#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232220.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232220_Fobs loop_ _publ_author_name 'Aznan, Aina Mardia Akhmad' 'Abdullah, Zanariah' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 4-Nitrobenzoic acid--N-(pyrimidin-2-yl)aniline (1/1) ; _journal_coeditor_code EZ2266 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3080 _journal_page_last o3081 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.209 _cell_angle_gamma 90.000 _cell_length_a 12.7754 _cell_length_b 25.7788 _cell_length_c 9.5813 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file ez2266Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 425.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4689.00 4537.76 66.05 o 3 0 0 8561.00 8160.81 108.57 o 4 0 0 44.07 93.99 9.92 o 5 0 0 1106.82 1122.43 37.10 o 6 0 0 249.84 295.94 21.23 o 7 0 0 82.58 34.49 66.12 o 8 0 0 72.49 95.26 22.39 o 9 0 0 1203.59 1230.70 65.00 o 10 0 0 394.84 533.47 53.64 o 11 0 0 3841.83 4003.06 154.05 o 12 0 0 300.05 265.96 43.17 o 13 0 0 74.55 110.52 30.06 o 14 0 0 1.78 11.07 13.12 o 15 0 0 289.42 341.52 54.88 o 16 0 0 187.65 155.60 40.39 o 2 1 0 38.21 36.99 4.57 o 3 1 0 3519.84 3322.08 48.94 o 4 1 0 1611.08 1523.06 31.20 o 5 1 0 46.74 69.01 6.69 o 6 1 0 2542.19 2616.92 43.92 o 7 1 0 104.76 21.77 24.51 o 8 1 0 24.97 22.59 8.10 o 9 1 0 1595.87 1678.29 64.18 o 10 1 0 55.65 91.08 21.13 o 11 1 0 87.31 68.27 17.38 o 12 1 0 29.16 23.03 9.74 o 13 1 0 186.73 196.60 27.67 o 14 1 0 173.03 176.13 27.46 o 15 1 0 1.39 4.94 8.61 o 16 1 0 288.27 292.00 37.40 o 1 2 0 888.99 835.43 21.02 o 2 2 0 6891.13 6119.77 84.75 o 3 2 0 47.65 43.32 6.06 o 4 2 0 5515.78 5379.47 83.15 o 5 2 0 563.27 602.85 22.58 o 6 2 0 1257.11 1305.50 36.39 o 7 2 0 284.23 295.77 23.12 o 8 2 0 687.94 725.97 38.79 o 9 2 0 775.30 730.18 35.67 o 10 2 0 178.81 190.09 40.17 o 11 2 0 177.41 149.57 21.49 o 12 2 0 90.21 126.28 21.65 o 13 2 0 182.71 169.15 34.77 o 14 2 0 0.02 -5.35 37.13 o 15 2 0 90.20 91.84 22.26 o 16 2 0 0.10 11.27 11.89 o 1 3 0 295.06 311.52 15.09 o 2 3 0 3576.57 3438.12 65.41 o 3 3 0 9283.16 9214.93 126.08 o 4 3 0 1578.53 1517.12 52.83 o 5 3 0 148.82 187.19 15.57 o 6 3 0 60.15 51.12 10.63 o 7 3 0 48.40 68.86 19.48 o 8 3 0 328.86 348.85 