#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/20/2232001.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232001_Fobs loop_ _publ_author_name 'Ara Jamal, Rifat' 'Ashiq, Uzma' 'Yousuf, Sammer' _publ_section_title ; (3Z)-3-Hydrazinylideneindolin-2-one ; _journal_coeditor_code NG5222 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2576 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.7211 _cell_length_b 11.4263 _cell_length_c 13.3693 _exptl_crystal_F_000 336.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file ng5222Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 92.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 75.90 63.39 2.29 o 4 0 0 7.42 7.84 0.94 o 1 1 0 14.69 16.50 1.03 o 2 1 0 76.65 73.29 1.37 o 3 1 0 272.77 293.64 6.71 o 4 1 0 12.07 13.81 0.70 o 5 1 0 1.65 0.97 0.72 o 0 2 0 5780.82 5049.22 118.42 o 1 2 0 338.65 296.31 2.73 o 2 2 0 0.09 0.13 0.16 o 3 2 0 213.10 212.23 4.55 o 4 2 0 19.44 20.62 0.79 o 5 2 0 14.07 14.37 1.17 o 1 3 0 58.16 59.91 1.09 o 2 3 0 84.46 86.22 1.24 o 3 3 0 215.91 223.39 2.73 o 4 3 0 5.70 6.17 0.61 o 5 3 0 79.07 74.09 2.27 o 0 4 0 8397.68 7929.38 248.92 o 1 4 0 671.95 720.40 7.26 o 2 4 0 60.06 54.36 1.27 o 3 4 0 84.04 88.03 1.44 o 4 4 0 0.14 0.19 0.37 o 5 4 0 2.79 2.47 0.71 o 1 5 0 5.42 2.22 0.62 o 2 5 0 295.51 305.12 3.92 o 3 5 0 2.86 2.19 0.39 o 4 5 0 97.49 95.65 2.27 o 5 5 0 53.67 52.84 2.03 o 0 6 0 329.32 330.30 4.88 o 1 6 0 377.66 431.89 5.46 o 2 6 0 125.32 133.29 2.31 o 3 6 0 165.80 163.39 2.88 o 4 6 0 74.05 73.27 2.10 o 5 6 0 25.87 29.52 1.68 o 1 7 0 107.20 108.82 2.01 o 2 7 0 14.10 11.62 0.77 o 3 7 0 122.96 124.91 2.51 o 4 7 0 238.35 244.95 4.10 o 0 8 0 316.31 300.01 6.97 o 1 8 0 0.15 0.46 0.31 o 2 8 0 0.56 0.26 0.33 o 3 8 0 15.62 13.60 0.96 o 4 8 0 9.32 8.19 1.67 o 1 9 0 0.08 0.22 0.32 o 2 9 0 71.19 71.75 1.89 o 3 9 0 6.43 7.17 0.82 o 4 9 0 31.03 31.31 1.34 o 0 10 0 21.26 16.84 1.70 o 1 10 0 78.26 73.69 1.93 o 2 10 0 14.58 14.96 1.08 o 3 10 0 81.78 79.47 2.22 o 1 11 0 21.39 22.77 1.48 o 2 11 0 5.13 5.04 0.71 o 3 11 0 1.12 0.91 0.58 o 0 12 0 75.32 84.31 3.96 o 1 12 0 121.37 121.51 3.45 o 2 12 0 0.21 1.31 0.53 o 1 13 0 1.44 3.19 1.05 o 1 0 1 516.71 515.03 5.14 o 2 0 1 461.91 472.59 5.23 o 3 0 1 28.31 31.04 1.06 o 4 0 1 23.55 24.74 0.96 o 5 0 1 0.01 -0.24 0.38 o 0 1 1 100.56 103.95 0.89 o 1 1 1 171.34 177.17 1.40 o 2 1 1 126.59 128.49 1.29 o 3 1 1 22.04 23.24 0.60 o 4 1 1 34.97 33.89 0.76 o 5 1 1 0.96 0.54 0.29 o 0 2 1 144.38 130.18 1.17 o 1 2 1 2.33 1.41 0.10 o 2 2 1 157.90 155.60 2.16 o 3 2 1 100.96 98.10 1.10 o 4 2 1 97.59 95.32 1.23 o 5 2 1 15.90 17.29 0.81 o 0 3 1 40.52 41.72 0.68 o 1 3 1 538.33 552.68 3.64 o 2 3 1 71.17 68.06 