#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232215.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232215_Fobs loop_ _publ_author_name 'Jiang, Guo-Qing' 'Li, Jian-Hua' 'Wang, Miao' 'Shi, Yu-Jun' _publ_section_title ; Hexa-\m~2~-acetato-\k^12^O:O'-(azido-\kN)bis(methanol-\kO)-\m~3~-oxido-trichromium(III) methanol monosolvate ; _journal_coeditor_code DS2137 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1483 _journal_volume 67 _journal_year 2011 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 130.484 _cell_angle_gamma 90.000 _cell_length_a 21.1647 _cell_length_b 10.6094 _cell_length_c 15.6407 _exptl_crystal_F_000 1364.00 _reflns_d_resolution_high 0.8144 _[local]_cod_data_source_file ds2137Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' y in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 491.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 22 2 -18 303.18 305.45 48.82 o 21 1 -17 38.41 192.79 141.46 o 23 1 -17 4.77 237.85 153.98 o 20 2 -17 1028.28 858.77 192.79 o 22 2 -17 567.68 1269.38 249.12 o 19 3 -17 143.45 388.08 284.17 o 21 3 -17 183.09 260.39 92.64 o 18 4 -17 9.57 76.36 304.20 o 20 4 -17 138.33 147.72 17.53 o 19 5 -17 91.07 73.86 256.63 o 20 0 -16 255.87 448.17 366.79 o 22 0 -16 71.54 71.36 33.80 o 19 1 -16 957.46 922.62 58.84 o 21 1 -16 161.42 281.67 331.74 o 23 1 -16 363.97 471.95 204.05 o 18 2 -16 96.68 133.95 192.79 o 20 2 -16 56.03 161.49 365.54 o 22 2 -16 168.02 244.11 163.99 o 17 3 -16 95.87 76.36 7.51 o 19 3 -16 367.93 389.33 257.88 o 21 3 -16 92.96 155.23 329.24 o 23 3 -16 118.10 294.19 107.66 o 18 4 -16 525.47 502.00 201.55 o 20 4 -16 103.79 123.93 117.67 o 22 4 -16 34.48 194.04 98.90 o 17 5 -16 1.39 27.54 180.27 o 19 5 -16 997.08 1554.81 336.75 o 21 5 -16 628.85 574.60 27.54 o 16 6 -16 44.29 78.87 364.29 o 18 6 -16 178.74 292.93 80.12 o 20 6 -16 295.28 552.07 360.54 o 17 1 -15 95.13 346.76 363.04 o 19 1 -15 249.33 192.59 58.53 o 21 1 -15 610.22 617.17 186.53 o 23 1 -15 114.59 132.70 25.04 o 16 2 -15 1125.47 1775.13 274.16 o 18 2 -15 603.54 623.43 96.39 o 20 2 -15 684.24 809.95 272.91 o 22 2 -15 528.65 1387.06 306.71 o 15 3 -15 181.10 364.29 174.01 o 17 3 -15 386.34 436.90 152.73 o 19 3 -15 282.29 525.78 254.13 o 21 3 -15 37.82 98.90 237.85 o 23 3 -15 120.35 167.75 371.80 o 16 4 -15 304.90 459.43 275.41 o 18 4 -15 483.77 1079.10 259.13 o 20 4 -15 241.49 271.65 47.57 o 22 4 -15 85.16 433.14 345.51 o 15 5 -15 1746.97 1728.82 92.64 o 17 5 -15 891.08 993.98 199.05 o 19 5 -15 874.12 860.03 51.33 o 21 5 -15 105.63 161.49 53.83 o 16 6 -15 4.22 71.36 137.70 o 18 6 -15 43.82 72.61 58.84 o 20 6 -15 