#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/20/2232083.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232083_Fobs loop_ _publ_author_name 'Wei, Bin' _publ_section_title ; Piperazine-1,4-diium naphthalene-1,5-disulfonate ; _journal_coeditor_code VM2121 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2811 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.005 _cell_angle_gamma 90.000 _cell_length_a 11.9968 _cell_length_b 7.2959 _cell_length_c 9.1453 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file vm2121Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 104.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 612.68 676.16 12.58 o 3 0 0 8395.79 8765.62 127.95 o 4 0 0 33.66 41.90 1.37 o 5 0 0 6000.72 6227.27 80.94 o 6 0 0 11.66 9.84 1.29 o 7 0 0 1004.33 997.05 14.47 o 8 0 0 59.67 49.25 2.22 o 9 0 0 897.84 905.73 15.70 o 10 0 0 650.65 673.57 13.07 o 11 0 0 43.05 40.00 4.14 o 12 0 0 4.54 5.39 1.83 o 13 0 0 162.96 170.13 6.13 o 14 0 0 118.22 120.94 11.35 o 15 0 0 263.94 265.37 18.17 o 1 1 0 96.25 94.89 0.70 o 2 1 0 0.04 1.21 0.24 o 3 1 0 0.07 1.10 0.23 o 4 1 0 2.98 3.29 0.37 o 5 1 0 1196.99 1368.76 17.89 o 6 1 0 256.35 297.29 4.25 o 7 1 0 80.48 79.87 2.07 o 8 1 0 393.83 434.68 6.34 o 9 1 0 46.29 49.16 1.77 o 10 1 0 79.90 91.24 2.50 o 11 1 0 12.53 10.93 1.48 o 12 1 0 1.88 1.93 1.12 o 13 1 0 1.39 3.52 1.48 o 14 1 0 52.93 53.84 4.59 o 15 1 0 7.22 14.40 5.17 o 0 2 0 5306.79 4469.16 58.60 o 1 2 0 4296.55 3850.53 23.06 o 2 2 0 1541.98 1345.13 12.24 o 3 2 0 1245.82 1148.29 7.35 o 4 2 0 181.12 173.31 3.02 o 5 2 0 105.98 94.56 1.56 o 6 2 0 188.59 210.81 2.49 o 7 2 0 581.39 607.87 6.43 o 8 2 0 20.69 25.59 2.01 o 9 2 0 2063.40 2014.38 31.54 o 10 2 0 18.44 24.58 2.25 o 11 2 0 71.93 60.12 2.71 o 12 2 0 231.76 235.56 6.13 o 13 2 0 54.26 45.99 3.55 o 14 2 0 94.97 103.53 5.24 o 15 2 0 188.34 178.97 11.95 o 1 3 0 4.23 5.87 0.56 o 2 3 0 310.29 333.61 3.38 o 3 3 0 628.41 655.50 6.71 o 4 3 0 5.97 4.91 1.84 o 5 3 0 0.51 4.73 0.84 o 6 3 0 403.35 415.07 6.55 o 7 3 0 79.31 86.07 2.42 o 8 3 0 48.25 37.45 1.99 o 9 3 0 160.79 154.25 3.82 o 10 3 0 37.69 34.46 2.08 o 11 3 0 3.94 6.80 1.99 o 12 3 0 31.15 35.78 2.90 o 13 3 0 93.38 91.91 5.00 o 14 3 0 0.36 -2.07 2.07 o 0 4 0 