0.76 o 3 3 1 85.56 89.81 1.21 o 4 3 1 54.72 53.87 1.07 o 5 3 1 20.18 21.04 0.88 o 0 4 1 288.43 307.64 3.43 o 1 4 1 80.07 76.02 0.83 o 2 4 1 457.27 456.98 3.32 o 3 4 1 28.54 31.46 0.59 o 4 4 1 29.60 31.01 0.86 o 5 4 1 35.21 35.07 1.07 o 0 5 1 26.60 31.70 0.86 o 1 5 1 453.56 470.61 3.66 o 2 5 1 130.56 138.82 1.89 o 3 5 1 53.41 54.32 1.05 o 4 5 1 23.07 21.98 0.76 o 5 5 1 3.42 3.42 0.49 o 0 6 1 102.89 130.28 2.06 o 1 6 1 46.23 46.81 0.68 o 2 6 1 83.35 85.32 1.26 o 3 6 1 79.26 78.86 1.33 o 4 6 1 20.96 22.24 0.79 o 5 6 1 28.25 29.46 1.46 o 0 7 1 317.74 342.44 4.25 o 1 7 1 46.28 42.40 0.76 o 2 7 1 13.87 10.94 0.53 o 3 7 1 95.28 88.80 1.47 o 4 7 1 32.91 35.34 1.07 o 0 8 1 0.53 0.63 0.32 o 1 8 1 225.05 217.02 2.04 o 2 8 1 109.86 110.90 1.70 o 3 8 1 61.98 58.88 1.16 o 4 8 1 7.38 7.08 0.56 o 0 9 1 480.66 469.03 5.67 o 1 9 1 248.84 237.77 2.63 o 2 9 1 117.71 116.10 1.74 o 3 9 1 61.30 56.97 1.19 o 4 9 1 8.01 8.36 0.62 o 0 10 1 41.32 35.75 1.25 o 1 10 1 83.07 86.13 1.48 o 2 10 1 56.15 54.94 1.14 o 3 10 1 82.43 79.50 2.31 o 0 11 1 84.46 82.16 2.58 o 1 11 1 10.45 9.13 0.62 o 2 11 1 64.65 58.50 1.24 o 3 11 1 2.80 3.58 0.48 o 0 12 1 59.72 58.14 3.07 o 1 12 1 16.26 18.57 0.93 o 2 12 1 11.96 14.62 0.83 o 0 13 1 59.35 77.94 3.96 o 1 13 1 37.54 36.22 1.35 o 0 0 2 443.15 437.01 10.42 o 1 0 2 145.63 128.29 1.43 o 2 0 2 6.40 4.89 0.54 o 3 0 2 87.18 93.61 2.18 o 4 0 2 128.45 123.80 3.16 o 5 0 2 0.70 1.26 0.49 o 0 1 2 2648.92 2585.08 18.14 o 1 1 2 8535.85 7928.15 44.17 o 2 1 2 161.14 164.14 1.50 o 3 1 2 93.85 92.64 1.21 o 4 1 2 7.60 7.99 0.63 o 5 1 2 2.94 3.55 0.43 o 0 2 2 341.70 325.73 2.58 o 1 2 2 1065.73 1001.11 5.80 o 2 2 2 447.31 462.18 3.14 o 3 2 2 54.61 57.89 0.88 o 4 2 2 11.98 13.18 0.50 o 5 2 2 141.30 153.77 2.33 o 0 3 2 78.78 70.00 0.84 o 1 3 2 684.77 698.17 3.97 o 2 3 2 97.84 99.75 1.04 o 3 3 2 9.85 11.46 0.42 o 4 3 2 5.44 5.69 0.38 o 5 3 2 15.45 15.05 0.84 o 0 4 2 1065.38 1104.66 8.12 o 1 4 2 140.22 155.22 1.30 o 2 4 2 263.10 288.25 2.20 o 3 4 2 56.80 52.98 0.83 o 4 4 2 40.14 42.09 1.02 o 5 4 2 37.73 39.58 1.20 o 0 5 2 22.67 25.70 0.65 o 1 5 2 1482.32 1526.50 8.90 o 2 5 2 149.05 150.35 1.42 o 3 5 2 3.70 3.55 0.33 o 4 5 2 38.82 40.19 0.96 o 5 5 2 13.68 16.65 0.90 o 0 6 2 69.39 79.02 1.29 o 1 6 2 66.24 71.79 0.77 o 2 6 2 101.34 99.99 1.12 o 3 6 2 94.65 97.34 1.59 o 4 6 2 60.93 61.17 1.21 o 5 6 2 72.16 76.75 1.69 o 0 7 2 122.12 113.14 1.70 o 1 7 2 80.91 83.43 1.11 o 2 7 2 30.05 27.43 0.70 o 3 7 2 35.78 35.97 0.87 o 4 7 2 5.98 5.48 0.60 o 0 8 2 282.72 275.86 3.22 o 1 8 2 118.43 113.98 1.33 o 2 8 2 75.51 75.78 1.22 o 3 8 2 43.96 41.05 0.97 o 4 8 2 51.88 50.06 1.16 o 0 9 2 6.05 3.76 0.45 o 1 9 2 82.53 80.84 1.36 o 2 9 2 25.77 