#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:29:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181244 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232237.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232237_Fobs loop_ _publ_author_name 'Kinfe, Henok H.' 'Mebrahtu, Fanuel M.' 'Muller, Alfred' _publ_section_title ; Phenyl 4,6-di-O-acetyl-2,3-dideoxy-1-thio-\a-D-erythro-hex-2-enopyranoside ; _journal_coeditor_code FJ2451 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2840 _journal_page_last o2841 _journal_volume 67 _journal_year 2011 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.291 _cell_angle_gamma 90.000 _cell_length_a 5.2330 _cell_length_b 13.4700 _cell_length_c 11.1760 _exptl_crystal_F_000 340.00 _reflns_d_resolution_high 0.7482 _cod_data_source_file fj2451Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_11cn_fm1_0m in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 114.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -17 0 18.14 17.94 1.20 o 2 -17 0 22.74 20.59 1.54 o 0 -16 0 244.14 240.56 8.71 o 1 -16 0 193.65 203.47 5.53 o 2 -16 0 62.64 60.95 1.62 o 3 -16 0 108.23 98.78 2.70 o 1 -15 0 1.58 2.22 0.94 o 2 -15 0 7.42 6.60 0.78 o 3 -15 0 8.24 9.37 0.94 o 0 -14 0 90.56 95.88 4.54 o 1 -14 0 175.05 176.19 4.67 o 2 -14 0 35.91 38.10 1.96 o 3 -14 0 28.44 27.50 1.51 o 4 -14 0 20.77 17.27 1.73 o 1 -13 0 21.73 25.35 1.64 o 2 -13 0 26.46 26.42 1.53 o 3 -13 0 16.19 15.98 1.26 o 4 -13 0 18.71 19.52 1.30 o 0 -12 0 559.36 526.72 14.96 o 1 -12 0 495.80 502.91 10.18 o 2 -12 0 115.16 111.38 2.76 o 3 -12 0 5.95 5.01 1.72 o 4 -12 0 82.61 82.38 2.33 o 5 -12 0 72.39 69.86 2.37 o 1 -11 0 632.13 623.49 12.27 o 2 -11 0 233.87 239.75 5.04 o 3 -11 0 14.42 11.11 1.09 o 4 -11 0 26.09 23.36 1.96 o 5 -11 0 56.18 56.66 2.08 o 0 -10 0 139.72 149.70 5.27 o 1 -10 0 192.18 179.60 3.30 o 2 -10 0 234.77 241.31 5.07 o 3 -10 0 244.32 242.57 8.46 o 4 -10 0 35.57 39.78 1.91 o 5 -10 0 35.77 38.54 2.81 o 1 -9 0 128.16 134.26 2.54 o 2 -9 0 282.48 298.69 7.30 o 3 -9 0 71.03 75.23 2.33 o 4 -9 0 11.94 11.15 1.18 o 5 -9 0 44.96 46.23 1.85 o 6 -9 0 64.92 67.31 4.41 o 0 -8 0 43.31 48.55 2.33 o 1 -8 0 235.71 259.89 4.26 o 2 -8 0 592.45 603.67 19.07 o 3 -8 0 328.81 316.93 6.56 o 4 -8 0 217.23 213.11 4.96 o 5 -8 0 122.71 126.36 3.11 o 6 -8 0 25.53 26.40 2.50 o 1 -7 0 676.27 792.79 11.71 o 2 -7 0 524.70 554.03 8.25 o 3 -7 0 178.53 181.44 3.25 o 4 -7 0 78.48 77.42 2.55 o 5 -7 0 45.13 42.31 1.72 o 6 -7 0 26.93 30.73 1.81 o 1 -6 0 143.53 141.10 2.43 o 2 -6 0 