#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:29:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181244 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232257.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232257_Fobs loop_ _publ_author_name 'Owczarzak, Anita M.' 'Kyros, Loukas' 'Hadjikakou, Sotiris K.' 'Kubicki, Maciej' _publ_section_title ; Bromidotris(triphenylphosphane)silver acetonitrile monosolvate monohydrate ; _journal_coeditor_code GO2030 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1507 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.103 _cell_angle_beta 87.161 _cell_angle_gamma 77.398 _cell_length_a 13.1894 _cell_length_b 13.7384 _cell_length_c 13.8299 _exptl_crystal_F_000 1052.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file go2030Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S065 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 378.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12489.96 10593.53 70.12 o 3 0 0 5599.34 6618.26 88.85 o 4 0 0 1516.88 1571.33 44.99 o 5 0 0 6801.65 7029.01 71.75 o 6 0 0 2063.95 1767.88 42.21 o 7 0 0 4995.38 5412.46 79.46 o 8 0 0 984.54 870.90 34.21 o 9 0 0 335.75 339.96 22.01 o 10 0 0 1130.84 1104.60 50.30 o 11 0 0 4238.55 4214.37 132.23 o 12 0 0 2497.78 2427.64 195.98 o 13 0 0 6.30 57.87 42.74 o 14 0 0 190.47 216.63 58.40 o 15 0 0 416.31 401.31 75.08 o -15 1 0 13.19 8.57 40.92 o -14 1 0 79.19 129.97 78.88 o -13 1 0 846.52 831.85 126.72 o -12 1 0 19.10 86.95 57.13 o -11 1 0 1856.15 2061.51 174.38 o -10 1 0 1074.83 1024.62 56.23 o -9 1 0 157.92 123.93 21.33 o -8 1 0 1334.83 1241.80 85.77 o -7 1 0 8046.35 8161.08 184.03 o -6 1 0 875.90 768.84 38.06 o -5 1 0 6504.08 6015.14 129.88 o -4 1 0 18.70 40.03 6.27 o -3 1 0 1763.74 1821.61 48.48 o -2 1 0 102.25 213.75 16.96 o 3 1 0 55769.32 61192.12 395.36 o 4 1 0 16766.57 15772.30 160.16 o 5 1 0 3798.04 3809.52 86.12 o 6 1 0 3994.96 4046.23 73.34 o 7 1 0 56.94 116.07 18.20 o 8 1 0 168.49 189.59 19.85 o 9 1 0 811.15 804.09 38.93 o 10 1 0 4146.28 3795.61 120.73 o 11 1 0 1452.34 1547.73 88.57 o 12 1 0 2328.45 2219.33 93.93 o 13 1 0 237.86 252.61 87.64 o 14 1 0 835.02 765.19 97.03 o 15 1 0 573.82 568.61 85.22 o 16 1 0 1929.41 1942.29 217.23 o -15 2 0 583.99 677.40 130.12 o -14 2 0 89.18 31.98 52.63 o -13 2 0 276.53 373.06 87.70 o -12 2 0 3348.70 3666.76 244.52 o -11 2 0 337.18 170.14 66.12 o -10 2 0 489.14 572.88 94.50 o -9 2 0 10.45 10.78 20.28 o -8 2 0 230.84 210.32 19.15 o -7 2 0 2436.53 2120.83 186.75 o -6 2 0 7974.56 8094.41 220.43 o -5 2 0 25.95 18.93 13.04 o -4 2 0 5702.10 6336.87 92.18 o -3 2 0 10.66 64.27 11.77 o -2 2 0 1409.05 1451.34 35.17 o -1 2 0 117.60 138.20 7.63 o 0 2 0 5832.93 5231.20 57.13 o 1 2 0 224.17 579.66 52.20 o 2 2 0 56.54 37.23 12.28 o 3 2 0 19745.67 18304.94 129.07 