1608.46 1691.04 22.76 o 1 4 0 21.06 27.09 1.52 o 2 4 0 63.28 38.43 1.13 o 3 4 0 764.70 756.59 7.58 o 4 4 0 14.13 12.36 1.28 o 5 4 0 78.73 71.91 2.37 o 6 4 0 348.08 339.14 6.91 o 7 4 0 58.65 68.04 2.37 o 8 4 0 84.54 81.57 2.79 o 9 4 0 110.73 108.22 3.41 o 10 4 0 112.99 113.99 5.62 o 11 4 0 71.14 73.94 6.27 o 12 4 0 11.34 16.29 2.77 o 13 4 0 2.38 7.80 3.44 o 14 4 0 6.04 8.99 3.43 o 1 5 0 471.82 478.09 6.43 o 2 5 0 117.37 137.15 2.65 o 3 5 0 1096.35 1117.97 12.57 o 4 5 0 384.49 382.34 6.71 o 5 5 0 244.86 244.46 5.37 o 6 5 0 1497.36 1478.04 21.22 o 7 5 0 81.23 77.12 2.85 o 8 5 0 92.29 87.82 2.92 o 9 5 0 0.81 2.23 1.71 o 10 5 0 280.35 267.93 7.99 o 11 5 0 124.06 123.01 5.48 o 12 5 0 411.17 395.66 11.87 o 13 5 0 108.35 103.04 7.18 o 0 6 0 556.81 551.46 11.67 o 1 6 0 39.62 43.31 3.77 o 2 6 0 549.53 511.05 7.76 o 3 6 0 1197.85 1175.93 17.53 o 4 6 0 95.45 99.80 3.48 o 5 6 0 54.47 49.21 2.51 o 6 6 0 5.01 6.89 2.38 o 7 6 0 65.72 64.11 3.78 o 8 6 0 135.13 123.88 5.30 o 9 6 0 30.56 34.54 3.33 o 10 6 0 0.86 0.78 2.05 o 11 6 0 87.49 96.45 5.89 o 1 7 0 103.05 105.94 3.62 o 2 7 0 286.02 275.74 5.64 o 3 7 0 1279.60 1289.77 21.60 o 4 7 0 194.91 192.82 5.36 o 5 7 0 6.88 6.63 1.61 o 6 7 0 261.23 262.60 8.24 o 7 7 0 103.89 97.67 5.00 o 8 7 0 57.47 50.62 4.02 o 9 7 0 1.45 -1.23 2.05 o 10 7 0 61.46 63.74 5.57 o 0 8 0 0.03 2.92 2.39 o 1 8 0 0.07 4.24 1.84 o 2 8 0 96.94 99.71 4.21 o 3 8 0 0.04 -1.64 1.64 o 4 8 0 13.09 17.00 2.50 o 5 8 0 77.50 79.04 5.05 o 6 8 0 22.73 28.09 3.11 o 7 8 0 14.54 18.58 5.38 o 8 8 0 4.56 0.86 2.56 o 1 9 0 21.58 24.26 3.26 o 2 9 0 8.06 11.60 6.26 o 3 9 0 108.60 108.11 7.88 o 4 9 0 81.23 72.65 6.04 o -15 1 1 2.52 0.79 2.32 o -14 1 1 542.96 549.81 12.21 o -13 1 1 30.99 31.12 2.51 o -12 1 1 501.73 517.98 10.00 o -11 1 1 129.01 128.09 3.19 o -10 1 1 5.89 4.68 0.98 o -9 1 1 346.78 339.20 5.10 o -8 1 1 1126.65 1169.03 12.71 o -7 1 1 872.72 842.52 8.78 o -6 1 1 417.39 430.74 4.62 o -5 1 1 9386.82 9285.56 65.10 o -4 1 1 491.74 436.92 7.78 o -3 1 1 4255.35 4166.61 20.52 o -2 1 1 7099.29 6339.51 41.45 o -1 1 1 637.19 583.80 2.93 o 0 1 1 5885.95 5161.52 41.50 o 1 1 1 5021.20 4490.54 35.58 o 2 1 1 6854.20 6131.75 38.36 o 3 1 1 433.36 485.76 3.87 o 4 1 1 1459.60 1389.91 10.35 o 5 1 1 3531.08 