#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:28:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181242 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/20/2232009.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232009_Fobs loop_ _publ_author_name 'Rivera, Augusto' 'Quiroga, Diego' 'R\'ios-Motta, Jaime' 'Fejfarov\'a, Karla' 'Du\n-propyl 4,4'-dihydroxy-3,3'-{[(3aRS,7aRS)-2,3,3a,4,5,6,7,7a-octahydro-1H-benzimidazole-1,3-diyl]bis(methylene)}dibenzoate ; _journal_coeditor_code NK2109 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2627 _journal_page_last o2628 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90 _cell_angle_beta 96.353(2) _cell_angle_gamma 90 _cell_length_a 15.8047(4) _cell_length_b 8.7762(3) _cell_length_c 19.0108(6) _exptl_crystal_F_000 1096 _reflns_d_resolution_high 0.8362 _cod_data_source_file nk2109Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 253.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2433.73 2085.07 60.53 o 4 0 0 5347.35 5260.84 140.93 o 6 0 0 391.67 268.71 26.59 o 8 0 0 2078.96 2180.11 80.36 o 10 0 0 0.32 7.31 10.36 < 12 0 0 386.49 489.25 24.81 o 14 0 0 842.71 892.80 30.07 o 16 0 0 171.10 174.21 14.81 o 18 0 0 143.50 109.79 13.30 o 1 1 0 1046.36 927.44 15.47 o 3 1 0 1398.49 1375.28 39.00 o 5 1 0 3947.32 3637.48 70.09 o 7 1 0 6998.06 6816.44 91.15 o 9 1 0 424.39 546.18 14.70 o 11 1 0 960.40 1165.57 21.44 o 13 1 0 352.84 331.38 15.44 o 15 1 0 1.14 8.21 7.60 < 17 1 0 280.16 280.01 13.35 o 0 2 0 16.45 27.66 10.25 < 2 2 0 269.25 208.72 13.18 o 4 2 0 3701.11 3470.80 53.18 o 6 2 0 331.97 348.00 23.12 o 8 2 0 351.14 346.71 17.26 o 10 2 0 559.73 525.64 13.13 o 12 2 0 2.86 8.92 6.25 < 14 2 0 13.65 18.64 6.93 < 16 2 0 21.73 18.82 6.99 < 18 2 0 2.90 -2.06 5.36 < 1 3 0 462.61 412.17 18.49 o 3 3 0 1409.68 1365.36 32.33 o 5 3 0 4146.12 4047.30 58.93 o 7 3 0 123.99 102.61 10.39 o 9 3 0 5158.71 4930.50 33.02 o 11 3 0 4.25 12.23 6.55 < 13 3 0 3277.62 3430.63 33.90 o 15 3 0 644.78 616.35 15.83 o 17 3 0 1.69 -7.96 5.76 < 0 4 0 344.05 233.43 23.46 o 2 4 0 17617.90 19123.10 124.52 o 4 4 0 20.08 31.24 13.92 < 6 4 0 3250.02 3668.83 37.93 o 8 4 0 73.49 59.96 7.00 o 10 4 0 24.27 35.54 7.70 o 12 4 0 13.74 21.57 