22.18 0.75 o 3 9 2 2.26 2.11 0.36 o 4 9 2 15.82 15.51 0.87 o 0 10 2 2.34 2.17 0.46 o 1 10 2 105.27 102.90 1.64 o 2 10 2 4.20 3.67 0.40 o 3 10 2 35.29 36.21 1.01 o 0 11 2 0.93 1.49 0.57 o 1 11 2 73.41 70.16 1.40 o 2 11 2 103.42 97.10 1.75 o 3 11 2 10.41 11.70 0.70 o 0 12 2 13.86 13.31 1.29 o 1 12 2 22.26 25.33 0.96 o 2 12 2 2.61 4.10 0.51 o 0 13 2 4.15 3.13 1.68 o 1 13 2 5.08 4.64 0.65 o 1 0 3 5246.43 5211.67 51.91 o 2 0 3 214.32 229.22 2.41 o 3 0 3 0.35 0.32 0.31 o 4 0 3 16.77 16.06 1.85 o 5 0 3 1.34 1.30 0.54 o 0 1 3 223.86 200.42 1.70 o 1 1 3 4666.49 4646.72 24.20 o 2 1 3 31.25 30.40 0.55 o 3 1 3 7.41 7.99 0.38 o 4 1 3 15.49 15.10 0.73 o 5 1 3 39.89 43.18 1.40 o 0 2 3 45.39 31.27 0.49 o 1 2 3 529.58 547.49 3.21 o 2 2 3 736.34 792.45 5.28 o 3 2 3 97.58 100.30 1.68 o 4 2 3 10.92 12.03 0.59 o 5 2 3 14.11 15.29 0.84 o 0 3 3 13.74 14.85 0.39 o 1 3 3 418.01 420.20 2.73 o 2 3 3 26.51 29.75 0.53 o 3 3 3 25.00 26.69 0.59 o 4 3 3 169.11 171.24 2.05 o 5 3 3 54.99 57.18 1.41 o 0 4 3 98.01 94.08 1.14 o 1 4 3 376.01 389.75 2.61 o 2 4 3 387.30 421.64 2.99 o 3 4 3 55.49 58.66 0.95 o 4 4 3 6.80 7.73 0.58 o 5 4 3 9.18 8.74 0.70 o 0 5 3 567.05 610.84 4.90 o 1 5 3 432.29 436.70 3.13 o 2 5 3 39.54 38.06 0.65 o 3 5 3 69.87 68.94 1.13 o 4 5 3 94.70 95.95 2.16 o 5 5 3 16.40 17.85 0.93 o 0 6 3 16.30 17.73 0.80 o 1 6 3 14.56 15.98 0.39 o 2 6 3 234.84 236.03 2.02 o 3 6 3 100.30 95.78 1.44 o 4 6 3 25.07 22.65 0.91 o 5 6 3 5.02 6.48 0.70 o 0 7 3 19.30 20.60 0.71 o 1 7 3 15.37 13.00 0.39 o 2 7 3 109.38 108.10 1.43 o 3 7 3 51.53 47.62 1.00 o 4 7 3 87.58 88.47 1.70 o 0 8 3 79.74 85.81 1.54 o 1 8 3 156.81 150.41 1.86 o 2 8 3 307.06 293.56 2.80 o 3 8 3 65.12 66.60 1.24 o 4 8 3 4.07 4.26 0.52 o 0 9 3 27.10 25.32 1.33 o 1 9 3 56.67 51.41 1.11 o 2 9 3 74.96 75.69 1.41 o 3 9 3 42.60 41.87 1.03 o 4 9 3 25.38 28.73 1.11 o 0 10 3 239.48 243.05 4.10 o 1 10 3 120.01 115.78 1.76 o 2 10 3 68.82 64.17 1.36 o 3 10 3 0.19 0.83 0.35 o 0 11 3 27.79 27.47 1.54 o 1 11 3 51.47 50.77 1.40 o 2 11 3 12.59 11.97 0.74 o 3 11 3 12.49 14.59 0.85 o 0 12 3 9.65 8.09 1.07 o 1 12 3 4.27 4.91 0.51 o 2 12 3 49.49 54.06 1.37 o 0 13 3 62.75 69.83 2.66 o 1 13 3 20.39 24.98 1.12 o 0 0 4 3127.21 3082.70 40.00 o 1 0 4 1898.59 1917.15 17.72 o 2 0 4 339.58 336.20 4.01 o 3 0 4 141.32 127.86 1.76 o 4 0 4 0.94 0.91 0.41 o 5 0 4 0.60 0.48 0.84 o 0 1 4 182.59 181.57 1.83 o 1 1 4 266.75 281.89 1.91 o 2 1 4 286.67 292.73 2.25 o 3 1 4 117.33 110.86 1.28 o 4 1 4 43.10 43.54 1.03 o 5 1 4 29.56 29.65 1.36 o 0 2 4 0.37 0.29 0.12 o 1 2 4 216.33 227.80 1.47 o 2 2 4 120.37 118.31 1.52 o 3 2 4 103.19 105.74 1.27 o 4 2 4 20.97 22.33 0.74 o 5 2 4 24.42 26.66 1.37 o 0 3 4 182.89 189.48 1.97 o 