#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:29:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181244 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232248.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232248_Fobs loop_ _publ_author_name 'Nistor, Alexandra' 'Shova, Sergiu' 'Cazacu, Maria' 'Lazar, Alina' _publ_section_title ; Hexakis(1H-imidazole-\kN^3^)iron(II) sulfate--1H-imidazole (1/2) ; _journal_coeditor_code GK2405 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1600 _journal_page_last m1601 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.813 _cell_angle_beta 69.949 _cell_angle_gamma 73.214 _cell_length_a 15.4091 _cell_length_b 15.4436 _cell_length_c 15.9883 _exptl_crystal_F_000 1448.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file gk2405Isup3.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' new' _shelx_refln_list_code 4 _shelx_f_calc_maximum 462.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6.04 110.83 27.09 o 3 0 0 30.73 24.28 10.90 o 4 0 0 212810.53 208760.42 1031.89 o 5 0 0 92.01 69.98 27.49 o 6 0 0 2879.73 2706.48 145.90 o 7 0 0 122.33 135.19 29.46 o 8 0 0 9664.00 9365.98 318.42 o 9 0 0 198.37 174.52 59.30 o 10 0 0 1660.21 1869.32 201.22 o 11 0 0 314.54 391.42 208.80 o 12 0 0 3346.85 3329.74 522.11 o 13 0 0 134.66 44.47 89.16 o 14 0 0 60.88 47.40 23.93 o 15 0 0 80.99 47.18 62.75 o 16 0 0 677.21 741.07 307.44 o -16 1 0 36.01 69.52 120.31 o -15 1 0 163.06 0.00 157.79 o -14 1 0 203.61 218.06 150.56 o -13 1 0 31.05 0.00 98.42 o -12 1 0 2.25 0.00 148.08 o -11 1 0 210.56 146.05 81.26 o -10 1 0 32.34 0.00 96.39 o -9 1 0 677.70 662.54 113.80 o -8 1 0 12.66 23.00 34.00 o -7 1 0 6680.81 6988.36 240.95 o -6 1 0 82.13 66.27 22.59 o -5 1 0 65.22 28.05 14.11 o -4 1 0 101.37 66.22 34.35 o -3 1 0 13378.61 12780.43 175.20 o -2 1 0 1.32 10.84 19.41 o 3 1 0 38.49 19.65 14.95 o 4 1 0 674.59 663.34 53.04 o 5 1 0 9.78 160.51 30.64 o 6 1 0 44.94 24.42 21.63 o 7 1 0 2398.55 2376.33 154.11 o 8 1 0 99.89 82.02 37.73 o 9 1 0 319.82 619.08 122.59 o 10 1 0 6.59 21.43 27.17 o 11 1 0 696.53 734.37 143.90 o 12 1 0 659.55 828.65 278.78 o 13 1 0 484.25 560.49 216.70 o 14 1 0 265.55 221.67 128.89 o 15 1 0 33.59 8.80 100.22 o 16 1 0 248.43 291.87 186.00 o 17 1 0 19.98 97.74 124.38 o -16 2 0 13.95 41.08 87.58 o -15 2 0 105.68 74.27 115.35 o -14 2 0 2489.11 2140.82 487.80 o -13 2 0 812.26 754.16 259.82 o -12 2 0 0.36 83.29 96.84 o -11 2 0 42.89 77.65 86.68 o -10 2 0 9133.90 10524.88 355.73 o -9 2 0 79.26 60.59 83.75 o -8 2 0 16.27 27.19 25.73 o -7 2 0 241.34 