7.56 < 14 4 0 336.42 335.40 13.19 o 16 4 0 146.35 151.59 9.95 o 1 5 0 540.13 633.78 34.20 o 3 5 0 22.50 8.96 8.20 < 5 5 0 115.54 133.71 10.58 o 7 5 0 19.22 20.25 6.26 o 9 5 0 1792.80 1861.76 26.28 o 11 5 0 367.30 364.90 13.11 o 13 5 0 363.38 367.57 13.38 o 15 5 0 284.55 278.98 13.13 o 0 6 0 1666.16 1680.48 63.80 o 2 6 0 152.01 119.88 14.91 o 4 6 0 0.17 13.89 9.37 < 6 6 0 356.34 356.40 16.49 o 8 6 0 447.88 452.66 17.34 o 10 6 0 484.44 503.55 15.74 o 12 6 0 15.65 29.37 9.61 o 14 6 0 150.72 160.05 10.73 o 1 7 0 292.44 321.27 22.30 o 3 7 0 65.15 104.10 17.39 o 5 7 0 125.15 113.73 14.82 o 7 7 0 375.39 402.45 19.66 o 9 7 0 12.37 35.80 10.76 o 11 7 0 0.06 8.27 8.61 < 13 7 0 1.33 10.22 8.34 < 0 8 0 0.31 11.01 21.87 < 2 8 0 48.83 43.14 17.25 < 4 8 0 1959.97 1776.75 40.20 o 6 8 0 1.48 6.78 11.78 < 8 8 0 131.10 86.56 10.59 o 10 8 0 129.48 124.53 10.79 o 12 8 0 8.78 35.75 15.16 < 1 9 0 227.52 204.45 19.33 o 3 9 0 1163.08 1202.06 35.81 o 5 9 0 139.52 131.06 13.11 o 7 9 0 1370.67 1446.94 30.62 o 9 9 0 1.29 56.30 16.29 o 0 10 0 2.74 27.09 23.26 < 2 10 0 97.56 65.33 16.01 o 4 10 0 319.29 315.27 23.58 o -17 1 1 314.99 326.88 14.40 o -15 1 1 207.62 199.28 11.70 o -13 1 1 577.11 547.51 19.91 o -11 1 1 558.74 659.03 15.79 o -9 1 1 687.02 717.90 17.47 o -7 1 1 563.17 498.70 29.60 o -5 1 1 6670.47 6818.20 94.46 o -3 1 1 14772.40 13837.60 147.89 o -1 1 1 244.02 239.91 12.39 o 1 1 1 7329.18 7631.58 54.68 o 3 1 1 26647.30 25991.50 161.65 o 5 1 1 144.30 108.38 15.98 o 7 1 1 4277.95 4428.61 62.89 o 9 1 1 358.40 418.85 12.79 o 11 1 1 315.33 333.48 13.20 o 13 1 1 183.66 202.38 12.48 o 15 1 1 576.36 592.04 17.28 o 17 1 1 14.15 9.88 6.40 < -18 2 1 15.43 -1.42 5.10 < -16 2 1 25.44 14.32 6.28 < -14 2 1 0.03 -0.90 7.70 < -12 2 1 2075.77 2022.26 27.58 o -10 2 1 614.85 557.78 13.82 o -8 2 1 88.11 84.33 13.39 o -6 2 1 2491.96 2389.37 50.15 o -4 2 1 5932.20 5739.61 68.57 o -2 2 1 8103.92 7594.17 58.37 o 0 2 1 266.41 215.47 13.20 o 2 2 1 440.87 394.64 19.50 o 4 2 1 196.01 212.13 16.81 o 6 2 1 2867.62 2926.76 53.62 o 8 2 1 551.20 513.26 19.66 o 10 2 1 13.51 14.49 6.04 < 12 2 1 42.92 49.16 7.55 o 14 2 1 1371.56 1462.96 23.70 o 16 2 1 263.46 252.48 11.87 o 18 2 1 60.49 76.01 8.50 o -17 3 1 184.23 149.48 