o 4 2 0 320.68 474.15 25.01 o 5 2 0 35941.14 37696.98 378.16 o 6 2 0 3370.00 4115.36 90.20 o 7 2 0 9.01 0.00 13.63 o 8 2 0 859.50 792.57 37.37 o 9 2 0 1087.03 1036.01 63.37 o 10 2 0 1037.97 1112.78 54.82 o 11 2 0 5241.41 5177.66 166.71 o 12 2 0 139.25 50.94 26.28 o 13 2 0 158.27 228.26 44.76 o 14 2 0 1105.52 1110.27 109.90 o 15 2 0 1147.69 1166.72 119.04 o 16 2 0 1216.18 1765.35 209.26 o -14 3 0 218.15 265.10 93.86 o -13 3 0 2552.93 2285.20 207.81 o -12 3 0 660.92 484.20 100.80 o -11 3 0 3920.41 4008.99 245.96 o -10 3 0 1043.76 884.63 111.42 o -9 3 0 32.29 89.51 52.10 o -8 3 0 1413.07 1528.88 93.03 o -7 3 0 6848.16 7067.80 182.26 o -6 3 0 929.58 1132.12 71.25 o -5 3 0 6275.84 5685.13 142.24 o -4 3 0 523.60 473.57 27.90 o -3 3 0 397.01 355.04 24.83 o -2 3 0 4465.07 4214.62 44.11 o -1 3 0 2446.03 2494.48 39.61 o 0 3 0 624.35 721.01 23.36 o 1 3 0 7432.75 7854.14 91.63 o 2 3 0 1646.06 1856.51 60.50 o 3 3 0 28214.44 29362.14 310.11 o 4 3 0 42424.37 43182.66 630.63 o 5 3 0 3129.95 3473.08 72.75 o 6 3 0 1437.94 1450.06 57.57 o 7 3 0 363.82 369.24 32.88 o 8 3 0 233.81 125.43 26.77 o 9 3 0 8752.10 9067.23 157.06 o 10 3 0 2141.09 2044.33 105.11 o 11 3 0 75.28 4.62 27.63 o 12 3 0 405.10 491.05 58.76 o 13 3 0 186.17 109.62 34.74 o 14 3 0 4.86 13.71 59.69 o 15 3 0 4957.58 5050.91 330.38 o 16 3 0 311.38 443.58 117.65 o -14 4 0 1104.18 902.18 144.79 o -13 4 0 1470.98 1744.01 186.49 o -12 4 0 988.41 913.08 130.62 o -11 4 0 89.04 154.93 53.34 o -10 4 0 2709.62 2672.65 197.03 o -9 4 0 1839.91 1802.29 110.71 o -8 4 0 472.48 438.16 54.33 o -7 4 0 4807.17 5052.67 161.22 o -6 4 0 5219.73 5202.70 243.23 o -5 4 0 1291.97 1275.59 130.26 o -4 4 0 1999.98 2282.86 72.09 o -3 4 0 1234.20 1012.79 27.82 o -2 4 0 373.54 383.75 17.04 o -1 4 0 3628.75 3168.43 67.67 o 0 4 0 5280.47 5026.96 69.19 o 1 4 0 526.06 461.29 24.26 o 2 4 0 96.20 56.03 13.78 o 3 4 0 1602.25 1449.39 63.47 o 4 4 0 6648.43 6680.29 127.98 o 5 4 0 8346.82 7824.00 198.52 o 6 4 0 1041.16 1139.71 94.52 o 7 4 0 336.86 399.92 50.67 o 8 4 0 5651.22 5734.87 163.34 o 9 4 0 17.74 16.82 27.82 o 10 4 0 388.29 459.11 54.33 o 11 4 0 1012.60 877.25 84.95 o 12 4 0 151.40 105.46 33.76 o 13 4 0 159.90 154.91 43.30 o 14 4 0 1009.29 1195.33 98.76 o 15 4 0 5.99 0.00 73.64 o -14 5 0 1820.14 1906.26 205.84 o -13 5 0 476.65 306.43 89.18 o -12 5 0 1451.47 1492.88 171.53 o -11 5 0 1066.62 904.97 126.40 o -10 5 0 186.73 110.31 38.66 o -9 5 0 5498.91 5537.46 194.29 o -8 5 0 2032.97 2077.63 114.52 o -7 5 0 640.99 621.36 61.88 o -6 5 0 4542.14 4442.32 146.71 o -5 5 0 662.24 514.29 35.33 o -4 5 0 1727.59 1748.54 163.37 o -3 5 0 1502.74 1313.94 39.24 o -2 5 0 14801.32 14654.77 112.69 o -1 5 0 681.33 757.03 29.96 o 0 5 0 2733.95 2614.07 61.22 o 1 5 0 134.27 168.32 18.65 o 2 5 0 176.84 202.26 23.30 o 3 5 0 5422.38 4785.10 122.66 o 