#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/20/2232080.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232080_Fobs loop_ _publ_author_name 'Udachin, Konstantin A.' 'Zaman, Md. Badruz' 'Ripmeester, John A.' _publ_section_title ; Bis(guanidinium) chloranilate ; _journal_coeditor_code VM2118 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2625 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.087 _cell_angle_gamma 90.000 _cell_length_a 19.5224 _cell_length_b 3.7316 _cell_length_c 18.4103 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.7194 _[local]_cod_data_source_file vm2118Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zam79 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 204.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5603.65 5601.91 48.32 o 4 0 0 607.92 492.50 4.35 o 6 0 0 1499.23 1369.47 11.15 o 8 0 0 574.77 602.72 6.76 o 10 0 0 423.52 343.08 5.80 o 12 0 0 7972.38 7638.27 53.85 o 14 0 0 1666.50 1462.68 12.21 o 16 0 0 294.69 323.07 8.79 o 18 0 0 157.80 169.28 9.88 o 20 0 0 149.23 138.67 7.36 o 22 0 0 19.58 27.85 5.17 o 24 0 0 26.17 39.34 6.19 o 1 1 0 1639.95 1826.22 14.84 o 3 1 0 206.78 238.75 6.82 o 5 1 0 545.41 514.86 7.81 o 7 1 0 863.73 958.66 12.65 o 9 1 0 1288.09 1511.97 16.22 o 11 1 0 29.29 14.05 1.94 o 13 1 0 1599.52 1543.71 17.07 o 15 1 0 2405.28 2330.64 18.51 o 17 1 0 445.11 411.53 5.82 o 19 1 0 0.18 -0.65 2.72 o 21 1 0 89.15 96.99 4.77 o 23 1 0 6.69 5.98 3.57 o 0 2 0 9563.49 10213.82 48.29 o 2 2 0 3951.69 4126.94 17.51 o 4 2 0 171.86 183.32 2.90 o 6 2 0 397.77 454.55 3.70 o 8 2 0 401.54 383.30 5.46 o 10 2 0 46.97 54.78 2.66 o 12 2 0 5992.16 5890.71 48.17 o 14 2 0 3541.31 3506.56 25.62 o 16 2 0 407.42 399.97 12.94 o 18 2 0 51.48 48.00 3.20 o 20 2 0 12.65 9.05 3.09 o 22 2 0 64.91 63.76 4.96 o 1 3 0 1372.34 1430.80 11.21 o 3 3 0 7.88 18.29 2.15 o 5 3 0 234.02 244.49 5.90 o 7 3 0 12.18 8.91 2.84 o 9 3 0 82.18 82.27 4.16 o 11 3 0 36.86 40.26 3.59 o 13 3 0 2222.12 2298.34 15.28 o 15 3 0 302.78 319.99 6.11 o 17 3 0 189.84 205.07 5.46 o 19 3 0 83.64 82.27 4.60 o 0 4 0 570.39 603.57 12.24 o 2 4 0 12.09 11.87 3.11 o 4 4 0 286.23 294.47 6.85 o 6 4 0 284.96 285.38 7.05 o 8 4 0 45.80 44.44 4.22 o 10 4 0 187.25 202.70 6.60 o 12 4 0 360.99 417.84 12.48 o 14 4 0 133.81 145.52 8.62 o 3 5 0 50.56 60.62 10.44 o 5 5 0 157.76 143.13 20.21 o -23 1 1 529.77 526.37 11.15 o -21 1 1 764.74 685.79 10.55 o -19 1 1 3.12 4.21 2.72 o -17 1 1 540.79 473.45 10.87 o -15 1 1 3398.11 3313.37 34.46 o -13 1 1 3321.98 3118.27 17.47 o -11 1 1 5705.88 5690.56 20.28 o -9 1 1 6035.85 6279.85 58.03 o -7 1 1 1750.33 1745.36 21.63 o -5 1 1 217.11 242.25 4.90 o -3 1 1 41634.16 40113.83 295.28 o -1 1 1 1585.73 1937.60 22.45 o 1 1 1 2212.23 2325.88 14.86 o 3 1 1 15095.04 14432.38 137.58 o 5 1 1 3198.04 3275.51 14.37 o 7 1 1 5571.64 5680.32 39.14 o 9 1 1 780.61 707.20 5.74 o 11 1 1 3.05 5.77 1.85 o 13 1 1 27.04 24.77 2.50 o 15 1 1 2081.92 2144.10 13.25 o 17 1 1 620.57 604.92 9.96 o 19 1 1 749.30 734.57 12.60 o 21 1 1 210.99 214.37 6.43 o 23 1 1 12.48 11.32 3.90 o -22 2 1 70.06 65.96 5.03 o -20 2 1 675.59 709.03 14.90 o -18 2 1 25.26 24.16 2.96 o -16 2 1 732.20 722.32 8.07 o -14 2 1 318.29 293.72 5.59 o -12 2 1 121.71 141.60 3.70 o -10 2 1 115.09 113.38 4.77 o -8 2 1 394.77 370.52 4.87 o -6 2 1 827.14 883.95 7.26 o -4 2 1 97.12 129.74 2.91 o -2 2 1 20.58 27.04 2.34 o 0 2 1 1111.06 1086.12 16.67 o 2 2 1 1760.12 1878.01 9.35 o 4 2 1 19.61 19.33 2.15 o 6 2 1 504.04 518.44 4.31 o 8 2 1 596.82 595.97 7.33 o 10 2 1 2208.66 2251.36 14.93 o 12 2 1 2935.72 2902.92 15.29 o 14 2 1 247.85 221.55 4.76 o 16 2 1 335.21 313.01 5.71 o 18 2 1 200.27 195.91 5.11 o 20 2 1 505.68 505.45 8.26 o 22 2 1 8.05 -0.24 6.04 o -19 3 1 15.92 20.70 3.54 o -17 3 1 211.83 224.57 5.64 o -15 3 1 402.14 427.55 6.86 o -13 3 1 0.99 4.90 2.92 o -11 3 1 1070.21 1057.86 12.07 o -9 3 1 1905.65 1907.31 15.76 o -7 3 1 18.56 13.18 2.82 o -5 3 1 9.36 7.12 2.57 o -3 3 1 22.18 16.96 2.31 o -1 3 1 62.71 67.02 3.35 o 1 3 1 2898.31 3028.53 60.65 o 3 3 1 2458.23 2677.68 21.05 o 5 3 1 20.81 19.09 2.81 o 7 3 1 179.55 182.30 5.15 o 9 3 1 494.65 488.21 8.04 o 11 3 1 404.02 410.50 7.88 o 13 3 1 445.38 462.42 14.60 o 15 3 1 297.62 315.41 8.16 o 17 3 1 659.34 670.39 16.59 o 19 3 1 862.79 930.99 11.67 o -14 4 1 66.10 69.75 5.08 o -12 4 1 597.82 660.26 13.08 o -10 4 1 170.69 178.54 6.15 o -8 4 1 395.02 424.57 11.02 o -6 4 1 756.76 797.97 11.06 o -4 4 1 237.46 242.74 6.38 o -2 4 1 628.42 617.16 13.85 o 0 4 1 114.78 120.36 4.77 o 2 4 1 375.73 393.14 8.72 o 4 4 1 1060.19 1125.04 20.04 o 6 4 1 730.71 760.84 12.60 o 8 4 1 225.37 230.89 7.68 o 10 4 1 168.94 173.39 10.44 o 12 4 1 182.90 185.06 10.17 o 14 4 1 773.76 782.32 37.31 o -5 5 1 26.52 22.68 7.88 o 3 5 1 104.22 111.37 9.55 o 5 5 1 131.27 127.73 8.91 o -24 0 2 944.66 891.85 17.90 o -22 0 2 1483.32 1422.21 51.19 o -20 0 2 1390.74 1371.91 27.20 o -18 0 2 20.13 8.51 3.89 o -16 0 2 6698.85 