278.56 59.45 o -6 2 0 20733.24 21346.12 644.01 o -5 2 0 117.81 118.27 30.34 o -4 2 0 1287.69 1271.78 74.79 o -3 2 0 32.82 65.84 24.91 o -2 2 0 13723.25 14118.65 340.16 o -1 2 0 336.96 316.92 60.04 o 0 2 0 184.80 165.69 33.18 o 1 2 0 130.00 129.79 28.67 o 2 2 0 26113.60 27982.94 280.61 o 3 2 0 784.34 795.17 54.91 o 4 2 0 463.00 416.02 45.78 o 5 2 0 741.21 680.74 56.48 o 6 2 0 17140.57 17598.93 411.76 o 7 2 0 16.81 0.00 10.73 o 8 2 0 793.10 905.38 130.99 o 9 2 0 32.32 0.00 26.33 o 10 2 0 5829.74 5881.95 386.98 o 11 2 0 368.30 564.48 129.85 o 12 2 0 172.90 170.85 62.75 o 13 2 0 6.28 100.68 145.14 o 14 2 0 2630.13 3221.84 578.09 o 15 2 0 44.65 0.00 129.79 o 16 2 0 4.34 0.00 86.00 o 17 2 0 110.93 140.40 110.61 o -16 3 0 24.73 110.83 88.94 o -15 3 0 127.12 258.46 198.87 o -14 3 0 1.94 60.95 79.46 o -13 3 0 293.17 586.67 259.36 o -12 3 0 47.78 42.21 53.50 o -11 3 0 1039.80 1062.29 305.19 o -10 3 0 67.72 67.57 28.67 o -9 3 0 31.73 21.32 27.89 o -8 3 0 55.55 37.24 25.17 o -7 3 0 2454.69 2565.07 158.04 o -6 3 0 128.67 134.26 30.46 o -5 3 0 736.36 868.16 175.84 o -4 3 0 428.90 518.72 89.86 o -3 3 0 2.46 0.00 19.20 o -2 3 0 129.18 124.89 37.21 o -1 3 0 173046.56 174524.83 1037.65 o 0 3 0 243.23 232.00 21.81 o 1 3 0 497.28 381.72 30.07 o 2 3 0 297.53 293.07 29.90 o 3 3 0 177522.23 182089.53 985.62 o 4 3 0 343.12 271.74 36.27 o 5 3 0 267.40 228.90 39.51 o 6 3 0 1153.86 1120.10 106.22 o 7 3 0 1190.33 1110.08 137.66 o 8 3 0 431.99 501.61 100.33 o 9 3 0 506.20 452.67 102.64 o 10 3 0 636.10 744.39 140.39 o 11 3 0 169.18 192.17 70.44 o 12 3 0 0.09 19.51 37.20 o 13 3 0 25.09 123.25 154.85 o 14 3 0 11.97 166.59 180.81 o 15 3 0 135.15 379.00 234.31 o 16 3 0 1.62 0.00 92.78 o 17 3 0 2.98 0.00 188.48 o -15 4 0 276.66 230.70 211.51 o -14 4 0 42.86 0.00 117.38 o -13 4 0 38.91 110.16 157.79 o -12 4 0 2843.39 2829.53 529.79 o -11 4 0 757.39 729.56 241.08 o -10 4 0 701.07 585.09 215.35 o -9 4 0 128.32 168.85 132.50 o -8 4 0 4665.26 4762.68 548.52 o -7 4 0 13.82 12.42 16.70 o -6 4 0 793.37 857.77 200.00 o -5 4 0 14.29 41.99 65.01 o -4 4 0 2783.69 2472.20 201.88 o -3 4 0 22.93 32.68 46.16 o -2 4 0 71.24 73.26 17.64 o -1 4 0 387.84 404.28 34.54 o 0 4 0 17662.99 17776.70 239.51 o 1 4 0 34.59 42.82 12.59 o 2 4 0 240.32 197.08 26.57 o 3 4 0 1727.59 1656.88 87.67 o 4 4 0 61961.54 62221.14 600.68 o 5 4 0 306.81 275.31 52.08 o 6 4 0 1612.37 1560.29 158.91 o 7 4 0 612.94 561.12 80.14 o 8 4 0 14172.80 12758.27 529.05 o 9 4 0 180.40 149.85 56.24 o 10 4 0 672.13 760.58 145.09 o 11 4 0 520.25 684.41 149.33 o 12 4 0 622.06 561.94 