37.33 30.27 1.10 o 3 -6 0 134.26 133.55 2.12 o 4 -6 0 160.83 158.89 5.11 o 5 -6 0 98.15 96.15 2.59 o 6 -6 0 63.09 67.37 2.35 o 1 -5 0 284.59 309.56 5.15 o 2 -5 0 2522.85 2831.23 39.69 o 3 -5 0 862.02 902.86 11.53 o 4 -5 0 105.83 101.79 2.33 o 5 -5 0 199.15 184.20 3.45 o 6 -5 0 92.67 90.10 2.69 o 0 -4 0 263.43 279.91 7.48 o 1 -4 0 411.08 426.17 5.67 o 2 -4 0 303.43 325.45 4.36 o 3 -4 0 832.10 854.23 10.89 o 4 -4 0 109.11 111.92 2.08 o 5 -4 0 13.96 13.73 0.92 o 6 -4 0 180.80 181.29 3.45 o 1 -3 0 3.99 2.49 0.18 o 2 -3 0 107.97 116.73 1.79 o 3 -3 0 14.96 16.80 0.66 o 4 -3 0 45.92 42.92 1.04 o 5 -3 0 212.08 205.10 3.13 o 6 -3 0 70.24 71.09 1.99 o 0 -2 0 778.75 878.36 21.82 o 1 -2 0 972.39 1008.40 13.68 o 2 -2 0 1353.60 1370.65 16.70 o 3 -2 0 731.01 741.00 9.42 o 4 -2 0 18.14 20.84 0.94 o 5 -2 0 49.11 51.28 1.32 o 6 -2 0 82.91 83.44 2.14 o 1 -1 0 485.60 475.22 5.81 o 2 -1 0 359.21 371.84 5.17 o 3 -1 0 104.92 110.01 2.28 o 4 -1 0 540.85 535.45 6.46 o 5 -1 0 119.32 112.31 2.60 o 6 -1 0 33.18 33.76 1.23 o 1 0 0 6670.83 6369.04 129.45 o 2 0 0 69.07 65.75 1.12 o 3 0 0 34.63 50.93 0.99 o 4 0 0 1.78 0.77 0.34 o 5 0 0 9.09 7.90 0.65 o 6 0 0 10.46 10.73 0.97 o 1 1 0 483.29 463.56 5.76 o 2 1 0 359.79 371.24 4.80 o 3 1 0 108.70 111.78 1.67 o 4 1 0 540.83 539.29 6.44 o 5 1 0 121.16 116.22 2.06 o 6 1 0 31.93 34.09 1.38 o 1 2 0 996.83 1049.62 17.65 o 2 2 0 1357.49 1360.54 19.18 o 3 2 0 732.34 739.52 9.39 o 4 2 0 16.06 17.44 0.71 o 5 2 0 51.33 50.06 1.28 o 6 2 0 83.87 85.10 2.50 o 1 3 0 4.04 2.91 0.20 o 2 3 0 111.38 120.14 1.93 o 3 3 0 16.45 17.98 0.69 o 4 3 0 43.05 39.52 0.99 o 5 3 0 214.53 210.12 4.53 o 6 3 0 67.98 66.13 2.21 o 1 4 0 420.89 442.06 6.25 o 2 4 0 311.87 341.31 5.24 o 3 4 0 840.16 868.79 14.19 o 4 4 0 107.50 112.59 2.10 o 5 4 0 13.10 10.18 0.77 o 6 4 0 178.11 173.79 4.81 o 1 5 0 286.62 314.67 4.20 o 2 5 0 2534.71 2840.33 39.29 o 3 5 0 865.20 929.97 11.46 o 4 5 0 104.64 97.04 2.26 o 5 5 0 201.29 186.74 4.62 o 6 5 0 96.72 85.39 4.60 o 1 6 0 147.02 142.74 2.73 o 2 6 0 42.12 36.78 0.89 o 3 6 0 130.50 129.21 2.50 o 4 6 0 156.67 146.67 6.93 o 5 6 0 99.88 96.57 3.07 o 6 6 0 61.57 63.72 5.64 o 1 7 0 672.69 803.28 13.70 o 2 7 0 521.96 567.84 15.90 o 3 7 0 174.79 179.83 3.16 o 4 7 0 82.45 80.40 2.51 o 5 7 0 48.07 44.94 3.31 o 6 7 0 25.68 28.09 3.13 o 1 8 0 236.58 264.84 4.77 o 2 8 0 589.20 627.74 15.26 o 3 8 0 325.99 319.98 6.32 o 4 8 0 213.73 204.21 4.84 o 5 8 0 123.24 126.72 3.68 o 6 8 0 25.34 26.32 1.95 o 1 9 0 128.51 137.26 2.69 o 2 9 0 284.66 305.76 7.04 o 3 9 0 73.56 75.92 