1 3 4 12.43 10.05 0.26 o 2 3 4 86.07 93.50 1.01 o 3 3 4 142.50 140.41 1.65 o 4 3 4 75.31 72.68 1.26 o 5 3 4 17.42 16.15 1.16 o 0 4 4 1759.05 1824.83 13.13 o 1 4 4 221.59 228.14 1.65 o 2 4 4 39.14 37.52 0.67 o 3 4 4 57.31 53.25 1.20 o 4 4 4 17.17 14.52 0.74 o 5 4 4 11.67 13.30 1.06 o 0 5 4 173.44 188.63 1.97 o 1 5 4 228.55 230.72 1.69 o 2 5 4 27.88 23.69 0.98 o 3 5 4 71.96 69.81 1.01 o 4 5 4 62.06 62.69 1.36 o 5 5 4 4.25 4.30 0.99 o 0 6 4 272.38 286.92 3.29 o 1 6 4 95.26 92.69 0.95 o 2 6 4 134.57 130.23 1.50 o 3 6 4 97.49 101.34 1.46 o 4 6 4 14.87 15.97 0.81 o 0 7 4 25.16 21.35 0.73 o 1 7 4 6.82 7.76 0.40 o 2 7 4 25.22 21.81 0.62 o 3 7 4 182.55 177.07 2.25 o 4 7 4 0.19 0.04 0.32 o 0 8 4 112.15 107.04 1.76 o 1 8 4 85.43 82.19 1.31 o 2 8 4 43.65 41.05 0.99 o 3 8 4 9.02 10.53 0.58 o 4 8 4 3.25 3.34 0.48 o 0 9 4 489.15 471.19 4.98 o 1 9 4 29.62 30.51 0.96 o 2 9 4 19.26 18.24 0.78 o 3 9 4 41.56 39.69 1.11 o 4 9 4 30.87 30.01 1.25 o 0 10 4 9.94 11.56 0.72 o 1 10 4 26.62 26.18 0.84 o 2 10 4 11.70 11.03 0.68 o 3 10 4 44.51 43.37 1.21 o 0 11 4 64.91 66.79 1.94 o 1 11 4 12.54 13.99 0.71 o 2 11 4 2.72 1.95 0.45 o 3 11 4 1.60 1.30 0.42 o 0 12 4 40.67 37.10 2.14 o 1 12 4 1.13 2.00 0.46 o 2 12 4 10.03 9.97 0.72 o 0 13 4 39.99 46.59 2.29 o 1 13 4 6.21 8.13 0.71 o 1 0 5 138.08 129.89 1.51 o 2 0 5 1226.78 1230.61 10.42 o 3 0 5 4.71 4.09 0.49 o 4 0 5 24.02 23.59 2.19 o 5 0 5 2.20 3.68 0.82 o 0 1 5 86.33 81.25 1.09 o 1 1 5 120.21 132.77 1.21 o 2 1 5 1057.64 1121.92 6.77 o 3 1 5 32.89 33.84 0.77 o 4 1 5 34.97 33.30 1.56 o 5 1 5 13.23 12.31 1.23 o 0 2 5 122.86 137.50 1.43 o 1 2 5 155.05 167.96 1.24 o 2 2 5 461.18 478.46 3.49 o 3 2 5 93.61 94.16 1.36 o 4 2 5 157.40 161.48 2.12 o 5 2 5 8.57 8.98 0.93 o 0 3 5 56.78 55.48 0.83 o 1 3 5 589.00 601.30 3.40 o 2 3 5 155.83 147.06 1.47 o 3 3 5 39.88 39.10 0.97 o 4 3 5 25.21 26.16 0.88 o 5 3 5 0.75 0.73 0.49 o 0 4 5 121.22 129.10 1.47 o 1 4 5 491.57 525.59 3.08 o 2 4 5 59.09 53.62 0.77 o 3 4 5 146.07 151.50 1.75 o 4 4 5 76.72 74.85 1.64 o 5 4 5 16.02 19.37 1.28 o 0 5 5 271.35 287.27 2.73 o 1 5 5 128.65 133.12 1.13 o 2 5 5 103.66 101.64 1.13 o 3 5 5 122.35 122.92 1.80 o 4 5 5 1.69 1.60 0.41 o 5 5 5 8.73 9.76 1.06 o 0 6 5 110.57 102.63 1.41 o 1 6 5 15.52 17.90 0.42 o 2 6 5 27.74 24.32 0.64 o 3 6 5 4.92 4.61 0.45 o 4 6 5 8.73 8.30 0.70 o 0 7 5 5.25 5.54 0.40 o 1 7 5 296.18 301.77 2.25 o 2 7 5 37.42 35.40 0.79 o 3 7 5 5.30 5.67 0.51 o 4 7 5 18.14 18.25 1.03 o 0 8 5 118.24 111.15 1.82 o 1 8 5 53.78 50.69 0.93 o 2 8 5 149.00 137.41 1.91 o 3 8 5 20.39 18.39 0.82 o 4 8 5 8.66 8.43 0.77 o 0 9 5 24.13 26.71 0.93 o 1 9 5 298.89 288.25 2.99 o 2 9 5 32.15 28.49 0.90 o 3 9 5 12.01 11.47 0.72 o 0 10 