26.95 o 9 3 0 520.55 588.99 30.65 o 10 3 0 1846.56 2041.49 74.04 o 11 3 0 141.96 178.83 24.19 o 12 3 0 307.64 342.11 28.32 o 13 3 0 147.93 172.05 26.18 o 14 3 0 48.74 36.43 21.50 o 15 3 0 0.33 -0.35 20.18 o 16 3 0 12.68 1.25 9.18 o 0 4 0 246.42 237.32 13.83 o 1 4 0 2077.05 1781.70 28.40 o 2 4 0 6678.11 6192.78 48.95 o 3 4 0 3554.18 3344.36 52.09 o 4 4 0 80.83 106.22 10.75 o 5 4 0 341.72 435.91 23.57 o 6 4 0 2.12 5.86 1.77 o 7 4 0 1845.71 1923.88 31.69 o 8 4 0 152.80 166.62 9.65 o 9 4 0 248.06 261.41 12.76 o 10 4 0 296.17 299.23 18.76 o 11 4 0 551.38 606.54 21.84 o 12 4 0 113.01 111.12 9.08 o 13 4 0 233.01 217.39 29.18 o 14 4 0 119.71 122.84 25.21 o 15 4 0 5.85 14.58 19.25 o 1 5 0 692.80 666.51 15.33 o 2 5 0 1295.38 1182.75 22.54 o 3 5 0 90.43 94.74 9.31 o 4 5 0 1542.35 1594.87 41.24 o 5 5 0 5391.28 5183.79 82.22 o 6 5 0 14.46 7.88 5.10 o 7 5 0 1141.33 1255.71 54.29 o 8 5 0 401.49 401.50 24.13 o 9 5 0 1170.26 1213.28 49.10 o 10 5 0 709.10 750.82 45.05 o 11 5 0 12.59 4.44 8.17 o 12 5 0 209.28 208.35 34.45 o 13 5 0 0.01 6.22 18.17 o 14 5 0 296.75 267.86 33.38 o 15 5 0 209.10 200.49 30.41 o 0 6 0 650.88 607.09 27.19 o 1 6 0 0.74 -0.96 2.30 o 2 6 0 70.24 45.53 5.02 o 3 6 0 610.09 624.33 24.71 o 4 6 0 5782.14 5690.01 79.22 o 5 6 0 4611.34 4513.61 77.20 o 6 6 0 94.08 165.99 13.59 o 7 6 0 146.66 167.77 31.21 o 8 6 0 28.40 42.53 8.65 o 9 6 0 173.98 197.18 22.30 o 10 6 0 9.24 17.22 9.54 o 11 6 0 0.45 8.54 19.26 o 12 6 0 28.46 47.73 21.48 o 13 6 0 246.98 247.14 31.22 o 14 6 0 28.39 1.86 9.21 o 15 6 0 78.18 72.03 38.22 o 1 7 0 510.98 442.28 14.54 o 2 7 0 2825.36 2554.37 36.94 o 3 7 0 73.20 65.01 6.53 o 4 7 0 72.62 48.83 4.84 o 5 7 0 1555.18 1473.69 45.04 o 6 7 0 76.37 83.36 10.01 o 7 7 0 2359.54 2374.23 53.87 o 8 7 0 204.38 206.04 18.77 o 9 7 0 303.82 313.49 22.43 o 10 7 0 88.87 76.34 15.50 o 11 7 0 66.40 72.95 16.08 o 12 7 0 1.12 -1.84 13.83 o 13 7 0 464.02 441.40 41.27 o 14 7 0 157.25 181.77 28.02 o 15 7 0 12.63 9.87 9.58 o 0 8 0 2389.43 1862.10 41.17 o 1 8 0 2005.15 1802.90 31.03 o 2 8 0 326.62 290.82 13.17 o 3 8 0 571.05 574.14 19.74 o 4 8 0 2.16 9.53 4.35 o 5 8 0 7.75 2.92 5.04 o 6 8 0 1595.54 1538.05 50.35 o 7 8 0 1097.64 1237.63 39.10 o 8 8 0 471.89 551.12 24.83 o 9 8 0 482.48 572.12 55.63 o 10 8 0 0.07 -7.49 7.59 o 11 