#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/21/2232145.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232145_Fobs loop_ _publ_author_name 'Wen, Hua-wen' 'Fang, Qi' _publ_section_title ; Thieno[3,4-d][1,3]dithiole-2-thione ; _journal_coeditor_code BG2422 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3097 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 3.9425 _cell_length_b 9.2588 _cell_length_c 19.2368 _exptl_crystal_F_000 384.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file bg2422Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fq09 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 21.87 24.67 1.33 o 4 0 0 1043.43 1036.20 11.30 o 1 1 0 123.87 122.31 1.28 o 2 1 0 136.31 119.35 1.65 o 3 1 0 45.90 45.43 1.71 o 4 1 0 0.94 2.11 1.66 o 5 1 0 9.50 10.06 4.23 o 0 2 0 1125.39 1088.67 13.43 o 1 2 0 2249.69 2224.02 8.65 o 2 2 0 2693.39 2578.53 10.92 o 3 2 0 12.76 16.63 1.44 o 4 2 0 232.57 229.34 3.72 o 5 2 0 46.90 45.21 3.86 o 1 3 0 4859.60 5050.62 20.12 o 2 3 0 33.86 32.29 1.11 o 3 3 0 420.61 423.35 3.99 o 4 3 0 56.18 58.93 2.66 o 0 4 0 3253.13 3430.65 23.33 o 1 4 0 4097.19 4281.20 17.54 o 2 4 0 324.90 314.16 2.74 o 3 4 0 88.15 83.87 2.14 o 4 4 0 100.79 112.02 3.38 o 1 5 0 315.99 313.35 2.49 o 2 5 0 159.11 167.48 2.32 o 3 5 0 16.21 21.18 1.90 o 4 5 0 28.64 29.96 2.89 o 0 6 0 1569.14 1574.29 18.80 o 1 6 0 1271.33 1223.31 8.50 o 2 6 0 1652.88 1633.87 12.12 o 3 6 0 460.01 461.74 6.84 o 4 6 0 5.15 5.02 3.16 o 1 7 0 7.40 8.67 1.94 o 2 7 0 54.77 49.72 3.32 o 3 7 0 1.37 0.56 2.69 o 4 7 0 5.30 12.88 4.82 o 0 8 0 96.32 91.03 4.90 o 1 8 0 173.81 179.71 4.94 o 2 8 0 22.28 23.59 2.92 o 3 8 0 54.22 62.70 4.61 o 1 9 0 225.65 251.84 8.03 o 2 9 0 0.64 -1.82 2.66 o 3 9 0 102.70 112.47 6.32 o 0 10 0 63.74 66.59 6.02 o 1 10 0 56.83 65.53 4.38 o 2 10 0 12.76 7.41 3.43 o 1 11 0 0.19 4.82 3.67 o 2 11 0 14.67 17.58 4.82 o 0 12 0 19.80 18.74 12.89 o 1 0 1 4886.93 5138.32 19.00 o 2 0 1 0.84 2.15 0.71 o 3 0 1 311.72 296.41 3.88 o 4 0 1 27.53 26.06 1.91 o -5 1 1 1.03 2.35 2.88 o -4 1 1 38.89 38.61 2.08 o -3 1 1 318.88 307.60 3.53 o -2 1 1 32.03 36.38 1.14 o -1 1 1 4279.49 4467.85 17.62 o 0 1 1 1082.52 1167.62 6.54 o 1 1 1 4334.58 4503.56 17.58 o 2 1 1 30.25 