2.70 o 4 9 0 11.95 9.00 0.99 o 5 9 0 44.80 47.53 2.11 o 1 10 0 201.05 191.38 3.80 o 2 10 0 237.41 246.33 4.76 o 3 10 0 248.34 244.28 5.11 o 4 10 0 35.46 38.11 1.76 o 5 10 0 34.95 38.01 1.99 o 1 11 0 633.00 637.56 15.57 o 2 11 0 232.23 238.24 5.27 o 3 11 0 15.00 10.26 1.72 o 4 11 0 24.68 23.32 1.50 o 5 11 0 54.98 54.92 2.37 o 1 12 0 492.43 492.52 12.63 o 2 12 0 108.84 103.40 2.44 o 3 12 0 7.17 5.59 0.73 o 4 12 0 85.97 82.60 2.67 o 5 12 0 73.59 70.48 3.31 o 1 13 0 22.06 24.03 1.35 o 2 13 0 25.73 28.66 1.29 o 3 13 0 16.12 15.66 1.53 o 4 13 0 20.00 20.64 1.41 o 1 14 0 170.86 173.74 5.03 o 2 14 0 37.04 40.55 1.41 o 3 14 0 28.50 27.67 1.33 o 4 14 0 20.48 17.99 1.41 o 1 15 0 1.41 0.61 0.61 o 2 15 0 6.92 6.79 0.68 o 3 15 0 7.43 8.05 0.85 o 1 16 0 186.23 192.00 5.76 o 2 16 0 60.95 59.71 2.82 o 3 16 0 109.05 102.68 4.66 o 2 17 0 23.57 24.52 1.84 o -2 -17 1 41.55 44.45 2.11 o -1 -17 1 1.01 2.65 0.73 o 0 -17 1 9.11 10.11 1.39 o 1 -17 1 0.51 2.57 1.59 o 2 -17 1 10.41 10.04 0.99 o -3 -16 1 61.64 61.55 2.08 o -2 -16 1 166.87 169.38 4.45 o -1 -16 1 203.55 207.04 4.11 o 0 -16 1 88.47 80.60 4.23 o 1 -16 1 190.68 195.44 7.72 o 2 -16 1 14.29 13.81 1.10 o 3 -16 1 145.08 143.16 4.01 o -3 -15 1 25.56 23.86 1.35 o -2 -15 1 26.33 26.22 1.63 o -1 -15 1 14.75 15.00 1.00 o 0 -15 1 20.05 24.73 1.93 o 1 -15 1 1.54 0.23 0.82 o 2 -15 1 39.54 37.97 1.61 o 3 -15 1 22.87 23.27 2.51 o -4 -14 1 47.74 44.71 1.76 o -3 -14 1 10.73 8.77 1.34 o -2 -14 1 101.61 92.16 2.07 o -1 -14 1 27.41 24.23 1.89 o 0 -14 1 53.13 53.14 2.50 o 1 -14 1 273.43 269.37 6.41 o 2 -14 1 227.53 228.88 7.91 o 3 -14 1 88.31 85.07 4.29 o 4 -14 1 71.66 75.29 2.81 o -4 -13 1 34.24 31.52 1.52 o -3 -13 1 10.49 9.03 0.87 o -2 -13 1 129.92 128.80 2.60 o -1 -13 1 185.29 186.84 3.57 o 0 -13 1 175.83 174.42 4.66 o 1 -13 1 89.90 85.30 3.19 o 2 -13 1 10.07 9.74 0.88 o 3 -13 1 77.66 83.53 2.64 o 4 -13 1 160.39 158.62 8.58 o -5 -12 1 31.96 36.14 2.10 o -4 -12 1 16.87 17.54 1.22 o -3 -12 1 23.89 21.61 1.13 o -2 -12 1 42.31 37.34 1.18 o -1 -12 1 4.56 5.86 0.63 o 0 -12 1 568.17 560.65 10.80 o 1 -12 1 57.31 55.51 2.21 o 2 -12 1 142.57 143.77 3.80 o 3 -12 1 190.00 193.20 4.62 o 4 -12 1 167.99 157.70 4.36 o 5 -12 1 18.93 16.99 1.39 o -5 -11 1 32.52 35.18 2.22 o -4 -11 1 383.60 379.12 6.62 o -3 -11 1 188.73 202.71 3.82 o -2 -11 1 125.44 119.48 2.90 o -1 -11 1 107.09 111.16 3.16 o 0 -11 1 708.49 695.95 13.44 o 1 -11 1 871.23 879.94 16.91 o 2 -11 1 2.62 4.27 0.63 o 3 -11 1 63.02 67.19 2.29 o 4 -11 1 31.43 33.80 1.85 o 5 -11 1 6.96 5.06 0.95 o -5 -10 1 