8 0 822.09 826.82 63.99 o 12 8 0 62.82 42.62 11.83 o 13 8 0 304.44 292.08 33.76 o 14 8 0 30.44 43.49 14.59 o 15 8 0 97.29 96.75 22.16 o 1 9 0 1938.35 1803.30 28.95 o 2 9 0 0.24 -0.44 2.94 o 3 9 0 681.27 613.86 21.27 o 4 9 0 437.46 477.26 19.97 o 5 9 0 129.90 137.49 7.93 o 6 9 0 5864.35 5954.79 100.05 o 7 9 0 3191.60 3441.87 66.03 o 8 9 0 1550.82 1628.32 42.67 o 9 9 0 170.86 230.46 19.63 o 10 9 0 212.95 228.43 25.89 o 11 9 0 144.42 128.82 28.17 o 12 9 0 117.28 145.15 22.80 o 13 9 0 6.95 24.38 12.31 o 14 9 0 19.86 18.53 12.22 o 15 9 0 978.97 952.45 65.66 o 0 10 0 17.80 29.55 5.90 o 1 10 0 3170.81 3463.73 42.29 o 2 10 0 1097.83 1152.43 28.60 o 3 10 0 6066.42 6236.71 69.55 o 4 10 0 919.36 911.70 30.96 o 5 10 0 1424.34 1535.31 33.92 o 6 10 0 2143.97 2155.68 77.74 o 7 10 0 61.66 61.92 10.23 o 8 10 0 1148.46 1308.49 60.72 o 9 10 0 22.17 25.79 7.13 o 10 10 0 238.29 316.02 30.76 o 11 10 0 0.49 8.49 16.26 o 12 10 0 15.22 16.85 10.50 o 13 10 0 466.43 423.01 41.15 o 14 10 0 54.67 51.24 18.19 o 15 10 0 809.90 810.47 61.23 o 1 11 0 52.28 83.33 7.11 o 2 11 0 3975.72 3902.40 57.06 o 3 11 0 2673.08 2708.53 47.52 o 4 11 0 283.55 355.28 18.25 o 5 11 0 183.32 182.48 19.47 o 6 11 0 1214.34 1255.84 24.35 o 7 11 0 947.07 1018.83 38.40 o 8 11 0 8.27 9.79 5.86 o 9 11 0 519.03 532.42 29.88 o 10 11 0 27.56 20.09 10.10 o 11 11 0 843.94 894.40 54.06 o 12 11 0 8.74 9.28 13.88 o 13 11 0 412.73 435.77 41.61 o 14 11 0 56.41 47.07 20.75 o 15 11 0 13.70 64.92 26.86 o 0 12 0 3794.38 3696.80 67.47 o 1 12 0 740.94 708.08 21.11 o 2 12 0 1316.98 1320.93 29.48 o 3 12 0 3482.16 3595.77 56.88 o 4 12 0 1956.01 2051.83 44.95 o 5 12 0 1812.27 1903.01 56.08 o 6 12 0 161.05 220.34 11.60 o 7 12 0 245.87 257.72 37.06 o 8 12 0 53.96 82.82 12.25 o 9 12 0 199.25 223.31 19.76 o 10 12 0 125.42 141.41 21.43 o 11 12 0 839.29 842.57 52.95 o 12 12 0 192.82 208.28 27.94 o 13 12 0 0.07 21.09 18.62 o 14 12 0 538.99 550.77 48.78 o 15 12 0 339.94 327.61 54.80 o 1 13 0 26.31 23.22 4.38 o 2 13 0 1434.07 1547.50 33.09 o 3 13 0 1730.72 1868.74 37.62 o 4 13 0 1289.92 1343.76 37.54 o 5 13 0 2908.14 3210.28 60.45 o 6 13 0 293.71 326.01 14.15 o 7 13 0 29.44 45.88 12.12 o 8 13 0 118.53 121.62 27.03 o 9 13 0 0.04 5.25 7.97 o 10 13 0 475.53 536.35 40.88 o 11 13 0 7.39 11.49 9.58 o 12 