#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232233.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232233_Fobs loop_ _publ_author_name 'Wu, Qi' _publ_section_title ; Potassium pentaborate ; _journal_coeditor_code FI2113 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i67 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 119.132 _cell_angle_gamma 90.000 _cell_length_a 7.6690 _cell_length_b 9.0445 _cell_length_c 12.2304 _exptl_crystal_F_000 471.95 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file fi2113Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kb in P2(1)/n New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 181.07 158.40 2.07 o 2 0 0 432.49 422.39 6.51 o 3 0 0 457.06 409.12 5.64 o 4 0 0 3216.86 3402.55 32.14 o 5 0 0 790.79 767.42 12.74 o 6 0 0 65.63 68.12 5.61 o 7 0 0 516.45 577.74 20.95 o 8 0 0 344.61 323.09 20.85 o 1 1 0 2580.42 2798.39 17.76 o 2 1 0 1458.83 1465.10 9.96 o 3 1 0 164.37 183.21 2.45 o 4 1 0 2357.18 2453.89 18.40 o 5 1 0 706.52 748.07 9.17 o 6 1 0 861.97 817.58 13.08 o 7 1 0 1055.36 1098.64 25.07 o 8 1 0 20.47 21.82 5.03 o 0 2 0 921.43 843.34 8.26 o 1 2 0 103.57 93.05 1.35 o 2 2 0 6189.10 7005.06 40.00 o 3 2 0 549.95 688.11 6.43 o 4 2 0 754.76 764.49 7.22 o 5 2 0 46.01 56.45 2.51 o 6 2 0 997.19 926.61 14.62 o 7 2 0 0.14 -0.43 1.74 o 8 2 0 11.22 15.46 4.11 o 1 3 0 98.83 109.30 2.01 o 2 3 0 8436.36 8692.16 54.98 o 3 3 0 163.91 140.33 2.12 o 4 3 0 30.38 32.15 1.59 o 5 3 0 465.03 470.79 6.77 o 6 3 0 438.49 393.99 8.06 o 7 3 0 259.98 259.40 8.46 o 0 4 0 1462.74 1636.64 16.86 o 1 4 0 20.22 19.98 0.90 o 2 4 0 1557.39 1564.52 11.49 o 3 4 0 190.19 199.41 3.04 o 4 4 0 898.99 894.87 8.87 o 5 4 0 99.64 102.88 3.47 o 6 4 0 26.86 19.15 1.99 o 7 4 0 21.46 21.79 3.39 o 1 5 0 816.70 892.38 7.26 o 2 5 0 10.45 5.08 0.70 o 3 5 0 0.87 -0.50 0.60 o 4 5 0 406.97 404.50 6.37 o 5 5 0 33.10 32.13 2.31 o 6 5 0 319.88 344.79 8.11 o 7 5 0 3.90 4.07 2.98 o 0 6 0 1809.46 2006.00 30.66 o 1 6 0 171.40 156.76 2.96 o 2 6 0 98.00 113.50 3.28 o 3 6 0 0.76 0.53 0.81 o 4 6 0 34.63 32.39 2.66 o 5 6 0 3.84 -0.38 1.28 o 6 6 0 1220.32 1161.57 20.66 o 1 7 0 102.74 84.99 3.11 o 2 7 0 157.48 158.99 3.74 o 3 7 0 17.23 9.75 1.29 o 4 7 0 793.15 782.05 10.85 o 5 7 0 