10.57 10.21 1.10 o -4 -10 1 23.63 21.89 1.26 o -3 -10 1 169.94 166.07 3.27 o -2 -10 1 627.78 656.65 12.20 o -1 -10 1 271.34 286.59 4.75 o 0 -10 1 613.85 628.55 12.09 o 1 -10 1 119.90 113.17 1.84 o 2 -10 1 53.93 55.09 1.74 o 3 -10 1 118.56 115.27 5.09 o 4 -10 1 122.38 121.48 3.56 o 5 -10 1 85.59 89.39 3.18 o -6 -9 1 35.54 36.81 1.97 o -5 -9 1 143.57 153.92 3.55 o -4 -9 1 67.71 65.87 1.94 o -3 -9 1 68.17 65.30 2.15 o -2 -9 1 367.85 365.20 8.45 o -1 -9 1 1051.62 1080.08 15.91 o 0 -9 1 22.84 22.62 1.21 o 1 -9 1 6.07 8.69 0.43 o 2 -9 1 98.94 96.02 2.47 o 3 -9 1 35.54 31.31 1.50 o 4 -9 1 27.98 24.41 1.56 o 5 -9 1 65.68 65.10 2.67 o -6 -8 1 31.85 34.04 1.90 o -5 -8 1 11.35 7.95 1.01 o -4 -8 1 74.65 68.42 1.96 o -3 -8 1 112.83 110.02 3.49 o -2 -8 1 249.24 274.70 7.50 o -1 -8 1 220.53 245.16 4.08 o 0 -8 1 529.49 573.08 10.88 o 1 -8 1 551.71 533.60 6.93 o 2 -8 1 768.25 771.70 14.32 o 3 -8 1 826.05 819.19 15.28 o 4 -8 1 84.68 82.26 3.25 o 5 -8 1 22.57 21.46 1.68 o 6 -8 1 86.19 92.60 2.90 o -6 -7 1 1.83 1.18 0.91 o -5 -7 1 73.08 72.65 2.56 o -4 -7 1 185.04 176.31 3.53 o -3 -7 1 49.41 44.14 1.25 o -2 -7 1 290.83 292.46 5.27 o -1 -7 1 581.64 637.46 9.52 o 0 -7 1 600.04 704.46 13.05 o 1 -7 1 561.31 598.22 7.71 o 2 -7 1 204.86 210.32 4.43 o 3 -7 1 99.06 111.07 2.28 o 4 -7 1 25.29 25.61 1.47 o 5 -7 1 38.39 41.18 2.02 o 6 -7 1 61.31 66.07 2.40 o -6 -6 1 78.13 80.26 2.52 o -5 -6 1 73.77 68.09 2.15 o -4 -6 1 80.79 86.39 1.86 o -3 -6 1 36.47 33.95 0.90 o -2 -6 1 113.53 143.51 2.65 o -1 -6 1 399.81 471.96 7.11 o 0 -6 1 1494.94 1678.73 29.69 o 1 -6 1 969.40 1054.99 15.25 o 2 -6 1 1187.56 1291.35 18.51 o 3 -6 1 539.36 563.83 7.35 o 4 -6 1 29.70 28.91 1.25 o 5 -6 1 19.07 16.66 1.66 o 6 -6 1 104.11 105.46 3.02 o -6 -5 1 28.86 31.03 1.72 o -5 -5 1 33.74 28.22 1.22 o -4 -5 1 330.11 319.04 4.72 o -3 -5 1 32.00 36.31 0.84 o -2 -5 1 1042.50 1145.43 16.13 o -1 -5 1 160.95 184.79 2.21 o 0 -5 1 1226.94 1378.48 24.41 o 1 -5 1 300.11 309.39 4.70 o 2 -5 1 18.36 16.64 0.54 o 3 -5 1 36.68 40.77 1.02 o 4 -5 1 75.52 77.61 1.97 o 5 -5 1 55.87 56.13 1.84 o 6 -5 1 153.74 151.78 3.68 o -6 -4 1 2.21 1.60 0.65 o -5 -4 1 135.54 127.59 2.54 o -4 -4 1 127.35 131.60 2.12 o -3 -4 1 53.46 57.91 1.12 o -2 -4 1 997.39 1046.98 12.97 o -1 -4 1 548.21 560.20 5.66 o 0 -4 1 913.89 1001.07 16.81 o 1 -4 1 432.71 471.90 5.86 o 2 -4 1 121.93 137.89 2.09 o 3 -4 1 69.33 62.34 1.30 o 4 -4 1 212.88 204.00 3.27 o 5 -4 1 144.47 144.34 3.16 o 6 -4 1 12.07 14.38 1.10 o -6 -3 1 316.58 327.39 6.01 o -5 -3 1 284.99 276.96 3.92 o -4 -3 1 