#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:28:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181242 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/20/2232030.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232030_Fobs loop_ _publ_author_name 'Howie, R. Alan' 'de Lima, Geraldo M.' 'Tiekink, Edward R. T.' 'Wardell, James L.' 'Wardell, Solange M. S. V.' _publ_section_title ; fac-(2-Amidoethyl-\k^2^C^1^,O)trichlorido(urea-\kO)tin(IV) ; _journal_coeditor_code QM2029 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1420 _journal_page_last m1421 _journal_volume 67 _journal_year 2011 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.1223 _cell_length_b 12.0180 _cell_length_c 16.0461 _exptl_crystal_F_000 1376.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file qm2029Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ot29 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 456.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2108.01 2270.46 121.26 o 6 0 0 7.24 -10.06 18.62 o 8 0 0 5914.65 6175.51 227.02 o 10 0 0 35.92 25.74 10.59 o 12 0 0 33986.02 37224.18 2036.77 o 14 0 0 35070.90 37788.58 3334.69 o 2 1 0 12811.87 12948.75 275.91 o 4 1 0 6913.75 6656.02 148.38 o 6 1 0 75259.05 73252.59 1981.73 o 8 1 0 51092.18 49817.55 1026.39 o 10 1 0 24886.48 25388.34 646.24 o 12 1 0 6153.21 6346.69 247.20 o 14 1 0 1728.00 1819.63 189.57 o 0 2 0 167224.42 136438.06 7389.53 o 4 2 0 30582.20 29836.33 781.17 o 6 2 0 1143.24 1075.18 29.52 o 8 2 0 1234.26 1225.05 32.49 o 10 2 0 12310.97 12144.79 358.00 o 12 2 0 17772.10 18032.40 948.30 o 14 2 0 17689.27 17558.49 1466.13 o 2 3 0 3890.34 3783.00 85.77 o 4 3 0 87467.05 88756.52 2125.72 o 6 3 0 52425.61 51884.11 1140.25 o 8 3 0 56577.18 57205.03 1437.96 o 10 3 0 12274.79 12216.06 412.11 o 12 3 0 126.15 86.19 27.55 o 14 3 0 708.85 726.54 71.20 o 0 4 0 194.92 1.23 26.34 o 2 4 0 62837.92 61305.83 1443.96 o 4 4 0 87259.26 90774.33 1836.46 o 6 4 0 10348.06 11010.38 257.65 o 8 4 0 4037.55 3860.24 138.30 o 10 4 0 38496.93 39534.42 1326.46 o 12 4 0 7179.53 7586.81 515.59 o 2 5 0 26250.42 26130.52 534.00 o 4 5 0 97517.07 94035.13 3794.65 o 6 5 0 50734.71 50414.13 1215.28 o 8 5 0 18230.76 18147.71 582.40 o 10 5 0 10315.79 10644.80 412.17 o 12 5 0 844.62 830.37 85.53 o 0 6 0 14316.86 13918.51 391.06 o 2 6 0 14517.08 14473.67 290.82 o 4 6 0 39266.95 38450.23 937.72 o 6 6 0 11608.84 12222.16 282.59 o 8 6 0 4361.24 4273.99 127.53 o 10 6 0 8712.23 8812.14 374.35 o 12 6 0 14426.31 15021.08 1332.73 o 2 7 0 62310.12 61457.22 1314.96 o 4 7 0 29045.43 29468.14 643.16 o 6 7 0 25094.82 25830.51 754.73 o 8 7 0 11447.70 11655.87 404.54 o 10 7 0 