33.85 115.17 40.06 o 15 7 -15 336.06 239.10 182.77 o 17 7 -15 2.57 23.79 260.39 o 19 7 -15 0.55 66.35 225.33 o 16 0 -14 81.21 80.12 13.77 o 18 0 -14 675.30 1480.95 300.45 o 20 0 -14 1617.97 1538.53 191.53 o 22 0 -14 378.72 415.62 290.43 o 15 1 -14 455.78 659.73 336.75 o 17 1 -14 597.15 532.80 108.71 o 19 1 -14 997.68 806.57 228.14 o 21 1 -14 2100.49 1737.58 25.04 o 23 1 -14 671.44 1224.32 255.38 o 14 2 -14 2848.94 2726.55 205.30 o 16 2 -14 376.86 353.02 77.62 o 18 2 -14 198.92 391.83 161.49 o 20 2 -14 306.12 368.05 107.66 o 22 2 -14 195.09 225.33 360.54 o 15 3 -14 83.77 90.13 28.79 o 17 3 -14 771.81 713.56 18.78 o 19 3 -14 580.13 679.76 343.01 o 21 3 -14 310.51 508.25 373.05 o 23 3 -14 420.77 604.65 316.72 o 14 4 -14 1176.38 1641.19 227.84 o 16 4 -14 721.01 831.23 191.53 o 18 4 -14 175.88 295.44 117.67 o 20 4 -14 366.77 481.97 321.73 o 22 4 -14 702.06 1142.95 141.46 o 13 5 -14 49.50 182.77 83.87 o 15 5 -14 153.00 464.44 321.73 o 17 5 -14 679.99 947.66 122.68 o 19 5 -14 250.49 282.92 264.14 o 21 5 -14 88.14 96.39 120.18 o 14 6 -14 991.68 1781.39 349.27 o 16 6 -14 1306.65 1077.85 296.69 o 18 6 -14 997.49 1362.02 177.76 o 20 6 -14 110.80 220.33 117.67 o 22 6 -14 22.42 192.79 152.73 o 13 7 -14 219.35 418.12 167.75 o 15 7 -14 56.23 309.21 255.38 o 17 7 -14 95.39 265.39 116.42 o 19 7 -14 240.70 296.69 291.68 o 14 8 -14 473.05 789.92 85.13 o 16 8 -14 234.14 401.85 304.20 o 18 8 -14 364.65 552.07 325.48 o 13 1 -13 164.71 200.30 224.08 o 15 1 -13 131.16 177.16 149.60 o 17 1 -13 1175.26 1211.80 264.14 o 19 1 -13 682.90 737.60 141.40 o 21 1 -13 214.68 425.92 131.55 o 23 1 -13 7.07 70.10 226.59 o 14 2 -13 371.71 466.94 110.16 o 16 2 -13 787.46 833.48 119.98 o 18 2 -13 3439.05 3382.52 327.99 o 20 2 -13 2324.22 1960.41 197.79 o 22 2 -13 1083.81 1209.29 112.67 o 13 3 -13 1126.45 928.88 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1043.05 1892.81 360.54 o 15 9 -13 249.51 334.25 91.39 o 14 0 -12 3045.49 2546.28 12.52 o 16 0 -12 2402.86 2585.09 145.22 o 18 0 -12 18.69 329.24 239.10 o 20 0 -12 216.54 363.04 311.71 o 22 0 -12 63.26 135.20 241.61 o 13 1 -12 1848.35 1876.54 205.30 o 15 1 -12 2377.86 2257.62 220.05 o 17 1 -12 1144.60 1019.69 157.73 o 19 1 -12 674.57 1105.51 199.67 o 21 1 -12 632.27 547.36 223.46 o 23 1 -12 751.01 552.07 52.58 o 12 2 -12 925.43 828.73 132.70 o 14 2 -12 159.96 180.27 210.31 o 16 2 -12 193.30 382.38 207.88 o 18 2 -12 321.94 256.63 259.13 o 20 2 -12 338.21 436.90 373.05 o 22 2 -12 392.49 423.13 110.16 o 11 3 -12 85.77 92.64 185.27 o 13 3 -12 206.70 212.82 11.27 o 15 3 -12 1572.73 1513.50 249.12 o 17 3 -12 416.66 236.60 85.13 o 19 3 -12 