294.72 285.57 3.84 o -3 -3 1 2.05 2.41 0.30 o -2 -3 1 392.89 387.10 5.07 o -1 -3 1 146.32 149.38 1.60 o 0 -3 1 2210.81 2445.47 34.01 o 1 -3 1 1445.24 1479.08 17.92 o 2 -3 1 304.11 327.61 4.33 o 3 -3 1 280.56 298.47 4.17 o 4 -3 1 79.35 77.25 1.64 o 5 -3 1 334.31 321.57 4.36 o 6 -3 1 47.76 50.88 1.68 o -6 -2 1 126.38 130.52 4.02 o -5 -2 1 85.88 87.76 1.76 o -4 -2 1 105.15 106.76 1.81 o -3 -2 1 594.29 630.65 9.41 o -2 -2 1 1966.61 2043.04 22.07 o -1 -2 1 998.41 1012.65 9.98 o 0 -2 1 1203.45 1261.45 19.56 o 1 -2 1 3100.64 3070.23 36.45 o 2 -2 1 1106.91 1141.25 14.13 o 3 -2 1 45.10 40.25 0.99 o 4 -2 1 150.17 133.47 2.36 o 5 -2 1 143.40 143.91 2.42 o 6 -2 1 54.33 57.19 1.79 o -6 -1 1 28.66 32.65 1.23 o -5 -1 1 215.60 212.38 3.15 o -4 -1 1 55.81 50.87 1.18 o -3 -1 1 481.41 498.24 6.59 o -2 -1 1 90.64 106.47 1.59 o -1 -1 1 23.43 25.69 0.57 o 0 -1 1 1354.07 1273.38 19.40 o 1 -1 1 1273.96 1244.41 14.95 o 2 -1 1 32.89 36.37 0.80 o 3 -1 1 426.37 403.63 5.41 o 4 -1 1 43.79 44.46 1.19 o 5 -1 1 29.81 27.86 1.01 o 6 -1 1 32.51 33.64 1.39 o -6 0 1 67.98 71.55 2.22 o -5 0 1 695.75 699.81 9.14 o -4 0 1 276.82 269.89 3.68 o -3 0 1 90.85 84.61 1.52 o -2 0 1 0.80 1.98 0.21 o -1 0 1 3257.27 3261.85 49.95 o 0 0 1 54.69 52.09 0.87 o 1 0 1 3589.51 3363.25 46.34 o 2 0 1 421.18 481.75 7.08 o 3 0 1 259.52 244.32 3.69 o 4 0 1 290.24 279.33 4.14 o 5 0 1 1.38 1.36 0.47 o 6 0 1 2.75 1.54 0.58 o -6 1 1 27.64 30.21 1.53 o -5 1 1 211.28 212.02 3.13 o -4 1 1 56.92 51.34 1.13 o -3 1 1 481.62 491.92 5.79 o -2 1 1 95.23 110.40 1.47 o -1 1 1 21.63 24.31 0.45 o 0 1 1 1347.13 1260.67 13.58 o 1 1 1 1271.35 1205.43 23.05 o 2 1 1 32.67 33.98 0.87 o 3 1 1 424.41 404.97 6.25 o 4 1 1 43.75 45.51 1.09 o 5 1 1 29.68 26.72 0.97 o 6 1 1 34.46 33.87 1.36 o -6 2 1 126.96 127.53 4.19 o -5 2 1 87.41 89.31 1.84 o -4 2 1 108.67 110.73 1.79 o -3 2 1 591.30 639.30 7.28 o -2 2 1 1957.08 2025.92 24.52 o -1 2 1 980.85 1005.69 10.91 o 0 2 1 1230.61 1262.52 22.67 o 1 2 1 3116.24 2985.07 97.23 o 2 2 1 1134.09 1160.81 19.85 o 3 2 1 42.89 38.32 1.15 o 4 2 1 147.48 132.55 2.08 o 5 2 1 139.77 142.14 2.55 o 6 2 1 53.93 60.00 1.77 o -6 3 1 321.32 331.13 11.42 o -5 3 1 290.06 292.07 5.42 o -4 3 1 303.23 298.39 4.23 o -3 3 1 2.61 3.14 0.37 o -2 3 1 393.97 394.07 5.03 o -1 3 1 146.06 149.02 1.94 o 0 3 1 2195.12 2381.03 44.75 o 1 3 1 1439.97 1491.29 38.07 o 2 3 1 303.34 328.85 4.29 o 3 3 1 277.59 300.54 4.62 o 4 3 1 76.86 76.31 1.97 o 5 3 1 328.81 316.31 4.84 o 6 3 1 46.32 45.90 2.30 o -6 4 1 2.26 2.51 0.95 o -5 4 1 134.16 127.86 3.44 o -4 