5 1.90 2.91 0.84 o 1 10 5 4.09 4.06 0.43 o 2 10 5 113.17 105.45 1.77 o 3 10 5 22.42 23.88 1.18 o 0 11 5 4.55 3.80 0.63 o 1 11 5 69.69 65.25 1.36 o 2 11 5 13.90 16.98 0.85 o 0 12 5 25.03 24.55 1.36 o 1 12 5 37.96 41.54 1.29 o 2 12 5 4.03 5.27 0.57 o 0 13 5 0.06 0.51 0.58 o 0 0 6 15.57 16.63 1.20 o 1 0 6 155.58 151.08 2.22 o 2 0 6 123.03 130.57 1.71 o 3 0 6 17.86 17.53 0.84 o 4 0 6 0.01 -0.11 0.55 o 5 0 6 18.15 19.04 1.62 o 0 1 6 221.44 209.04 2.60 o 1 1 6 67.25 75.41 0.77 o 2 1 6 1129.57 1142.69 6.92 o 3 1 6 50.24 48.80 0.93 o 4 1 6 29.13 26.66 1.14 o 5 1 6 1.39 1.92 0.52 o 0 2 6 119.33 119.83 1.36 o 1 2 6 183.56 210.95 1.89 o 2 2 6 817.95 830.92 5.90 o 3 2 6 110.39 103.54 1.42 o 4 2 6 175.02 168.19 2.86 o 5 2 6 5.22 4.89 0.75 o 0 3 6 180.92 197.18 1.98 o 1 3 6 77.65 74.75 0.90 o 2 3 6 148.37 150.85 2.02 o 3 3 6 2.56 2.09 0.28 o 4 3 6 1.65 2.09 0.42 o 5 3 6 3.58 4.07 0.70 o 0 4 6 0.16 0.37 0.17 o 1 4 6 96.63 107.85 0.97 o 2 4 6 35.49 36.56 0.89 o 3 4 6 142.53 140.19 1.69 o 4 4 6 32.06 31.90 1.40 o 5 4 6 2.25 4.00 0.67 o 0 5 6 0.05 0.36 0.18 o 1 5 6 100.59 105.89 1.05 o 2 5 6 279.22 284.26 2.31 o 3 5 6 100.18 98.07 1.47 o 4 5 6 25.10 24.69 1.75 o 0 6 6 134.18 139.31 1.75 o 1 6 6 31.90 31.90 0.57 o 2 6 6 211.29 199.68 2.52 o 3 6 6 17.37 19.40 0.89 o 4 6 6 18.52 18.99 1.47 o 0 7 6 30.46 27.70 0.76 o 1 7 6 6.02 6.76 0.32 o 2 7 6 166.48 161.35 1.84 o 3 7 6 30.83 34.35 1.12 o 4 7 6 17.81 20.67 1.26 o 0 8 6 7.49 8.60 0.70 o 1 8 6 194.66 187.49 2.31 o 2 8 6 127.86 118.83 1.77 o 3 8 6 54.05 56.28 1.44 o 4 8 6 0.27 1.12 0.64 o 0 9 6 6.02 6.64 0.57 o 1 9 6 16.74 16.78 0.63 o 2 9 6 32.13 31.14 1.17 o 3 9 6 3.48 4.76 0.61 o 0 10 6 111.62 110.31 2.43 o 1 10 6 33.67 29.32 0.90 o 2 10 6 4.30 5.17 0.51 o 3 10 6 15.89 17.50 1.06 o 0 11 6 0.93 0.71 0.44 o 1 11 6 4.03 4.63 0.55 o 2 11 6 21.18 20.38 0.90 o 0 12 6 2.85 1.97 0.62 o 1 12 6 7.21 8.60 0.99 o 1 0 7 316.45 329.71 4.18 o 2 0 7 13.34 14.54 1.03 o 3 0 7 0.19 0.44 0.42 o 4 0 7 5.13 4.62 0.86 o 5 0 7 1.25 0.62 0.64 o 0 1 7 2.79 2.28 0.25 o 1 1 7 185.59 189.42 1.69 o 2 1 7 35.62 35.12 0.80 o 3 1 7 59.95 61.19 1.84 o 4 1 7 12.13 11.83 0.97 o 5 1 7 1.07 0.64 0.45 o 0 2 7 83.38 81.42 1.11 o 1 2 7 52.15 57.60 0.85 o 2 2 7 25.79 25.52 0.58 o 3 2 7 92.05 88.56 1.86 o 4 2 7 10.91 11.74 0.86 o 5 2 7 2.43 2.31 0.64 o 0 3 7 133.31 135.70 2.01 o 1 3 7 66.90 69.19 1.08 o 2 3 7 12.07 11.64 0.38 o 3 3 7 188.25 180.70 2.54 o 4 3 7 24.14 22.61 1.01 o 5 3 7 7.77 8.70 0.93 o 0 4 7 131.43 145.50 1.71 o 1 4 7 105.42 100.51 0.96 o 2 4 7 27.40 27.54 0.58 o 3 4 7 2.23 2.26 0.49 o 4 4 7 18.20 19.45 1.20 o 0 5 7 110.38 109.60 1.48 o 1 5 7 112.33 112.53 1.07 o 2 5 7 36.83 37.34 0.80 o 3 5 7 10.31 