9.54 o -15 3 1 1666.81 1711.16 25.09 o -13 3 1 493.91 499.04 14.28 o -11 3 1 548.14 509.79 13.86 o -9 3 1 437.16 452.98 11.11 o -7 3 1 4011.19 3936.77 53.95 o -5 3 1 64.28 90.27 14.42 o -3 3 1 188.25 169.80 13.19 o -1 3 1 396.85 344.82 17.60 o 1 3 1 99.88 146.72 11.11 o 3 3 1 638.00 707.14 24.02 o 5 3 1 0.45 7.86 15.16 < 7 3 1 1291.57 1325.06 26.86 o 9 3 1 973.75 998.19 16.24 o 11 3 1 72.00 101.55 9.04 o 13 3 1 5163.23 5509.62 39.53 o 15 3 1 36.23 29.68 6.41 o 17 3 1 91.63 88.22 7.78 o -16 4 1 335.87 312.92 11.82 o -14 4 1 1188.93 1266.69 20.52 o -12 4 1 168.49 176.20 10.12 o -10 4 1 254.30 250.49 10.92 o -8 4 1 1068.28 964.07 15.64 o -6 4 1 2831.90 2879.17 34.46 o -4 4 1 3175.07 3572.55 57.07 o -2 4 1 6309.86 7080.21 74.79 o 0 4 1 920.80 851.84 26.36 o 2 4 1 9379.12 10686.40 104.01 o 4 4 1 5193.70 5799.73 86.80 o 6 4 1 1321.13 1184.17 20.09 o 8 4 1 3125.79 3021.83 32.67 o 10 4 1 16.37 26.93 7.87 o 12 4 1 17.54 18.61 8.51 < 14 4 1 300.52 310.99 12.81 o 16 4 1 214.73 186.68 12.77 o -15 5 1 3.36 13.29 7.23 < -13 5 1 674.14 643.15 16.69 o -11 5 1 262.41 289.79 11.33 o -9 5 1 14.72 19.48 6.61 < -7 5 1 93.01 107.30 8.07 o -5 5 1 848.71 824.79 19.41 o -3 5 1 32.00 52.13 8.60 o -1 5 1 12.97 42.27 12.25 o 1 5 1 1004.26 1127.28 34.40 o 3 5 1 818.93 829.18 21.28 o 5 5 1 577.65 630.86 16.06 o 7 5 1 35.68 12.86 6.88 < 9 5 1 2114.77 2217.52 28.42 o 11 5 1 65.24 92.48 9.76 o 13 5 1 284.61 302.26 14.04 o 15 5 1 29.32 16.77 6.91 < -14 6 1 17.61 35.36 9.30 o -12 6 1 252.09 280.52 12.86 o -10 6 1 184.07 199.73 12.91 o -8 6 1 23.58 22.24 8.18 < -6 6 1 282.10 256.26 14.48 o -4 6 1 203.75 220.61 16.96 o -2 6 1 1833.36 1773.85 46.75 o 0 6 1 954.62 1133.75 39.24 o 2 6 1 476.60 483.74 26.21 o 4 6 1 368.59 449.02 23.67 o 6 6 1 145.84 126.48 12.80 o 8 6 1 1.73 -17.52 9.70 < 10 6 1 208.01 222.67 11.82 o 12 6 1 73.45 75.06 9.79 o 14 6 1 61.62 75.53 9.91 o -13 7 1 138.68 196.62 13.46 o -11 7 1 1.34 17.11 8.93 < -9 7 1 182.55 225.46 15.27 o -7 7 1 64.54 66.72 12.63 o -5 7 1 116.66 109.32 13.64 o -3 7 1 445.79 437.01 27.29 o -1 7 1 860.45 830.12 31.12 o 1 7 1 2559.17 2582.74 55.18 o 3 7 1 681.15 739.29 30.31 o 5 7 1 958.85 947.87 31.08 o 7 7 1 0.13 -14.28 12.39 < 9 7 1 62.28 49.60 9.57 o 11 