48.28 52.27 4.45 o 6 7 0 4.54 5.82 2.16 o 0 8 0 561.51 564.90 25.93 o 1 8 0 51.45 52.98 3.01 o 2 8 0 703.16 678.03 9.23 o 3 8 0 14.91 17.24 1.89 o 4 8 0 713.04 710.27 11.66 o 5 8 0 0.03 1.31 1.66 o 1 9 0 148.42 140.44 5.08 o 2 9 0 2084.45 2097.02 25.76 o 3 9 0 58.85 55.36 4.39 o 4 9 0 24.21 28.49 3.08 o 0 10 0 1493.12 1484.31 37.49 o 1 10 0 1.25 -0.12 1.78 o 2 10 0 203.75 194.78 7.73 o 3 10 0 1.15 2.49 2.26 o 1 11 0 68.28 93.82 7.10 o -8 1 1 1198.43 1151.65 30.30 o -7 1 1 0.39 -0.08 1.81 o -6 1 1 192.72 180.22 4.83 o -5 1 1 157.56 117.89 3.55 o -4 1 1 2192.63 2417.66 18.73 o -3 1 1 1419.76 1433.01 10.34 o -2 1 1 5022.66 4796.62 30.71 o -1 1 1 172.98 225.16 2.57 o 0 1 1 410.53 395.00 3.17 o 1 1 1 381.75 314.52 2.51 o 2 1 1 3268.18 3332.46 19.92 o 3 1 1 1410.98 1530.97 10.73 o 4 1 1 545.56 513.06 4.61 o 5 1 1 2210.94 2289.48 24.77 o 6 1 1 204.80 207.91 6.11 o 7 1 1 290.81 288.55 9.17 o -8 2 1 304.18 305.54 9.22 o -7 2 1 591.68 573.30 10.95 o -6 2 1 1218.47 1209.36 15.86 o -5 2 1 10.89 9.81 1.27 o -4 2 1 254.45 241.87 3.04 o -3 2 1 1966.36 2073.80 16.98 o -2 2 1 17224.42 17402.86 132.96 o -1 2 1 2679.81 2797.12 21.18 o 0 2 1 6216.85 6064.05 33.25 o 1 2 1 898.84 902.60 6.17 o 2 2 1 7.97 2.27 0.55 o 3 2 1 9.33 1.47 0.62 o 4 2 1 162.36 136.06 2.93 o 5 2 1 36.28 49.85 2.92 o 6 2 1 97.14 106.21 5.03 o 7 2 1 1.85 2.86 2.19 o -8 3 1 97.59 93.68 7.42 o -7 3 1 47.43 57.24 3.99 o -6 3 1 39.62 44.99 3.03 o -5 3 1 0.77 1.60 0.90 o -4 3 1 46.46 64.41 2.62 o -3 3 1 1473.09 1653.03 13.89 o -2 3 1 1675.53 1605.02 12.67 o -1 3 1 0.41 0.55 0.35 o 0 3 1 319.64 311.60 2.65 o 1 3 1 559.49 511.13 5.02 o 2 3 1 1486.17 1414.88 10.17 o 3 3 1 382.84 401.25 4.33 o 4 3 1 68.69 71.37 2.64 o 5 3 1 1.36 1.93 1.13 o 6 3 1 20.47 27.87 3.23 o 7 3 1 25.20 15.58 3.38 o -8 4 1 2.54 0.60 2.34 o -7 4 1 399.94 385.46 11.28 o -6 4 1 17.65 22.32 2.04 o -5 4 1 322.88 349.22 5.09 o -4 4 1 478.02 413.68 4.77 o -3 4 1 296.20 234.12 4.25 o -2 4 1 83.14 75.39 1.52 o -1 4 1 2025.03 1854.37 17.63 o 0 4 1 4151.71 4251.43 25.43 o 1 4 1 543.92 552.04 5.07 o 2 4 1 1.43 2.90 0.61 o 3 4 1 2216.97 2360.04 17.86 o 4 4 1 1671.57 1635.94 16.40 o 5 4 1 1010.49 977.57 12.01 o 6 4 1 343.61 326.18 6.75 o 7 4 1 124.73 133.10 8.05 o -7 5 1 85.40 82.32 