4 5 0 5329.97 4878.95 130.37 o 5 5 0 687.71 699.52 76.76 o 6 5 0 2643.38 2607.97 148.18 o 7 5 0 557.42 699.13 84.99 o 8 5 0 1251.60 961.31 99.27 o 9 5 0 2576.51 2356.65 161.76 o 10 5 0 962.24 840.71 104.98 o 11 5 0 197.53 196.15 84.22 o 12 5 0 200.40 234.00 48.16 o 13 5 0 3.54 0.00 33.85 o 14 5 0 19.68 63.66 32.12 o 15 5 0 2873.40 2785.73 245.39 o -13 6 0 2169.86 1970.10 205.01 o -12 6 0 139.17 262.97 87.99 o -11 6 0 432.89 534.21 77.11 o -10 6 0 78.57 96.21 38.05 o -9 6 0 59.15 55.76 36.12 o -8 6 0 1166.83 1279.21 96.65 o -7 6 0 1742.76 1741.04 118.53 o -6 6 0 1969.19 1871.15 44.34 o -5 6 0 996.23 1274.15 80.00 o -4 6 0 6087.12 5917.77 91.92 o -3 6 0 2689.64 2372.42 51.86 o -2 6 0 17695.19 18617.57 153.98 o -1 6 0 6541.61 6056.40 90.28 o 0 6 0 3423.81 3849.40 74.73 o 1 6 0 1476.81 1544.37 49.13 o 2 6 0 12750.75 11613.79 281.64 o 3 6 0 55.98 77.40 18.36 o 4 6 0 5827.27 5760.45 214.22 o 5 6 0 6062.21 6225.34 231.08 o 6 6 0 944.61 894.49 93.53 o 7 6 0 753.42 751.27 88.88 o 8 6 0 7755.92 7762.86 286.09 o 9 6 0 78.94 112.86 39.39 o 10 6 0 1192.25 1349.38 130.36 o 11 6 0 91.19 128.26 52.37 o 12 6 0 354.49 443.75 85.16 o 13 6 0 157.46 193.80 69.93 o 14 6 0 879.23 714.96 110.06 o 15 6 0 0.72 0.00 60.36 o -12 7 0 903.10 868.00 138.85 o -11 7 0 5.93 17.19 38.54 o -10 7 0 2.72 0.00 35.25 o -9 7 0 2596.18 2688.79 146.09 o -8 7 0 126.75 113.72 35.77 o -7 7 0 100.71 111.50 32.30 o -6 7 0 293.01 296.07 27.16 o -5 7 0 686.14 775.77 66.98 o -4 7 0 499.41 496.02 31.80 o -3 7 0 1042.75 938.19 36.87 o -2 7 0 4391.62 4433.98 82.53 o -1 7 0 14357.72 14822.84 173.46 o 0 7 0 452.12 406.30 39.14 o 1 7 0 11202.69 11912.09 167.74 o 2 7 0 6067.68 5869.40 159.82 o 3 7 0 6307.33 5212.98 207.42 o 4 7 0 25.17 87.91 35.09 o 5 7 0 1151.38 1072.76 105.86 o 6 7 0 0.45 0.00 43.88 o 7 7 0 129.04 41.24 40.24 o 8 7 0 2192.36 1964.86 152.54 o 9 7 0 8592.17 8340.66 321.92 o 10 7 0 35.97 112.54 57.89 o 11 7 0 470.08 463.15 88.38 o 12 7 0 346.90 305.66 75.70 o 13 7 0 4.33 56.47 45.84 o 14 7 0 740.82 783.01 120.69 o 15 7 0 653.04 634.11 114.01 o -12 8 0 75.34 25.48 59.40 o -11 8 0 308.13 327.49 64.43 o -10 8 0 426.38 368.40 65.36 o -9 8 0 3.69 0.00 38.13 o -8 8 0 1306.23 1153.98 94.94 o -7 8 0 725.44 686.84 73.50 o -6 8 0 1730.39 1671.62 66.19 o -5 8 0 317.80 255.98 24.47 o -4 8 0 97.84 94.21 22.01 o -3 8 0 595.07 627.23 41.62 o -2 8 0 6137.92 5759.11 101.86 o -1 8 0 5367.89 5082.64 110.00 o 0 8 0 2597.94 2862.05 86.22 o 1 8 0 446.34 374.52 46.02 o 2 8 0 13549.68 13723.88 164.12 o 3 8 0 5057.22 5060.85 214.60 o 4 8 0 4399.34 4235.46 204.02 o 5 8 0 88.04 114.02 49.94 o 6 8 0 1596.21 1724.05 141.10 o 7 8 0 2512.39 2212.41 164.63 o 8 8 0 69.29 108.88 48.31 o 9 8 0 624.07 753.75 107.52 o 10 8 0 27.39 0.00 52.38 o 11 8 0 51.22 79.53 52.42 o 12 8 0 24.96 0.00 54.05 o 13 8 0 2258.61 