36.48 1.13 o 3 1 1 318.34 302.05 3.39 o 4 1 1 38.03 40.28 2.09 o 5 1 1 1.09 4.29 2.95 o -5 2 1 8.67 8.09 3.22 o -4 2 1 8.01 8.25 1.76 o -3 2 1 328.17 321.08 3.65 o -2 2 1 340.73 322.24 2.70 o -1 2 1 423.04 412.31 2.43 o 0 2 1 39.99 45.11 1.18 o 1 2 1 428.43 412.21 2.45 o 2 2 1 337.62 317.98 2.54 o 3 2 1 324.68 316.90 3.38 o 4 2 1 8.30 8.11 1.93 o 5 2 1 8.46 9.66 3.10 o -4 3 1 120.65 124.54 3.31 o -3 3 1 175.86 176.87 3.04 o -2 3 1 301.02 307.72 2.66 o -1 3 1 63.75 68.34 1.15 o 0 3 1 209.02 210.96 2.27 o 1 3 1 68.34 72.24 1.17 o 2 3 1 293.69 301.43 2.50 o 3 3 1 177.37 178.13 2.66 o 4 3 1 123.12 127.63 3.56 o -4 4 1 35.04 35.96 2.41 o -3 4 1 93.21 96.88 2.27 o -2 4 1 1730.75 1703.51 7.94 o -1 4 1 282.18 292.55 2.33 o 0 4 1 23.02 21.56 1.39 o 1 4 1 291.65 302.95 2.25 o 2 4 1 1742.33 1707.18 8.11 o 3 4 1 94.10 100.16 2.41 o 4 4 1 34.83 36.06 2.47 o -4 5 1 110.48 111.37 3.91 o -3 5 1 53.01 57.03 2.17 o -2 5 1 498.84 499.24 4.15 o -1 5 1 45.61 42.04 1.24 o 0 5 1 1161.27 1211.95 8.02 o 1 5 1 44.13 41.90 1.12 o 2 5 1 492.36 493.56 3.90 o 3 5 1 52.30 52.26 2.75 o 4 5 1 111.29 108.44 4.33 o -4 6 1 82.58 94.08 5.39 o -3 6 1 56.62 55.09 2.81 o -2 6 1 20.60 17.10 1.91 o -1 6 1 59.40 58.78 2.14 o 0 6 1 749.60 711.55 6.46 o 1 6 1 56.74 57.17 2.07 o 2 6 1 20.44 20.95 1.97 o 3 6 1 58.67 61.70 3.23 o 4 6 1 80.88 84.61 4.59 o -4 7 1 63.59 61.67 6.39 o -3 7 1 140.14 140.42 5.25 o -2 7 1 1447.47 1371.71 12.82 o -1 7 1 1683.27 1610.36 12.11 o 0 7 1 280.37 272.07 5.72 o 1 7 1 1678.89 1578.65 12.64 o 2 7 1 1442.06 1394.97 12.86 o 3 7 1 143.18 136.31 5.19 o 4 7 1 64.39 64.31 6.46 o -3 8 1 22.84 25.27 3.85 o -2 8 1 12.32 15.85 2.82 o -1 8 1 5.37 3.59 2.21 o 0 8 1 132.74 127.93 3.97 o 1 8 1 4.84 7.63 2.14 o 2 8 1 12.79 13.20 2.75 o 3 8 1 22.24 23.37 3.77 o -3 9 1 104.94 97.49 6.12 o -2 9 1 114.18 123.86 5.00 o -1 9 1 231.33 240.50 5.87 o 0 9 1 501.33 468.35 6.90 o 1 9 1 231.17 243.43 5.85 o 2 9 1 117.15 114.37 4.88 o 3 9 1 105.92 108.29 6.34 o -2 10 1 102.69 98.81 5.62 o -1 10 1 45.42 45.67 3.92 o 0 10 1 554.12 551.96 8.43 o 1 10 1 46.60 49.48 3.98 o 2 10 1 100.76 108.48 5.44 o -2 11 1 157.43 154.01 8.49 o -1 11 1 205.09 210.94 7.06 o 0 11 1 133.64 131.72 5.70 o 1 11 1 204.51 202.96 7.42 o 2 11 1 