618.09 644.71 126.44 o 21 3 -12 742.46 1429.62 296.69 o 23 3 -12 386.99 500.74 16.27 o 12 4 -12 1123.25 933.89 190.28 o 14 4 -12 644.27 558.33 344.26 o 16 4 -12 18.12 95.14 297.94 o 18 4 -12 1156.64 930.13 210.31 o 20 4 -12 354.02 450.67 370.55 o 22 4 -12 72.51 169.00 111.42 o 11 5 -12 1450.89 1788.91 235.35 o 13 5 -12 484.38 527.03 163.99 o 15 5 -12 265.16 426.88 160.24 o 17 5 -12 410.98 475.71 96.39 o 19 5 -12 571.99 481.97 1.25 o 21 5 -12 67.30 210.31 245.36 o 10 6 -12 1517.06 2135.67 280.42 o 12 6 -12 178.51 311.71 131.45 o 14 6 -12 175.95 304.20 338.00 o 16 6 -12 118.75 305.45 138.96 o 18 6 -12 404.44 395.59 309.21 o 20 6 -12 1062.28 1238.09 112.67 o 22 6 -12 534.83 727.33 51.33 o 11 7 -12 38.28 80.12 30.04 o 13 7 -12 726.65 652.22 42.56 o 15 7 -12 57.38 36.30 136.45 o 17 7 -12 91.96 81.37 133.95 o 19 7 -12 122.87 108.91 21.28 o 21 7 -12 203.94 464.44 319.22 o 12 8 -12 2789.64 3079.57 359.28 o 14 8 -12 1221.62 1020.26 35.05 o 16 8 -12 1358.56 1648.70 170.25 o 18 8 -12 1851.81 1263.12 12.52 o 20 8 -12 669.67 838.74 296.69 o 11 9 -12 579.14 503.25 142.71 o 13 9 -12 733.90 992.72 176.51 o 15 9 -12 519.45 445.66 301.70 o 17 9 -12 420.91 518.27 175.26 o 12 10 -12 0.96 12.52 301.70 o 11 1 -11 549.12 627.18 108.91 o 13 1 -11 1173.13 1259.76 187.78 o 15 1 -11 133.72 222.74 97.02 o 17 1 -11 1248.76 1534.87 298.57 o 19 1 -11 386.44 446.29 237.23 o 21 1 -11 138.29 220.21 110.48 o 23 1 -11 1164.23 1586.10 374.31 o 10 2 -11 3161.34 3420.08 246.62 o 12 2 -11 4527.55 4372.74 68.85 o 14 2 -11 5095.85 4387.07 131.55 o 16 2 -11 3543.40 3407.31 207.95 o 18 2 -11 917.91 996.58 254.75 o 20 2 -11 285.32 379.31 363.04 o 22 2 -11 43.42 83.87 133.95 o 11 3 -11 1558.07 2056.80 205.30 o 13 3 -11 33.59 108.91 327.99 o 15 3 -11 229.31 291.68 201.55 o 17 3 -11 407.74 547.06 345.51 o 19 3 -11 966.46 1374.54 350.52 o 21 3 -11 504.23 528.28 118.93 o 23 3 -11 408.96 332.99 1.25 o 10 4 -11 184.63 272.91 343.01 o 12 4 -11 271.06 481.97 206.56 o 14 4 -11 1506.30 1195.52 12.52 o 16 4 -11 1625.99 1872.78 310.46 o 18 4 -11 1069.36 1557.31 180.27 o 20 4 -11 1066.59 1336.98 120.18 o 22 4 -11 814.38 1035.29 316.72 o 9 5 -11 1424.40 1607.39 120.18 o 11 5 -11 2006.92 1950.39 130.19 o 13 5 -11 464.75 603.40 177.76 o 15 5 -11 153.46 336.75 196.54 o 17 5 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1038.70 1055.32 75.11 o 14 0 -10 4868.80 4953.60 236.60 o 16 0 -10 1692.05 1374.54 28.79 o 18 0 -10 2118.83 2023.00 61.34 o 20 0 -10 2075.95 2219.54 299.19 o 22 0 -10 685.19 1220.56 257.88 o 9 1 -10 7448.48 6904.00 310.46 o 11 1 -10 10018.49 8766.37 52.58 o 13 1 -10 5404.06 5026.34 114.42 