13 0 2134.75 2236.68 90.20 o 13 13 0 846.20 778.67 87.08 o 14 13 0 3.12 21.09 10.95 o 0 14 0 356.99 496.76 30.09 o 1 14 0 103.58 128.86 9.94 o 2 14 0 1509.65 1679.19 35.82 o 3 14 0 403.50 432.15 18.90 o 4 14 0 121.88 140.30 11.25 o 5 14 0 12.12 9.03 5.92 o 6 14 0 195.38 200.07 13.22 o 7 14 0 371.40 395.07 14.70 o 8 14 0 429.26 471.83 50.69 o 9 14 0 19.90 36.71 11.39 o 10 14 0 8.30 4.68 7.57 o 11 14 0 127.29 125.75 21.32 o 12 14 0 1775.45 1802.05 96.62 o 13 14 0 265.52 233.45 31.13 o 14 14 0 263.93 297.03 36.84 o 1 15 0 2257.84 2334.98 42.98 o 2 15 0 22.18 11.97 5.17 o 3 15 0 357.10 413.36 18.99 o 4 15 0 5.31 6.80 4.16 o 5 15 0 328.17 335.33 32.17 o 6 15 0 351.62 324.59 21.94 o 7 15 0 377.57 365.44 18.42 o 8 15 0 0.56 5.62 6.70 o 9 15 0 2.94 5.72 12.35 o 10 15 0 1191.16 1246.81 63.01 o 11 15 0 1.60 4.84 7.67 o 12 15 0 302.33 322.72 64.23 o 13 15 0 255.17 286.50 35.10 o 14 15 0 238.56 253.61 46.50 o 0 16 0 738.80 736.16 35.51 o 1 16 0 1645.77 1536.78 36.23 o 2 16 0 38.20 32.47 6.12 o 3 16 0 208.02 208.22 14.51 o 4 16 0 89.89 104.64 10.50 o 5 16 0 261.03 279.40 19.46 o 6 16 0 10.02 6.07 7.04 o 7 16 0 92.03 92.57 9.57 o 8 16 0 389.59 371.46 48.25 o 9 16 0 1.40 -16.35 13.62 o 10 16 0 38.17 59.71 20.41 o 11 16 0 130.00 96.16 19.70 o 12 16 0 30.65 47.56 15.58 o 13 16 0 162.86 167.89 28.00 o 14 16 0 3.21 27.12 15.32 o 1 17 0 23.51 41.68 6.95 o 2 17 0 86.05 79.31 9.07 o 3 17 0 97.80 74.82 9.18 o 4 17 0 163.98 169.25 13.43 o 5 17 0 25.32 20.26 6.51 o 6 17 0 403.54 363.49 27.66 o 7 17 0 361.15 384.84 24.09 o 8 17 0 226.00 321.60 45.60 o 9 17 0 13.93 -11.50 19.20 o 10 17 0 3.35 3.25 9.47 o 11 17 0 0.01 -13.16 9.88 o 12 17 0 77.83 84.18 19.21 o 13 17 0 254.95 254.31 33.70 o 0 18 0 1865.51 1995.72 62.24 o 1 18 0 941.06 926.80 32.97 o 2 18 0 865.32 946.77 30.71 o 3 18 0 144.89 144.20 12.52 o 4 18 0 529.41 487.30 26.21 o 5 18 0 0.05 6.50 5.81 o 6 18 0 789.23 786.05 35.12 o 7 18 0 12.20 15.84 14.43 o 8 18 0 237.31 210.36 38.19 o 9 18 0 82.35 80.22 24.60 o 10 18 0 281.11 313.26 33.43 o 11 18 0 2.79 2.58 13.34 o 12 18 0 128.49 127.06 23.64 o 13 18 0 0.24 -21.66 15.92 o 1 19 0 194.91 213.81 16.90 o 2 19 0 923.85 991.65 32.44 o 3 19 0 1.01 16.68 7.41 o 4 19 0 11.45 10.92 5.94 o 5 19 0 439.40 432.20 26.12 o 6 19 0 1255.43 1243.38 