4 1 130.88 137.52 2.06 o -3 4 1 56.67 65.25 1.73 o -2 4 1 995.98 1061.73 12.84 o -1 4 1 541.28 560.48 6.80 o 1 4 1 414.92 464.46 7.99 o 2 4 1 131.71 148.47 2.32 o 3 4 1 72.81 66.20 1.33 o 4 4 1 213.92 211.83 3.29 o 5 4 1 139.62 137.73 2.63 o 6 4 1 13.06 16.21 1.55 o -6 5 1 27.23 28.16 1.99 o -5 5 1 32.33 27.08 3.56 o 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110.85 2.76 o -2 8 1 254.88 277.88 4.24 o -1 8 1 229.08 251.64 4.55 o 1 8 1 543.33 540.77 7.62 o 2 8 1 754.24 798.73 19.69 o 3 8 1 815.64 831.64 14.87 o 4 8 1 81.58 79.16 2.51 o 5 8 1 20.87 16.57 2.08 o 6 8 1 87.90 94.78 3.42 o -6 9 1 35.67 36.64 2.16 o -5 9 1 140.09 147.82 4.15 o -4 9 1 63.43 58.69 2.20 o -3 9 1 63.76 58.65 3.25 o -2 9 1 368.15 366.28 5.47 o -1 9 1 1053.89 1096.55 18.64 o 1 9 1 6.35 9.81 0.61 o 2 9 1 99.06 100.10 5.27 o 3 9 1 36.64 32.30 1.38 o 4 9 1 28.46 26.51 1.47 o 5 9 1 66.10 67.56 2.58 o -5 10 1 10.77 9.15 1.96 o -4 10 1 22.73 19.43 1.41 o -3 10 1 170.20 165.98 3.80 o -2 10 1 634.27 657.96 14.96 o -1 10 1 272.14 288.62 5.29 o 1 10 1 114.11 109.00 2.34 o 2 10 1 50.18 53.01 1.59 o 3 10 1 117.91 115.99 2.94 o 4 10 1 125.97 123.85 3.37 o 5 10 1 86.91 85.46 2.98 o -5 11 1 32.46 33.72 1.94 o -4 11 1 385.24 372.92 7.75 o -3 11 1 185.10 201.65 6.80 o -2 11 1 126.43 122.11 2.67 o -1 11 1 109.69 111.94 3.43 o 1 11 1 874.41 919.07 21.95 o 2 11 1 2.61 4.54 0.56 o 3 11 1 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212.27 3.35 o 0 -6 9 55.17 53.47 1.65 o 1 -6 9 1.61 1.23 1.41 o 2 -6 9 203.19 211.01 5.15 o 3 -6 9 227.59 240.92 5.80 o 4 -6 9 60.31 63.87 5.27 o -5 -5 9 25.74 27.59 5.39 o -4 -5 9 48.66 50.95 1.81 o -3 -5 9 43.71 44.60 2.25 o -2 -5 9 204.83 202.98 3.82 o -1 -5 9 539.35 514.39 7.02 o 0 -5 9 40.68 38.88 1.18 o 1 -5 9 77.23 78.70 2.02 o 2 -5 9 196.91 203.29 4.98 o 3 -5 9 77.36 73.61 2.81 o 4 -5 9 61.15 60.79 2.72 o -5 -4 9 28.58 28.77 1.65 o -4 -4 9 209.28 218.63 8.44 o -3 -4 9 84.28 80.22 3.13 o -2 -4 9 169.44 167.83 2.85 o -1 -4 9 111.43 106.67 2.09 o 0 -4 9 229.64 223.75 3.46 o 1 -4 9 368.00 362.66 5.22 o 2 -4 9 96.48 90.13 1.94 o 3 -4 9 138.23 133.20 3.90 o 4 -4 9 40.70 41.56 2.25 o -5 -3 9 30.25 27.75 1.63 o -4 -3 9 130.55 129.52 3.02 o -3 -3 9 254.97 244.43 3.89 o -2 -3 9 93.97 92.26 1.88 o -1 -3 9 20.06 21.42 1.15 o 0 -3 9 203.21 192.79 3.09 o 1 -3 9 47.29 51.40 1.53 o 2 -3 9 37.63 36.24 1.32 o 3 -3 9 31.54 31.45 1.31 o 4 -3 9 88.00 81.86 5.58 o -6 -2 9 29.91 34.94 3.43 o -5 -2 9 82.50 87.40 2.52 o -4 -2 9 160.00 152.90 2.90 o -3 -2 9 119.74 102.16 2.13 o -2 -2 9 