5277.57 5695.64 297.19 o 12 7 0 6564.93 7214.06 683.34 o 0 8 0 60390.02 60782.96 1792.35 o 2 8 0 15540.18 15419.59 323.58 o 4 8 0 2661.52 2570.63 79.02 o 6 8 0 2852.41 2937.52 121.69 o 8 8 0 531.52 441.42 32.83 o 10 8 0 4314.30 4112.91 236.86 o 12 8 0 12416.84 12734.33 1382.11 o 2 9 0 7080.83 6881.18 185.81 o 4 9 0 9171.65 9208.12 246.62 o 6 9 0 20133.23 21262.13 740.23 o 8 9 0 8380.22 7994.30 438.44 o 10 9 0 6057.78 5826.00 412.65 o 0 10 0 19234.55 19215.00 774.56 o 2 10 0 17911.84 18710.74 647.70 o 4 10 0 6217.71 6437.09 212.61 o 6 10 0 222.39 149.79 30.90 o 8 10 0 1878.39 1727.58 115.63 o 10 10 0 3658.21 3806.85 372.09 o 2 11 0 1356.57 1487.24 79.23 o 4 11 0 9643.74 9908.09 329.36 o 6 11 0 7310.79 7995.38 446.53 o 8 11 0 15805.05 16239.49 1003.18 o 10 11 0 4622.73 4596.22 380.24 o 0 12 0 4009.18 3978.13 291.19 o 2 12 0 16258.09 16681.83 654.40 o 4 12 0 2143.23 2328.93 143.48 o 6 12 0 726.29 836.02 75.04 o 8 12 0 642.92 391.93 74.51 o 2 13 0 53.56 -31.82 31.82 o 4 13 0 3498.74 3562.63 231.61 o 6 13 0 6455.81 6115.02 440.78 o 0 14 0 14019.03 15117.85 1350.36 o 2 14 0 2568.88 2701.70 301.00 o 4 14 0 70.37 153.36 46.61 o 6 14 0 59.04 108.99 58.92 o 2 15 0 6444.23 6540.78 445.90 o 2 1 1 3.11 3.47 4.60 o 3 1 1 460.28 438.30 12.53 o 4 1 1 12115.53 12350.77 178.79 o 5 1 1 4060.73 4377.43 65.54 o 6 1 1 2830.31 2745.97 45.16 o 7 1 1 4305.62 4197.76 69.62 o 8 1 1 1825.99 1862.85 33.79 o 9 1 1 367.24 356.60 13.01 o 10 1 1 1854.27 1887.76 44.97 o 11 1 1 337.13 387.04 15.58 o 12 1 1 102.80 117.60 17.66 o 13 1 1 0.38 -6.82 16.42 o 14 1 1 1.87 -1.90 13.83 o 0 2 1 4516.68 4277.69 121.40 o 1 2 1 1306.24 1367.45 24.16 o 2 2 1 1925.75 2039.86 35.13 o 3 2 1 40097.42 40216.43 613.50 o 4 2 1 5204.05 5167.69 86.24 o 5 2 1 10541.81 10980.46 179.40 o 6 2 1 91.63 103.86 9.12 o 7 2 1 707.26 714.80 23.17 o 8 2 1 6674.95 6622.23 103.88 o 9 2 1 4267.02 4298.30 75.27 o 10 2 1 592.40 659.09 28.36 o 11 2 1 9.01 -1.03 11.59 o 12 2 1 2757.93 2625.42 108.94 o 13 2 1 62.68 78.25 31.08 o 14 2 1 466.51 496.75 46.39 o 1 3 1 31.45 40.22 8.04 o 2 3 1 13228.85 13302.03 221.51 o 3 3 1 1177.75 1074.02 21.12 o 4 3 1 7430.20 7453.58 119.04 o 5 3 1 13.54 5.83 6.01 o 6 3 1 3184.24 3083.22 56.12 o 7 3 1 2404.97 2323.05 39.16 o 8 3 1 98.74 103.44 9.23 o 9 3 1 1335.15 1343.21 34.40 o 10 3 1 465.51 350.35 19.22 o 11 3 1 1005.10 991.77 60.28 o 12 3 1 225.72 210.70 27.57 o 13 3 1 451.71 607.20 44.18 o 14 3 1 521.63 556.46 48.55 o 0 4 1 5700.51 5728.48 127.54 o 1 4 1 22664.23 22989.28 375.67 o 2 4 1 1175.03 1186.69 24.22 o 3 4 1 12678.07 13381.22 217.65 o 4 4 1 6144.85 6047.95 97.43 o 5 4 1 8633.50 8819.94 166.34 o 6 4 1 1717.06 1641.72 35.81 o 