6021.50 73.17 o -14 0 2 2255.94 2219.77 16.99 o -12 0 2 1206.87 1135.15 15.06 o -10 0 2 1140.68 935.42 11.91 o -8 0 2 40217.49 39655.95 107.34 o -6 0 2 602.90 687.09 16.80 o -4 0 2 8121.89 7516.44 63.69 o -2 0 2 1148.92 1335.07 17.63 o 0 0 2 544.97 651.71 10.93 o 2 0 2 308.61 252.35 2.41 o 4 0 2 27971.12 26494.74 102.06 o 6 0 2 10921.19 10697.78 64.87 o 8 0 2 12171.35 12732.13 97.70 o 10 0 2 264.49 296.89 4.62 o 12 0 2 3295.84 3423.51 35.77 o 14 0 2 21.98 26.02 5.45 o 16 0 2 10.11 15.75 3.92 o 18 0 2 2997.73 2846.30 33.53 o 20 0 2 1116.46 995.90 17.90 o 22 0 2 95.09 82.38 6.83 o -23 1 2 397.90 372.96 8.38 o -21 1 2 12.24 8.74 2.99 o -19 1 2 0.83 -2.53 2.53 o -17 1 2 301.60 268.82 5.08 o -15 1 2 1116.73 1130.24 13.08 o -13 1 2 0.41 2.44 1.81 o -11 1 2 81.30 76.53 2.81 o -9 1 2 578.71 656.20 8.25 o -7 1 2 1415.21 1380.22 10.74 o -5 1 2 25.06 45.15 8.59 o -3 1 2 2684.23 3009.37 14.31 o -1 1 2 20219.29 20878.18 149.30 o 1 1 2 4088.46 4288.49 63.47 o 3 1 2 1701.68 1755.33 28.38 o 5 1 2 431.11 436.48 6.50 o 7 1 2 600.45 567.18 10.28 o 9 1 2 2415.94 2457.37 44.97 o 11 1 2 245.73 211.40 4.17 o 13 1 2 7.19 10.43 2.11 o 15 1 2 3.97 2.88 2.17 o 17 1 2 1221.25 1139.86 17.81 o 19 1 2 154.07 155.57 5.49 o 21 1 2 41.40 42.53 4.13 o -22 2 2 220.33 234.77 7.35 o -20 2 2 443.41 455.99 7.29 o -18 2 2 5.79 7.19 2.59 o -16 2 2 3.40 1.74 2.30 o -14 2 2 1084.28 1109.79 9.78 o -12 2 2 742.49 774.43 7.35 o -10 2 2 1653.73 1696.52 10.46 o -8 2 2 3180.33 3094.42 19.42 o -6 2 2 4929.23 4846.28 24.82 o -4 2 2 58.02 57.31 2.21 o -2 2 2 1111.59 1248.99 9.01 o 0 2 2 5568.34 5703.05 74.19 o 2 2 2 1783.63 1942.58 14.15 o 4 2 2 6012.81 6042.76 40.63 o 6 2 2 3256.13 3318.39 32.88 o 8 2 2 1383.38 1304.05 15.73 o 10 2 2 481.29 482.32 9.45 o 12 2 2 291.51 299.03 6.16 o 14 2 2 68.58 68.25 3.17 o 16 2 2 2499.51 2509.96 16.09 o 18 2 2 1281.92 1270.24 12.26 o 20 2 2 1622.37 1669.91 16.59 o -19 3 2 38.07 38.55 3.78 o -17 3 2 309.93 341.88 6.57 o -15 3 2 189.73 183.97 4.83 o -13 3 2 12.00 14.00 2.62 o -11 3 2 96.36 98.71 4.51 o -9 3 2 1902.85 1970.49 16.24 o -7 3 2 249.55 233.27 7.63 o -5 3 2 256.45 247.55 4.80 o -3 3 2 400.97 396.32 6.35 o -1 3 2 174.45 197.61 4.64 o 1 3 2 547.52 573.99 7.46 o 3 3 2 1149.65 1233.08 15.48 o 5 3 2 4919.39 5202.96 30.11 o 7 3 2 34.15 33.67 3.29 o 9 3 2 0.15 -1.17 2.88 o 11 3 2 1009.08 1085.90 28.69 o 13 3 2 244.75 248.65 5.42 o 15 3 2 9.42 10.36 2.86 o 17 3 2 244.96 255.57 6.40 o -16 4 2 10.77 6.33 4.54 o -14 4 