158.34 161.67 7.75 o 0 12 1 76.45 80.53 6.19 o 1 0 2 11087.24 11486.91 46.46 o 2 0 2 7851.60 7769.44 29.93 o 3 0 2 558.48 539.58 4.55 o 4 0 2 16.59 15.54 1.94 o 5 0 2 3.30 -0.99 2.98 o -5 1 2 1.49 0.23 2.78 o -4 1 2 58.50 57.45 2.50 o -3 1 2 63.27 63.76 1.95 o -2 1 2 694.41 713.09 4.51 o -1 1 2 58.64 61.19 1.16 o 0 1 2 1215.05 1263.23 6.87 o 1 1 2 58.40 64.05 1.01 o 2 1 2 694.35 715.73 4.28 o 3 1 2 64.86 66.43 1.96 o 4 1 2 57.73 60.26 2.70 o 5 1 2 1.60 2.01 3.08 o -5 2 2 9.65 15.83 3.23 o -4 2 2 152.80 152.35 3.56 o -3 2 2 235.87 234.49 3.12 o -2 2 2 591.14 578.72 3.79 o -1 2 2 716.61 732.43 3.83 o 0 2 2 1399.29 1382.70 7.53 o 1 2 2 711.65 724.38 3.75 o 2 2 2 581.88 572.19 3.73 o 3 2 2 235.26 225.37 3.15 o 4 2 2 156.01 153.45 3.79 o 5 2 2 9.24 7.70 3.41 o -4 3 2 201.16 202.19 4.06 o -3 3 2 530.60 529.19 4.50 o -2 3 2 370.47 354.94 2.89 o -1 3 2 1790.96 1775.72 8.27 o 0 3 2 3484.31 3576.88 17.79 o 1 3 2 1796.36 1798.71 7.78 o 2 3 2 376.15 366.65 2.96 o 3 3 2 522.22 525.13 4.71 o 4 3 2 200.63 199.12 4.48 o -4 4 2 61.34 64.34 2.87 o -3 4 2 604.31 605.24 4.95 o -2 4 2 581.44 585.13 3.91 o -1 4 2 410.78 419.28 3.11 o 0 4 2 806.89 844.75 5.94 o 1 4 2 408.23 424.97 2.88 o 2 4 2 571.13 576.15 4.05 o 3 4 2 604.97 602.63 5.05 o 4 4 2 62.43 65.94 3.04 o -4 5 2 18.85 20.55 2.59 o -3 5 2 63.43 62.00 2.12 o -2 5 2 280.94 272.40 3.01 o -1 5 2 1012.45 1078.80 8.86 o 0 5 2 179.28 192.99 2.79 o 1 5 2 1012.17 1074.02 6.04 o 2 5 2 283.17 282.73 3.24 o 3 5 2 64.65 63.23 2.38 o 4 5 2 19.12 22.50 2.75 o -4 6 2 84.88 86.87 4.56 o -3 6 2 185.33 177.94 4.26 o -2 6 2 306.38 309.50 4.56 o -1 6 2 1695.18 1637.47 10.57 o 0 6 2 1588.65 1533.80 10.89 o 1 6 2 1700.76 1651.24 11.19 o 2 6 2 299.90 309.34 4.51 o 3 6 2 186.74 184.07 4.79 o 4 6 2 84.72 87.42 4.71 o -4 7 2 8.98 17.02 5.46 o -3 7 2 333.27 335.47 7.03 o -2 7 2 25.41 25.08 2.81 o -1 7 2 663.84 635.79 7.33 o 0 7 2 32.85 28.94 2.57 o 1 7 2 660.48 628.99 7.22 o 2 7 2 26.79 25.81 2.70 o 3 7 2 333.25 338.35 7.58 o 4 7 2 8.36 4.82 4.04 o -3 8 2 15.58 20.89 3.85 o -2 8 2 27.54 29.15 3.05 o -1 8 2 48.21 54.43 3.08 o 0 8 2 0.24 -1.16 1.95 o 1 8 2 47.83 51.17 2.98 o 2 8 2 29.00 22.96 3.13 o 3 8 2 15.65 23.69 4.09 o -3 9 2 98.35 103.01 6.77 o -2 9 2 2.78 