#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232252.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232252_Fobs loop_ _publ_author_name 'Nayak, Susanta K.' 'Venugopala, K. N.' 'Govender, Thavendran' 'Kruger, Hendrik G.' 'Maguire, Glenn E. M.' 'Row, Tayur N. Guru' _publ_section_title ; Ethyl 4-(1,3-benzodioxol-5-yl)-6-methyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate ; _journal_coeditor_code GK2420 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3069 _journal_page_last o3070 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.178 _cell_angle_gamma 90.000 _cell_length_a 12.5102 _cell_length_b 7.2054 _cell_length_c 17.0881 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file gk2420Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LTD4 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 208.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 496.24 489.70 17.66 o 3 0 0 12755.09 11932.35 293.33 o 4 0 0 4849.90 4724.26 75.13 o 5 0 0 8.63 7.44 2.19 o 6 0 0 141.36 124.54 9.70 o 7 0 0 2169.04 2236.78 67.40 o 8 0 0 135.48 141.61 20.15 o 9 0 0 56.08 65.22 11.34 o 10 0 0 3579.54 3458.09 253.18 o 11 0 0 364.82 423.74 31.78 o 12 0 0 115.06 147.62 25.66 o 13 0 0 8.53 16.37 7.01 o 14 0 0 63.31 57.53 14.02 o 1 1 0 7304.71 7776.46 45.08 o 2 1 0 140.76 137.75 4.75 o 3 1 0 8103.07 8224.90 71.55 o 4 1 0 4574.35 4434.35 51.60 o 5 1 0 730.79 661.74 23.61 o 6 1 0 627.30 639.62 18.42 o 7 1 0 91.48 71.63 5.87 o 8 1 0 975.50 843.89 23.73 o 9 1 0 16.25 18.25 3.47 o 10 1 0 1321.40 1363.51 64.10 o 11 1 0 50.43 32.11 6.76 o 12 1 0 244.95 232.05 20.24 o 13 1 0 40.28 26.79 7.71 o 14 1 0 104.92 96.60 14.91 o 0 2 0 0.80 1.16 0.97 o 1 2 0 3695.72 3767.33 27.94 o 2 2 0 369.43 376.10 9.90 o 3 2 0 3.63 4.68 1.18 o 4 2 0 5245.64 5383.28 62.59 o 5 2 0 598.49 598.52 15.10 o 6 2 0 6.04 6.59 1.67 o 7 2 0 232.90 195.88 8.98 o 8 2 0 73.77 68.53 7.85 o 9 2 0 338.57 361.81 18.52 o 10 2 0 148.63 161.54 12.76 o 11 2 0 194.96 205.44 16.79 o 12 2 0 356.18 441.00 33.80 o 13 2 0 352.03 395.40 33.71 o 14 2 0 341.96 369.60 35.00 o 1 3 0 170.67 192.28 7.22 o 2 3 0 41.13 64.54 4.61 o 3 3 0 457.07 514.82 13.55 o 4 3 0 4218.65 4361.44 43.33 o 5 3 0 828.89 806.42 21.41 o 6 3 0 1177.66 1291.33 41.50 o 7 3 0 388.36 328.49 12.95 o 8 3 0 100.64 99.79 9.14 o 9 3 0 186.25 