#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/20/2232012.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232012_Fobs loop_ _publ_author_name 'Wu, Xiang-Xiang' 'Wan, Yan' 'Ng, Seik Weng' _publ_section_title ; 3,6-Dibromonaphthalene-2,7-diyl bis(trifluoromethanesulfonate) ; _journal_coeditor_code NK2112 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2698 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.169 _cell_angle_gamma 90.000 _cell_length_a 5.2413 _cell_length_b 26.4499 _cell_length_c 12.4291 _exptl_crystal_F_000 1120.00 _reflns_d_resolution_high 0.7699 _[local]_cod_data_source_file nk2112Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 260.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2775.28 2671.08 53.96 o 4 0 0 129.48 162.80 23.04 o 6 0 0 921.00 917.53 79.41 o 1 1 0 21371.66 21552.56 192.45 o 2 1 0 16606.96 17186.19 107.85 o 3 1 0 10.70 35.37 9.11 o 4 1 0 1477.01 1500.10 44.65 o 5 1 0 121.84 113.54 16.08 o 6 1 0 220.68 268.84 33.18 o 1 2 0 665.89 540.63 9.63 o 2 2 0 3872.47 3559.00 49.24 o 3 2 0 114.92 179.41 10.62 o 4 2 0 3464.67 3574.66 79.02 o 5 2 0 91.76 86.60 12.56 o 6 2 0 11.95 68.98 18.37 o 1 3 0 382.89 389.88 8.98 o 2 3 0 1145.95 1155.10 35.55 o 3 3 0 9871.55 9767.27 192.90 o 4 3 0 2682.00 2703.30 45.23 o 5 3 0 2866.53 3037.27 58.20 o 6 3 0 1165.84 1216.65 64.13 o 0 4 0 2020.06 2105.20 46.44 o 1 4 0 1273.88 1229.92 22.80 o 2 4 0 14404.17 14891.41 152.66 o 3 4 0 279.82 318.43 17.45 o 4 4 0 6161.63 6289.41 83.26 o 5 4 0 30.01 47.50 14.61 o 6 4 0 170.63 118.86 33.14 o 1 5 0 33824.43 34943.24 263.52 o 2 5 0 473.60 498.45 17.97 o 3 5 0 2968.90 3009.13 51.50 o 4 5 0 6264.33 6223.20 109.11 o 5 5 0 417.61 394.23 28.16 o 6 5 0 1382.42 1478.76 133.97 o 0 6 0 46776.57 49406.23 539.85 o 1 6 0 275.36 302.92 8.63 o 2 6 0 7019.87 6828.06 51.43 o 3 6 0 832.06 772.76 17.93 o 4 6 0 3595.01 3717.73 71.01 o 5 6 0 114.65 146.10 27.16 o 6 6 0 260.77 207.79 23.83 o 1 7 0 1249.15 1127.28 24.02 o 2 7 0 49.27 50.39 8.06 o 3 7 0 4.34 20.44 13.43 o 4 7 0 3286.37 3087.09 69.30 o 5 7 0 1339.49 1528.81 59.79 o 6 7 0 1071.17 1081.22 69.25 o 0 8 0 7535.01 7887.19 103.96 o 1 8 0 248.82 239.25 8.77 o 2 8 0 4187.33 4299.82 48.86 o 3 8 0 1704.13 1491.30 39.83 o 4 8 0 3369.16 3526.13 94.72 o 5 8 0 13.10 54.39 15.97 o 6 8 0 55.80 39.43 15.09 o 1 9 0 6017.66 5891.26 67.96 o 2 9 0 9482.36 9850.80 124.61 o 3 9 0 287.37 300.31 28.50 o 4 