7 4 1 6870.61 7006.89 124.47 o 8 4 1 142.25 185.46 13.53 o 9 4 1 250.22 266.98 17.61 o 10 4 1 3083.46 2985.31 73.65 o 11 4 1 2401.29 2392.80 99.63 o 12 4 1 1158.84 1208.99 88.54 o 13 4 1 176.93 234.12 31.52 o 1 5 1 4163.64 4053.00 100.20 o 2 5 1 402.40 389.49 14.04 o 3 5 1 1101.95 1220.21 26.09 o 4 5 1 6.82 24.29 7.32 o 5 5 1 11728.62 11910.04 191.83 o 6 5 1 8293.61 8034.82 135.56 o 7 5 1 2.67 15.75 11.10 o 8 5 1 59.17 79.72 12.52 o 9 5 1 1443.60 1541.49 45.02 o 10 5 1 372.71 368.49 21.21 o 11 5 1 175.27 192.10 23.95 o 12 5 1 1149.10 1281.65 86.92 o 13 5 1 1040.67 876.36 85.31 o 0 6 1 1905.54 1924.00 53.33 o 1 6 1 2013.32 2100.88 56.13 o 2 6 1 180.50 265.61 13.28 o 3 6 1 3645.91 4044.43 69.48 o 4 6 1 15510.24 15622.75 268.47 o 5 6 1 5038.77 5350.71 93.03 o 6 6 1 6078.50 6158.58 110.65 o 7 6 1 8942.16 9340.79 185.16 o 8 6 1 11590.63 11326.59 231.66 o 9 6 1 2252.64 2178.28 61.80 o 10 6 1 1455.38 1434.35 62.16 o 11 6 1 2124.72 2168.90 144.66 o 13 6 1 352.11 295.78 42.45 o 1 7 1 14176.03 14229.12 256.02 o 2 7 1 491.65 478.70 17.89 o 3 7 1 7393.36 7510.53 120.68 o 4 7 1 75.56 83.46 9.49 o 5 7 1 4097.71 4145.57 110.74 o 6 7 1 4365.98 4433.36 103.95 o 7 7 1 730.83 704.74 32.03 o 8 7 1 2870.36 3018.28 102.79 o 9 7 1 2223.06 2071.80 66.75 o 10 7 1 588.53 680.74 49.01 o 11 7 1 515.95 487.88 48.99 o 12 7 1 111.52 353.13 84.43 o 0 8 1 6827.47 6920.94 150.93 o 1 8 1 0.99 19.34 7.78 o 2 8 1 10015.17 9789.32 153.21 o 3 8 1 659.12 679.07 28.29 o 4 8 1 398.15 408.35 23.42 o 5 8 1 4681.74 4638.63 134.37 o 6 8 1 1182.94 1223.32 40.70 o 7 8 1 6813.08 6458.87 149.60 o 8 8 1 1.65 -4.48 11.11 o 9 8 1 7171.08 7135.68 255.52 o 10 8 1 131.69 169.03 23.67 o 11 8 1 1336.94 1103.25 132.26 o 12 8 1 563.57 641.95 95.78 o 1 9 1 17748.91 17932.57 307.17 o 2 9 1 14.27 28.51 7.78 o 3 9 1 10832.10 10830.97 211.96 o 4 9 1 5342.18 5268.17 121.93 o 5 9 1 226.56 241.39 17.06 o 6 9 1 201.57 179.28 22.37 o 7 9 1 1.47 1.65 15.18 o 8 9 1 4388.80 4315.09 141.26 o 9 9 1 189.22 194.76 29.14 o 10 9 1 5979.55 5961.39 320.68 o 11 9 1 3979.91 3413.22 236.59 o 0 10 1 19373.79 19734.28 526.18 o 1 10 1 641.42 620.41 28.03 o 2 10 1 12466.98 12643.39 278.15 o 3 10 1 1563.49 1483.33 51.89 o 4 10 1 1551.95 1671.05 59.35 o 5 10 1 7183.52 7360.12 174.26 o 6 10 1 1918.41 1812.25 82.82 o 7 10 1 6503.78 6255.04 224.82 o 8 10 1 2633.21 2463.78 115.91 o 9 10 1 7001.47 7100.89 329.03 o 10 10 1 138.44 109.96 85.75 o 11 10 1 479.22 466.21 57.76 o 1 11 1 9937.20 10330.58 257.05 o 2 11 1 202.84 229.77 19.85 o 3 11 1 6365.10 6531.72 249.19 o 4 11 1 1589.69 1675.98 79.99 o 5 11 1 171.07 159.61 28.77 o 6 11 1 4566.67 5066.63 174.46 o 7 11 1 98.13 95.89 27.75 o 8 