4.80 o -6 5 1 199.14 201.75 5.81 o -5 5 1 181.51 167.66 5.17 o -4 5 1 14.18 14.29 1.15 o -3 5 1 14.50 23.74 1.11 o -2 5 1 1311.23 1257.10 9.84 o -1 5 1 272.70 297.74 3.49 o 0 5 1 25.21 7.57 0.64 o 1 5 1 540.76 586.05 5.06 o 2 5 1 988.34 972.28 8.03 o 3 5 1 232.00 216.10 3.61 o 4 5 1 409.66 421.32 7.93 o 5 5 1 479.12 453.18 9.65 o 6 5 1 108.75 103.90 5.77 o 7 5 1 146.56 133.60 8.70 o -7 6 1 436.76 468.50 11.28 o -6 6 1 7.38 9.10 2.02 o -5 6 1 396.36 386.73 7.03 o -4 6 1 390.77 379.91 6.38 o -3 6 1 59.61 48.01 1.84 o -2 6 1 3.25 1.67 0.68 o -1 6 1 340.48 343.55 4.77 o 0 6 1 126.31 125.36 2.14 o 1 6 1 16.54 18.39 1.28 o 2 6 1 10.16 10.20 1.08 o 3 6 1 599.55 592.93 7.50 o 4 6 1 330.05 289.31 6.67 o 5 6 1 90.27 80.69 4.31 o 6 6 1 127.25 145.87 10.94 o -6 7 1 97.83 107.00 4.85 o -5 7 1 378.97 386.31 7.17 o -4 7 1 776.83 773.64 10.57 o -3 7 1 119.51 111.41 4.34 o -2 7 1 2992.01 2923.10 24.11 o -1 7 1 805.96 830.36 9.77 o 0 7 1 19.22 17.73 1.06 o 1 7 1 228.38 237.55 4.52 o 2 7 1 157.59 139.02 3.54 o 3 7 1 163.26 175.60 4.62 o 4 7 1 57.95 56.91 3.11 o 5 7 1 100.78 104.66 5.07 o 6 7 1 17.89 20.82 2.98 o -6 8 1 47.49 47.67 3.68 o -5 8 1 17.52 27.41 3.16 o -4 8 1 75.74 76.39 3.95 o -3 8 1 17.64 21.57 1.86 o -2 8 1 572.95 543.87 8.92 o -1 8 1 91.61 97.51 4.23 o 0 8 1 717.65 702.91 10.34 o 1 8 1 83.57 64.60 3.76 o 2 8 1 1448.10 1428.37 17.79 o 3 8 1 274.86 292.78 6.02 o 4 8 1 115.61 108.06 6.91 o 5 8 1 50.03 45.78 3.68 o -5 9 1 0.22 2.55 1.84 o -4 9 1 514.47 540.06 10.94 o -3 9 1 8.17 11.00 2.08 o -2 9 1 0.43 -0.23 1.40 o -1 9 1 157.44 156.54 5.38 o 0 9 1 77.03 82.67 4.90 o 1 9 1 200.67 203.58 5.97 o 2 9 1 24.21 25.60 2.79 o 3 9 1 25.55 21.45 2.94 o 4 9 1 42.09 39.00 3.48 o -3 10 1 147.45 162.19 6.84 o -2 10 1 101.37 121.84 9.36 o -1 10 1 145.52 144.95 5.60 o 0 10 1 280.09 287.18 9.82 o 1 10 1 1000.26 1014.77 18.30 o 2 10 1 0.82 -0.45 2.12 o 3 10 1 308.75 299.05 8.08 o -1 11 1 157.97 166.67 9.14 o 0 11 1 0.01 -1.26 2.69 o -8 0 2 90.39 90.47 11.42 o -7 0 2 307.99 310.36 11.10 o -6 0 2 13.21 9.30 2.33 o -5 0 2 1985.56 1833.94 45.33 o -4 0 2 3641.59 3360.76 41.65 o -3 0 2 5335.77 5441.95 46.67 o -2 0 2 2444.23 2523.78 23.42 o -1 0 2 23.62 15.05 0.79 o 0 0 2 1144.07 1065.27 11.94 o 1 0 2 2912.33 