9 0 1116.70 1206.54 50.58 o 5 9 0 4595.84 4909.74 169.11 o 6 9 0 17.68 51.68 14.42 o 0 10 0 3763.01 3622.87 118.58 o 1 10 0 5728.04 5644.94 62.17 o 2 10 0 231.88 272.61 21.47 o 3 10 0 4953.62 4904.98 212.13 o 4 10 0 2685.47 2949.12 76.98 o 5 10 0 63.87 52.65 20.65 o 6 10 0 22.77 39.54 12.01 o 1 11 0 1586.17 1531.65 53.98 o 2 11 0 6817.73 6658.92 88.20 o 3 11 0 67.45 82.87 35.78 o 4 11 0 239.87 287.07 26.90 o 5 11 0 843.87 1027.88 81.80 o 6 11 0 82.12 86.65 17.97 o 0 12 0 16893.77 17736.15 407.40 o 1 12 0 6834.25 6451.00 86.41 o 2 12 0 603.29 578.15 20.75 o 3 12 0 21.91 56.68 16.70 o 4 12 0 1503.49 1538.65 60.45 o 5 12 0 185.38 194.27 26.33 o 6 12 0 0.22 36.99 13.34 o 1 13 0 8998.10 9064.90 239.04 o 2 13 0 673.43 759.31 18.10 o 3 13 0 4384.62 4202.90 146.79 o 4 13 0 68.47 115.23 17.09 o 5 13 0 771.89 834.20 45.28 o 6 13 0 0.39 38.34 14.71 o 0 14 0 15.76 34.30 9.14 o 1 14 0 21454.32 21355.73 309.61 o 2 14 0 1253.50 1284.07 28.80 o 3 14 0 127.94 137.77 24.38 o 4 14 0 235.53 259.13 22.63 o 5 14 0 244.23 291.17 30.69 o 6 14 0 73.28 71.49 23.36 o 1 15 0 6508.74 6536.09 103.87 o 2 15 0 506.82 451.51 21.00 o 3 15 0 6655.70 6362.68 206.11 o 4 15 0 85.34 64.24 41.51 o 5 15 0 181.97 188.51 22.41 o 6 15 0 417.42 353.19 50.52 o 0 16 0 8148.00 8228.48 219.92 o 1 16 0 6135.09 6260.04 107.81 o 2 16 0 5.79 17.53 6.01 o 3 16 0 83.12 126.71 19.61 o 4 16 0 533.91 509.72 65.03 o 5 16 0 385.45 396.01 39.21 o 6 16 0 1.17 -8.10 24.26 o 1 17 0 1537.96 1624.21 87.45 o 2 17 0 6617.63 6358.31 91.25 o 3 17 0 4898.38 4868.65 190.52 o 4 17 0 0.10 40.65 20.02 o 5 17 0 286.81 248.28 39.49 o 0 18 0 2488.38 2535.70 432.72 o 1 18 0 110.89 92.13 19.39 o 2 18 0 2197.36 1965.07 55.40 o 3 18 0 3495.28 3522.81 211.85 o 4 18 0 913.73 995.40 194.16 o 5 18 0 65.21 102.12 44.66 o 1 19 0 1078.34 1088.04 54.11 o 2 19 0 915.90 848.59 29.04 o 3 19 0 15.25 52.98 15.01 o 4 19 0 1197.73 1114.30 53.29 o 5 19 0 1822.32 1868.98 123.80 o 0 20 0 1849.15 1981.17 116.11 o 1 20 0 377.33 397.89 28.05 o 2 20 0 67.55 74.74 12.37 o 3 20 0 2262.80 2347.28 148.92 o 4 20 0 470.70 464.81 59.55 o 5 20 0 2.62 40.89 16.98 o 1 21 0 55.87 68.11 16.16 o 2 21 0 1158.21 1054.48 124.27 o 3 21 0 586.41 544.40 71.16 o 4 21 0 358.21 380.97 33.91 o 5 21 0 607.37 671.92 59.56 o 0 22 0 183.01 202.69 41.10 o 1 22 0 2886.57 2760.71 115.63 o 2 22 0 2834.27 2632.67 188.89 o 3 22 0 510.71 537.07 36.98 o 4 22 0 346.81 368.06 38.02 o 