o 15 1 -10 480.41 683.67 192.46 o 17 1 -10 279.92 237.39 55.71 o 19 1 -10 1453.04 1517.29 23.68 o 21 1 -10 812.54 879.63 82.00 o 23 1 -10 1102.72 970.19 71.36 o 10 2 -10 4903.68 4933.57 161.49 o 12 2 -10 4859.35 4375.12 155.59 o 14 2 -10 2633.54 2290.12 125.78 o 16 2 -10 2661.18 2606.11 78.91 o 18 2 -10 299.54 499.61 178.55 o 20 2 -10 527.76 481.97 374.31 o 22 2 -10 456.48 652.22 226.59 o 9 3 -10 6703.05 5893.75 57.59 o 11 3 -10 7514.77 7091.78 275.41 o 13 3 -10 7061.68 5861.61 144.59 o 15 3 -10 2699.69 2312.18 36.30 o 17 3 -10 261.15 548.31 292.93 o 19 3 -10 188.42 212.82 67.60 o 21 3 -10 42.28 189.03 209.06 o 23 3 -10 286.29 388.08 132.70 o 8 4 -10 1901.80 2079.34 287.93 o 10 4 -10 1395.33 1751.35 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230.34 o 14 8 -10 1119.29 1244.35 215.32 o 16 8 -10 329.14 356.78 191.53 o 18 8 -10 57.53 48.82 31.30 o 20 8 -10 116.80 102.65 91.39 o 9 9 -10 759.64 668.49 329.24 o 11 9 -10 68.13 204.05 97.64 o 13 9 -10 41.80 152.73 345.51 o 15 9 -10 69.14 219.08 306.71 o 17 9 -10 700.60 850.01 45.07 o 10 10 -10 500.35 474.45 95.14 o 12 10 -10 511.64 659.73 353.02 o 14 10 -10 70.26 73.86 32.55 o 16 10 -10 2.16 6.26 2.50 o 11 11 -10 154.74 307.96 133.95 o 9 1 -9 499.15 449.42 87.63 o 11 1 -9 710.06 730.19 204.61 o 13 1 -9 4739.68 5105.82 228.59 o 15 1 -9 3315.17 2978.38 56.48 o 17 1 -9 1947.08 1736.41 488.22 o 19 1 -9 804.94 930.20 165.87 o 21 1 -9 728.48 726.70 153.85 o 23 1 -9 186.50 229.09 363.04 o 8 2 -9 14806.14 16123.93 338.00 o 10 2 -9 17054.80 16075.11 97.64 o 12 2 -9 2151.63 2810.66 177.26 o 14 2 -9 1121.04 1101.34 28.27 o 16 2 -9 454.18 492.57 198.61 o 18 2 -9 1679.32 2044.11 207.18 o 20 2 -9 1600.02 1266.88 40.06 o 22 2 -9 462.53 491.98 190.28 o 7 3 -9 528.60 632.19 148.97 o 9 3 -9 4120.12 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4 -8 12955.94 12695.09 133.95 o 14 4 -8 2945.51 2691.49 284.17 o 16 4 -8 476.05 684.77 364.29 o 18 4 -8 44.75 106.41 180.27 o 20 4 -8 172.25 329.24 242.86 o 22 4 -8 501.46 587.12 161.49 o 9 5 -8 2945.64 3213.48 276.66 o 11 5 -8 3818.42 3655.43 73.86 o 13 5 -8 2297.37 2199.51 77.62 o 15 5 -8 700.58 692.28 126.44 o 17 5 -8 202.17 384.32 370.55 o 19 5 -8 86.41 102.65 309.21 o 21 5 -8 167.05 460.68 305.45 o 6 6 -8 7034.24 6458.33 133.95 o 8 6 -8 3861.28 3692.34 121.43 o 10 6 -8 2990.59 3395.04 305.45 o 12 6 -8 704.05 567.09 42.56 o 14 6 -8 354.22 504.50 219.08 o 16 6 -8 140.40 295.44 126.44 o 18 6 -8 293.07 459.43 266.65 o 20 6 -8 165.63 301.70 307.96 o 22 6 -8 874.80 822.47 199.05 o 7 7 -8 990.24 993.69 232.93 o 9 7 -8 168.88 153.98 247.87 o 11 7 -8 171.07 230.34 234.10 