2659.21 20.71 o 2 0 2 1420.15 1416.51 13.05 o 3 0 2 51.64 24.30 1.11 o 4 0 2 110.58 117.50 3.89 o 5 0 2 12.34 10.16 2.12 o 6 0 2 63.20 69.04 7.90 o 7 0 2 568.26 580.91 28.65 o -8 1 2 200.99 204.97 9.75 o -7 1 2 91.77 64.92 5.97 o -6 1 2 166.30 193.77 4.56 o -5 1 2 567.49 530.13 6.45 o -4 1 2 420.51 448.47 4.71 o -3 1 2 520.07 645.06 4.71 o -2 1 2 1073.90 1093.62 7.66 o -1 1 2 2648.78 2592.87 16.15 o 0 1 2 37.34 23.21 0.71 o 1 1 2 72.80 66.01 1.07 o 2 1 2 3221.11 3261.20 21.22 o 3 1 2 144.18 138.70 2.08 o 4 1 2 4.58 2.07 0.68 o 5 1 2 1069.92 1020.28 12.00 o 6 1 2 758.69 723.24 14.19 o 7 1 2 299.25 302.19 10.37 o -8 2 2 197.40 186.86 7.62 o -7 2 2 112.56 127.76 6.41 o -6 2 2 417.46 421.34 7.90 o -5 2 2 79.66 76.64 2.55 o -4 2 2 17.01 14.59 0.86 o -3 2 2 2188.74 2200.36 15.50 o -2 2 2 10596.46 11347.83 74.93 o -1 2 2 289.93 204.95 2.17 o 0 2 2 990.91 877.40 5.70 o 1 2 2 1252.16 1249.85 8.04 o 2 2 2 375.06 368.19 4.77 o 3 2 2 3822.12 3918.53 24.33 o 4 2 2 190.80 182.07 4.24 o 5 2 2 35.94 37.20 2.20 o 6 2 2 654.87 648.14 13.22 o 7 2 2 87.23 73.61 7.61 o -8 3 2 40.32 51.58 4.35 o -7 3 2 7.26 14.41 2.27 o -6 3 2 1738.55 1675.75 18.88 o -5 3 2 691.68 697.65 7.19 o -4 3 2 358.59 338.70 4.94 o -3 3 2 720.35 745.41 7.45 o -2 3 2 5696.89 5647.27 40.21 o -1 3 2 6327.05 6104.16 40.22 o 0 3 2 0.20 2.73 0.37 o 1 3 2 412.99 268.12 2.75 o 2 3 2 1174.76 1112.49 8.67 o 3 3 2 1213.82 1233.94 11.27 o 4 3 2 2318.00 2204.15 20.03 o 5 3 2 17.70 20.97 1.95 o 6 3 2 44.45 49.31 3.54 o 7 3 2 1.74 0.94 2.53 o -8 4 2 0.01 -0.44 2.06 o -7 4 2 12.85 9.25 1.95 o -6 4 2 1028.30 1006.10 13.65 o -5 4 2 811.51 752.93 8.12 o -4 4 2 1010.22 1106.80 12.18 o -3 4 2 31.31 32.47 1.56 o -2 4 2 265.90 301.04 3.98 o -1 4 2 44.63 83.38 1.66 o 0 4 2 539.09 541.79 4.42 o 1 4 2 2261.11 2425.37 15.37 o 2 4 2 214.70 224.05 2.98 o 3 4 2 3.13 8.46 1.09 o 4 4 2 57.38 56.56 2.82 o 5 4 2 0.09 0.52 1.18 o 6 4 2 329.64 292.95 7.12 o 7 4 2 307.15 386.89 15.51 o -7 5 2 0.48 0.19 1.55 o -6 5 2 128.82 135.20 4.69 o -5 5 2 138.70 134.76 3.39 o -4 5 2 595.04 557.04 7.43 o -3 5 2 5.68 6.15 0.92 o -2 5 2 518.70 516.25 5.10 o -1 5 2 218.99 166.79 2.45 o 0 5 2 6077.71 6198.85 35.11 o 1 5 2 160.22 143.27 2.23 o 2 5 2 582.03 570.12 6.46 o 3 5 2 61.18 