5 22 0 130.81 188.29 30.53 o 1 23 0 2211.21 2433.54 82.47 o 2 23 0 869.58 826.93 59.80 o 3 23 0 104.90 60.97 14.42 o 4 23 0 616.19 784.98 53.14 o 5 23 0 267.77 269.40 37.54 o 0 24 0 1435.86 1668.64 130.47 o 1 24 0 3363.48 3524.76 78.21 o 2 24 0 167.92 160.75 21.59 o 3 24 0 458.80 501.49 41.24 o 4 24 0 790.45 881.87 65.66 o 1 25 0 182.49 209.68 23.59 o 2 25 0 577.75 653.22 54.58 o 3 25 0 1136.13 1106.74 59.33 o 4 25 0 500.13 515.76 52.44 o 0 26 0 1575.88 1935.32 128.00 o 1 26 0 175.72 219.71 28.28 o 2 26 0 683.39 727.03 83.96 o 3 26 0 546.08 547.28 72.62 o 4 26 0 0.76 67.06 20.67 o 1 27 0 58.87 55.57 16.16 o 2 27 0 3388.64 3591.54 125.42 o 3 27 0 4.69 92.64 28.54 o 4 27 0 148.48 110.02 33.70 o 0 28 0 4319.67 4599.12 180.43 o 1 28 0 4.13 25.64 12.10 o 2 28 0 97.62 152.86 32.59 o 3 28 0 168.45 151.58 34.23 o 1 29 0 588.44 606.39 50.54 o 2 29 0 1335.55 1473.85 130.60 o 3 29 0 150.17 156.10 31.25 o 0 30 0 148.10 172.92 36.48 o 1 30 0 547.67 556.09 45.13 o 2 30 0 1258.85 1407.20 106.00 o 3 30 0 183.63 203.29 58.33 o 1 31 0 27.11 56.85 39.27 o 2 31 0 25.06 103.39 39.62 o 0 32 0 222.46 181.90 43.47 o 1 32 0 789.29 867.35 84.10 o 2 32 0 29.04 87.24 26.36 o 1 33 0 185.23 246.01 54.64 o 0 34 0 229.21 289.88 125.90 o -5 0 1 8413.03 9427.21 274.76 o -3 0 1 7478.45 7482.47 114.78 o -1 0 1 9635.15 9457.07 139.37 o 1 0 1 3589.83 3650.39 103.63 o 3 0 1 1849.63 1477.68 98.44 o 5 0 1 1417.14 1384.33 62.47 o -6 1 1 771.73 876.09 78.35 o -5 1 1 1420.98 1454.58 58.92 o -4 1 1 536.05 498.32 19.88 o -3 1 1 2869.26 2806.79 56.39 o -2 1 1 4394.70 4330.40 87.55 o -1 1 1 4006.78 3862.32 54.64 o 1 1 1 5379.97 5056.51 50.95 o 2 1 1 2004.83 1889.36 25.28 o 3 1 1 12387.22 12673.28 212.49 o 4 1 1 1308.36 1274.10 39.87 o 5 1 1 713.03 797.18 38.95 o 6 1 1 158.61 149.97 24.25 o -6 2 1 1.36 50.79 15.00 o -5 2 1 2346.62 2446.04 61.51 o -4 2 1 1347.72 1317.75 41.10 o -3 2 1 11204.45 11452.90 109.95 o -2 2 1 1497.69 1530.65 44.70 o -1 2 1 958.11 785.72 22.12 o 1 2 1 2454.78 2443.43 37.69 o 2 2 1 6684.50 6963.36 79.30 o 3 2 1 17.52 43.29 8.90 o 4 2 1 93.60 92.07 8.09 o 5 2 1 814.77 945.25 51.56 o 6 2 1 313.09 311.37 33.55 o -6 3 1 1239.25 1245.96 55.01 o -5 3 1 388.49 379.30 25.18 o -4 3 1 13.34 40.75 10.45 o -3 3 1 1366.99 1360.45 41.04 o -2 3 1 19468.66 18949.30 258.73 o -1 3 1 3334.95 3541.86 48.65 o 0 3 1 8.75 60.58 6.29 o 1 3 1 16545.69 17218.10 101.98 o 2 3 1 4937.35 4839.62 83.39 