2 19.01 22.80 4.31 o -12 4 2 746.24 805.43 12.92 o -10 4 2 230.64 236.71 6.88 o -8 4 2 102.47 109.93 4.99 o -6 4 2 129.37 137.99 5.23 o -4 4 2 142.92 142.21 5.27 o -2 4 2 288.66 287.03 11.73 o 0 4 2 574.71 610.88 19.42 o 2 4 2 259.90 274.06 19.99 o 4 4 2 532.51 525.07 27.20 o 6 4 2 605.54 563.99 21.21 o 8 4 2 288.97 290.11 17.99 o 10 4 2 78.31 74.81 9.55 o 12 4 2 102.33 100.12 6.75 o 14 4 2 285.19 272.73 19.21 o -7 5 2 708.46 784.88 17.66 o -5 5 2 149.59 171.48 9.48 o 3 5 2 697.25 639.87 26.98 o 5 5 2 156.46 150.91 9.42 o -25 1 3 812.64 854.28 19.78 o -23 1 3 1290.79 1247.46 14.52 o -21 1 3 849.55 770.71 16.22 o -19 1 3 56.63 47.03 3.12 o -17 1 3 1048.60 1024.11 8.76 o -15 1 3 2343.67 2192.90 13.37 o -13 1 3 2.24 1.76 1.90 o -11 1 3 10017.25 10380.50 57.20 o -9 1 3 3595.80 3639.20 39.79 o -7 1 3 1293.94 1308.52 9.00 o -5 1 3 14423.36 13983.41 65.90 o -3 1 3 15638.75 16125.78 71.34 o -1 1 3 21663.18 21708.70 168.21 o 1 1 3 13680.47 13539.80 71.98 o 3 1 3 7884.56 7951.65 49.20 o 5 1 3 4636.93 4367.92 49.71 o 7 1 3 3254.99 3342.26 48.78 o 9 1 3 2.06 3.49 1.72 o 11 1 3 3553.80 3631.51 45.17 o 13 1 3 1.90 3.21 2.12 o 15 1 3 2127.79 1978.55 19.06 o 17 1 3 1543.16 1436.55 12.69 o 19 1 3 705.64 665.58 10.48 o 21 1 3 0.53 -3.63 4.17 o -22 2 3 4.81 3.05 3.36 o -20 2 3 387.98 401.72 6.80 o -18 2 3 165.70 176.77 4.55 o -16 2 3 185.40 176.29 5.95 o -14 2 3 30.78 34.10 2.60 o -12 2 3 879.35 947.50 8.08 o -10 2 3 637.30 616.26 8.79 o -8 2 3 1197.18 1131.46 7.24 o -6 2 3 801.88 901.44 7.43 o -4 2 3 2542.44 2980.95 28.44 o -2 2 3 1650.99 1761.72 24.30 o 0 2 3 2.58 1.51 1.66 o 2 2 3 4752.31 4931.66 35.35 o 4 2 3 2011.43 2068.04 19.55 o 6 2 3 36.81 37.25 1.89 o 8 2 3 209.15 200.85 3.86 o 10 2 3 1588.94 1546.86 24.29 o 12 2 3 1075.00 1045.80 9.33 o 14 2 3 260.38 270.48 5.71 o 16 2 3 75.27 79.49 4.90 o 18 2 3 49.03 57.48 3.74 o 20 2 3 425.22 445.97 19.33 o -21 3 3 147.20 169.94 5.86 o -19 3 3 305.24 338.45 7.96 o -17 3 3 438.02 465.06 7.40 o -15 3 3 38.83 39.98 3.09 o -13 3 3 33.29 39.98 2.99 o -11 3 3 476.09 499.21 15.51 o -9 3 3 1500.06 1511.39 14.06 o -7 3 3 321.87 300.09 6.34 o -5 3 3 170.08 154.70 3.63 o -3 3 3 22.66 23.06 2.75 o -1 3 3 1410.66 1464.70 18.96 o 1 3 3 1078.87 1090.97 9.04 o 3 3 3 3016.51 2979.16 40.40 o 5 3 3 974.97 989.05 9.55 o 7 3 3 1373.37 1445.59 29.08 o 9 3 3 1568.00 1657.60 22.79 o 11 3 3 1256.35 1366.79 35.81 o 13 3 3 494.99 534.42 18.36 o 15 3 3 429.77 436.32 8.92 o 17 3 3 90.53 94.91 4.60 