58.64 2.59 o 4 5 2 914.29 886.09 13.21 o 5 5 2 216.33 206.27 8.41 o 6 5 2 151.38 173.71 6.52 o -7 6 2 295.59 290.67 8.45 o -6 6 2 1.38 -1.22 1.35 o -5 6 2 219.56 245.71 5.08 o -4 6 2 4939.31 4818.37 35.78 o -3 6 2 1525.95 1489.94 12.95 o -2 6 2 0.20 0.98 0.62 o -1 6 2 824.30 706.62 8.14 o 0 6 2 1162.48 1104.22 9.01 o 1 6 2 3093.72 3107.37 25.24 o 2 6 2 1347.68 1259.77 11.69 o 3 6 2 616.76 578.93 8.17 o 4 6 2 886.27 905.23 13.14 o 5 6 2 6.72 2.51 1.98 o 6 6 2 728.82 769.81 16.45 o -6 7 2 108.06 116.84 4.72 o -5 7 2 2.23 1.98 1.35 o -4 7 2 87.84 86.67 3.04 o -3 7 2 0.28 3.23 1.01 o -2 7 2 78.35 97.26 2.78 o -1 7 2 131.19 131.34 3.56 o 0 7 2 709.60 762.46 8.67 o 1 7 2 145.43 118.78 3.72 o 2 7 2 518.03 555.40 7.83 o 3 7 2 36.98 40.94 2.64 o 4 7 2 190.56 188.69 6.80 o 5 7 2 31.48 33.72 3.65 o -6 8 2 63.82 58.87 3.85 o -5 8 2 10.49 8.88 1.97 o -4 8 2 73.37 65.78 3.40 o -3 8 2 39.23 45.49 2.50 o -2 8 2 844.81 810.76 11.78 o -1 8 2 87.52 82.19 3.71 o 0 8 2 633.00 650.72 9.59 o 1 8 2 413.02 418.08 7.78 o 2 8 2 30.11 25.23 2.53 o 3 8 2 1358.84 1329.74 15.99 o 4 8 2 3.54 0.57 2.18 o 5 8 2 25.23 21.78 2.93 o -5 9 2 108.31 104.72 6.04 o -4 9 2 327.61 319.55 7.42 o -3 9 2 19.61 18.06 2.38 o -2 9 2 1173.93 1098.96 16.03 o -1 9 2 241.56 260.33 6.47 o 0 9 2 157.28 160.25 6.80 o 1 9 2 15.67 12.77 2.69 o 2 9 2 2.51 3.49 1.82 o 3 9 2 0.05 -2.73 1.82 o 4 9 2 416.54 412.41 9.76 o -4 10 2 2.62 2.25 2.48 o -3 10 2 151.31 143.26 6.76 o -2 10 2 12.92 13.54 2.68 o -1 10 2 20.56 24.27 2.77 o 0 10 2 2183.93 2121.76 34.58 o 1 10 2 196.27 191.01 6.83 o 2 10 2 7.30 8.76 2.60 o -1 11 2 195.33 207.56 9.71 o 0 11 2 56.79 61.32 7.13 o -8 1 3 293.65 278.03 8.70 o -7 1 3 56.36 63.40 4.61 o -6 1 3 1642.35 1738.26 17.13 o -5 1 3 779.25 765.56 7.73 o -4 1 3 20.68 26.04 1.23 o -3 1 3 27.30 30.85 0.76 o -2 1 3 1001.95 920.58 6.33 o -1 1 3 3126.66 3081.14 18.09 o 0 1 3 22.98 23.55 0.72 o 1 1 3 189.71 153.22 1.67 o 2 1 3 2573.85 2514.74 15.00 o 3 1 3 106.77 122.70 2.21 o 4 1 3 2677.93 2591.27 22.06 o 5 1 3 298.25 303.36 6.66 o 6 1 3 25.02 22.64 4.83 o 7 1 3 35.50 43.26 4.60 o -8 2 3 15.40 7.29 2.56 o -7 2 3 156.34 121.80 4.39 o -6 2 3 268.11 247.44 5.10 o -5 2 3 87.18 84.08 2.28 o -4 2 3 971.53 971.63 8.83 o -3 2 3 544.91 420.35 