o 3 3 1 171.46 160.07 9.28 o 4 3 1 4829.83 4849.04 78.91 o 5 3 1 1036.13 1142.72 40.53 o 6 3 1 336.59 341.76 28.29 o -6 4 1 92.67 65.39 25.20 o -5 4 1 227.10 245.40 29.91 o -4 4 1 2364.53 2339.97 57.57 o -3 4 1 3839.13 3769.47 42.91 o -2 4 1 1442.08 1495.74 32.75 o -1 4 1 66681.13 72497.32 374.32 o 0 4 1 9198.25 9423.65 95.93 o 1 4 1 16967.86 16073.11 113.60 o 2 4 1 971.25 1069.21 22.43 o 3 4 1 9160.03 9233.85 103.71 o 4 4 1 52.52 82.34 12.17 o 5 4 1 1377.76 1476.98 51.13 o 6 4 1 781.69 974.09 92.71 o -6 5 1 1186.53 1347.22 143.25 o -5 5 1 0.36 32.72 14.71 o -4 5 1 28.22 45.23 10.46 o -3 5 1 7333.89 7568.29 127.13 o -2 5 1 901.82 912.00 23.59 o -1 5 1 21891.32 22576.38 119.71 o 0 5 1 1355.68 1416.73 20.85 o 1 5 1 12062.49 12723.94 129.82 o 2 5 1 1813.83 2069.31 69.12 o 3 5 1 6977.14 6727.28 92.00 o 4 5 1 1656.59 1542.11 41.27 o 5 5 1 850.67 865.58 52.06 o 6 5 1 693.89 764.16 47.01 o -6 6 1 195.03 220.63 27.63 o -5 6 1 271.81 260.73 45.26 o -4 6 1 175.70 191.83 14.54 o -3 6 1 15.99 54.53 14.26 o -2 6 1 15342.66 15746.11 145.27 o -1 6 1 31626.25 32680.51 355.82 o 0 6 1 56.19 58.48 3.61 o 1 6 1 1887.71 1703.74 29.22 o 2 6 1 8254.91 9041.20 94.97 o 3 6 1 7403.86 7319.92 108.08 o 4 6 1 2626.13 2626.32 53.26 o 5 6 1 690.65 793.64 46.04 o 6 6 1 226.50 135.70 23.13 o -6 7 1 10.90 38.17 16.57 o -5 7 1 16.83 60.82 28.47 o -4 7 1 395.53 396.19 26.64 o -3 7 1 14.84 38.61 8.39 o -2 7 1 2934.78 3069.87 29.50 o -1 7 1 15193.06 15331.22 136.89 o 0 7 1 9243.67 9282.14 108.81 o 1 7 1 18072.33 18538.64 269.80 o 2 7 1 9957.45 10243.18 129.72 o 3 7 1 208.22 210.12 14.54 o 4 7 1 147.68 116.38 12.74 o 5 7 1 160.35 187.21 20.38 o 6 7 1 1.68 38.34 26.28 o -6 8 1 136.00 129.28 27.43 o -5 8 1 107.27 136.60 39.71 o -4 8 1 52.64 44.97 12.78 o -3 8 1 1079.27 1010.73 31.09 o -2 8 1 7456.03 7314.83 106.96 o -1 8 1 6485.41 6050.88 34.95 o 0 8 1 33773.41 35329.74 303.74 o 1 8 1 495.57 612.28 14.31 o 3 8 1 1673.21 1665.38 43.61 o 4 8 1 921.81 928.45 41.30 o 5 8 1 803.24 833.11 53.06 o 6 8 1 336.42 362.53 40.40 o -6 9 1 54.06 88.60 18.22 o -5 9 1 497.07 498.84 53.44 o -4 9 1 1943.60 1867.01 87.21 o -3 9 1 5.90 33.40 14.15 o -2 9 1 8654.13 8655.52 165.68 o -1 9 1 4820.40 4428.48 32.73 o 0 9 1 32533.92 34814.21 352.57 o 1 9 1 2930.06 2758.14 45.49 o 2 9 1 41001.68 25116.71 6684.86 o 3 9 1 731.47 785.79 29.21 o 4 9 1 279.92 264.92 23.75 o 5 9 1 733.28 656.74 47.55 o 6 9 1 300.93 