135.85 o 13 4 0 20.31 50.45 30.12 o 14 4 0 40.03 106.77 111.06 o 15 4 0 590.56 618.27 269.97 o 16 4 0 163.03 134.76 174.04 o 17 4 0 36.41 0.00 154.63 o -15 5 0 14.01 0.00 36.34 o -14 5 0 47.81 219.41 155.08 o -13 5 0 3.32 0.00 100.45 o -12 5 0 117.68 246.27 176.52 o -11 5 0 47.81 132.28 127.76 o -10 5 0 46.86 124.83 109.25 o -9 5 0 27.64 12.19 70.88 o -8 5 0 57.06 119.64 87.13 o -7 5 0 430.82 658.68 206.77 o -6 5 0 75.92 146.72 102.48 o -5 5 0 4.92 18.06 50.79 o -4 5 0 290.01 227.08 101.13 o -3 5 0 367.59 440.01 83.55 o -2 5 0 336.37 335.26 40.79 o -1 5 0 0.55 4.40 10.72 o 0 5 0 2.95 8.21 10.66 o 1 5 0 1105.67 1365.11 73.82 o 2 5 0 200.69 228.88 30.15 o 3 5 0 460.21 524.67 51.06 o 4 5 0 1219.76 1122.97 92.57 o 5 5 0 8194.57 8601.51 283.92 o 6 5 0 13.58 14.54 12.11 o 7 5 0 13.59 2.37 19.30 o 8 5 0 1112.32 1157.61 126.38 o 9 5 0 608.23 661.12 126.00 o 10 5 0 164.82 177.06 67.62 o 11 5 0 301.69 331.79 100.09 o 12 5 0 17.00 16.82 17.15 o 13 5 0 7.31 44.37 65.01 o 14 5 0 92.79 219.41 193.45 o 15 5 0 75.53 289.61 201.35 o 16 5 0 16.82 114.45 121.67 o 17 5 0 10.97 99.10 168.62 o -14 6 0 312.94 215.57 177.42 o -13 6 0 73.65 104.96 143.56 o -12 6 0 34.37 156.21 146.72 o -11 6 0 21.39 115.57 95.71 o -10 6 0 1677.23 2224.12 437.69 o -9 6 0 351.73 540.62 210.38 o -8 6 0 513.60 534.75 195.48 o -7 6 0 139.53 161.40 112.86 o -6 6 0 3490.13 4019.12 457.10 o -5 6 0 136.31 206.32 100.90 o -4 6 0 119.24 198.42 90.29 o -3 6 0 4.02 7.83 9.24 o -2 6 0 657.03 579.23 60.53 o -1 6 0 6.91 17.00 17.36 o 0 6 0 132.22 147.10 22.79 o 1 6 0 240.93 239.03 32.42 o 2 6 0 15449.53 15491.38 276.10 o 3 6 0 58.38 35.69 20.22 o 4 6 0 7.17 7.67 13.85 o 5 6 0 1196.12 1170.73 107.61 o 6 6 0 4692.00 4390.50 280.74 o 7 6 0 224.13 168.22 57.04 o 8 6 0 7.40 55.55 41.38 o 9 6 0 2082.57 2192.60 236.05 o 10 6 0 2068.46 2147.41 249.67 o 11 6 0 13.54 10.45 32.39 o 12 6 0 16.95 33.99 31.94 o 13 6 0 100.12 51.50 36.41 o 14 6 0 2123.87 2190.83 312.57 o 15 6 0 0.14 89.16 117.61 o 16 6 0 4.55 65.24 115.57 o -14 7 0 20.37 0.00 114.90 o -13 7 0 97.88 139.05 151.69 o -12 7 0 257.46 418.73 212.19 o -11 7 0 839.41 937.46 300.45 o -10 7 0 220.85 361.39 178.55 o -9 7 0 459.85 786.89 254.17 o -8 7 0 83.32 13.77 34.76 o -7 7 0 2414.39 2377.16 374.71 o -6 7 0 312.09 496.38 181.94 o -5 7 0 5.00 47.18 76.30 o -4 7 0 81.53 98.19 54.85 o -3 7 0 972.82 984.86 92.61 o -2 7 0 38.78 41.99 18.04 o -1 7 0 244.29 350.63 43.11 o 0 7 0 121.28 128.42 27.90 o 1 7 0 578.22 575.60 57.51 o 2 7 0 41.36 33.08 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o -7 11 0 729.85 