4.36 o -2 2 3 9231.24 9527.98 64.66 o -1 2 3 194.26 199.50 2.25 o 0 2 3 2396.65 2403.08 13.94 o 1 2 3 110.45 140.46 1.66 o 2 2 3 6885.37 7236.52 46.63 o 3 2 3 6.77 8.10 0.83 o 4 2 3 553.02 519.88 6.12 o 5 2 3 129.07 129.40 4.30 o 6 2 3 1618.59 1502.14 25.18 o 7 2 3 303.00 320.73 11.44 o -8 3 3 5.22 2.05 2.03 o -7 3 3 55.17 61.99 3.79 o -6 3 3 5.70 4.09 1.32 o -5 3 3 0.66 2.49 0.78 o -4 3 3 13.24 5.67 0.88 o -3 3 3 1.02 0.46 0.60 o -2 3 3 2347.34 2492.95 17.32 o -1 3 3 437.72 529.99 4.66 o 0 3 3 20.34 12.12 0.57 o 1 3 3 2242.22 2209.08 13.80 o 2 3 3 882.16 851.98 6.82 o 3 3 3 300.18 325.46 4.22 o 4 3 3 533.79 563.29 7.91 o 5 3 3 572.07 565.39 8.79 o 6 3 3 402.63 447.81 11.77 o -8 4 3 624.44 647.03 14.33 o -7 4 3 118.99 125.11 5.20 o -6 4 3 1332.91 1329.33 16.51 o -5 4 3 596.23 633.74 9.09 o -4 4 3 11469.75 11733.34 80.46 o -3 4 3 355.46 314.76 4.53 o -2 4 3 110.09 97.19 2.08 o -1 4 3 332.07 347.76 3.87 o 0 4 3 5106.47 4949.48 33.36 o 1 4 3 1136.74 1113.59 8.28 o 2 4 3 67.02 47.82 1.49 o 3 4 3 436.88 396.79 5.32 o 4 4 3 313.44 307.55 5.69 o 5 4 3 7.81 4.12 1.60 o 6 4 3 784.26 803.78 14.37 o -8 5 3 544.35 599.68 19.26 o -7 5 3 111.64 111.58 4.36 o -6 5 3 1249.96 1233.74 14.93 o -5 5 3 9.85 14.29 1.62 o -4 5 3 26.84 34.48 1.94 o -3 5 3 384.17 405.03 6.07 o -2 5 3 2109.89 2289.49 18.04 o -1 5 3 592.55 517.49 4.98 o 0 5 3 97.37 107.29 2.15 o 1 5 3 865.72 881.16 7.07 o 2 5 3 1504.05 1362.97 13.76 o 3 5 3 16.41 12.06 1.63 o 4 5 3 509.99 491.22 9.34 o 5 5 3 179.82 213.12 6.57 o 6 5 3 4.51 0.44 2.03 o -7 6 3 8.29 7.60 2.14 o -6 6 3 225.52 194.07 6.41 o -5 6 3 142.41 140.17 4.68 o -4 6 3 255.40 239.87 5.03 o -3 6 3 362.80 374.81 4.65 o -2 6 3 19.97 29.52 1.61 o -1 6 3 398.58 399.78 4.50 o 0 6 3 484.13 473.23 5.53 o 1 6 3 377.65 402.42 5.62 o 2 6 3 359.07 358.05 6.36 o 3 6 3 9.61 13.41 1.78 o 4 6 3 3.97 5.39 1.74 o 5 6 3 0.45 2.92 2.09 o -7 7 3 5.94 4.86 1.98 o -6 7 3 357.09 373.13 10.34 o -5 7 3 350.39 352.40 6.00 o -4 7 3 152.65 140.96 3.76 o -3 7 3 34.68 35.74 1.92 o -2 7 3 3377.36 3324.62 29.44 o -1 7 3 24.09 21.09 1.92 o 0 7 3 191.05 189.27 4.08 o 1 7 3 290.79 306.52 6.29 o 2 7 3 1196.57 1134.94 13.53 o 3 7 3 15.79 17.93 1.99 o 4 7 3 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