8.97 0.64 o 4 5 7 3.80 4.78 0.78 o 0 6 7 106.66 108.93 2.28 o 1 6 7 78.36 77.86 0.92 o 2 6 7 123.38 113.30 1.46 o 3 6 7 28.13 26.91 1.02 o 4 6 7 6.96 8.06 0.99 o 0 7 7 40.06 42.27 1.00 o 1 7 7 26.13 27.36 0.55 o 2 7 7 21.10 20.05 0.65 o 3 7 7 43.99 38.75 1.18 o 4 7 7 15.20 19.58 1.26 o 0 8 7 69.96 67.24 1.28 o 1 8 7 136.46 128.98 1.82 o 2 8 7 22.52 21.21 0.78 o 3 8 7 7.27 9.19 0.73 o 0 9 7 45.87 49.93 1.26 o 1 9 7 55.54 54.29 0.98 o 2 9 7 54.86 51.48 1.33 o 3 9 7 35.69 34.65 1.27 o 0 10 7 66.82 65.23 1.84 o 1 10 7 66.83 63.89 1.31 o 2 10 7 58.07 58.48 1.49 o 3 10 7 8.78 9.93 0.97 o 0 11 7 24.48 25.65 1.33 o 1 11 7 29.35 30.90 0.97 o 2 11 7 10.94 12.84 1.23 o 0 12 7 0.05 0.91 0.55 o 1 12 7 18.33 20.03 1.59 o 0 0 8 480.12 509.96 6.92 o 1 0 8 0.75 2.02 0.42 o 2 0 8 23.44 24.19 0.98 o 3 0 8 712.28 690.13 10.01 o 4 0 8 2.29 1.30 0.61 o 0 1 8 2.30 3.99 0.34 o 1 1 8 82.38 89.62 1.08 o 2 1 8 6.67 6.62 0.44 o 3 1 8 381.75 364.07 4.95 o 4 1 8 2.67 1.86 0.52 o 0 2 8 58.73 57.60 1.16 o 1 2 8 94.49 98.43 1.05 o 2 2 8 21.15 22.25 0.69 o 3 2 8 84.29 83.54 1.84 o 4 2 8 5.79 5.37 0.67 o 0 3 8 847.35 917.10 7.15 o 1 3 8 77.43 76.86 0.79 o 2 3 8 238.19 227.59 2.29 o 3 3 8 489.54 472.92 4.90 o 4 3 8 8.32 8.38 0.71 o 0 4 8 6.86 6.21 0.40 o 1 4 8 108.53 112.47 1.07 o 2 4 8 10.61 11.72 0.45 o 3 4 8 106.05 99.29 1.85 o 4 4 8 19.26 18.44 1.22 o 0 5 8 20.86 19.10 0.68 o 1 5 8 13.57 16.11 0.41 o 2 5 8 90.87 92.94 1.72 o 3 5 8 5.70 6.97 0.60 o 4 5 8 7.07 7.29 0.83 o 0 6 8 0.23 0.01 0.21 o 1 6 8 12.65 11.65 0.38 o 2 6 8 16.23 16.35 0.65 o 3 6 8 40.57 40.97 1.45 o 4 6 8 7.99 8.53 0.89 o 0 7 8 333.09 345.03 3.49 o 1 7 8 195.36 189.04 1.64 o 2 7 8 10.00 9.25 0.54 o 3 7 8 16.31 13.15 0.97 o 4 7 8 6.88 6.62 0.80 o 0 8 8 3.50 4.51 0.44 o 1 8 8 31.23 31.02 0.93 o 2 8 8 18.00 18.06 0.85 o 3 8 8 11.48 11.76 0.97 o 0 9 8 66.16 61.63 1.50 o 1 9 8 102.11 96.35 1.35 o 2 9 8 0.09 0.39 0.33 o 3 9 8 27.31 30.96 1.59 o 0 10 8 21.23 19.88 1.17 o 1 10 8 2.78 2.13 0.34 o 2 10 8 25.63 27.56 1.11 o 0 11 8 25.99 33.32 1.55 o 1 11 8 19.07 19.97 1.19 o 2 11 8 2.61 2.13 0.48 o 0 12 8 2.89 4.85 0.78 o 1 0 9 196.24 197.21 2.95 o 2 0 9 0.14 0.24 0.29 o 3 0 9 15.65 13.37 1.20 o 4 0 9 1.45 2.18 1.03 o 0 1 9 7.16 6.13 0.63 o 1 1 9 46.07 43.82 0.82 o 2 1 9 51.81 50.92 1.04 o 3 1 9 22.90 20.62 0.89 o 4 1 9 12.62 12.98 0.95 o 0 2 9 1.11 1.22 0.23 o 1 2 9 121.35 121.67 1.38 o 2 2 9 36.52 33.60 0.86 o 3 2 9 17.81 15.65 0.79 o 4 2 9 13.12 13.35 0.98 o 0 3 9 6.78 7.32 0.42 o 1 3 9 13.73 13.69 0.42 o 2 3 9 43.57 43.54 0.92 o 3 3 9 19.41 19.05 0.79 o 4 3 9 9.96 10.54 0.91 o 0 4 9 96.38 99.37 1.43 o 1 4 9 18.37 16.90 0.46 o 2 4 9 80.38 70.29 1.19 o 3 4 9 8.56 6.03 0.58 o 4 4 