11 1 6767.05 6400.42 287.88 o 9 11 1 823.41 730.09 74.25 o 10 11 1 2413.27 2236.87 158.98 o 0 12 1 8984.02 8917.03 524.85 o 1 12 1 584.26 432.57 53.49 o 2 12 1 2296.59 2304.23 83.80 o 3 12 1 2915.88 2904.14 116.97 o 4 12 1 2114.05 2170.02 94.77 o 5 12 1 6290.14 6583.89 295.03 o 6 12 1 444.11 403.61 52.27 o 7 12 1 7937.73 7631.41 377.69 o 8 12 1 774.79 790.12 75.62 o 9 12 1 2803.78 2648.62 211.30 o 1 13 1 6720.64 7287.66 240.44 o 2 13 1 193.90 109.22 39.67 o 3 13 1 1450.79 1435.09 109.74 o 4 13 1 1165.80 1443.63 92.75 o 5 13 1 6324.13 6707.33 311.55 o 6 13 1 12219.20 11794.79 474.77 o 7 13 1 182.14 31.21 50.70 o 0 14 1 2063.47 2299.56 153.79 o 1 14 1 2878.21 2694.25 128.18 o 2 14 1 1469.52 1292.02 97.69 o 3 14 1 2803.78 2742.61 135.28 o 4 14 1 4437.52 4370.68 226.45 o 5 14 1 4852.45 4702.62 207.23 o 6 14 1 2225.66 1944.09 109.01 o 1 15 1 5133.08 4856.22 245.60 o 2 15 1 2372.90 2567.99 134.09 o 3 15 1 5013.42 5046.66 268.41 o 1 0 2 5227.41 5689.41 145.01 o 2 0 2 16259.41 16618.04 381.17 o 3 0 2 30187.23 28905.84 628.44 o 4 0 2 38816.17 38875.80 776.57 o 5 0 2 57680.38 57914.24 1202.65 o 6 0 2 3619.68 3406.09 72.18 o 7 0 2 62684.04 62020.38 1326.59 o 8 0 2 5653.73 5719.24 129.95 o 9 0 2 21954.34 21696.30 458.38 o 10 0 2 7006.16 6902.43 200.37 o 11 0 2 11367.31 11534.64 350.25 o 12 0 2 4578.83 4730.84 215.83 o 13 0 2 24.31 27.22 18.82 o 14 0 2 611.99 375.62 77.81 o 1 1 2 141983.00 149368.38 8489.26 o 2 1 2 2250.71 2143.24 41.50 o 3 1 2 10356.62 9340.64 143.79 o 4 1 2 3119.96 3040.28 54.55 o 5 1 2 7964.68 7395.21 126.35 o 6 1 2 4551.07 4520.83 79.77 o 7 1 2 696.59 703.66 31.21 o 8 1 2 581.95 509.89 18.42 o 9 1 2 3961.26 3830.08 69.95 o 10 1 2 150.07 136.05 10.23 o 11 1 2 6629.29 6743.79 130.16 o 12 1 2 1091.57 1130.35 55.08 o 13 1 2 21009.81 21782.44 974.00 o 14 1 2 1214.24 1369.77 79.67 o 0 2 2 24508.79 24827.22 591.17 o 1 2 2 19034.81 17869.38 294.69 o 2 2 2 15882.38 15924.32 254.07 o 3 2 2 23140.39 22487.78 350.51 o 4 2 2 4103.51 4023.85 61.18 o 5 2 2 47130.55 46776.66 702.72 o 6 2 2 1910.55 1857.81 36.40 o 7 2 2 64179.35 65313.72 1165.56 o 8 2 2 266.74 314.28 15.89 o 9 2 2 24784.07 25090.26 421.32 o 10 2 2 4909.68 4893.15 104.89 o 11 2 2 5471.56 5287.49 136.52 o 12 2 2 2601.83 2256.63 200.73 o 13 2 2 0.78 23.29 20.80 o 14 2 2 1367.87 1239.51 99.12 o 1 3 2 39359.06 37734.99 624.95 o 2 3 2 14536.96 14685.81 225.39 o 3 3 2 93833.91 94599.68 1463.05 o 4 3 2 11350.67 11526.61 197.29 o 5 3 2 4806.82 4792.14 75.60 o 6 3 2 224.45 165.32 13.11 o 7 3 2 46.72 47.03 6.75 o 8 3 2 1416.21 1366.54 31.26 o 9 3 2 6653.56 6674.47 128.83 o 10 3 2 4695.69 4725.58 108.80 o 11 3 2 19629.04 19287.57 558.41 o 12 3 