4.07 2.81 o -1 9 2 405.70 395.62 8.64 o 0 9 2 497.45 526.77 7.71 o 1 9 2 402.52 387.63 6.85 o 2 9 2 2.78 2.41 3.01 o 3 9 2 98.93 104.14 6.96 o -2 10 2 39.29 38.50 4.53 o -1 10 2 104.32 104.43 5.02 o 0 10 2 11.13 9.49 2.82 o 1 10 2 103.71 104.88 5.30 o 2 10 2 39.40 41.21 4.20 o -2 11 2 153.14 163.19 8.67 o -1 11 2 115.83 95.73 6.13 o 0 11 2 171.71 157.21 6.82 o 1 11 2 117.30 112.75 5.95 o 2 11 2 154.05 178.80 8.80 o 1 0 3 17244.39 17609.81 73.44 o 2 0 3 336.76 365.01 2.84 o 3 0 3 903.76 872.02 6.39 o 4 0 3 2.59 5.21 1.78 o 5 0 3 193.18 195.57 5.84 o -5 1 3 21.15 21.75 3.15 o -4 1 3 17.52 14.01 1.97 o -3 1 3 23.64 23.51 1.48 o -2 1 3 791.58 791.26 4.74 o -1 1 3 662.94 669.20 3.79 o 0 1 3 2193.16 2329.20 12.34 o 1 1 3 662.39 661.18 3.58 o 2 1 3 791.99 785.54 4.63 o 3 1 3 24.90 24.41 1.52 o 4 1 3 17.88 24.04 2.17 o 5 1 3 21.26 32.12 3.83 o -5 2 3 91.12 94.49 4.45 o -4 2 3 74.36 71.92 2.83 o -3 2 3 593.01 574.56 4.82 o -2 2 3 145.72 150.56 2.01 o -1 2 3 3369.01 3354.48 14.50 o 0 2 3 4026.79 4110.98 20.39 o 1 2 3 3322.24 3301.63 13.55 o 2 2 3 140.39 144.49 1.89 o 3 2 3 592.00 575.49 4.91 o 4 2 3 73.73 72.06 3.31 o 5 2 3 91.76 94.43 5.07 o -4 3 3 13.50 10.57 1.99 o -3 3 3 252.22 257.83 3.25 o -2 3 3 70.72 72.46 1.59 o -1 3 3 51.52 47.92 1.52 o 0 3 3 377.82 406.14 3.10 o 1 3 3 52.10 49.26 1.24 o 2 3 3 68.95 69.29 1.52 o 3 3 3 252.45 255.31 3.36 o 4 3 3 14.11 12.45 2.07 o -4 4 3 296.39 309.62 4.95 o -3 4 3 424.85 428.26 3.97 o -2 4 3 484.45 480.98 3.58 o -1 4 3 1727.94 1709.94 8.26 o 0 4 3 7067.94 7518.29 33.58 o 1 4 3 1714.09 1686.02 9.96 o 2 4 3 485.65 484.48 4.03 o 3 4 3 425.78 436.42 4.30 o 4 4 3 298.00 302.50 5.12 o -4 5 3 22.06 24.21 2.80 o -3 5 3 88.78 92.98 2.38 o -2 5 3 14.32 13.02 1.27 o -1 5 3 273.47 296.32 2.74 o 0 5 3 24.27 31.07 1.32 o 1 5 3 276.82 299.51 2.75 o 2 5 3 13.66 13.52 1.27 o 3 5 3 91.55 92.40 2.73 o 4 5 3 21.94 19.42 2.89 o -4 6 3 95.96 106.74 7.86 o -3 6 3 177.82 178.22 4.11 o -2 6 3 828.11 808.01 7.00 o -1 6 3 191.41 179.54 3.21 o 0 6 3 1387.25 1324.02 10.29 o 1 6 3 195.34 186.72 4.13 o 2 6 3 821.35 808.14 7.73 o 3 6 3 176.00 177.89 4.74 o 4 6 3 96.62 101.85 5.97 o -4 7 3 33.91 44.61 7.11 o -3 7 3 71.35 76.10 4.56 o -2 7 3 378.83 370.68 6.41 o -1 7 3 