7 1 3.56 25.02 9.16 < 13 7 1 135.93 114.58 14.85 o -12 8 1 167.35 199.34 20.54 o -10 8 1 5.37 40.32 7.20 o -8 8 1 86.56 103.46 10.88 o -6 8 1 42.04 13.59 11.47 < -4 8 1 165.57 201.26 13.74 o -2 8 1 508.19 515.15 28.90 o 0 8 1 314.31 310.52 24.55 o 2 8 1 606.23 666.74 32.13 o 4 8 1 498.31 397.60 20.33 o 6 8 1 515.09 559.98 22.63 o 8 8 1 381.90 357.95 16.23 o 10 8 1 18.41 3.14 8.48 < 12 8 1 2.99 30.31 22.27 < -9 9 1 141.74 163.54 15.01 o -7 9 1 1.96 -2.74 8.86 < -5 9 1 733.79 631.74 22.75 o -3 9 1 1648.29 1705.04 43.93 o -1 9 1 91.49 88.55 16.32 o 1 9 1 36.89 40.53 14.27 < 3 9 1 421.31 395.35 27.49 o 5 9 1 98.32 70.54 17.03 o 7 9 1 2359.09 2336.07 38.33 o 9 9 1 160.31 173.16 20.38 o -4 10 1 1.24 -1.96 11.73 < -2 10 1 187.54 129.16 18.74 o 0 10 1 139.04 124.59 19.40 o 2 10 1 101.46 57.85 22.58 < 4 10 1 112.62 91.64 15.07 o -18 0 2 2.38 -12.92 8.05 < -16 0 2 184.12 191.98 17.76 o -14 0 2 105.58 71.76 12.18 o -12 0 2 121.49 157.48 15.64 o -10 0 2 4752.12 4989.78 50.48 o -8 0 2 13958.20 15706.20 210.64 o -6 0 2 10033.20 8693.17 128.48 o -4 0 2 66167.00 62621.40 453.56 o -2 0 2 37188.70 38684.40 152.29 o 0 0 2 641.43 595.21 13.64 o 2 0 2 326.25 352.63 29.93 o 4 0 2 22108.80 21083.80 284.82 o 6 0 2 3840.77 3938.12 87.80 o 8 0 2 3094.20 2899.70 93.03 o 10 0 2 290.12 212.83 13.76 o 12 0 2 3.95 -5.43 11.45 < 14 0 2 40.08 34.14 11.82 < 16 0 2 116.28 114.38 12.29 o 18 0 2 34.00 36.59 8.53 o -17 1 2 35.37 42.38 8.63 o -15 1 2 25.66 20.28 8.15 < -13 1 2 380.17 365.08 17.26 o -11 1 2 426.84 365.54 13.02 o -9 1 2 749.89 748.06 17.86 o -7 1 2 19.01 21.59 16.05 < -5 1 2 1911.54 1968.43 41.16 o -3 1 2 6646.77 6110.26 82.63 o -1 1 2 26287.70 25466.10 156.43 o 1 1 2 2338.73 2217.85 27.05 o 3 1 2 31617.90 30378.90 176.09 o 5 1 2 1628.81 1506.64 46.33 o 7 1 2 257.28 292.63 15.95 o 9 1 2 0.78 21.20 6.02 o 11 1 2 1832.37 1766.30 27.39 o 13 1 2 292.53 270.22 11.76 o 15 1 2 1603.29 1737.85 27.88 o 17 1 2 90.95 88.68 8.98 o -18 2 2 0.04 -3.62 5.00 < -16 2 2 3.51 5.00 7.25 < -14 2 2 2.16 8.24 7.87 < -12 2 2 167.78 179.82 10.70 o -10 2 2 8.57 1.27 6.13 < -8 2 2 1741.45 1601.89 36.22 o -6 2 2 59.53 48.27 15.01 o -4 2 2 225.68 276.07 18.01 o -2 2 2 1039.15 876.59 24.04 o 0 2 2 7545.87 7135.97 