9 8.69 7.63 0.86 o 0 5 9 14.75 15.18 0.60 o 1 5 9 136.94 137.05 1.38 o 2 5 9 51.87 54.62 1.04 o 3 5 9 5.01 5.26 0.56 o 4 5 9 5.91 7.65 0.86 o 0 6 9 16.99 18.36 0.69 o 1 6 9 64.97 64.57 0.92 o 2 6 9 82.44 86.69 1.65 o 3 6 9 14.70 14.83 0.84 o 4 6 9 17.75 23.04 1.39 o 0 7 9 118.77 116.32 1.79 o 1 7 9 64.02 60.33 0.93 o 2 7 9 1.34 1.34 0.35 o 3 7 9 16.98 17.62 1.15 o 0 8 9 58.64 58.33 1.24 o 1 8 9 9.23 9.42 0.50 o 2 8 9 45.29 42.90 1.42 o 3 8 9 22.06 22.10 1.26 o 0 9 9 184.77 168.72 2.34 o 1 9 9 6.33 5.93 0.46 o 2 9 9 61.15 61.50 1.75 o 0 10 9 13.65 18.47 1.13 o 1 10 9 23.89 25.79 0.93 o 2 10 9 11.98 12.31 0.96 o 0 11 9 0.01 0.27 0.47 o 1 11 9 2.38 2.63 0.59 o 0 0 10 162.75 158.66 4.55 o 1 0 10 44.99 45.61 1.51 o 2 0 10 13.53 13.74 0.90 o 3 0 10 7.39 5.97 0.74 o 4 0 10 5.04 4.56 0.94 o 0 1 10 168.91 175.80 2.69 o 1 1 10 139.00 141.33 1.75 o 2 1 10 125.27 116.60 2.13 o 3 1 10 19.42 17.90 0.85 o 4 1 10 25.55 23.09 1.23 o 0 2 10 19.46 21.43 0.64 o 1 2 10 2.75 3.69 0.35 o 2 2 10 186.79 180.20 2.22 o 3 2 10 24.02 23.08 1.32 o 4 2 10 94.50 84.33 2.17 o 0 3 10 5.77 6.30 0.42 o 1 3 10 18.80 17.70 0.53 o 2 3 10 108.82 102.87 2.01 o 3 3 10 6.23 6.42 0.55 o 4 3 10 16.83 14.33 0.94 o 0 4 10 44.51 44.36 0.95 o 1 4 10 19.10 19.07 0.56 o 2 4 10 105.68 98.09 1.80 o 3 4 10 28.53 28.75 1.09 o 4 4 10 17.92 13.72 0.92 o 0 5 10 1.28 1.74 0.30 o 1 5 10 112.59 112.22 1.37 o 2 5 10 65.31 58.99 1.12 o 3 5 10 3.23 2.34 0.48 o 0 6 10 10.75 11.18 0.60 o 1 6 10 30.79 30.81 0.71 o 2 6 10 11.65 11.41 0.67 o 3 6 10 2.49 3.33 0.49 o 0 7 10 2.70 2.31 0.37 o 1 7 10 7.53 7.18 0.43 o 2 7 10 24.85 25.77 0.99 o 3 7 10 11.94 12.93 1.26 o 0 8 10 55.33 55.36 1.42 o 1 8 10 72.49 72.11 1.19 o 2 8 10 16.14 15.60 0.87 o 3 8 10 9.91 11.44 0.99 o 0 9 10 14.22 13.36 1.47 o 1 9 10 2.17 2.44 0.36 o 2 9 10 14.93 15.47 1.04 o 0 10 10 29.79 33.64 1.51 o 1 10 10 2.88 2.40 0.42 o 1 0 11 45.79 42.56 1.32 o 2 0 11 131.89 119.72 2.79 o 3 0 11 6.24 5.18 0.96 o 4 0 11 4.89 6.80 1.16 o 0 1 11 17.47 18.53 1.19 o 1 1 11 12.54 10.90 0.55 o 2 1 11 89.29 87.66 1.63 o 3 1 11 4.88 3.88 0.45 o 4 1 11 39.19 40.65 1.55 o 0 2 11 6.17 6.44 0.63 o 1 2 11 84.25 85.40 1.29 o 2 2 11 14.92 14.16 0.79 o 3 2 11 3.25 3.20 0.43 o 4 2 11 54.64 47.41 1.48 o 0 3 11 2.05 2.65 0.44 o 1 3 11 139.49 137.22 1.70 o 2 3 11 12.62 12.08 0.61 o 3 3 11 10.17 11.23 0.69 o 4 3 11 17.26 15.70 1.22 o 0 4 11 8.80 8.98 0.62 o 1 4 11 132.45 131.48 1.66 o 2 4 11 22.28 22.34 0.77 o 3 4 11 0.58 0.30 0.36 o 0 5 11 62.52 65.81 1.77 o 1 5 11 39.54 39.35 0.89 o 2 5 11 34.80 32.23 0.87 o 3 5 11 8.90 8.10 0.70 o 0 6 11 91.03 90.78 1.80 o 1 6 11 18.38 18.10 0.78 o 2 6 11 1.70 1.04 0.31 o 3 6 11 3.98 5.62 0.58 o 0 7 11 