o 13 7 -8 798.93 723.57 25.04 o 15 7 -8 559.19 701.04 206.56 o 17 7 -8 847.22 642.20 3.76 o 19 7 -8 421.22 662.23 321.73 o 21 7 -8 465.83 495.74 161.49 o 6 8 -8 3861.22 3247.62 123.31 o 8 8 -8 255.56 381.82 158.99 o 10 8 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2600.10 25.26 o 16 2 -7 2801.67 2734.79 170.25 o 18 2 -7 578.30 540.80 148.27 o 20 2 -7 356.46 383.07 68.85 o 22 2 -7 295.16 424.38 88.88 o 5 3 -7 3427.32 3322.43 127.69 o 7 3 -7 5949.12 5511.93 151.47 o 9 3 -7 5073.39 5316.64 226.59 o 11 3 -7 12687.67 11815.04 123.93 o 13 3 -7 3427.58 3704.25 132.70 o 15 3 -7 1802.33 1818.79 137.70 o 17 3 -7 382.24 380.56 80.12 o 19 3 -7 2104.61 1975.43 60.09 o 21 3 -7 365.75 418.12 81.37 o 6 4 -7 6572.08 6952.82 336.75 o 8 4 -7 12377.03 11122.13 51.34 o 10 4 -7 4793.43 4334.11 78.24 o 12 4 -7 493.97 673.50 182.77 o 14 4 -7 3138.89 3021.99 194.04 o 16 4 -7 1749.32 1651.20 48.82 o 18 4 -7 1487.05 1815.19 186.53 o 20 4 -7 2156.07 2202.02 116.42 o 22 4 -7 1503.42 1975.43 249.12 o 5 5 -7 5292.62 5530.71 265.39 o 7 5 -7 5612.47 5226.98 70.10 o 9 5 -7 5606.67 5522.48 133.27 o 11 5 -7 1998.36 2337.22 132.70 o 13 5 -7 15.54 73.86 117.67 o 15 5 -7 136.12 285.42 143.96 o 17 5 -7 599.37 610.91 35.05 o 19 5 -7 338.67 302.95 286.68 o 21 5 -7 1470.12 2254.60 360.54 o 6 6 -7 1118.78 1083.97 17.39 o 8 6 -7 1110.94 1192.02 84.17 o 10 6 -7 1163.50 1435.29 294.19 o 12 6 -7 5626.93 4812.14 16.27 o 14 6 -7 1878.25 1932.87 78.87 o 16 6 -7 1000.89 1404.58 128.94 o 18 6 -7 459.00 624.68 202.80 o 20 6 -7 779.25 1698.77 343.01 o 22 6 -7 1196.36 1936.62 370.55 o 5 7 -7 793.12 815.69 194.73 o 7 7 -7 547.69 571.00 87.83 o 9 7 -7 73.72 123.27 123.84 o 11 7 -7 5.53 98.90 259.13 o 13 7 -7 569.99 518.27 266.65 o 15 7 -7 1960.05 2275.88 158.99 o 17 7 -7 1966.01 1857.76 26.29 o 19 7 -7 764.81 1806.43 358.03 o 21 7 -7 84.62 266.65 246.62 o 4 8 -7 1124.35 1611.14 275.41 o 6 8 -7 1089.11 1000.23 339.25 o 8 8 -7 291.78 358.77 94.42 o 10 8 -7 82.39 148.97 254.13 o 12 8 -7 515.82 510.76 366.79 o 14 8 -7 1818.33 1791.41 41.31 o 16 8 -7 721.33 624.68 96.39 o 18 8 -7 314.09 364.29 133.95 o 5 9 -7 1093.59 1054.83 240.36 o 7 9 -7 349.45 427.51 169.51 o 9 9 -7 1011.00 1842.73 374.31 o 11 9 -7 1845.06 2012.99 142.71 o 13 9 -7 74.24 225.33 241.61 o 15 9 -7 120.22 165.25 343.01 o 17 9 -7 96.25 296.69 281.67 o 4 10 -7 492.14 475.71 169.00 o 6 10 -7 2356.13 2315.94 172.76 o 8 10 -7 1219.94 1732.57 260.39 o 10 10 -7 1784.63 1564.82 23.79 o 12 10 -7 1684.59 2040.53 179.02 o 14 10 -7 1334.03 1141.69 16.27 o 16 10 -7 539.59 525.78 210.31 o 5 11 -7 242.62 222.83 40.06 o 13 11 -7 439.54 797.43 358.03 