81.06 o 2 2 2 6568.07 6370.93 61.90 o 4 2 2 1201.99 1043.78 27.50 o 6 2 2 1179.57 1048.36 24.80 o 8 2 2 937.56 927.76 18.59 o 10 2 2 6074.64 6461.15 42.52 o 12 2 2 2090.46 2119.97 29.12 o 14 2 2 390.49 400.24 13.63 o 16 2 2 547.92 568.20 15.86 o 18 2 2 255.02 223.97 16.34 o -17 3 2 1058.17 1030.24 23.83 o -15 3 2 41.38 28.10 7.00 o -13 3 2 696.36 742.18 16.04 o -11 3 2 3721.31 3714.17 34.87 o -9 3 2 1405.97 1316.55 18.47 o -7 3 2 5653.47 5649.95 59.25 o -5 3 2 326.02 354.45 22.18 o -3 3 2 7296.87 7279.13 68.36 o -1 3 2 231.01 193.34 14.52 o 1 3 2 1923.83 1821.48 37.29 o 3 3 2 1676.19 1654.11 36.84 o 5 3 2 26512.00 28983.50 200.17 o 7 3 2 1241.28 1166.61 21.97 o 9 3 2 208.43 192.82 9.08 o 11 3 2 221.60 231.16 11.73 o 13 3 2 68.45 51.34 7.92 o 15 3 2 477.97 480.01 14.02 o 17 3 2 744.06 762.16 20.48 o -16 4 2 43.39 49.50 7.23 o -14 4 2 242.24 252.43 9.89 o -12 4 2 852.78 882.49 18.37 o -10 4 2 5941.97 6009.11 40.52 o -8 4 2 118.70 119.14 7.09 o -6 4 2 10093.00 10622.90 61.40 o -4 4 2 675.75 659.12 33.25 o -2 4 2 398.73 440.88 25.52 o 0 4 2 4.69 15.09 14.72 < 2 4 2 104.33 96.50 16.54 o 4 4 2 1096.59 1227.92 42.18 o 6 4 2 1548.12 1527.16 22.79 o 8 4 2 68.47 80.67 7.87 o 10 4 2 8.56 25.34 8.15 o 12 4 2 31.57 24.54 8.43 < 14 4 2 5.29 1.67 7.62 < 16 4 2 2.97 4.08 6.72 < -15 5 2 0.16 0.57 6.54 < -13 5 2 300.03 314.60 11.99 o -11 5 2 298.45 274.68 11.40 o -9 5 2 156.95 133.03 8.34 o -7 5 2 1115.59 1135.25 20.52 o -5 5 2 2373.42 2460.22 34.09 o -3 5 2 2906.04 3338.81 46.22 o -1 5 2 635.31 630.99 28.98 o 1 5 2 1370.69 1443.26 35.38 o 3 5 2 1.72 0.02 6.94 < 5 5 2 1.81 -3.14 5.49 < 7 5 2 0.16 4.75 7.27 < 9 5 2 926.96 983.96 21.29 o 11 5 2 298.98 314.30 14.34 o 13 5 2 62.35 73.83 9.28 o 15 5 2 5.66 5.49 6.62 < -14 6 2 65.99 58.83 8.27 o -12 6 2 78.38 81.31 8.99 o -10 6 2 500.16 545.51 17.45 o -8 6 2 533.45 567.14 17.55 o -6 6 2 7.05 19.41 9.24 < -4 6 2 20.53 29.56 8.94 o -2 6 2 293.83 313.84 18.04 o 0 6 2 102.92 86.99 12.78 o 2 6 2 39.69 38.83 9.39 o 4 6 2 130.66 116.25 12.12 o 6 6 2 46.19 65.65 9.90 o 8 6 2 610.52 612.76 18.95 o 10 6 2 156.99 153.80 12.17 o 12 6 2 573.54 570.76 17.11 o 14 6 2 59.99 91.98 11.19 o -13 7 2 133.88 165.10 12.74 o -11 7 2 85.74 103.29 10.31 o -9 