3.99 4.47 0.53 o 1 7 11 43.57 40.00 1.05 o 2 7 11 22.03 24.96 1.00 o 3 7 11 14.76 14.99 1.09 o 0 8 11 103.27 105.36 2.07 o 1 8 11 72.09 75.07 1.48 o 2 8 11 4.95 8.28 0.70 o 0 9 11 28.38 29.57 1.43 o 1 9 11 14.69 16.35 1.02 o 0 10 11 19.01 19.93 1.39 o 0 0 12 162.48 178.56 5.32 o 1 0 12 10.05 10.09 1.53 o 2 0 12 50.72 47.72 1.59 o 3 0 12 0.07 -0.20 0.43 o 0 1 12 182.17 196.12 4.08 o 1 1 12 2.56 2.29 0.33 o 2 1 12 9.59 8.64 0.59 o 3 1 12 20.90 20.54 0.92 o 0 2 12 6.77 8.22 0.74 o 1 2 12 19.06 19.87 0.69 o 2 2 12 0.69 0.45 0.28 o 3 2 12 3.37 3.44 0.45 o 0 3 12 12.21 12.27 0.87 o 1 3 12 31.96 30.40 0.88 o 2 3 12 20.20 17.60 0.73 o 3 3 12 20.29 20.82 1.05 o 0 4 12 126.05 134.04 2.60 o 1 4 12 13.50 14.42 0.69 o 2 4 12 37.28 34.92 1.12 o 3 4 12 9.00 8.57 0.96 o 0 5 12 20.46 22.97 1.09 o 1 5 12 40.06 40.83 1.51 o 2 5 12 1.81 1.71 0.35 o 3 5 12 2.61 3.23 0.53 o 0 6 12 65.91 69.09 3.29 o 1 6 12 18.20 17.32 0.77 o 2 6 12 0.66 1.30 0.37 o 0 7 12 43.10 40.21 2.00 o 1 7 12 14.31 14.43 0.85 o 2 7 12 1.55 0.91 0.39 o 0 8 12 5.00 7.46 1.60 o 1 8 12 5.69 5.68 0.60 o 0 9 12 37.53 40.30 1.99 o 1 0 13 81.19 77.84 2.52 o 2 0 13 10.78 9.97 1.40 o 3 0 13 0.04 -0.21 0.51 o 0 1 13 13.15 15.07 1.01 o 1 1 13 128.15 126.42 2.31 o 2 1 13 6.24 6.38 0.59 o 3 1 13 2.23 0.93 0.36 o 0 2 13 68.92 69.57 2.26 o 1 2 13 23.93 26.08 1.31 o 2 2 13 3.02 2.70 0.38 o 3 2 13 1.08 0.29 0.32 o 0 3 13 8.48 9.21 0.82 o 1 3 13 4.31 5.70 0.60 o 2 3 13 25.80 25.15 1.04 o 3 3 13 3.17 3.49 0.51 o 0 4 13 3.24 2.69 0.50 o 1 4 13 56.52 54.67 1.49 o 2 4 13 26.57 24.69 0.87 o 0 5 13 130.50 133.95 3.54 o 1 5 13 10.80 10.40 0.71 o 2 5 13 2.41 2.76 0.49 o 0 6 13 8.72 8.40 0.82 o 1 6 13 4.41 5.65 0.55 o 2 6 13 16.98 15.54 0.94 o 0 7 13 11.01 12.40 0.99 o 1 7 13 13.04 16.49 1.03 o 0 8 13 0.44 0.16 0.45 o 0 0 14 21.12 19.52 2.04 o 1 0 14 44.96 47.65 2.03 o 2 0 14 4.63 2.55 0.69 o 0 1 14 49.96 50.80 2.08 o 1 1 14 72.35 72.47 1.79 o 2 1 14 3.23 3.46 0.55 o 0 2 14 41.65 38.60 2.18 o 1 2 14 8.48 8.99 0.69 o 2 2 14 3.20 2.58 0.46 o 0 3 14 5.69 5.64 1.59 o 1 3 14 23.31 25.50 1.05 o 2 3 14 0.30 0.29 0.34 o 0 4 14 50.70 52.89 4.79 o 1 4 14 23.86 24.48 1.03 o 2 4 14 2.55 2.11 0.55 o 0 5 14 0.12 1.86 0.61 o 1 5 14 73.43 79.06 2.62 o 2 5 14 13.61 16.25 1.07 o 0 6 14 0.86 1.96 0.78 o 1 6 14 4.40 5.15 0.61 o 1 0 15 32.87 34.71 1.83 o 2 0 15 10.41 8.87 1.15 o 0 1 15 7.92 6.54 1.00 o 1 1 15 12.86 15.05 0.91 o 2 1 15 4.65 3.33 0.56 o 0 2 15 12.45 10.41 1.21 o 1 2 15 2.79 1.97 0.43 o 0 3 15 30.26 32.19 1.82 o 1 3 15 3.66 3.80 0.53 o 0 4 15 23.31 26.84 1.75 o 1 4 15 17.46 19.33 0.99 o 0 5 15 10.02 12.58 2.04 o 0 0 16 271.28 287.53 8.43 o 0 1 16 3.12 5.48 1.08 o 0 2 16 23.26 23.66 1.76 o