168.14 12.25 o 10 3 0 2.73 4.34 3.73 o 11 3 0 401.09 403.06 30.52 o 12 3 0 1.60 6.57 5.67 o 13 3 0 1.43 0.00 7.69 o 0 4 0 3.08 0.00 2.56 o 1 4 0 3349.21 3347.35 35.47 o 2 4 0 553.45 658.09 15.86 o 3 4 0 396.86 356.52 12.90 o 4 4 0 537.47 574.20 16.14 o 5 4 0 175.44 191.04 10.85 o 6 4 0 630.60 681.47 21.83 o 7 4 0 174.73 167.36 10.47 o 8 4 0 262.37 256.87 15.25 o 9 4 0 822.76 851.10 32.64 o 10 4 0 147.24 143.07 13.91 o 11 4 0 671.04 693.77 35.34 o 12 4 0 272.39 309.42 28.70 o 13 4 0 75.45 95.09 17.36 o 1 5 0 718.23 702.44 18.56 o 2 5 0 2.03 0.00 1.81 o 3 5 0 112.89 115.04 7.85 o 4 5 0 287.59 259.06 14.83 o 5 5 0 14.27 16.08 3.92 o 6 5 0 418.48 379.59 20.85 o 7 5 0 2247.17 2296.62 66.64 o 8 5 0 107.09 126.27 12.78 o 9 5 0 409.74 412.79 23.40 o 10 5 0 0.01 0.00 3.66 o 11 5 0 19.52 7.58 4.04 o 12 5 0 0.34 0.00 5.37 o 0 6 0 872.23 876.11 61.04 o 1 6 0 59.02 56.34 8.92 o 2 6 0 24.44 22.30 5.22 o 3 6 0 857.95 870.38 31.21 o 4 6 0 946.55 915.16 36.52 o 5 6 0 15.53 10.29 5.05 o 6 6 0 1257.74 1243.94 53.51 o 7 6 0 167.02 177.07 15.59 o 8 6 0 129.76 117.09 15.26 o 9 6 0 0.21 1.65 3.32 o 10 6 0 10.54 8.13 5.51 o 1 7 0 64.64 45.46 11.30 o 2 7 0 246.08 215.47 23.58 o 3 7 0 1347.41 1350.76 58.73 o 4 7 0 233.18 266.85 24.36 o 5 7 0 58.03 52.75 11.90 o 6 7 0 7.22 0.27 3.79 o 7 7 0 225.30 228.11 21.73 o 8 7 0 364.00 401.85 34.83 o 9 7 0 0.17 0.00 5.01 o 0 8 0 132.33 101.25 24.61 o 1 8 0 24.79 24.89 9.12 o 2 8 0 9.27 6.46 7.67 o 3 8 0 63.92 70.25 13.72 o 4 8 0 11.17 15.58 7.99 o 5 8 0 7.70 7.74 7.61 o 6 8 0 0.15 3.42 7.38 o -14 1 1 17.57 19.79 7.28 o -13 1 1 0.35 4.23 5.62 o -12 1 1 386.00 404.12 27.12 o -11 1 1 78.57 89.51 13.18 o -10 1 1 85.29 87.00 12.28 o -9 1 1 158.81 141.86 11.49 o -8 1 1 16.82 14.16 3.76 o -7 1 1 2593.84 2531.09 71.55 o -6 1 1 139.94 111.73 8.52 o -5 1 1 1037.23 1191.55 36.73 o -4 1 1 174.28 179.86 9.25 o -3 1 1 6116.31 6247.66 178.44 o -2 1 1 53.28 45.16 3.39 o -1 1 1 6087.97 6247.60 48.47 o 0 1 1 7.11 12.65 1.60 o 1 1 1 1526.88 1721.93 17.57 o 2 1 1 7328.19 7174.78 112.12 o 3 1 1 1635.70 1669.21 19.57 o 4 1 1 364.71 381.66 10.01 o 5 1 1 223.77 223.33 9.04 o 6 1 1 1340.57 1379.33 27.60 o 7 1 1 1740.49 1712.50 52.29 o 8 1 1 747.56 775.75 25.20 o 9 1 1 102.29 89.99 7.00 o 10 1 1 25.62 32.00 5.48 o 11 1 1 327.59 326.00 23.84 o 12 1 1 133.82 126.55 