7 2 508.02 593.63 20.13 o -7 7 2 23.33 13.73 9.51 < -5 7 2 139.52 116.03 13.06 o -3 7 2 1087.46 1098.14 40.96 o -1 7 2 644.24 681.21 28.60 o 1 7 2 688.88 766.64 35.84 o 3 7 2 794.92 791.97 31.84 o 5 7 2 551.42 568.88 24.25 o 7 7 2 1.37 -1.05 12.04 < 9 7 2 99.81 94.44 10.78 o 11 7 2 273.52 259.25 14.75 o 13 7 2 143.34 143.65 20.46 o -12 8 2 514.67 755.57 32.26 o -10 8 2 33.49 62.76 7.33 o -8 8 2 125.52 88.99 10.17 o -6 8 2 978.36 945.69 29.69 o -4 8 2 1857.74 1871.78 42.39 o -2 8 2 504.69 488.56 28.16 o 0 8 2 2980.23 3292.10 63.40 o 2 8 2 11.47 7.01 16.53 < 4 8 2 16.10 26.01 14.48 < 6 8 2 3.35 2.90 10.28 < 8 8 2 258.21 269.61 14.29 o 10 8 2 17.13 19.82 9.37 < -9 9 2 21.93 66.88 11.84 o -7 9 2 130.28 88.12 9.65 o -5 9 2 102.19 69.85 15.66 o -3 9 2 769.27 764.69 27.10 o -1 9 2 87.33 89.00 15.66 o 1 9 2 44.08 27.12 14.06 < 3 9 2 1011.24 1030.62 40.05 o 5 9 2 80.26 94.87 11.35 o 7 9 2 387.36 440.28 21.16 o 9 9 2 95.44 71.86 22.32 o -4 10 2 3.44 -19.90 17.74 < -2 10 2 21.80 -0.87 17.89 < 0 10 2 23.15 -9.77 14.32 < 2 10 2 131.46 138.78 19.23 o 4 10 2 533.62 549.23 46.16 o -17 1 3 30.71 30.98 8.68 o -15 1 3 1.08 2.80 8.24 < -13 1 3 217.90 206.14 12.61 o -11 1 3 265.60 262.58 12.46 o -9 1 3 876.70 923.19 18.74 o -7 1 3 930.32 804.03 34.55 o -5 1 3 4698.50 4390.97 60.24 o -3 1 3 328.55 296.39 21.43 o -1 1 3 20642.50 19203.10 122.01 o 1 1 3 3514.05 3452.84 29.75 o 3 1 3 63609.10 64485.10 315.61 o 5 1 3 966.71 877.37 36.44 o 7 1 3 49.01 38.02 9.73 o 9 1 3 990.41 922.61 16.11 o 11 1 3 395.24 359.06 13.09 o 13 1 3 249.95 241.71 11.93 o 15 1 3 65.10 60.96 8.47 o 17 1 3 79.76 78.44 8.16 o -18 2 3 14.28 3.40 4.79 < -16 2 3 0.85 5.03 6.45 < -14 2 3 237.42 216.63 12.20 o -12 2 3 34.01 39.89 7.69 o -10 2 3 174.69 138.37 8.43 o -8 2 3 14.08 23.26 10.12 < -6 2 3 168.62 91.24 16.53 o -4 2 3 465.22 459.34 22.90 o -2 2 3 2128.41 2101.60 37.16 o 0 2 3 3800.79 3714.04 54.08 o 2 2 3 2298.12 2262.79 38.56 o 4 2 3 3.72 7.27 10.85 < 6 2 3 1376.51 1520.87 29.09 o 8 2 3 2309.23 2244.88 24.72 o 10 2 3 129.37 174.21 9.02 o 12 2 3 826.75 861.64 19.06 o 14 2 3 337.95 343.36 13.33 o 16 2 3 453.61 450.48 15.42 o 18 2 3 682.73 683.30 41.58 o -17 3 3 63.58 56.28 7.19 o -15 3 3 92.69 80.03 9.53 o -13 3 