54.42 75.39 6.22 o 0 7 3 3126.00 2916.41 19.62 o 1 7 3 54.40 61.36 3.08 o 2 7 3 378.84 373.26 8.22 o 3 7 3 72.50 72.32 4.52 o 4 7 3 35.21 37.57 5.81 o -3 8 3 2.55 2.87 3.59 o -2 8 3 220.61 223.94 5.62 o -1 8 3 87.07 90.24 3.58 o 0 8 3 72.77 75.49 3.28 o 1 8 3 89.05 93.34 3.60 o 2 8 3 221.24 228.30 6.11 o 3 8 3 2.39 1.25 3.45 o -3 9 3 8.86 15.81 4.53 o -2 9 3 85.27 77.08 4.54 o -1 9 3 49.46 50.80 3.45 o 0 9 3 127.66 121.14 5.42 o 1 9 3 49.86 43.14 3.17 o 2 9 3 85.97 83.67 4.66 o 3 9 3 8.76 11.75 4.58 o -2 10 3 195.90 176.50 7.06 o -1 10 3 312.68 307.01 7.19 o 0 10 3 3.00 4.03 2.81 o 1 10 3 311.44 301.33 7.71 o 2 10 3 195.50 204.07 6.86 o -1 11 3 45.56 51.01 5.21 o 0 11 3 59.13 60.16 4.52 o 1 11 3 45.63 52.10 4.82 o 0 0 4 5753.30 6260.28 52.03 o 1 0 4 12525.30 12784.69 51.79 o 2 0 4 108.07 106.98 2.88 o 3 0 4 454.37 435.30 4.38 o 4 0 4 7.02 6.32 1.84 o 5 0 4 16.39 23.04 3.16 o -5 1 4 41.30 38.82 3.53 o -4 1 4 86.23 85.86 2.97 o -3 1 4 169.81 168.74 2.86 o -2 1 4 66.73 71.92 1.60 o -1 1 4 293.77 300.76 2.55 o 0 1 4 2426.96 2594.93 14.43 o 1 1 4 306.82 308.08 2.34 o 2 1 4 68.21 73.73 1.57 o 3 1 4 166.83 162.83 2.84 o 4 1 4 86.05 80.10 2.98 o 5 1 4 40.90 36.03 3.41 o -4 2 4 37.85 41.28 2.42 o -3 2 4 24.37 28.07 1.61 o -2 2 4 1027.20 1014.69 5.93 o -1 2 4 367.63 379.78 2.92 o 0 2 4 1.20 2.79 0.69 o 1 2 4 365.00 381.18 2.55 o 2 2 4 1015.08 1011.03 5.41 o 3 2 4 25.82 28.16 1.84 o 4 2 4 37.67 36.86 2.40 o -4 3 4 76.02 76.62 2.97 o -3 3 4 54.67 50.34 1.94 o -2 3 4 2244.22 2189.81 10.75 o -1 3 4 306.81 327.27 2.60 o 0 3 4 3129.31 3293.14 15.94 o 1 3 4 295.83 319.97 2.32 o 2 3 4 2234.66 2181.35 9.95 o 3 3 4 53.93 51.71 1.98 o 4 3 4 75.58 72.32 2.84 o -4 4 4 111.43 108.74 3.55 o -3 4 4 33.23 37.39 1.79 o -2 4 4 129.34 126.23 2.89 o -1 4 4 897.80 949.30 5.34 o 0 4 4 351.92 346.87 3.01 o 1 4 4 889.18 934.82 5.23 o 2 4 4 128.67 125.39 2.59 o 3 4 4 34.66 33.55 1.82 o 4 4 4 113.23 110.12 3.49 o -4 5 4 0.44 0.02 2.22 o -3 5 4 593.77 580.64 5.09 o -2 5 4 6.36 6.19 1.13 o -1 5 4 866.98 873.31 5.25 o 0 5 4 554.56 511.34 4.15 o 1 5 4 857.77 872.32 5.79 o 2 5 4 7.01 9.42 1.24 o 3 5 4 594.28 592.56 5.50 o 4 5 4 0.53 -1.51 2.86 o -4 6 4 13.39 18.42 3.59 o -3 6 4 367.07 366.84 5.04 o -2 6 4 5.93 