13.61 o 13 1 1 64.87 58.92 13.13 o 14 1 1 26.10 19.95 7.81 o -14 2 1 36.38 51.70 13.30 o -13 2 1 28.63 36.83 12.15 o -12 2 1 7.29 8.16 7.53 o -11 2 1 654.65 607.82 35.11 o -10 2 1 1697.40 1759.82 46.87 o -9 2 1 42.74 33.63 5.76 o -8 2 1 564.23 570.69 22.09 o -7 2 1 407.52 423.98 17.66 o -6 2 1 10.04 3.27 1.85 o -5 2 1 341.35 332.50 11.70 o -4 2 1 2090.87 2063.64 27.78 o -3 2 1 141.67 121.82 7.20 o -2 2 1 104.12 109.51 5.71 o -1 2 1 5499.83 5468.16 47.71 o 0 2 1 849.91 819.24 12.04 o 1 2 1 40.84 58.19 3.62 o 2 2 1 2076.52 2061.59 23.46 o 3 2 1 2344.84 2325.29 58.41 o 4 2 1 317.27 362.04 9.30 o 5 2 1 892.03 893.59 22.50 o 6 2 1 455.59 463.20 14.91 o 7 2 1 20.04 19.65 3.14 o 8 2 1 40.35 34.35 4.41 o 9 2 1 98.80 105.46 9.50 o 10 2 1 7.78 6.36 4.28 o 11 2 1 90.98 73.21 12.26 o 12 2 1 9.95 5.47 5.73 o 13 2 1 28.00 11.53 9.58 o 14 2 1 10.75 12.13 7.77 o -14 3 1 19.08 7.33 7.15 o -13 3 1 18.64 20.69 10.28 o -12 3 1 1.25 0.00 6.26 o -11 3 1 0.01 0.81 4.58 o -10 3 1 373.29 352.91 22.02 o -9 3 1 77.42 81.79 10.25 o -8 3 1 214.55 227.20 13.48 o -7 3 1 233.42 232.43 12.88 o -6 3 1 649.36 603.73 17.15 o -5 3 1 782.27 798.40 18.98 o -4 3 1 218.33 236.46 10.48 o -3 3 1 105.54 147.53 7.60 o -2 3 1 457.47 432.45 13.19 o -1 3 1 1322.85 1628.57 25.19 o 0 3 1 437.89 411.32 10.29 o 1 3 1 872.27 925.49 17.21 o 2 3 1 1226.54 1281.12 22.11 o 3 3 1 2002.75 2001.72 31.59 o 4 3 1 5.68 5.60 1.81 o 5 3 1 833.73 853.49 26.24 o 6 3 1 354.76 348.16 13.67 o 7 3 1 168.70 160.51 9.21 o 8 3 1 4.79 0.63 2.28 o 9 3 1 31.12 27.39 5.07 o 10 3 1 5.41 5.09 3.52 o 11 3 1 225.59 209.40 22.73 o 12 3 1 5.03 2.03 4.53 o 13 3 1 367.38 388.50 34.33 o -13 4 1 142.46 168.77 22.46 o -12 4 1 96.78 83.66 15.47 o -11 4 1 561.04 573.76 36.04 o -10 4 1 168.63 182.38 16.56 o -9 4 1 539.09 564.67 25.01 o -8 4 1 88.89 72.00 7.27 o -7 4 1 10.18 12.49 3.04 o -6 4 1 141.84 134.84 9.19 o -5 4 1 1.90 0.32 2.16 o -4 4 1 609.69 680.28 20.23 o -3 4 1 2.24 3.55 1.68 o -2 4 1 0.87 0.00 1.33 o -1 4 1 32.23 32.83 4.44 o 0 4 1 132.00 161.29 8.84 o 1 4 1 663.50 671.79 14.53 o 2 4 1 287.54 358.86 10.77 o 3 4 1 80.85 66.99 5.68 o 4 4 1 0.31 2.43 2.07 o 5 4 1 173.67 165.07 8.73 o 6 4 1 603.61 626.83 20.82 o 7 4 1 1941.85 2063.96 36.29 o 8 4 1 599.87 591.84 24.36 o 9 4 1 178.82 162.52 13.62 o 10 4 1 94.01 85.52 10.15 o 11 4 1 53.01 