o -16 4 3 303.08 323.15 8.78 o -14 4 3 140.02 141.97 9.36 o -12 4 3 1042.73 1069.49 16.73 o -10 4 3 583.60 582.09 14.58 o -8 4 3 727.43 725.57 15.49 o -6 4 3 307.84 307.19 8.02 o -4 4 3 292.59 280.95 6.82 o -2 4 3 125.08 120.99 4.71 o 0 4 3 409.92 417.36 13.56 o 2 4 3 568.18 544.12 13.66 o 4 4 3 165.09 156.26 8.46 o 6 4 3 340.39 330.64 11.99 o 8 4 3 7.33 6.54 5.28 o 10 4 3 109.25 112.07 8.73 o 12 4 3 761.35 674.64 26.65 o -7 5 3 9.70 3.12 5.29 o -5 5 3 260.25 260.39 9.61 o -3 5 3 12.52 4.22 8.88 o -1 5 3 271.48 237.17 15.77 o 3 5 3 116.12 108.50 8.88 o -24 0 4 685.21 654.24 15.07 o -22 0 4 114.18 90.14 6.20 o -20 0 4 3969.98 3662.89 41.30 o -18 0 4 7239.94 6583.93 43.33 o -16 0 4 6877.28 6869.17 68.31 o -14 0 4 1.77 5.99 4.93 o -12 0 4 214.81 252.70 4.68 o -10 0 4 884.72 888.14 14.62 o -8 0 4 16423.75 15856.46 47.21 o -6 0 4 16868.89 16080.63 134.43 o -4 0 4 7727.48 7596.89 92.76 o -2 0 4 870.59 760.45 41.08 o 0 0 4 8520.37 8458.08 37.69 o 2 0 4 8.65 13.75 1.31 o 4 0 4 5868.33 5833.40 29.78 o 6 0 4 13.93 47.90 2.99 o 8 0 4 1721.36 1411.92 9.56 o 10 0 4 5626.39 5789.98 32.95 o 12 0 4 32.29 49.75 3.09 o 14 0 4 38.77 67.23 4.74 o 16 0 4 2574.18 2276.65 24.65 o 18 0 4 12.17 11.23 4.20 o 20 0 4 1210.06 1278.44 21.04 o 22 0 4 754.99 784.14 17.66 o -25 1 4 3.23 2.44 3.68 o -23 1 4 44.14 44.50 4.07 o -21 1 4 52.19 56.01 3.89 o -19 1 4 13.42 15.66 2.56 o -17 1 4 370.17 319.85 5.09 o -15 1 4 10.36 13.87 2.09 o -13 1 4 8.48 4.07 1.84 o -11 1 4 184.71 171.45 2.83 o -9 1 4 45.10 33.31 1.50 o -7 1 4 5122.49 5636.50 51.16 o -5 1 4 11608.09 12037.73 41.99 o -3 1 4 1916.61 2196.11 10.38 o -1 1 4 1933.70 1831.42 18.04 o 1 1 4 6868.82 7022.61 43.78 o 3 1 4 99.26 123.74 3.26 o 5 1 4 791.77 863.82 7.37 o 7 1 4 1034.54 1138.74 7.73 o 9 1 4 929.32 894.87 7.24 o 11 1 4 13.46 19.90 2.26 o 13 1 4 312.30 292.05 4.96 o 15 1 4 583.94 527.30 6.94 o 17 1 4 86.99 93.02 4.53 o 19 1 4 43.26 50.29 4.01 o 21 1 4 58.61 54.92 4.54 o -24 2 4 44.18 41.17 5.73 o -22 2 4 546.07 601.05 10.64 o -20 2 4 1160.01 1222.08 14.53 o -18 2 4 1062.60 1062.36 10.01 o -16 2 4 98.96 97.61 3.46 o -14 2 4 1177.56 1119.96 13.94 o -12 2 4 26.91 27.49 2.36 o -10 2 4 55.00 43.06 2.46 o -8 2 4 4313.22 4228.42 23.27 o -6 2 4 3005.46 3037.48 16.28 o -4 2 4 10155.10 10373.26 47.50 o -2 2 4 1436.27 1448.66 16.25 o 0 2 4 178.24 192.38 3.09 o 2 2 4 8.35 1.03 1.60 o 4 2 4 5589.55 6061.10 42.46 o 6 2 4 452.80 452.70 10.90 o 8 2 4 4535.84 4492.92 64.43 o 10 2 4 42.80 