2 1639.70 1626.77 98.05 o 13 3 2 4998.37 4874.14 250.73 o 14 3 2 199.29 195.86 27.82 o 0 4 2 12658.30 12330.02 245.43 o 1 4 2 5356.07 5241.53 77.43 o 2 4 2 6413.24 6396.00 102.78 o 3 4 2 37528.96 38142.36 566.48 o 4 4 2 54.92 103.96 8.03 o 5 4 2 68159.14 67743.06 1121.11 o 6 4 2 370.80 342.21 13.25 o 7 4 2 24284.95 24445.74 451.07 o 8 4 2 306.22 341.72 18.78 o 9 4 2 31270.05 31581.62 664.00 o 10 4 2 62.64 99.14 12.58 o 11 4 2 1873.89 1786.83 67.07 o 12 4 2 1983.11 1954.98 99.86 o 1 5 2 43725.77 42542.74 622.06 o 2 5 2 4724.69 4893.00 117.12 o 3 5 2 57059.61 56327.10 909.61 o 4 5 2 2435.90 2469.30 57.71 o 5 5 2 7619.86 7852.76 137.87 o 6 5 2 5796.35 6028.70 113.41 o 7 5 2 380.60 376.32 17.20 o 8 5 2 7149.05 7259.65 160.88 o 9 5 2 11224.38 11121.74 254.39 o 10 5 2 3642.91 3543.81 90.97 o 11 5 2 14108.89 15170.43 619.78 o 12 5 2 0.71 23.13 19.73 o 13 5 2 6747.83 6903.30 477.98 o 0 6 2 7206.92 6963.01 197.55 o 1 6 2 8762.70 8549.13 133.12 o 2 6 2 1465.71 1496.72 41.89 o 3 6 2 31679.15 31632.92 585.61 o 4 6 2 128.43 114.59 13.27 o 5 6 2 28091.01 27956.05 456.52 o 6 6 2 0.03 0.74 12.95 o 7 6 2 24609.67 25679.18 581.62 o 8 6 2 287.22 250.64 18.10 o 9 6 2 13452.21 13106.82 309.08 o 10 6 2 12.44 16.07 17.05 o 11 6 2 4899.07 5016.19 226.14 o 12 6 2 2.83 27.10 21.79 o 13 6 2 709.83 710.06 62.33 o 1 7 2 61969.52 63370.98 998.29 o 2 7 2 8238.59 8400.85 136.46 o 3 7 2 9466.65 9559.15 184.28 o 4 7 2 651.16 678.98 21.75 o 5 7 2 15947.45 16332.93 308.60 o 6 7 2 16625.07 16362.68 458.11 o 7 7 2 614.61 475.63 28.47 o 8 7 2 10469.75 10469.14 264.70 o 9 7 2 3018.01 3220.01 92.76 o 10 7 2 9.29 75.37 25.91 o 11 7 2 7760.01 7413.85 336.44 o 12 7 2 1168.07 1135.20 81.13 o 0 8 2 153.80 185.58 21.42 o 1 8 2 18935.10 18867.67 310.06 o 2 8 2 3124.62 3030.28 71.47 o 3 8 2 11395.25 11258.72 214.90 o 4 8 2 2063.53 2281.85 113.79 o 5 8 2 17131.46 17680.05 370.20 o 6 8 2 83.24 93.13 16.65 o 7 8 2 24644.56 24266.00 569.90 o 8 8 2 793.52 801.79 54.60 o 9 8 2 2051.78 2029.33 99.87 o 10 8 2 329.36 381.27 39.40 o 11 8 2 10990.49 11072.08 694.91 o 12 8 2 1.59 25.79 55.33 o 1 9 2 34613.24 34707.49 702.31 o 2 9 2 263.57 331.89 21.15 o 3 9 2 12501.04 12618.14 367.89 o 4 9 2 249.50 248.88 19.63 o 5 9 2 4744.80 4880.21 111.39 o 6 9 2 4473.30 4249.41 124.39 o 7 9 2 4.32 -10.63 12.70 o 8 9 2 2316.89 2327.20 120.90 o 9 9 2 4147.95 4133.92 147.16 o 10 9 2 6.11 7.70 34.92 o 11 9 2 8618.65 8896.07 578.96 o 0 10 2 4987.03 5235.58 162.77 o 1 10 2 81.59 151.39 17.42 o 2 10 2 994.29 930.97 34.19 o 3 10 2 10036.40 10525.44 242.44 o 4 10 2 26.42 63.26 43.43 o 5 10 2 13197.67 13718.40 338.30 o 6 10 2 15.36 -12.88 14.73 o 7 10 2 7194.78 7445.88 274.99 