3 166.04 172.65 8.87 o -11 3 3 24.04 20.61 7.10 < -9 3 3 88.64 67.84 5.71 o -7 3 3 616.46 629.68 16.87 o -5 3 3 25.27 24.90 12.82 < -3 3 3 7.35 14.69 11.16 < -1 3 3 1466.22 1355.64 33.63 o 1 3 3 573.01 618.99 23.70 o 3 3 3 538.57 493.92 22.28 o 5 3 3 11325.00 12590.50 93.04 o 7 3 3 776.33 766.88 16.66 o 9 3 3 2268.01 2356.90 24.97 o 11 3 3 398.29 409.80 13.86 o 13 3 3 154.14 153.45 11.22 o 15 3 3 5.78 4.32 6.88 < 17 3 3 282.39 249.47 14.52 o -16 4 3 2.06 11.15 6.74 < -14 4 3 16.20 11.47 6.66 < -12 4 3 453.89 491.95 13.81 o -10 4 3 9365.66 9328.83 50.29 o -8 4 3 727.46 644.34 13.70 o -6 4 3 5288.91 5602.84 45.47 o -4 4 3 1329.24 1209.41 43.29 o -2 4 3 2017.40 2193.33 51.87 o 0 4 3 293.91 370.78 25.62 o 2 4 3 0.12 12.64 11.16 < 4 4 3 1766.83 1800.56 40.69 o 6 4 3 954.35 1093.97 19.57 o 8 4 3 745.16 773.46 17.55 o 10 4 3 38.80 60.09 9.53 o 12 4 3 1.32 13.46 9.75 < 14 4 3 120.93 107.33 11.06 o 16 4 3 282.23 288.04 14.22 o -15 5 3 1811.49 1863.66 28.71 o -13 5 3 302.31 329.62 11.20 o -11 5 3 0.03 3.91 6.93 < -9 5 3 0.78 8.11 7.08 < -7 5 3 444.88 387.78 12.04 o -5 5 3 49.75 48.10 7.56 o -3 5 3 5088.76 5773.42 60.56 o -1 5 3 1.78 -6.34 10.66 < 1 5 3 3417.83 3416.22 54.17 o 3 5 3 109.56 85.61 7.72 o 5 5 3 280.28 290.28 12.06 o 7 5 3 156.40 161.35 9.79 o 9 5 3 94.96 98.59 9.66 o 11 5 3 25.87 40.27 10.99 o 13 5 3 28.51 17.12 7.93 < 15 5 3 43.99 52.46 8.34 o -14 6 3 133.21 159.36 10.02 o -12 6 3 32.02 10.55 9.08 < -10 6 3 13.10 19.51 7.40 < -8 6 3 16.06 23.21 7.38 o -6 6 3 122.93 84.64 10.69 o -4 6 3 526.75 512.79 20.90 o -2 6 3 1400.25 1479.07 34.43 o 0 6 3 111.84 110.24 14.13 o 2 6 3 246.34 214.24 17.01 o 4 6 3 784.18 729.15 21.62 o 6 6 3 0.55 0.70 8.92 < 8 6 3 126.46 128.84 11.26 o 10 6 3 147.22 159.50 12.45 o 12 6 3 288.33 281.73 14.09 o 14 6 3 132.93 131.21 18.04 o -13 7 3 1.27 -2.06 9.60 < -11 7 3 1.38 24.65 8.15 o -9 7 3 106.21 91.96 11.28 o -7 7 3 253.65 220.76 15.45 o -5 7 3 1991.52 1921.57 38.89 o -3 7 3 492.26 505.66 31.86 o -1 7 3 1099.55 1116.95 39.08 o 1 7 3 223.16 216.38 24.12 o 3 7 3 262.97 212.03 20.00 o 5 7 3 3.83 2.44 10.98 < 7 7 3 1873.54 1569.29 32.00 o 9 7 3 425.52 488.27 21.76 o 11 7 3 14.97 0.71 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