45.49 8.83 o 12 4 1 4.10 0.00 6.69 o -12 5 1 0.04 0.00 6.26 o -11 5 1 54.89 62.80 10.11 o -10 5 1 6.89 7.66 4.43 o -9 5 1 50.39 47.31 8.06 o -8 5 1 48.96 42.65 5.84 o -7 5 1 182.55 209.00 12.59 o -6 5 1 6.30 0.95 2.39 o -5 5 1 9.27 7.55 4.72 o -4 5 1 212.03 207.43 13.21 o -3 5 1 1911.94 1965.84 36.85 o -2 5 1 976.72 906.14 48.31 o -1 5 1 2890.49 2922.00 51.25 o 0 5 1 1.03 0.88 2.53 o 1 5 1 166.95 165.59 8.05 o 2 5 1 126.88 123.66 7.08 o 3 5 1 17.37 15.18 2.44 o 4 5 1 174.43 151.92 8.63 o 5 5 1 277.99 266.35 12.36 o 6 5 1 323.16 343.44 16.31 o 7 5 1 1260.85 1271.91 32.78 o 8 5 1 248.75 254.52 16.74 o 9 5 1 94.56 100.10 11.05 o 10 5 1 8.21 4.42 5.07 o 11 5 1 5.12 8.47 5.04 o -11 6 1 108.93 137.10 21.13 o -10 6 1 12.80 11.07 6.48 o -9 6 1 84.47 68.58 11.28 o -8 6 1 166.75 182.85 17.40 o -7 6 1 33.28 38.86 7.58 o -6 6 1 896.08 946.11 37.59 o -5 6 1 300.97 293.99 20.06 o -4 6 1 436.94 394.85 21.90 o -3 6 1 43.60 43.64 6.81 o -2 6 1 657.45 663.05 31.97 o -1 6 1 188.44 164.23 15.81 o 0 6 1 31.16 29.82 7.65 o 1 6 1 571.15 597.84 35.51 o 2 6 1 2985.76 3034.58 93.41 o 3 6 1 45.90 42.31 7.96 o 4 6 1 442.24 419.60 25.11 o 5 6 1 10.89 8.93 3.63 o 6 6 1 141.30 155.70 14.65 o 7 6 1 71.64 69.12 10.06 o 8 6 1 19.65 23.70 6.86 o 9 6 1 47.18 50.14 11.75 o 10 6 1 29.61 23.48 8.31 o -9 7 1 27.67 19.04 7.64 o -8 7 1 5.25 0.00 10.13 o -7 7 1 104.19 102.16 14.75 o -6 7 1 179.71 222.57 19.87 o -5 7 1 92.17 90.15 12.81 o -4 7 1 32.54 21.21 8.20 o -3 7 1 440.49 474.61 34.49 o -2 7 1 363.02 338.77 29.22 o -1 7 1 344.60 345.93 29.40 o 0 7 1 284.38 267.50 25.96 o 1 7 1 87.16 67.70 13.45 o 2 7 1 605.10 580.46 38.33 o 3 7 1 315.57 332.89 27.33 o 4 7 1 17.15 10.42 5.45 o 5 7 1 120.98 138.89 17.90 o 6 7 1 36.82 48.78 13.26 o 7 7 1 17.20 6.12 5.75 o 8 7 1 131.22 136.34 20.61 o -6 8 1 161.50 153.99 19.78 o -5 8 1 144.54 166.16 20.54 o -4 8 1 368.80 388.98 33.87 o -3 8 1 136.86 145.22 20.77 o -2 8 1 0.84 3.68 6.90 o -1 8 1 21.27 14.10 10.98 o 0 8 1 153.46 175.59 22.79 o 1 8 1 823.39 806.54 48.81 o 2 8 1 302.14 329.34 31.05 o 3 8 1 130.45 117.75 18.04 o 4 8 1 46.67 15.97 7.89 o 5 8 1 75.15 65.53 13.39 o 6 8 1 634.79 689.41 42.45 o -15 0 2 266.72 273.05 35.96 o -14 0 2 497.92 502.18 66.14 o -13 0 2 73.70 65.90 14.57 o -12 0 2 3.86 5.23 9.91 o -11 0 2 111.63 113.28 19.71 o -10 0 2 211.01 