3653.66 27.34 o 6 1 1 325.97 334.66 3.83 o 7 1 1 612.53 601.50 6.64 o 8 1 1 14.61 20.88 1.09 o 9 1 1 31.65 31.32 1.47 o 10 1 1 499.12 461.85 7.10 o 11 1 1 458.83 466.79 11.26 o 12 1 1 43.35 43.26 2.08 o 13 1 1 352.32 350.17 11.10 o 14 1 1 124.49 127.18 6.68 o 15 1 1 244.08 246.13 12.69 o -15 2 1 9.36 10.88 4.92 o -14 2 1 31.91 31.01 3.50 o -13 2 1 15.53 17.12 2.32 o -12 2 1 15.68 15.38 1.94 o -11 2 1 33.79 25.77 2.07 o -10 2 1 84.97 102.61 3.38 o -9 2 1 67.31 73.76 2.58 o -8 2 1 151.83 149.24 2.49 o -7 2 1 363.64 404.29 5.97 o -6 2 1 137.81 134.56 1.71 o -5 2 1 1333.65 1405.65 18.86 o -4 2 1 383.65 472.40 6.10 o -3 2 1 47.48 46.81 0.84 o -2 2 1 183.89 160.34 2.26 o -1 2 1 13.36 16.63 1.27 o 0 2 1 231.96 223.82 2.78 o 1 2 1 2034.95 1920.04 16.70 o 2 2 1 1191.29 1225.08 8.33 o 3 2 1 456.08 535.98 4.15 o 4 2 1 104.45 97.27 1.27 o 5 2 1 23.59 32.41 0.80 o 6 2 1 173.15 169.30 2.25 o 7 2 1 253.74 253.72 3.38 o 8 2 1 106.46 105.81 3.90 o 9 2 1 4.32 7.71 1.08 o 10 2 1 86.60 88.17 2.78 o 11 2 1 74.31 79.16 3.62 o 12 2 1 30.71 28.57 4.32 o 13 2 1 0.45 5.85 2.29 o 14 2 1 26.86 24.84 3.36 o -14 3 1 116.34 124.92 6.09 o -13 3 1 2.37 0.62 2.03 o -12 3 1 207.59 199.92 5.62 o -11 3 1 50.60 56.13 4.06 o -10 3 1 63.88 67.69 2.85 o -9 3 1 138.32 137.23 3.70 o -8 3 1 107.51 102.47 2.97 o -7 3 1 958.14 948.82 15.26 o -6 3 1 53.37 62.19 1.99 o -5 3 1 998.97 971.81 12.20 o -4 3 1 3049.07 3183.40 36.57 o -3 3 1 183.64 174.33 3.78 o -2 3 1 1501.91 1557.92 20.00 o -1 3 1 1392.74 1560.00 14.10 o 0 3 1 198.56 168.71 3.19 o 1 3 1 13.62 15.43 0.76 o 2 3 1 155.36 213.24 2.73 o 3 3 1 334.71 344.74 3.49 o 4 3 1 671.57 671.25 6.00 o 5 3 1 124.38 107.40 2.62 o 6 3 1 8.39 17.19 1.15 o 7 3 1 21.61 22.17 1.74 o 8 3 1 8.15 10.85 1.76 o 9 3 1 242.16 265.82 7.08 o 10 3 1 197.09 185.32 5.76 o 11 3 1 152.86 152.84 5.46 o 12 3 1 53.44 46.97 3.61 o 13 3 1 172.64 174.25 8.04 o 14 3 1 195.58 185.49 7.46 o -14 4 1 17.81 19.84 4.41 o -13 4 1 47.64 47.15 4.15 o -12 4 1 0.01 1.35 1.71 o -11 4 1 178.51 191.14 6.15 o -10 4 1 81.77 79.89 3.44 o -9 4 1 410.76 418.12 8.28 o -8 4 1 1189.29 1139.97 20.00 o -7 4 1 153.07 151.32 3.87 o -6 4 1 457.13 428.72 7.07 o -5 4 1 83.79 88.52 2.50 o -4 4 1 332.08 308.13 4.97 o -3 4 1 66.36 76.39 2.20 