347.97 333.04 4.90 o -1 -2 9 254.42 231.71 3.59 o 0 -2 9 565.99 538.27 7.19 o 1 -2 9 232.94 232.73 4.10 o 2 -2 9 20.85 22.92 1.13 o 3 -2 9 34.05 28.99 1.60 o 4 -2 9 15.85 15.02 1.23 o -6 -1 9 87.43 93.86 3.51 o -5 -1 9 27.02 30.00 1.89 o -4 -1 9 56.76 55.17 1.59 o -3 -1 9 9.94 9.16 1.06 o -2 -1 9 161.52 153.93 3.59 o -1 -1 9 25.39 27.85 0.95 o 0 -1 9 36.33 34.79 1.19 o 1 -1 9 141.99 132.85 2.74 o 2 -1 9 32.70 32.51 1.30 o 3 -1 9 58.18 56.17 1.79 o 4 -1 9 90.48 88.73 2.20 o -6 0 9 25.00 28.33 2.64 o -5 0 9 3.72 4.06 1.16 o -4 0 9 0.21 2.49 0.57 o -3 0 9 85.75 98.91 2.07 o -2 0 9 90.10 89.50 1.84 o -1 0 9 334.56 300.19 4.40 o 0 0 9 397.05 372.63 5.27 o 1 0 9 378.66 348.59 5.80 o 2 0 9 82.77 79.04 2.05 o 3 0 9 55.49 55.33 1.79 o 4 0 9 19.54 27.07 1.55 o -6 1 9 89.78 95.61 6.74 o -5 1 9 26.41 31.06 1.93 o -4 1 9 55.41 54.09 1.57 o -3 1 9 9.43 8.31 0.72 o -2 1 9 161.86 153.19 2.67 o -1 1 9 25.47 28.69 1.06 o 0 1 9 36.20 35.25 1.25 o 1 1 9 140.42 132.75 2.76 o 2 1 9 34.33 34.56 1.32 o 3 1 9 60.47 55.50 1.79 o 4 1 9 89.19 92.66 2.55 o -5 2 9 80.48 84.59 2.50 o -4 2 9 162.76 148.55 3.30 o -3 2 9 121.31 104.16 2.13 o -2 2 9 356.89 342.48 4.90 o -1 2 9 249.05 234.47 3.59 o 0 2 9 550.49 525.79 8.28 o 1 2 9 225.33 221.64 4.10 o 2 2 9 18.34 21.99 1.13 o 3 2 9 37.02 33.82 1.39 o 4 2 9 17.15 16.62 1.56 o -5 3 9 28.28 25.85 1.55 o -4 3 9 128.86 127.40 3.00 o -3 3 9 251.89 244.76 7.96 o -2 3 9 93.45 93.48 1.91 o -1 3 9 19.97 20.13 1.31 o 0 3 9 203.52 196.78 3.61 o 1 3 9 47.09 49.45 1.53 o 2 3 9 38.71 36.03 1.53 o 3 3 9 33.10 34.19 1.78 o 4 3 9 87.94 79.48 2.95 o -5 4 9 29.78 27.79 1.86 o -4 4 9 211.12 216.45 5.47 o -3 4 9 80.04 79.94 2.15 o -2 4 9 174.71 171.44 3.35 o -1 4 9 114.25 110.51 2.27 o 0 4 9 227.90 220.81 3.99 o 1 4 9 368.42 362.60 6.04 o 2 4 9 93.05 86.08 2.77 o 3 4 9 134.82 131.38 3.77 o 4 4 9 40.20 38.91 2.08 o -5 5 9 26.08 25.15 3.25 o -4 5 9 49.99 52.98 2.70 o -3 5 9 43.52 45.97 1.95 o -2 5 9 206.82 198.06 3.77 o -1 5 9 540.80 522.52 8.14 o 0 5 9 40.33 39.48 1.65 o 1 5 9 77.94 78.98 2.51 o 2 5 9 197.95 199.27 4.86 o 3 5 9 80.17 75.23 2.69 o 4 5 9 58.14 57.20 2.51 o -5 6 9 60.08 66.17 5.70 o -4 6 9 59.52 56.41 2.34 o -3 6 9 102.63 94.82 2.94 o -2 6 9 618.73 579.38 11.10 o -1 6 9 228.17 216.15 4.90 o 0 6 9 53.77 55.58 3.07 o 1 6 9 2.44 2.39 0.69 o 2 6 9 202.93 208.37 7.17 o 3 6 9 223.81 218.11 5.50 o 4 6 9 59.80 65.40 2.73 o -5 7 9 38.81 39.90 3.62 o -4 7 9 21.93 20.48 2.21 o -3 7 9 53.67 51.12 2.12 o -2 7 9 76.95 71.44 2.38 o -1 7 9 74.05 69.49 2.30 o 0 7 9 1.51 1.41 