189.81 23.54 o -9 0 2 227.92 197.87 15.52 o -8 0 2 552.34 567.82 35.79 o -7 0 2 4131.01 4110.58 88.79 o -6 0 2 2802.61 3108.96 70.86 o -5 0 2 11244.15 10783.02 121.95 o -4 0 2 43509.82 38742.62 1091.60 o -3 0 2 42524.57 41867.00 896.26 o -2 0 2 467.32 486.55 18.36 o -1 0 2 24.07 10.70 2.26 o 0 0 2 4303.12 4616.78 78.54 o 1 0 2 1889.61 1857.14 33.79 o 2 0 2 2684.40 2812.65 55.17 o 3 0 2 1428.91 1417.83 38.45 o 4 0 2 301.15 295.85 17.10 o 5 0 2 338.80 345.31 17.84 o 6 0 2 1091.31 1097.24 61.64 o 7 0 2 3070.25 3302.79 73.25 o 8 0 2 1213.82 1264.18 48.68 o 9 0 2 1.38 0.00 5.37 o 10 0 2 867.25 850.85 45.23 o 11 0 2 533.65 562.81 31.02 o 12 0 2 422.46 400.94 30.68 o 13 0 2 777.20 853.09 72.58 o 14 0 2 86.20 60.71 21.18 o -15 1 2 257.09 300.52 27.60 o -14 1 2 85.46 83.69 12.82 o -13 1 2 129.12 139.85 16.34 o -12 1 2 283.01 319.46 22.59 o -11 1 2 78.02 75.18 13.85 o -10 1 2 35.76 43.59 7.42 o -9 1 2 326.74 314.39 19.35 o -8 1 2 2675.83 2469.60 100.46 o -7 1 2 5414.39 5427.16 102.61 o -6 1 2 420.84 356.89 20.90 o -5 1 2 1312.28 1373.93 56.83 o -4 1 2 205.56 193.55 12.79 o -3 1 2 366.47 370.59 12.95 o -2 1 2 61.14 47.78 3.57 o -1 1 2 1565.61 1825.02 69.44 o 0 1 2 30.82 38.12 2.69 o 1 1 2 11364.47 11991.58 70.00 o 2 1 2 337.92 349.70 9.48 o 3 1 2 1215.65 1227.97 17.75 o 4 1 2 1052.40 941.19 16.59 o 5 1 2 2323.56 2313.87 35.42 o 6 1 2 112.50 78.88 5.62 o 7 1 2 313.89 289.08 11.48 o 8 1 2 174.17 160.34 9.12 o 9 1 2 624.26 626.67 22.44 o 10 1 2 20.31 16.83 4.98 o 11 1 2 714.32 701.10 37.15 o 12 1 2 164.66 173.72 18.82 o 13 1 2 31.75 30.67 9.14 o 14 1 2 66.29 87.34 14.91 o -14 2 2 138.73 196.97 20.97 o -13 2 2 90.47 125.59 18.89 o -12 2 2 404.35 394.56 30.04 o -11 2 2 968.03 958.95 36.71 o -10 2 2 3.45 7.87 4.02 o -9 2 2 1257.87 1349.30 62.98 o -8 2 2 575.96 590.57 27.25 o -7 2 2 1546.61 1534.58 46.81 o -6 2 2 196.86 248.83 13.65 o -5 2 2 257.19 262.50 12.99 o -4 2 2 216.94 186.68 9.59 o -3 2 2 1769.48 1660.46 41.38 o -2 2 2 3208.94 3406.34 36.88 o -1 2 2 3897.43 4021.68 37.64 o 0 2 2 6.48 12.61 2.02 o 1 2 2 1351.84 1428.92 18.34 o 2 2 2 44.95 41.34 3.58 o 3 2 2 341.30 313.14 9.60 o 4 2 2 0.75 0.58 0.87 o 5 2 2 0.51 0.79 0.89 o 6 2 2 564.92 626.66 15.66 o 7 2 2 783.09 800.56 19.81 o 8 2 2 893.78 838.40 26.28 o 9 2 2 3506.57 3664.17 62.02 o 10 2 2 297.37 291.53 23.78 