o -2 4 1 4.27 8.18 0.75 o -1 4 1 895.33 918.33 11.72 o 0 4 1 181.09 183.49 2.89 o 1 4 1 936.14 992.93 10.16 o 2 4 1 44.23 42.22 1.25 o 3 4 1 5.57 8.78 0.74 o 4 4 1 411.78 432.87 5.72 o 5 4 1 58.78 53.71 2.98 o 6 4 1 411.15 391.59 6.02 o 7 4 1 1506.63 1488.71 28.33 o 8 4 1 122.08 119.04 4.28 o 9 4 1 19.81 23.80 2.30 o 10 4 1 415.30 409.07 10.54 o 11 4 1 63.56 65.91 4.14 o 12 4 1 76.02 78.91 4.36 o 13 4 1 9.29 9.11 3.89 o -13 5 1 45.17 52.59 5.34 o -12 5 1 11.70 10.18 3.16 o -11 5 1 56.65 62.25 5.17 o -10 5 1 1.84 8.99 2.17 o -9 5 1 139.00 126.57 3.97 o -8 5 1 286.67 271.86 6.26 o -7 5 1 64.11 62.31 2.68 o -6 5 1 37.97 36.09 2.13 o -5 5 1 988.85 1025.46 15.13 o -4 5 1 92.75 95.44 2.92 o -3 5 1 539.95 527.00 7.48 o -2 5 1 70.13 75.12 1.97 o -1 5 1 62.82 55.24 2.16 o 0 5 1 705.44 675.06 10.07 o 1 5 1 47.02 55.35 2.04 o 2 5 1 529.07 547.31 7.20 o 3 5 1 107.88 105.87 2.28 o 4 5 1 227.19 210.58 3.30 o 5 5 1 718.22 713.68 10.75 o 6 5 1 2.28 5.72 1.08 o 7 5 1 18.80 18.41 2.07 o 8 5 1 54.48 55.51 3.54 o 9 5 1 52.67 54.55 3.23 o 10 5 1 4.98 4.00 1.95 o 11 5 1 76.19 74.27 4.84 o 12 5 1 66.23 67.68 4.84 o -12 6 1 21.75 23.43 4.29 o -11 6 1 300.77 299.97 12.16 o -10 6 1 47.72 55.90 4.10 o -9 6 1 115.84 111.25 4.92 o -8 6 1 452.01 420.46 9.21 o -7 6 1 16.05 23.44 4.34 o -6 6 1 472.38 455.49 9.13 o -5 6 1 17.89 20.55 1.99 o -4 6 1 59.51 52.76 3.25 o -3 6 1 175.07 183.67 4.58 o -2 6 1 1629.76 1608.66 20.18 o -1 6 1 374.65 383.42 7.45 o 0 6 1 152.26 148.28 3.51 o 1 6 1 923.31 950.73 12.82 o 2 6 1 170.80 173.49 3.85 o 3 6 1 540.02 512.53 7.55 o 4 6 1 12.40 10.60 1.80 o 5 6 1 339.86 346.90 7.11 o 6 6 1 20.97 23.46 2.67 o 7 6 1 168.50 174.87 6.04 o 8 6 1 702.97 673.04 16.02 o 9 6 1 35.82 32.47 3.22 o 10 6 1 116.67 118.21 5.55 o 11 6 1 57.75 61.55 4.44 o -10 7 1 87.73 79.58 6.16 o -9 7 1 22.83 28.31 4.28 o -8 7 1 20.45 20.91 3.42 o -7 7 1 117.45 115.67 5.19 o -6 7 1 12.93 15.02 2.14 o -5 7 1 100.46 104.51 4.05 o -4 7 1 88.44 88.85 3.85 o -3 7 1 291.72 293.59 7.08 o -2 7 1 21.61 23.95 2.31 o -1 7 1 135.71 139.46 4.20 o 0 7 1 245.96 230.58 5.61 o 1 7 1 0.81 3.65 1.51 o 2 7 1 82.56 71.09 2.71 o 3 7 1 37.66 46.41 3.27 o 4 7 1 252.59 242.94 6.19 o 5 7 1 6.89 11.11 2.32 o 6 7 1 12.30 20.50 2.87 o 7 7 1 