o 4 12 -7 211.59 286.68 76.36 o 6 0 -6 20055.30 22594.79 261.64 o 8 0 -6 20227.16 19380.01 329.24 o 10 0 -6 17051.38 14902.12 63.84 o 12 0 -6 5317.51 4956.11 286.68 o 14 0 -6 596.92 598.79 116.56 o 16 0 -6 1738.42 1902.82 316.72 o 18 0 -6 1054.58 1330.72 121.43 o 20 0 -6 1308.08 2180.74 366.79 o 22 0 -6 1811.48 1927.86 185.27 o 5 1 -6 5950.24 6151.63 314.22 o 7 1 -6 4652.78 4917.28 210.31 o 9 1 -6 6885.04 7138.15 192.16 o 11 1 -6 3113.92 3672.19 172.13 o 13 1 -6 1547.96 1620.39 89.88 o 15 1 -6 1140.66 1123.20 29.79 o 17 1 -6 1468.02 1466.33 80.12 o 19 1 -6 118.79 120.65 50.07 o 21 1 -6 133.23 96.14 78.24 o 23 1 -6 157.49 206.56 182.77 o 4 2 -6 5535.97 6308.11 368.05 o 6 2 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590.73 51.92 o 13 5 -6 1614.96 2361.00 301.70 o 15 5 -6 1405.79 1526.01 151.47 o 17 5 -6 255.89 349.27 331.74 o 19 5 -6 262.27 388.08 284.17 o 21 5 -6 360.24 299.19 146.47 o 4 6 -6 3430.28 3337.70 122.46 o 6 6 -6 1246.92 1633.34 126.44 o 8 6 -6 67.69 103.90 230.15 o 10 6 -6 118.85 219.94 120.00 o 12 6 -6 2245.77 2078.70 120.80 o 14 6 -6 79.89 230.34 244.11 o 16 6 -6 1492.99 2096.86 241.61 o 18 6 -6 1041.35 1608.64 274.16 o 20 6 -6 1393.44 2010.48 269.15 o 3 7 -6 858.85 779.91 53.83 o 5 7 -6 254.15 373.76 86.57 o 7 7 -6 1898.94 2212.71 151.22 o 9 7 -6 2000.59 2605.35 256.54 o 11 7 -6 1712.53 2016.88 152.66 o 13 7 -6 910.82 1462.17 222.83 o 15 7 -6 2453.33 2367.26 160.24 o 17 7 -6 2364.24 2662.70 241.61 o 19 7 -6 1339.10 1294.42 165.25 o 2 8 -6 953.65 1046.55 150.22 o 4 8 -6 1675.00 1898.79 190.67 o 6 8 -6 1203.40 1852.21 217.95 o 8 8 -6 1137.28 928.70 50.70 o 10 8 -6 1643.00 2217.04 358.03 o 12 8 -6 1039.45 1279.40 191.53 o 14 8 -6 991.97 1502.23 133.95 o 16 8 -6 475.58 538.30 102.65 o 18 8 -6 71.99 140.21 100.15 o 3 9 -6 4862.38 4649.40 47.57 o 5 9 -6 4355.17 3668.22 170.25 o 7 9 -6 1425.41 1586.47 144.39 o 9 9 -6 440.98 323.91 104.53 o 11 9 -6 970.13 838.74 132.70 o 13 9 -6 427.02 455.68 70.10 o 15 9 -6 228.29 231.59 55.08 o 17 9 -6 83.31 76.36 97.64 o 2 10 -6 441.80 473.20 58.84 o 4 10 -6 398.88 369.30 47.57 o 6 10 -6 614.08 588.37 259.13 o 8 10 -6 1774.23 1820.06 58.40 o 10 10 -6 1395.09 1363.27 25.04 o 12 10 -6 516.83 572.10 224.08 o 14 10 -6 543.37 459.43 71.36 o 16 10 -6 1.25 67.92 206.84 o 3 11 -6 321.47 386.82 251.62 o 5 11 -6 374.94 538.30 170.25 o 7 11 -6 410.67 376.81 68.85 o 9 11 -6 304.35 440.65 255.38 o 11 11 -6 186.47 242.86 56.33 o 13 11 -6 22.31 76.84 127.11 o 2 12 -6 51.69 73.86 5.01 o 4 12 -6 192.85 349.27 147.72 o 6 12 -6 212.54 214.07 10.01 o 5 1 -5 15436.26 16105.66 813.08 o 7 1 -5 19263.62 22126.29 231.84 