45.14 o 7 19 0 2471.64 2436.33 59.40 o 8 19 0 510.89 531.70 60.21 o 9 19 0 44.33 38.91 18.93 o 10 19 0 899.13 921.19 57.29 o 11 19 0 237.81 218.06 29.41 o 12 19 0 2.57 -27.92 19.63 o 13 19 0 649.10 601.44 70.18 o 0 20 0 1604.31 1613.14 134.57 o 1 20 0 77.16 94.77 10.56 o 2 20 0 1.03 6.70 5.39 o 3 20 0 178.39 206.04 18.36 o 4 20 0 716.93 675.14 32.71 o 5 20 0 1867.30 1729.92 69.76 o 6 20 0 1575.30 1629.65 66.67 o 7 20 0 0.88 3.39 4.84 o 8 20 0 2238.56 2254.28 124.68 o 9 20 0 36.37 32.04 21.89 o 10 20 0 1608.00 1533.38 111.12 o 11 20 0 0.17 10.26 9.09 o 12 20 0 57.46 31.55 25.15 o 1 21 0 177.39 164.71 19.94 o 2 21 0 19.43 34.65 11.73 o 3 21 0 1127.97 1109.45 41.82 o 4 21 0 4624.86 4769.21 109.16 o 5 21 0 247.34 198.84 23.55 o 6 21 0 44.27 78.98 16.92 o 7 21 0 2.99 -2.69 14.24 o 8 21 0 90.48 63.78 23.59 o 9 21 0 0.99 -13.08 15.12 o 10 21 0 297.04 352.95 57.03 o 11 21 0 198.96 239.95 31.85 o 12 21 0 2.00 -0.89 10.15 o 0 22 0 421.55 424.45 45.82 o 1 22 0 182.83 160.76 20.82 o 2 22 0 3529.65 3350.29 90.68 o 3 22 0 1081.75 1108.74 52.97 o 4 22 0 2136.74 2260.76 85.79 o 5 22 0 89.19 70.77 14.95 o 6 22 0 617.61 589.80 42.00 o 7 22 0 882.91 931.75 80.40 o 8 22 0 107.14 110.82 29.99 o 9 22 0 69.28 82.17 26.68 o 10 22 0 375.34 372.40 57.10 o 11 22 0 151.70 122.73 23.24 o 12 22 0 57.65 52.72 19.90 o 1 23 0 1277.67 1092.02 52.61 o 2 23 0 531.85 575.17 39.07 o 3 23 0 79.11 110.38 17.94 o 4 23 0 1129.41 1105.03 55.37 o 5 23 0 48.89 94.10 36.50 o 6 23 0 579.31 534.25 40.62 o 7 23 0 175.79 230.67 41.95 o 8 23 0 25.74 20.75 19.10 o 9 23 0 509.76 528.81 66.89 o 10 23 0 996.62 1024.45 94.79 o 11 23 0 62.21 89.69 25.83 o 0 24 0 465.04 475.14 50.79 o 1 24 0 111.90 78.93 15.73 o 2 24 0 11.46 10.31 8.21 o 3 24 0 1247.29 1224.07 58.33 o 4 24 0 67.88 44.04 18.31 o 5 24 0 38.49 45.93 13.95 o 6 24 0 223.43 164.46 27.26 o 7 24 0 146.86 116.95 30.27 o 8 24 0 502.99 499.19 62.80 o 9 24 0 38.29 134.84 38.08 o 10 24 0 126.66 87.63 30.03 o 11 24 0 0.10 21.11 15.14 o 1 25 0 66.78 62.75 13.99 o 2 25 0 1.05 -19.22 15.48 o 3 25 0 484.63 508.20 38.95 o 4 25 0 141.24 95.25 18.66 o 5 25 0 130.06 140.73 21.70 o 6 25 0 30.58 16.56 9.37 o 7 25 0 134.76 179.03 39.74 o 8 25 0 106.10 69.03 24.35 o 9 25 0 139.34 88.11 27.22 o 0 26 0 373.50 333.00 44.88 o 1 26 0 