0.24 2.90 2.10 o 8 7 1 6.05 7.44 2.34 o 9 7 1 111.17 104.13 5.41 o 10 7 1 11.89 22.80 3.83 o -8 8 1 41.45 40.32 6.07 o -7 8 1 16.71 26.92 5.42 o -6 8 1 71.96 76.03 6.14 o -5 8 1 46.21 47.66 3.38 o -4 8 1 20.50 22.15 2.53 o -3 8 1 0.69 3.66 1.93 o -2 8 1 415.16 402.42 9.77 o -1 8 1 207.85 205.48 5.94 o 0 8 1 5.26 5.29 1.59 o 1 8 1 167.55 162.55 5.27 o 2 8 1 177.34 161.28 5.39 o 3 8 1 281.15 263.28 9.36 o 4 8 1 14.90 23.78 3.07 o 5 8 1 7.17 8.62 2.63 o 6 8 1 37.68 39.18 4.08 o 7 8 1 98.50 108.72 5.63 o 8 8 1 91.34 89.43 6.71 o -4 9 1 0.03 -0.02 2.12 o -3 9 1 4.40 -0.19 2.46 o -2 9 1 5.09 3.87 2.59 o -1 9 1 2.15 2.43 2.17 o 0 9 1 6.02 7.95 3.28 o 1 9 1 4.51 7.75 2.89 o 2 9 1 9.68 9.28 5.30 o 3 9 1 0.75 -0.01 1.82 o 4 9 1 24.77 22.24 3.75 o -15 0 2 20.89 35.24 6.11 o -14 0 2 449.15 449.25 17.10 o -13 0 2 139.51 154.73 5.87 o -12 0 2 623.77 635.87 14.98 o -11 0 2 0.35 2.09 1.47 o -10 0 2 454.50 497.22 11.89 o -9 0 2 817.51 791.76 14.16 o -8 0 2 869.61 899.71 14.80 o -7 0 2 2293.53 2348.42 31.15 o -6 0 2 59.85 60.60 2.90 o -5 0 2 374.95 338.61 8.68 o -4 0 2 1426.87 1527.49 16.21 o -3 0 2 4508.37 4283.74 37.60 o -2 0 2 105.66 102.19 1.85 o -1 0 2 3986.15 3716.02 29.97 o 0 0 2 11007.28 10606.43 93.89 o 1 0 2 5977.16 5601.69 42.91 o 2 0 2 1841.71 1615.90 23.84 o 3 0 2 32.86 38.21 1.14 o 4 0 2 97.66 71.33 1.64 o 5 0 2 643.35 696.68 9.36 o 6 0 2 3186.75 3404.71 64.86 o 7 0 2 28.59 38.34 1.74 o 8 0 2 451.37 448.83 11.71 o 9 0 2 471.41 419.16 41.24 o 10 0 2 175.56 162.01 6.75 o 11 0 2 123.06 141.69 6.19 o 12 0 2 22.87 24.24 3.80 o 13 0 2 455.66 466.11 16.38 o 14 0 2 2.38 -1.39 4.52 o -15 1 2 9.29 15.79 3.16 o -14 1 2 35.94 35.89 2.93 o -13 1 2 12.50 12.88 2.42 o -12 1 2 138.99 158.80 14.52 o -11 1 2 50.62 48.79 2.20 o -10 1 2 16.42 16.98 1.37 o -9 1 2 988.31 1002.20 12.23 o -8 1 2 45.17 33.64 1.35 o -7 1 2 1.16 1.03 0.59 o -6 1 2 8.00 10.10 0.91 o -5 1 2 27.16 35.58 1.06 o -4 1 2 1260.83 1357.11 17.85 o -3 1 2 16.69 20.47 0.71 o -2 1 2 194.14 207.37 4.10 o -1 1 2 3396.31 3340.03 15.44 o 0 1 2 3226.49 3093.73 15.33 o 1 1 2 2112.93 2079.05 10.48 o 2 1 2 332.46 337.51 2.38 o 3 1 2 1254.61 1271.97 14.21 o 4 1 2 1231.97 1334.09 18.59 o 5 1 2 1.26 0.34 0.54 o 6 1 2 223.27 226.56 2.94 o 7 1 2 14.57 