o 9 1 -5 15849.39 16962.60 1011.50 o 11 1 -5 3178.97 3543.12 170.17 o 13 1 -5 599.47 755.43 74.79 o 15 1 -5 3380.60 3382.35 120.56 o 17 1 -5 1973.93 1965.25 105.94 o 19 1 -5 940.73 1836.48 366.79 o 21 1 -5 937.16 1076.66 127.24 o 23 1 -5 716.31 731.08 261.64 o 4 2 -5 7855.87 7390.97 5.01 o 6 2 -5 4839.40 4743.86 118.93 o 8 2 -5 5190.97 5135.31 200.97 o 10 2 -5 3891.56 3806.81 130.44 o 12 2 -5 1555.59 1784.13 148.66 o 14 2 -5 807.61 799.72 50.68 o 16 2 -5 1195.15 962.18 84.22 o 18 2 -5 845.91 824.97 135.20 o 20 2 -5 91.53 205.30 110.16 o 22 2 -5 245.80 517.02 292.93 o 3 3 -5 17272.57 17269.38 148.97 o 5 3 -5 2377.94 2080.63 207.18 o 7 3 -5 18269.95 17456.96 362.41 o 9 3 -5 17450.48 17024.56 681.18 o 11 3 -5 2640.90 2642.37 134.03 o 13 3 -5 2825.24 2801.42 105.78 o 15 3 -5 1880.64 2285.88 115.67 o 17 3 -5 1697.05 1896.56 110.16 o 19 3 -5 185.43 251.62 48.82 o 21 3 -5 471.47 724.83 353.02 o 4 4 -5 17581.71 17780.30 128.32 o 6 4 -5 4668.19 4635.00 117.05 o 8 4 -5 14454.29 14293.74 519.52 o 10 4 -5 8970.18 8277.41 61.97 o 12 4 -5 5852.96 5384.01 79.04 o 14 4 -5 2835.15 2465.54 100.77 o 16 4 -5 598.89 582.11 105.16 o 18 4 -5 480.42 706.05 351.77 o 20 4 -5 85.95 404.35 369.30 o 22 4 -5 106.04 287.18 109.41 o 3 5 -5 774.34 671.87 96.83 o 5 5 -5 241.95 317.86 53.83 o 7 5 -5 2376.72 2505.48 43.81 o 9 5 -5 3609.48 3642.83 118.30 o 11 5 -5 3865.31 3978.17 170.54 o 13 5 -5 91.95 171.36 31.09 o 15 5 -5 1373.92 1510.99 194.04 o 17 5 -5 477.22 610.91 309.21 o 19 5 -5 505.08 702.29 246.62 o 21 5 -5 90.87 138.79 71.72 o 2 6 -5 11664.79 10972.54 264.14 o 4 6 -5 9361.08 8767.92 155.23 o 6 6 -5 3676.37 3520.00 206.03 o 8 6 -5 4534.27 4302.09 39.51 o 10 6 -5 4543.92 4909.64 222.21 o 12 6 -5 2061.56 2071.52 223.46 o 14 6 -5 1844.38 1979.19 137.70 o 16 6 -5 825.40 1010.25 142.71 o 18 6 -5 1541.76 1236.84 262.89 o 20 6 -5 1174.20 1117.53 162.12 o 1 7 -5 745.18 817.46 221.58 o 3 7 -5 2909.13 3387.54 153.77 o 5 7 -5 810.31 801.20 104.56 o 7 7 -5 1825.07 1845.65 246.62 o 9 7 -5 982.04 838.23 45.07 o 11 7 -5 309.33 208.42 104.20 o 13 7 -5 2010.21 1778.60 306.71 o 15 7 -5 2326.38 2519.99 327.99 o 17 7 -5 729.79 851.26 107.66 o 19 7 -5 71.88 128.26 193.28 o 2 8 -5 2363.44 2923.09 242.86 o 4 8 -5 1665.23 1883.60 88.88 o 6 8 -5 1202.23 1010.26 85.13 o 8 8 -5 375.91 627.18 277.91 o 10 8 -5 133.56 145.34 16.27 o 12 8 -5 1410.19 1888.75 146.39 o 14 8 -5 1512.92 1688.76 52.58 o 16 8 -5 595.15 517.02 12.52 o 18 8 -5 142.81 207.20 194.50 o 1 9 -5 418.70 599.64 214.07 o 3 9 -5 197.70 327.99 165.25 o 5 9 -5 493.02 556.51 81.39 o 7 9 -5 1572.68 1586.61 176.05 o 9 9 -5 1420.34 2077.12 