4.01 3.85 7.38 o 2 26 0 8.38 -9.30 15.19 o 3 26 0 7.54 16.30 10.40 o 4 26 0 2.17 4.86 7.53 o 5 26 0 115.71 114.01 20.61 o 6 26 0 124.68 106.78 19.66 o 7 26 0 23.77 15.32 16.50 o 8 26 0 204.09 276.39 49.77 o 9 26 0 65.61 56.75 27.18 o 1 27 0 26.55 15.25 9.52 o 2 27 0 327.39 332.70 32.64 o 3 27 0 28.72 25.83 17.83 o 4 27 0 48.36 64.86 16.23 o 5 27 0 10.37 4.96 9.05 o 6 27 0 0.28 2.46 11.50 o 7 27 0 310.69 389.75 56.71 o 8 27 0 28.15 54.49 24.06 o 0 28 0 36.67 46.26 23.56 o 1 28 0 602.32 566.23 43.01 o 2 28 0 38.17 52.10 15.86 o 3 28 0 346.88 291.07 31.61 o 4 28 0 65.78 80.24 17.94 o 5 28 0 3.03 12.42 10.71 o 6 28 0 88.34 69.69 16.99 o 7 28 0 217.41 292.37 34.03 o 8 28 0 39.57 21.37 15.78 o 1 29 0 36.61 22.85 10.40 o 2 29 0 1.41 4.59 10.19 o 3 29 0 124.30 131.83 30.33 o 4 29 0 2.68 -2.63 10.51 o 5 29 0 36.22 52.35 19.92 o 6 29 0 16.84 12.80 12.96 o 7 29 0 156.57 188.63 29.50 o 0 30 0 10.55 23.55 17.77 o 1 30 0 92.02 145.35 23.61 o 2 30 0 15.28 22.76 16.23 o 3 30 0 283.91 330.61 63.53 o 4 30 0 148.51 101.16 38.20 o 5 30 0 126.79 126.09 23.06 o 6 30 0 3.16 20.98 12.74 o 7 30 0 253.04 342.77 50.61 o 1 31 0 133.18 194.91 27.67 o 2 31 0 1.43 5.86 14.05 o 3 31 0 110.04 168.82 73.22 o 4 31 0 54.14 37.00 14.13 o 5 31 0 145.66 206.89 29.45 o 6 31 0 26.69 65.49 25.71 o 0 32 0 46.26 36.14 15.49 o 1 32 0 49.60 52.69 16.28 o 2 32 0 3.58 0.83 9.40 o 3 32 0 276.43 335.23 37.12 o 4 32 0 0.47 -9.78 15.64 o 1 33 0 0.17 -1.78 11.63 o 2 33 0 10.89 15.10 11.71 o -16 1 1 187.40 181.48 32.79 o -15 1 1 283.01 313.09 36.33 o -14 1 1 14.32 31.82 13.97 o -13 1 1 180.98 207.38 26.80 o -12 1 1 3.42 9.93 7.47 o -11 1 1 177.15 179.83 22.54 o -10 1 1 531.93 530.80 25.20 o -9 1 1 20.75 12.89 6.87 o -8 1 1 567.64 568.96 34.95 o -7 1 1 3797.95 3877.83 54.59 o -6 1 1 155.50 161.16 10.21 o -5 1 1 48.81 38.33 4.84 o -4 1 1 409.09 425.39 13.04 o -3 1 1 219.46 218.18 7.82 o -2 1 1 11368.94 10462.06 113.21 o -1 1 1 1134.53 999.78 20.38 o 1 1 1 499.47 450.83 18.30 o 2 1 1 196.96 191.83 9.36 o 3 1 1 52203.90 50438.29 1097.81 o 4 1 1 1311.52 1520.63 42.50 o 5 1 1 1540.53 1540.18 47.30 o 6 1 1 483.30 510.54 31.08 o 7 1 1 594.90 617.11 43.27 o 8 1 1 2.71 5.33 3.99 o 9 1 1 2105.89 2147.78 74.86 o 10 1 1 55.89 37.24 10.73 o 11 1 1 6.13 -3.60 6.48 o 12 1 1 953.26 