333.98 39.70 o -6 10 1 428.06 379.45 40.02 o -5 10 1 193.59 248.09 39.04 o -4 10 1 848.22 852.90 38.62 o -3 10 1 7447.09 7312.66 141.68 o -2 10 1 8945.76 9007.70 214.78 o -1 10 1 260.37 289.25 10.05 o 0 10 1 7774.35 8041.93 118.72 o 1 10 1 254.48 260.67 9.38 o 2 10 1 6.56 42.32 9.38 o 3 10 1 1515.46 1470.71 45.58 o 4 10 1 455.93 417.24 37.35 o 5 10 1 329.86 316.47 67.47 o 6 10 1 277.91 235.48 61.96 o -6 11 1 136.87 107.63 24.95 o -5 11 1 1272.44 1311.13 57.61 o -4 11 1 2296.98 2203.72 56.63 o -3 11 1 1136.88 1128.63 53.35 o -2 11 1 56.83 68.01 7.51 o -1 11 1 261.86 303.41 11.80 o 0 11 1 688.93 623.05 23.98 o 1 11 1 4348.44 4569.72 101.04 o 2 11 1 8123.50 7545.42 103.61 o 3 11 1 396.19 469.90 35.82 o 4 11 1 2721.70 2720.00 73.43 o 5 11 1 4172.22 4073.37 136.18 o 6 11 1 0.58 25.11 15.48 o -6 12 1 149.06 154.93 48.28 o -5 12 1 1468.98 1359.57 58.67 o -4 12 1 5714.07 5850.05 241.71 o -3 12 1 81.96 96.62 14.43 o -2 12 1 39.75 55.88 3.63 o -1 12 1 6702.94 6504.61 63.80 o 0 12 1 65.67 101.40 12.45 o 1 12 1 435.71 417.74 15.87 o 2 12 1 91.92 98.05 7.13 o 3 12 1 5892.87 6010.57 107.20 o 4 12 1 657.54 636.85 26.59 o 5 12 1 106.12 87.55 24.31 o 6 12 1 2142.08 2309.76 216.23 o -6 13 1 1581.09 1468.54 215.82 o -5 13 1 18.98 51.33 13.71 o -4 13 1 18.38 59.06 23.18 o -3 13 1 569.07 507.51 35.11 o -2 13 1 5698.44 5487.81 97.52 o -1 13 1 1106.91 1051.28 32.76 o 0 13 1 2749.49 2914.30 71.27 o 1 13 1 1433.70 1472.23 39.95 o 2 13 1 125.40 99.85 7.70 o 3 13 1 2656.85 2608.32 69.87 o 4 13 1 4594.89 5070.72 168.52 o 5 13 1 227.40 210.42 42.39 o 6 13 1 188.15 218.86 48.58 o -6 14 1 318.60 237.89 70.66 o -5 14 1 159.16 227.22 39.38 o -4 14 1 4742.69 4994.39 227.89 o -3 14 1 24.61 19.49 10.01 o -2 14 1 12192.79 11826.31 158.59 o -1 14 1 647.67 637.19 36.26 o 0 14 1 2460.75 2650.46 51.71 o 1 14 1 4656.86 4911.49 65.71 o 2 14 1 5279.05 5276.78 91.28 o 3 14 1 336.44 389.90 63.30 o 4 14 1 1019.42 1079.37 82.00 o 5 14 1 231.24 228.88 39.74 o 6 14 1 622.03 592.27 56.27 o -6 15 1 1260.61 1110.81 133.87 o -5 15 1 14.10 48.30 18.15 o -4 15 1 4.45 27.54 24.29 o -3 15 1 87.38 104.32 58.16 o -2 15 1 7089.80 6761.82 126.55 o -1 15 1 4938.32 5046.13 102.38 o 0 15 1 11.65 39.48 16.06 o 1 15 1 5889.69 5825.85 97.73 o 2 15 1 183.03 176.14 33.82 o 3 15 1 17.06 26.11 12.69 o 4 15 1 1212.43 1355.10 52.97 o 5 15 1 442.38 478.69 41.65 o 6 15 1 385.74 402.07 53.39 o -6 16 1 10.73 29.65 31.90 o -5 