41.00 2.80 o 12 2 4 407.88 408.10 6.16 o 14 2 4 532.03 541.40 7.41 o 16 2 4 2.09 6.24 2.71 o 18 2 4 148.60 144.71 4.92 o 20 2 4 271.49 270.06 7.88 o -21 3 4 5.09 6.12 3.71 o -19 3 4 305.91 289.94 7.59 o -17 3 4 476.91 477.49 7.50 o -15 3 4 89.34 84.40 3.68 o -13 3 4 1.34 3.48 2.30 o -11 3 4 1239.70 1219.71 13.05 o -9 3 4 2.80 2.20 3.15 o -7 3 4 145.35 117.37 4.90 o -5 3 4 705.83 691.84 17.16 o -3 3 4 965.69 917.46 14.01 o -1 3 4 28.84 26.89 2.84 o 1 3 4 499.45 532.27 6.69 o 3 3 4 339.46 322.68 4.66 o 5 3 4 4.17 5.27 2.86 o 7 3 4 1643.46 1723.97 34.87 o 9 3 4 3273.33 3481.01 46.70 o 11 3 4 1290.24 1366.34 40.77 o 13 3 4 342.92 349.68 11.51 o 15 3 4 23.08 30.32 5.50 o 17 3 4 240.09 232.91 8.05 o -16 4 4 65.07 66.57 5.21 o -14 4 4 0.11 2.72 3.72 o -12 4 4 12.37 2.31 3.79 o -10 4 4 286.14 275.95 7.28 o -8 4 4 1172.18 1181.45 25.40 o -6 4 4 224.89 222.23 7.15 o -4 4 4 118.62 107.43 4.93 o -2 4 4 42.20 40.67 4.01 o 0 4 4 32.07 30.92 4.84 o 2 4 4 66.24 56.91 5.65 o 4 4 4 164.81 150.57 8.37 o 6 4 4 1481.04 1432.36 23.55 o 8 4 4 637.97 633.56 16.49 o 10 4 4 417.08 387.14 13.71 o 12 4 4 163.27 149.73 9.96 o -7 5 4 122.17 143.50 9.10 o -5 5 4 753.29 807.42 21.20 o -3 5 4 69.40 68.62 10.88 o 1 5 4 81.27 61.51 10.88 o 3 5 4 30.21 33.08 13.55 o -25 1 5 288.22 265.04 7.54 o -23 1 5 15.94 12.88 3.41 o -21 1 5 1239.36 1190.09 13.10 o -19 1 5 3006.96 3165.62 16.78 o -17 1 5 4975.85 4733.92 20.56 o -15 1 5 495.21 496.86 8.77 o -13 1 5 359.78 337.20 4.50 o -11 1 5 80.20 70.77 1.99 o -9 1 5 442.53 551.12 3.71 o -7 1 5 531.62 453.99 8.92 o -5 1 5 8722.55 8256.51 66.40 o -3 1 5 7006.04 6883.74 52.92 o -1 1 5 725.07 636.29 3.37 o 1 1 5 3517.51 3967.62 42.75 o 3 1 5 8109.86 8732.65 83.96 o 5 1 5 142.29 162.52 6.02 o 7 1 5 3591.72 3652.01 13.44 o 9 1 5 4906.01 4816.79 36.98 o 11 1 5 2969.23 2980.63 28.63 o 13 1 5 69.89 68.56 3.08 o 15 1 5 1712.42 1638.53 12.19 o 17 1 5 247.30 220.93 7.05 o 19 1 5 456.67 430.74 8.89 o 21 1 5 920.25 977.62 23.49 o -24 2 5 52.23 63.33 5.23 o -22 2 5 28.97 34.59 3.50 o -20 2 5 30.45 30.68 3.09 o -18 2 5 143.91 121.92 3.94 o -16 2 5 650.29 656.50 8.17 o -14 2 5 178.84 151.60 3.79 o -12 2 5 6.42 10.50 2.12 o -10 2 5 1658.98 1822.31 10.61 o -8 2 5 2141.37 2340.18 15.67 o -6 2 5 5866.52 5952.82 28.64 o -4 2 5 4521.52 4971.04 21.62 o -2 2 5 139.34 163.38 3.10 o 0 2 5 88.37 96.17 2.58 o 2 2 5 2815.49 2771.50 15.31 o 4 2 5 0.90 -1.34 1.54 o 6 2 5 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