148.24 o 11 9 -5 383.73 418.34 72.61 o 13 9 -5 994.04 893.83 242.86 o 15 9 -5 41.23 101.11 63.34 o 17 9 -5 28.98 74.91 88.92 o 0 10 -5 2514.89 1880.29 16.27 o 2 10 -5 6841.70 6266.80 47.57 o 4 10 -5 5407.59 5231.51 171.50 o 6 10 -5 1621.43 2140.68 246.62 o 8 10 -5 617.58 565.04 159.15 o 10 10 -5 122.87 180.63 78.18 o 12 10 -5 1133.51 1070.44 56.03 o 14 10 -5 865.49 687.28 282.92 o 1 11 -5 1154.26 1817.70 230.34 o 3 11 -5 1155.85 1175.49 272.91 o 5 11 -5 657.97 1017.76 274.16 o 7 11 -5 2221.06 1852.69 148.24 o 9 11 -5 995.87 1374.25 231.71 o 11 11 -5 335.74 414.36 83.87 o 13 11 -5 4.77 45.86 104.35 o 0 12 -5 673.67 853.77 240.36 o 2 12 -5 260.11 320.48 135.20 o 4 12 -5 191.88 336.75 115.17 o 6 12 -5 356.45 398.09 147.72 o 8 12 -5 254.71 321.01 77.19 o 10 12 -5 127.09 334.25 271.65 o 4 0 -4 8953.86 9102.26 88.88 o 6 0 -4 76555.20 80963.91 77.62 o 8 0 -4 5377.47 6082.78 187.78 o 10 0 -4 11693.76 11726.15 356.78 o 14 0 -4 58086.01 54160.38 167.75 o 16 0 -4 15950.17 14809.48 85.13 o 18 0 -4 4912.77 4098.58 17.53 o 3 1 -4 4722.97 5022.45 216.57 o 5 1 -4 33085.55 35584.10 232.77 o 7 1 -4 12417.35 12506.99 163.37 o 9 1 -4 1132.30 1368.86 97.55 o 11 1 -4 101.98 332.05 164.14 o 13 1 -4 1116.88 1157.97 181.52 o 15 1 -4 862.41 996.48 225.33 o 17 1 -4 483.42 538.30 176.51 o 19 1 -4 94.16 105.16 150.22 o 4 2 -4 8342.41 8650.73 409.98 o 6 2 -4 23086.54 24015.03 435.07 o 8 2 -4 17980.11 18812.43 130.39 o 10 2 -4 8110.01 7547.23 239.35 o 12 2 -4 2470.83 2795.58 65.77 o 14 2 -4 441.26 649.71 200.30 o 16 2 -4 137.00 160.24 244.11 o 18 2 -4 390.08 479.46 317.97 o 3 3 -4 8521.96 8586.60 108.22 o 5 3 -4 13249.77 13174.68 70.83 o 7 3 -4 17948.12 19798.12 215.03 o 9 3 -4 15173.92 14173.56 96.78 o 11 3 -4 4868.53 4788.51 266.11 o 13 3 -4 1467.29 1339.58 198.42 o 15 3 -4 301.91 413.19 82.76 o 17 3 -4 184.81 146.37 242.55 o 19 3 -4 1524.91 1449.65 210.31 o 21 3 -4 794.66 709.80 55.08 o 2 4 -4 3114.18 3695.06 166.30 o 4 4 -4 258.96 380.88 60.36 o 6 4 -4 3091.34 3400.48 140.20 o 8 4 -4 7399.65 7165.98 159.62 o 10 4 -4 2335.39 2399.07 105.90 o 12 4 -4 1549.20 2119.32 211.56 o 14 4 -4 1057.50 1198.74 90.56 o 16 4 -4 4358.00 4062.96 201.30 o 18 4 -4 2200.30 2487.44 301.70 o 20 4 -4 1102.61 1617.22 178.39 o 1 5 -4 749.73 712.31 254.13 o 3 5 -4 2470.60 2643.53 60.72 o 5 5 -4 3267.38 3582.31 136.45 o 7 5 -4 11.37 65.44 116.47 o 9 5 -4 1069.50 1084.98 43.53 o 11 5 -4 3063.49 2962.94 209.06 o 13 5 -4 1509.35 1399.29 152.98 o 15 5 -4 155.30 341.74 238.04 o 17 5 -4 84.76 90.13 33.80 o 19 5 -4 243.76 447.60 155.06 o 21 5 -4 404.79 584.51 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