14.70 1.09 o 8 1 2 64.87 66.94 1.76 o 9 1 2 258.12 253.72 4.44 o 10 1 2 5.39 7.52 1.96 o 11 1 2 8.64 7.91 1.52 o 12 1 2 27.38 22.12 2.15 o 13 1 2 47.94 38.73 3.70 o 14 1 2 0.43 0.60 2.10 o -15 2 2 1.41 1.93 3.13 o -14 2 2 38.84 34.46 2.70 o -13 2 2 35.14 35.24 2.80 o -12 2 2 380.75 390.14 8.21 o -11 2 2 44.31 43.52 2.51 o -10 2 2 543.42 599.71 10.56 o -9 2 2 912.55 937.03 14.04 o -8 2 2 1128.25 1129.88 13.00 o -7 2 2 1714.01 1692.93 17.18 o -6 2 2 149.84 178.30 2.81 o -5 2 2 1641.66 1532.40 20.21 o -4 2 2 660.11 715.24 8.12 o -3 2 2 1780.84 1827.39 27.57 o -2 2 2 1482.37 1540.07 10.54 o -1 2 2 0.15 8.47 0.65 o 0 2 2 4406.68 4028.88 38.51 o 1 2 2 146.76 179.93 2.08 o 2 2 2 141.27 96.18 1.79 o 3 2 2 560.76 570.48 6.82 o 4 2 2 28.08 51.79 1.51 o 5 2 2 215.52 234.45 4.66 o 6 2 2 226.66 221.30 5.47 o 7 2 2 22.65 25.55 1.15 o 8 2 2 757.73 758.09 11.13 o 9 2 2 397.74 413.08 7.42 o 10 2 2 288.83 269.21 5.72 o 11 2 2 171.72 181.59 6.94 o 12 2 2 3.51 4.35 1.78 o 13 2 2 333.48 317.87 9.33 o 14 2 2 89.60 88.24 5.70 o -14 3 2 21.96 33.36 3.98 o -13 3 2 66.52 61.08 3.34 o -12 3 2 8.09 1.28 1.43 o -11 3 2 2.13 3.50 1.64 o -10 3 2 310.34 279.36 6.76 o -9 3 2 7.54 8.02 1.32 o -8 3 2 7.06 9.02 2.25 o -7 3 2 130.37 132.67 3.79 o -6 3 2 666.71 668.00 10.15 o -5 3 2 60.88 60.09 1.82 o -4 3 2 70.99 51.02 1.32 o -3 3 2 279.63 319.98 3.40 o -2 3 2 86.54 86.55 2.09 o -1 3 2 302.64 326.10 4.13 o 0 3 2 747.90 770.60 15.13 o 1 3 2 309.65 314.07 8.04 o 2 3 2 853.46 966.14 11.50 o 3 3 2 306.59 291.64 4.95 o 4 3 2 107.09 110.38 2.25 o 5 3 2 99.16 110.27 3.54 o 6 3 2 316.30 314.01 5.25 o 7 3 2 281.83 260.39 5.53 o 8 3 2 125.78 111.47 3.00 o 9 3 2 68.85 75.90 3.51 o 10 3 2 47.42 47.13 4.08 o 11 3 2 9.42 10.76 2.03 o 12 3 2 288.29 276.85 8.76 o 13 3 2 50.82 52.07 4.14 o 14 3 2 32.89 35.70 4.92 o -14 4 2 24.73 27.02 4.45 o -13 4 2 12.89 22.21 3.60 o -12 4 2 144.97 143.48 5.85 o -11 4 2 1.65 1.67 1.31 o -10 4 2 267.99 274.93 6.41 o -9 4 2 287.35 280.52 7.20 o -8 4 2 81.32 79.22 3.96 o -7 4 2 584.06 586.94 9.64 o -6 4 2 75.38 82.52 3.22 o -5 4 2 784.92 794.37 19.24 o -4 4 2 488.46 485.42 5.37 o -3 4 2 246.90 243.18 4.12 o -2 4 2 705.29 694.84 7.66 o -1 4 2 14.34 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