0.61 o 1 7 9 176.30 173.12 4.33 o 2 7 9 158.29 154.43 4.07 o 3 7 9 84.56 84.72 2.95 o 4 7 9 82.87 80.36 3.08 o -5 8 9 62.57 60.58 2.63 o -4 8 9 90.42 87.58 3.07 o -3 8 9 25.51 27.75 1.84 o -2 8 9 1.91 0.54 0.56 o -1 8 9 104.76 94.11 4.17 o 0 8 9 124.53 125.99 3.38 o 1 8 9 167.32 171.63 4.33 o 2 8 9 195.03 189.90 4.77 o 3 8 9 5.08 5.74 0.99 o 4 8 9 141.96 137.47 4.20 o -4 9 9 52.99 52.86 3.25 o -3 9 9 25.58 26.45 1.56 o -2 9 9 116.92 118.92 3.92 o -1 9 9 70.48 69.31 2.38 o 0 9 9 31.86 29.46 1.52 o 1 9 9 34.39 32.29 1.69 o 2 9 9 55.32 48.85 2.45 o 3 9 9 87.52 83.75 3.86 o -4 10 9 2.16 1.54 1.04 o -3 10 9 68.30 65.00 3.62 o -2 10 9 66.74 63.91 2.34 o -1 10 9 115.25 110.26 3.16 o 0 10 9 52.43 50.36 2.08 o 1 10 9 137.12 137.61 5.70 o 2 10 9 230.75 223.94 5.42 o 3 10 9 21.25 22.74 1.73 o -4 11 9 31.32 32.17 1.86 o -3 11 9 11.12 11.10 1.20 o -2 11 9 39.20 40.65 1.85 o -1 11 9 16.86 16.04 1.25 o 0 11 9 132.29 135.74 3.64 o 1 11 9 69.42 63.09 2.34 o 2 11 9 8.33 7.97 1.08 o 3 11 9 19.41 25.13 1.86 o -3 12 9 3.25 1.53 0.78 o -2 12 9 175.81 158.11 4.20 o -1 12 9 231.59 227.13 5.29 o 0 12 9 167.44 172.62 4.29 o 1 12 9 162.05 158.62 4.23 o 2 12 9 121.90 125.66 3.73 o -2 13 9 32.14 32.74 1.73 o -1 13 9 149.34 149.62 7.54 o 0 13 9 35.11 36.33 1.78 o 1 13 9 3.93 5.50 0.94 o -1 14 9 63.30 59.31 2.25 o 0 14 9 194.60 189.99 4.72 o -1 -13 10 16.41 18.41 1.90 o 0 -13 10 58.97 63.63 3.56 o -2 -12 10 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288.05 5.17 o 3 0 10 72.51 72.21 2.15 o 4 0 10 87.04 90.50 2.59 o -5 1 10 27.43 26.24 1.58 o -4 1 10 23.16 27.55 1.43 o -3 1 10 17.92 22.56 1.26 o -2 1 10 9.18 10.98 0.76 o -1 1 10 23.73 22.87 0.95 o 0 1 10 203.66 200.10 4.39 o 1 1 10 89.60 87.13 2.22 o 2 1 10 6.81 4.55 0.71 o 3 1 10 2.78 2.76 0.68 o 4 1 10 74.48 77.19 3.13 o -5 2 10 3.47 5.84 1.06 o -4 2 10 43.65 44.79 1.72 o -3 2 10 43.76 36.00 1.92 o -2 2 10 110.95 108.18 2.21 o -1 2 10 69.97 67.58 1.61 o 0 2 10 66.69 66.29 1.84 o 1 2 10 53.38 53.38 1.67 o 2 2 10 109.79 110.63 4.08 o 3 2 10 12.76 10.47 1.21 o 4 2 10 76.38 72.46 2.90 o -5 3 10 35.93 36.43 5.21 o -4 3 10 25.08 23.34 1.43 o -3 3 10 151.01 143.58 3.61 o -2 3 10 75.04 67.87 1.96 o -1 3 10 91.52 85.70 1.87 o 0 3 10 191.88 193.24 4.25 o 1 3 10 99.47 94.06 2.33 o 2 3 10 28.84 30.11 1.65 o 3 3 10 46.86 46.66 2.17 o 4 3 10 0.00 0.37 0.78 o -5 4 10 94.32 98.21 3.46 o -4 4 10 75.50 78.92 2.86 o -3 4 10 13.83 15.86 1.13 o -2 4 10 205.30 200.52 4.55 o -1 4 10 208.78 202.98 3.84 o 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