 145.14 16.18 o 6 12 0 497.97 459.49 35.84 o 7 12 0 91.85 135.12 27.73 o 8 12 0 182.12 199.59 31.14 o 9 12 0 182.62 203.16 32.92 o -12 13 0 316.31 291.45 36.72 o -11 13 0 78.22 103.88 27.57 o -10 13 0 233.20 147.75 29.31 o -9 13 0 323.11 262.20 34.56 o -8 13 0 5.40 -16.02 17.85 o -7 13 0 545.62 591.64 40.50 o -6 13 0 6.53 26.45 18.65 o -5 13 0 811.72 796.54 57.39 o -4 13 0 135.77 117.14 30.22 o -3 13 0 288.96 219.23 26.45 o -2 13 0 280.43 334.42 25.08 o -1 13 0 652.48 625.25 26.22 o 0 13 0 1783.15 1671.96 77.12 o 1 13 0 114.25 96.22 16.07 o 2 13 0 553.83 578.59 25.17 o 3 13 0 347.10 343.57 20.70 o 4 13 0 105.94 67.42 20.89 o 6 13 0 10.89 3.07 18.96 o 7 13 0 244.56 292.96 36.30 o 8 13 0 28.30 20.40 21.65 o -11 14 0 166.62 150.83 30.95 o -10 14 0 105.77 126.51 30.54 o -9 14 0 99.35 138.21 28.55 o -8 14 0 16.51 12.17 18.97 o -7 14 0 36.21 21.64 20.77 o -6 14 0 306.55 301.89 34.09 o -5 14 0 184.14 138.27 27.08 o -4 14 0 459.49 418.88 23.74 o -3 14 0 122.85 108.36 15.87 o -2 14 0 791.37 734.86 80.69 o -1 14 0 654.33 600.98 36.23 o 0 14 0 19.38 3.98 12.44 o 1 14 0 628.60 678.63 41.20 o 2 14 0 56.59 28.43 27.72 o 3 14 0 98.22 81.85 15.09 o 4 14 0 181.25 167.92 27.72 o 6 14 0 135.36 212.50 32.87 o 7 14 0 0.36 -25.63 17.08 o -10 15 0 137.49 96.35 28.87 o -9 15 0 5.66 -2.85 20.86 o -8 15 0 346.27 325.76 39.09 o -7 15 0 627.36 629.49 44.87 o -6 15 0 75.88 75.84 24.71 o -5 15 0 1578.42 1589.59 65.38 o -4 15 0 204.31 261.53 33.78 o -3 15 0 307.48 302.55 34.19 o -2 15 0 246.85 217.56 22.63 o -1 15 0 22.26 -13.79 11.71 o 0 15 0 552.42 479.99 25.53 o 1 15 0 22.49 -13.81 14.08 o 2 15 0 76.22 55.27 14.24 o 3 15 0 4.30 6.53 17.85 o 4 15 0 283.91 288.54 35.24 o -9 16 0 359.96 409.94 44.12 o -8 16 0 92.29 87.60 27.27 o -7 16 0 40.93 16.50 20.67 o -6 16 0 470.30 446.17 39.91 o -5 16 0 85.86 120.76 27.65 o -4 16 0 744.72 735.03 46.46 o -3 16 0 48.46 26.98 21.00 o -2 16 0 79.04 36.72 21.12 o -1 16 0 121.08 117.31 26.49 o 0 16 0 109.38 131.77 18.48 o 1 16 0 635.50 664.35 30.31 o 2 16 0 3.71 -17.08 11.39 o 3 16 0 121.96 99.38 24.45 o 4 16 0 47.63 68.75 26.27 o -7 17 0 309.28 256.04 37.64 o -6 17 0 1.09 3.62 19.97 o -5 17 0 206.90 279.32 37.04 o -4 17 0 25.24 22.66 21.00 o -3 17 0 404.94 427.52 39.65 o -2 17 0 139.30 132.46 28.54 o -1 17 0 26.64 11.53 20.62 o 1 17 0 33.40 9.87 18.72 o 0 -17 1 270.20 247.76 33.05 o 1 -17 1 2.47 -6.12 17.13 o 2 -17 1 227.50 307.10 36.95 o 3 -17 1 225.65 88.33 26.99 o 4 -17 1 0.33 3.65 21.49 o 5 -17 1 279.26 354.94 39.89 o 6 -17 1 33.92 25.98 21.65 o -3 -16 1 39.09 45.34 23.10 o -2 -16 1 154.34 198.77 20.19 o 0 -16 1 50.18 56.77 21.58 o 1 -16 1 129.56 92.73 24.59 o 2 -16 1 111.86 118.81 27.47 o 3 -16 1 330.09 273.41 34.39 o 4 -16 1 536.90 513.65 41.18 o 5 -16 1 1.04 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