895.29 57.02 o 13 1 1 2.88 1.43 9.62 o 14 1 1 20.85 3.37 17.34 o 15 1 1 127.60 94.26 22.13 o -16 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43.32 o -5 19 2 55.09 43.56 8.53 o -4 19 2 848.13 859.11 32.94 o -3 19 2 152.74 145.98 16.04 o -2 19 2 674.67 691.74 34.19 o -1 19 2 263.83 246.94 18.34 o 0 19 2 911.03 945.66 36.03 o 1 19 2 463.25 460.49 25.98 o 2 19 2 65.63 75.49 11.78 o 3 19 2 470.93 491.02 101.17 o 4 19 2 431.92 415.31 33.06 o 5 19 2 437.09 439.22 35.13 o 6 19 2 122.12 125.42 28.90 o 7 19 2 508.12 487.37 18.50 o 8 19 2 837.04 980.60 84.08 o 9 19 2 131.16 185.85 39.40 o 10 19 2 561.20 728.59 78.60 o 11 19 2 12.51 31.94 14.94 o 12 19 2 960.30 961.57 93.64 o -12 20 2 42.02 51.14 23.15 o -11 20 2 0.21 0.26 6.56 o -10 20 2 161.34 151.74 21.77 o -9 20 2 35.62 19.68 15.35 o -8 20 2 1942.65 1960.51 69.23 o -7 20 2 75.53 71.12 13.44 o -6 20 2 121.84 109.21 10.98 o -5 20 2 10.07 -1.67 4.88 o -4 20 2 1360.31 1357.83 65.38 o -3 20 2 95.29 108.85 12.63 o -2 20 2 8152.58 7885.50 137.88 o -1 20 2 163.98 168.51 17.76 o 0 20 2 370.15 345.51 22.65 o 1 20 2 871.39 859.55 36.42 o 2 20 2 843.77 794.67 43.95 o 3 20 2 2.82 3.16 8.30 o 4 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653.43 59.82 o 3 23 2 230.89 211.54 25.61 o 4 23 2 399.81 349.34 64.39 o 5 23 2 0.55 1.12 7.94 o 6 23 2 3837.93 3949.31 116.68 o 7 23 2 115.22 103.51 31.49 o 8 23 2 382.34 315.59 50.92 o 9 23 2 114.70 131.16 33.83 o 10 23 2 364.54 329.94 55.22 o -10 24 2 10.19 -26.50 18.74 o -9 24 2 12.89 13.94 14.02 o -8 24 2 81.23 67.85 24.19 o -7 24 2 0.81 -13.01 18.68 o -6 24 2 277.33 304.93 39.31 o -5 24 2 662.14 617.42 41.19 o -4 24 2 349.56 356.72 31.44 o -3 24 2 193.88 149.47 20.35 o -2 24 2 12.27 5.73 7.30 o -1 24 2 677.65 701.97 56.89 o 0 24 2 4.92 1.02 7.35 o 1 24 2 194.34 189.09 37.67 o 2 24 2 1438.71 1443.76 64.71 o 3 24 2 544.77 514.22 39.79 o 4 24 2 429.87 455.10 38.75 o 5 24 2 28.03 12.22 11.52 o 6 24 2 760.00 694.07 50.39 o 7 24 2 149.54 127.83 32.55 o 8 24 2 6.44 7.90 14.65 o 9 24 2 40.85 30.93 17.77 o -10 25 2 21.74 91.10 31.26 o -9 25 2 160.93 168.09 38.71 o -8 25 2 90.82 79.82 25.96 o -7 25 2 308.75 287.27 48.14 o -6 25 2 113.33 89.48 16.94 o -5 25 2 0.91 3.37 13.64 o -4 25 2 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