o 11 2 2 155.68 189.73 19.05 o 12 2 2 277.23 295.58 24.93 o 13 2 2 11.40 0.00 4.71 o -14 3 2 0.73 1.87 7.10 o -13 3 2 115.29 130.77 22.25 o -12 3 2 80.49 65.68 14.88 o -11 3 2 449.16 451.19 26.23 o -10 3 2 1.21 0.00 3.77 o -9 3 2 810.68 805.26 31.69 o -8 3 2 1041.89 1050.32 35.46 o -7 3 2 492.74 493.52 19.76 o -6 3 2 26.89 11.55 2.96 o -5 3 2 184.03 172.86 10.09 o -4 3 2 323.31 331.54 12.94 o -3 3 2 609.47 650.17 14.44 o -2 3 2 1191.70 1221.29 19.35 o -1 3 2 148.33 138.83 7.20 o 0 3 2 2825.46 2949.46 30.55 o 1 3 2 1957.44 2008.54 23.18 o 2 3 2 1234.06 1272.87 19.54 o 3 3 2 1733.85 1754.11 27.54 o 4 3 2 53.57 27.28 3.83 o 5 3 2 2145.06 2107.99 41.52 o 6 3 2 444.49 400.99 15.37 o 7 3 2 53.66 44.67 5.73 o 8 3 2 47.96 46.93 5.68 o 9 3 2 23.15 18.59 4.13 o 10 3 2 68.74 59.79 10.73 o 11 3 2 154.80 153.25 17.54 o 12 3 2 314.13 298.23 25.84 o 13 3 2 56.45 66.25 13.58 o -13 4 2 91.03 84.39 16.03 o -12 4 2 163.87 208.85 22.30 o -11 4 2 10.92 0.00 3.49 o -10 4 2 19.19 22.09 5.14 o -9 4 2 384.63 369.72 20.15 o -8 4 2 814.56 781.98 27.73 o -7 4 2 63.81 56.34 7.58 o -6 4 2 467.23 432.48 16.23 o -5 4 2 418.61 414.46 14.56 o -4 4 2 89.55 77.96 5.95 o -3 4 2 599.68 546.23 17.19 o -2 4 2 462.35 412.50 12.02 o -1 4 2 8.71 18.40 3.47 o 0 4 2 463.78 439.92 16.96 o 1 4 2 357.00 383.24 11.73 o 2 4 2 568.70 602.03 14.38 o 3 4 2 763.05 817.82 18.25 o 4 4 2 7.56 7.67 2.34 o 5 4 2 171.97 181.65 9.25 o 6 4 2 71.28 84.61 7.55 o 7 4 2 537.00 517.72 20.17 o 8 4 2 2410.90 2487.35 55.50 o 9 4 2 142.43 148.87 13.12 o 10 4 2 77.05 74.71 9.80 o 11 4 2 3.96 2.36 6.10 o 12 4 2 44.69 29.00 8.98 o -12 5 2 463.84 528.55 36.85 o -11 5 2 382.90 427.66 28.23 o -10 5 2 703.61 685.53 32.20 o -9 5 2 87.45 70.46 8.94 o -8 5 2 794.85 804.69 25.56 o -7 5 2 122.73 124.57 9.48 o -6 5 2 4.72 4.43 2.03 o -5 5 2 183.15 160.49 9.73 o -4 5 2 8.93 8.51 2.07 o -3 5 2 193.89 176.74 9.87 o -2 5 2 152.72 153.41 11.08 o -1 5 2 60.53 76.76 7.83 o 0 5 2 34.24 21.46 4.17 o 1 5 2 4.37 7.04 1.73 o 2 5 2 1022.16 1031.28 32.44 o 3 5 2 76.55 60.48 5.18 o 4 5 2 2531.32 2484.77 49.58 o 5 5 2 656.27 649.53 19.63 o 6 5 2 109.00 120.67 8.98 o 7 5 2 78.46 65.05 7.45 o 8 5 2 7.32 2.97 3.64 o 9 5 2 521.86 529.58 25.97 o 10 5 2 24.31 7.12 4.75 o 11 5 2 9.60 13.71 5.19 o -11 6 2 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