16 1 466.45 492.70 57.81 o -4 16 1 2556.70 2588.25 200.17 o -3 16 1 234.20 190.28 23.00 o -2 16 1 2217.90 1931.16 44.33 o -1 16 1 4572.91 4624.19 102.34 o 0 16 1 2433.90 2383.63 57.05 o 1 16 1 21.30 41.38 10.96 o 2 16 1 2901.35 3037.04 52.90 o 3 16 1 4248.85 4053.20 153.42 o 4 16 1 247.03 268.45 22.61 o 5 16 1 11.63 37.29 17.37 o 6 16 1 1278.81 1194.90 191.54 o -5 17 1 121.52 80.63 33.94 o -4 17 1 27.39 38.74 14.51 o -3 17 1 2365.92 2267.11 101.45 o -2 17 1 1530.27 1433.70 57.81 o -1 17 1 633.29 575.79 28.49 o 0 17 1 6376.68 6666.72 125.85 o 1 17 1 100.81 109.08 34.46 o 2 17 1 1942.12 1829.81 48.96 o 3 17 1 2.44 20.57 30.91 o 4 17 1 306.34 389.75 40.71 o 5 17 1 1979.60 2103.77 84.78 o -5 18 1 769.72 876.99 72.08 o -4 18 1 55.55 45.72 14.22 o -3 18 1 939.96 967.76 74.51 o -2 18 1 14113.13 13414.65 263.43 o -1 18 1 2095.63 2196.17 123.36 o 0 18 1 5992.14 5786.60 153.07 o 1 18 1 0.51 7.74 18.64 o 2 18 1 276.21 295.08 32.22 o 3 18 1 165.49 234.66 49.42 o 4 18 1 4649.89 4539.79 174.13 o 5 18 1 261.48 188.73 39.26 o -5 19 1 9.36 44.52 17.03 o -4 19 1 43.64 61.99 27.23 o -3 19 1 65.06 67.71 14.69 o -2 19 1 4746.45 4456.85 152.00 o -1 19 1 1081.64 1026.71 48.94 o 0 19 1 3287.44 3629.77 73.28 o 1 19 1 27.55 49.66 26.45 o 2 19 1 3647.53 3485.84 80.39 o 3 19 1 1533.70 1698.27 138.22 o 4 19 1 23.74 31.51 11.16 o 5 19 1 32.60 33.34 16.13 o -5 20 1 673.93 749.65 65.96 o -4 20 1 23.49 104.06 21.70 o -3 20 1 32.83 54.40 10.86 o -2 20 1 693.01 579.76 82.81 o -1 20 1 895.67 1040.87 48.97 o 0 20 1 6729.32 6999.11 130.14 o 1 20 1 1867.68 1909.81 65.26 o 2 20 1 776.39 711.29 46.46 o 3 20 1 18.15 38.40 18.36 o 4 20 1 1777.02 1778.31 99.40 o 5 20 1 117.94 77.75 28.19 o -5 21 1 126.95 93.31 24.71 o -4 21 1 191.97 133.11 57.55 o -3 21 1 559.84 530.72 36.92 o -2 21 1 595.01 487.57 41.30 o -1 21 1 0.72 77.73 18.99 o 0 21 1 2963.54 3305.01 103.48 o 1 21 1 12483.66 13286.04 300.97 o 2 21 1 5120.96 5104.15 138.99 o 3 21 1 798.69 700.42 47.48 o 4 21 1 66.77 29.78 22.14 o 5 21 1 146.30 169.82 37.46 o -5 22 1 114.27 100.90 25.78 o -4 22 1 840.66 950.50 118.79 o -3 22 1 597.09 624.20 92.78 o -2 22 1 860.95 832.05 86.48 o -1 22 1 1391.51 1669.77 58.15 o 0 22 1 13.35 75.48 13.47 o 1 22 1 46.81 114.77 30.61 o 2 22 1 26.35 52.70 11.76 o 3 22 1 1715.62 1416.01 127.97 o 4 22 1 85.05 75.96 15.19 o 5 22 1 111.27 105.75 26.14 o -5 23 1 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