774.71 223.47 o -6 11 0 0.03 0.00 110.61 o -5 11 0 238.56 125.96 92.10 o -4 11 0 81.72 165.46 90.97 o -3 11 0 2837.14 2945.78 361.85 o -2 11 0 174.55 118.53 50.81 o -1 11 0 434.79 389.84 107.90 o 0 11 0 1.22 0.00 46.95 o 1 11 0 1454.05 1432.03 190.29 o 2 11 0 12.34 5.45 12.79 o 3 11 0 1196.62 1118.86 140.31 o 4 11 0 1.30 0.00 13.54 o 5 11 0 403.69 317.89 80.78 o 6 11 0 42.89 49.71 35.12 o 7 11 0 54.91 4.73 29.02 o 8 11 0 183.35 143.48 56.26 o 9 11 0 731.09 844.99 164.24 o 10 11 0 152.22 186.22 63.74 o 11 11 0 268.72 259.49 83.86 o 12 11 0 6.42 0.00 53.01 o 13 11 0 198.05 149.42 67.44 o 14 11 0 353.04 514.89 211.28 o 15 11 0 429.64 573.35 235.89 o -9 12 0 1.50 0.00 85.33 o -8 12 0 1761.88 1371.54 318.73 o -7 12 0 2.89 0.00 51.92 o -6 12 0 32.54 81.71 110.16 o -5 12 0 12.90 69.07 81.04 o -4 12 0 7172.67 7096.27 606.54 o -3 12 0 1.87 3.84 46.50 o -2 12 0 474.25 429.79 125.51 o -1 12 0 522.83 612.41 133.41 o 0 12 0 3285.84 3631.77 330.02 o 1 12 0 39.60 51.24 31.83 o 2 12 0 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116.87 78.53 o 0 9 17 127.95 88.03 88.49 o 1 9 17 18.98 79.01 79.46 o 2 9 17 102.85 160.27 108.35 o 3 9 17 126.50 144.47 110.38 o 4 9 17 166.95 304.51 150.34 o 5 9 17 27.99 0.00 23.02 o 6 9 17 173.53 235.89 143.11 o 7 9 17 4.40 73.81 60.95 o 8 9 17 270.12 598.96 408.12 o 9 9 17 0.93 50.52 197.29 o 10 9 17 67.60 172.75 102.71 o 11 9 17 86.34 264.88 121.94 o 12 9 17 565.63 618.83 174.41 o 13 9 17 7.07 0.00 166.81 o 3 10 17 42.01 15.80 42.66 o 4 10 17 9.17 7.67 51.01 o 5 10 17 37.50 124.60 102.48 o 6 10 17 0.29 39.28 86.91 o 7 10 17 35.51 144.86 392.43 o 8 10 17 176.21 330.80 221.78 o 9 10 17 5.76 96.66 256.54 o 10 10 17 34.65 9.24 150.90 o 11 10 17 0.33 17.86 34.91 o 12 10 17 251.96 69.42 125.05 o 5 11 17 99.37 748.29 356.43 o 6 11 17 406.89 1015.56 381.03 o 7 11 17 9.12 546.49 314.22 o 8 11 17 98.98 432.05 263.88 o 9 11 17 5.41 190.06 169.97 o 10 11 17 321.67 274.71 185.32 o 11 11 17 2.66 133.41 107.45 o 12 11 17 452.81 254.62 75.85 o 3 12 17 157.86 651.91 334.76 o 4 12 17 19.05 691.41 314.22 o 5 12 17 56.85 465.68 271.33 o 6 12 17 429.33 695.70 313.99 o 7 12 17 288.58 520.31 262.75 o 8 12 17 9.11 0.00 120.31 o 9 12 17 57.13 90.74 97.52 o 10 12 17 157.32 220.54 149.21 o 11 12 17 7.78 0.00 182.39 o 5 13 17 18.18 374.71 233.86 o 6 13 17 122.56 385.55 232.95 o 7 13 17 0.49 259.82 197.06 o 8 13 17 628.19 651.01 258.24 o 9 13 17 18.08 0.00 178.10 o 3 1 18 44.77 0.00 90.74 o 4 1 18 21.09 0.00 125.05 o 5 1 18 53.64 160.27 150.56 o 6 1 18 220.29 144.69 140.86 o 7 1 18 1.71 0.00 117.38 