6.56 1.60 o -1 6 4 1363.95 1309.56 9.05 o 0 6 4 5.63 8.59 1.45 o 1 6 4 1349.44 1321.18 10.04 o 2 6 4 6.08 2.69 1.54 o 3 6 4 363.66 370.66 7.85 o 4 6 4 13.43 22.13 3.98 o -4 7 4 24.64 23.35 5.56 o -3 7 4 332.30 335.66 6.64 o -2 7 4 62.91 64.70 5.82 o -1 7 4 1281.03 1196.07 10.07 o 0 7 4 0.10 2.06 1.91 o 1 7 4 1271.83 1197.26 10.57 o 2 7 4 62.69 64.31 3.44 o 3 7 4 331.25 339.20 7.62 o 4 7 4 25.42 34.16 5.71 o -3 8 4 18.18 19.74 3.73 o -2 8 4 73.45 76.13 4.28 o -1 8 4 95.45 94.35 3.65 o 0 8 4 3.64 0.48 2.11 o 1 8 4 94.95 95.31 3.66 o 2 8 4 74.01 77.95 4.20 o 3 8 4 18.95 11.85 6.34 o -3 9 4 78.95 82.39 5.82 o -2 9 4 516.57 524.25 9.05 o -1 9 4 287.92 282.84 6.12 o 0 9 4 0.98 6.19 2.54 o 1 9 4 292.20 289.85 5.74 o 2 9 4 514.65 523.25 13.99 o 3 9 4 78.63 90.59 10.04 o -2 10 4 2.32 0.11 3.48 o -1 10 4 0.72 -1.70 3.27 o 0 10 4 112.56 115.86 4.81 o 1 10 4 0.76 1.22 3.13 o 2 10 4 2.27 -0.57 3.58 o -1 11 4 231.42 230.54 8.67 o 0 11 4 266.38 279.22 10.93 o 1 11 4 232.98 237.78 12.45 o 1 0 5 3294.58 3371.34 14.23 o 2 0 5 164.89 162.84 2.13 o 3 0 5 1651.89 1605.74 10.94 o 4 0 5 60.97 72.80 2.94 o 5 0 5 24.38 31.72 3.33 o -5 1 5 17.61 13.91 5.96 o -4 1 5 27.78 30.08 2.21 o -3 1 5 9.34 8.66 1.45 o -2 1 5 873.22 890.63 5.39 o -1 1 5 362.52 392.15 2.71 o 0 1 5 1604.09 1679.77 10.50 o 1 1 5 361.17 389.73 2.64 o 2 1 5 890.52 897.69 5.18 o 3 1 5 10.02 9.87 1.47 o 4 1 5 28.07 35.03 2.33 o 5 1 5 18.09 15.36 4.25 o -4 2 5 50.86 56.26 2.64 o -3 2 5 419.79 416.09 4.28 o -2 2 5 621.51 601.45 4.41 o -1 2 5 1935.15 2013.03 9.81 o 0 2 5 57.81 70.50 1.58 o 1 2 5 1929.32 1991.72 9.65 o 2 2 5 616.94 591.69 4.15 o 3 2 5 422.10 413.67 4.36 o 4 2 5 50.40 55.51 2.93 o -4 3 5 4.51 5.64 1.91 o -3 3 5 71.94 73.35 2.22 o -2 3 5 222.60 234.07 2.85 o -1 3 5 590.94 621.88 4.37 o 0 3 5 5.57 4.69 0.85 o 1 3 5 581.30 615.86 3.86 o 2 3 5 221.05 233.22 2.41 o 3 3 5 72.43 77.07 2.37 o 4 3 5 4.85 4.36 1.86 o -4 4 5 143.30 143.23 3.82 o -3 4 5 316.69 305.83 3.89 o -2 4 5 484.07 474.40 4.20 o -1 4 5 1959.28 1970.03 10.33 o 0 4 5 587.91 542.42 4.04 o 1 4 5 1967.03 1982.69 9.65 o 2 4 5 487.61 475.51 3.79 o 3 4 5 317.26 306.29 3.91 o 4 4 5 143.00 153.67 4.16 o -4 5 5 80.27 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