o 8 10 2 1.94 -17.79 17.79 o 9 10 2 12523.32 12860.68 467.73 o 10 10 2 222.37 127.03 41.04 o 1 11 2 9621.00 9423.23 241.86 o 2 11 2 4371.09 4433.04 124.96 o 3 11 2 23128.04 23491.41 765.29 o 4 11 2 2612.14 2555.32 87.76 o 5 11 2 801.23 791.70 48.67 o 6 11 2 196.27 143.56 35.22 o 7 11 2 125.30 133.98 33.09 o 8 11 2 327.63 280.27 43.51 o 9 11 2 3707.12 3916.70 242.10 o 10 11 2 941.19 600.01 91.26 o 0 12 2 944.16 1038.53 73.30 o 1 12 2 461.50 324.09 46.04 o 2 12 2 605.34 598.83 41.16 o 3 12 2 2415.49 2512.76 95.59 o 4 12 2 1.13 -20.77 20.77 o 5 12 2 8792.38 8964.60 291.98 o 6 12 2 74.49 156.03 55.50 o 7 12 2 5392.90 5303.29 207.46 o 8 12 2 174.81 197.58 40.42 o 9 12 2 7773.25 8387.06 596.68 o 1 13 2 9308.96 9351.33 320.30 o 2 13 2 3662.17 3739.19 135.68 o 3 13 2 4460.34 3905.34 192.59 o 4 13 2 1442.85 1236.53 82.56 o 5 13 2 186.11 95.58 36.43 o 6 13 2 94.26 154.96 32.73 o 7 13 2 218.27 249.95 46.75 o 0 14 2 118.06 74.78 49.55 o 1 14 2 1477.91 1371.15 73.84 o 2 14 2 27.48 6.58 30.34 o 3 14 2 605.57 570.74 55.54 o 4 14 2 942.18 775.22 71.90 o 5 14 2 1795.57 1786.44 161.85 o 6 14 2 345.49 339.41 57.57 o 1 15 2 6220.71 5964.94 256.84 o 2 15 2 13.76 -6.09 30.45 o 3 15 2 15.79 29.80 26.90 o 1 1 3 473.83 397.17 15.57 o 2 1 3 22009.03 22603.55 403.93 o 3 1 3 272.16 329.63 9.58 o 4 1 3 108.90 124.36 7.25 o 5 1 3 4.84 -1.59 8.17 o 6 1 3 3466.61 3465.42 62.52 o 7 1 3 1502.44 1540.15 34.62 o 8 1 3 2281.00 2221.21 53.34 o 9 1 3 337.40 354.25 15.56 o 10 1 3 1.41 26.25 6.34 o 11 1 3 1934.56 1966.66 49.05 o 12 1 3 2315.09 2284.72 112.05 o 13 1 3 0.22 -2.29 9.46 o 14 1 3 347.14 297.93 35.09 o 0 2 3 2196.56 1967.53 63.74 o 1 2 3 4.71 -5.64 5.64 o 2 2 3 4899.14 5067.46 82.66 o 3 2 3 17451.54 17118.96 277.35 o 4 2 3 1.60 13.61 6.39 o 5 2 3 224.31 236.18 10.59 o 6 2 3 2190.31 2260.51 38.66 o 7 2 3 17616.87 17978.36 307.43 o 8 2 3 10.54 42.68 11.28 o 9 2 3 226.58 200.81 17.39 o 10 2 3 436.15 407.93 33.73 o 11 2 3 770.05 743.21 34.12 o 12 2 3 18.65 81.45 16.33 o 13 2 3 627.32 629.32 37.61 o 14 2 3 17.42 2.02 13.95 o 1 3 3 3356.81 3190.85 50.87 o 2 3 3 39745.80 39675.11 587.74 o 3 3 3 18064.89 18293.89 400.22 o 4 3 3 450.24 447.77 13.45 o 5 3 3 1707.04 1749.39 41.87 o 6 3 3 4750.93 4701.07 80.50 o 7 3 3 332.81 345.11 15.38 o 8 3 3 7377.00 7260.06 133.91 o 9 3 3 1161.00 1140.36 27.04 o 10 3 3 20.47 9.96 6.23 o 11 3 3 4955.72 5076.78 196.24 o 12 3 3 1207.50 1141.73 67.45 o 13 3 3 208.83 151.00 26.42 o 14 3 3 124.26 173.20 27.95 o 0 4 3 10125.34 9503.75 189.84 o 1 4 3 3141.56 3111.59 51.51 o 2 4 3 14109.89 13264.82 230.93 o 3 4 3 1683.53 1502.43 26.63 o 4 4 3 301.06 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