o 2 2 18 129.79 33.86 71.56 o 3 2 18 716.60 885.54 317.15 o 4 2 18 21.62 63.43 84.65 o 5 2 18 29.62 48.53 84.65 o 6 2 18 336.08 245.59 176.52 o 7 2 18 602.34 572.45 226.86 o 8 2 18 2.76 0.00 39.05 o 1 3 18 20.38 0.68 15.80 o 2 3 18 33.06 31.83 61.62 o 3 3 18 19.13 82.17 92.10 o 4 3 18 1042.71 1151.22 341.76 o 5 3 18 21.34 0.00 44.92 o 6 3 18 156.70 198.42 165.01 o 7 3 18 0.42 0.00 58.46 o 8 3 18 198.82 232.95 142.44 o 9 3 18 11.31 4.06 37.92 o 1 4 18 400.45 451.46 220.54 o 2 4 18 17.49 8.13 28.44 o 3 4 18 105.00 34.76 47.40 o 4 4 18 185.76 205.19 142.89 o 5 4 18 416.82 476.06 219.41 o 6 4 18 74.53 186.23 145.14 o 7 4 18 147.79 214.67 131.83 o 8 4 18 461.42 445.82 221.44 o 9 4 18 123.60 191.87 163.20 o 10 4 18 4.97 0.00 125.05 o 1 5 18 0.37 128.44 136.12 o 2 5 18 199.31 187.81 139.05 o 3 5 18 35.28 36.34 62.75 o 4 5 18 17.39 44.02 44.69 o 5 5 18 26.59 38.15 24.60 o 6 5 18 207.60 248.75 155.53 o 7 5 18 0.48 28.89 69.52 o 8 5 18 0.41 41.31 80.36 o 9 5 18 103.15 86.45 43.34 o 10 5 18 208.59 249.88 162.53 o 11 5 18 12.14 236.73 435.09 o 1 6 18 339.04 378.55 193.68 o 2 6 18 201.03 252.82 177.42 o 3 6 18 8.50 115.80 73.59 o 4 6 18 27.79 68.40 66.59 o 5 6 18 54.40 142.66 120.09 o 6 6 18 53.65 153.27 135.21 o 7 6 18 416.87 550.78 246.27 o 8 6 18 51.62 47.85 61.17 o 9 6 18 1.27 10.61 60.50 o 10 6 18 145.92 156.43 104.06 o 11 6 18 487.49 752.35 207.18 o 1 7 18 0.07 133.63 146.72 o 2 7 18 3.35 0.00 102.93 o 3 7 18 152.62 258.91 157.11 o 4 7 18 327.16 360.49 189.39 o 5 7 18 10.54 50.79 60.72 o 6 7 18 53.39 11.96 43.11 o 7 7 18 25.77 128.67 100.90 o 8 7 18 357.64 299.32 164.33 o 9 7 18 1.19 0.00 73.36 o 10 7 18 134.34 123.48 303.27 o 11 7 18 67.82 360.44 191.53 o 2 8 18 0.71 0.00 88.03 o 3 8 18 2.60 0.45 56.88 o 4 8 18 70.46 49.21 7.45 o 5 8 18 152.93 175.39 108.35 o 6 8 18 0.32 42.66 44.02 o 7 8 18 182.85 194.35 121.67 o 8 8 18 195.27 295.25 181.49 o 9 8 18 4.32 217.61 551.80 o 10 8 18 76.67 198.58 227.08 o 11 8 18 33.89 22.36 176.41 o 2 9 18 149.86 147.40 119.41 o 3 9 18 9.63 37.70 53.95 o 4 9 18 12.01 70.43 60.95 o 5 9 18 7.65 35.44 56.66 o 6 9 18 245.34 272.00 139.73 o 7 9 18 33.69 0.00 39.28 o 8 9 18 50.10 260.95 431.93 o 9 9 18 14.82 90.21 243.11 o 10 9 18 3.53 78.99 215.35 o 11 9 18 1.24 65.19 135.78 o 6 10 18 167.73 151.24 105.87 o 7 10 18 165.03 497.37 401.91 o 8 10 18 9.05 71.19 288.14 o 9 10 18 2.48 100.74 269.18 o 10 10 18 124.58 128.04 174.60 o 6 11 18 88.69 628.88 337.69 o 7 11 18 13.09 981.93 385.55 o 8 11 18 468.09 810.14 341.08 o 9 11 18 24.76 397.28 249.88 o 6 6 19 4.64 93.45 121.44 o