2189.07 195.38 o 14 8 0 9.94 0.00 62.77 o 15 8 0 854.24 912.78 138.06 o -11 9 0 147.06 65.98 46.10 o -10 9 0 367.00 266.98 101.47 o -9 9 0 4936.50 5068.26 211.26 o -8 9 0 228.79 213.59 51.66 o -7 9 0 2279.86 2220.65 211.97 o -6 9 0 39.31 1.72 29.15 o -5 9 0 410.55 398.45 30.85 o -4 9 0 162.47 201.01 40.30 o -3 9 0 925.78 925.51 53.79 o -2 9 0 3175.24 3279.43 82.51 o -1 9 0 1420.77 1334.33 78.22 o 0 9 0 1850.53 1776.26 93.26 o 1 9 0 7079.66 7190.23 126.61 o 2 9 0 3173.64 3094.73 83.26 o 3 9 0 2911.48 2541.45 162.83 o 4 9 0 247.88 214.16 55.26 o 5 9 0 270.71 278.84 60.61 o 6 9 0 1542.23 1585.39 143.53 o 7 9 0 1633.94 1537.29 141.95 o 8 9 0 702.51 757.39 108.76 o 9 9 0 2289.66 2212.72 185.78 o 10 9 0 1.33 33.63 56.92 o 11 9 0 479.29 492.49 97.85 o 12 9 0 826.27 671.13 117.23 o 13 9 0 780.34 609.31 112.40 o 14 9 0 962.40 1082.72 151.99 o 15 9 0 7.57 0.00 63.81 o -10 10 0 1046.17 1083.55 109.83 o -9 10 0 36.54 24.68 45.26 o -8 10 0 3696.75 4077.54 213.55 o -7 10 0 188.12 153.59 47.18 o -6 10 0 1322.10 1197.87 115.55 o -5 10 0 813.26 922.86 84.84 o -4 10 0 2773.92 3041.73 95.54 o -3 10 0 158.97 110.71 39.99 o -2 10 0 3989.76 3893.89 117.91 o -1 10 0 2707.24 2391.71 108.82 o 0 10 0 599.81 793.83 69.36 o 1 10 0 1927.45 1776.78 68.94 o 2 10 0 4226.47 3978.97 100.88 o 3 10 0 3818.17 3683.95 205.08 o 4 10 0 4201.23 3975.46 218.71 o 5 10 0 1302.30 1228.88 130.49 o 6 10 0 2428.76 2269.72 175.68 o 7 10 0 4213.65 3973.63 239.32 o 8 10 0 2305.98 2530.37 197.71 o 9 10 0 607.43 624.01 107.64 o 10 10 0 372.37 370.36 88.67 o 11 10 0 92.08 69.11 57.96 o 12 10 0 187.86 175.98 74.11 o 13 10 0 874.44 935.43 144.50 o 14 10 0 1.93 2.43 56.79 o -9 11 0 1664.79 1527.51 127.06 o -8 11 0 326.93 269.16 67.26 o -7 11 0 327.51 266.91 56.12 o -6 11 0 462.45 495.03 80.41 o -5 11 0 42.23 81.82 55.97 o -4 11 0 3510.98 3520.84 163.30 o -3 11 0 2603.67 2796.41 101.49 o -2 11 0 19.85 53.77 24.15 o -1 11 0 472.07 470.13 57.94 o 0 11 0 242.02 299.91 107.82 o 1 11 0 10.34 0.00 23.15 o 2 11 0 6317.70 6480.99 135.01 o 3 11 0 696.15 608.32 93.70 o 4 11 0 3971.73 3768.74 221.76 o 5 11 0 218.52 185.03 69.84 o 6 11 0 4359.50 4229.46 249.74 o 7 11 0 1950.72 1836.44 170.18 o 8 11 0 2238.33 2306.43 194.37 o 9 11 0 86.58 135.65 66.46 o 10 11 0 229.94 45.80 52.21 o 11 11 0 608.74 488.33 102.02 o 12 11 0 150.56 124.62 68.23 o 13 11 0 132.85 206.02 71.14 o 14 11 0 1455.15 1455.13 183.06 o -8 12 0 753.49 690.57 101.70 o -7 12 0 750.94 697.36 88.54 o -6 12 0 47.41 91.11 50.07 o -5 12 0 2883.95 2911.32 159.30 o -4 12 0 710.24 556.83 74.00 o -3 12 0 1986.75 2048.21 128.49 o -2 12 0 454.24 466.33 49.15 o -1 12 0 4.07 0.00 24.34 o 0 12 0 534.27 537.28 45.62 o 1 12 0 1295.96 1384.48 74.87 o 2 12 0 18.67 116.31 55.17 o 3 12 0 3879.22 3858.97 230.02 o 4 12 0 739.92 668.82 103.57 o 5 12 0 3095.82 2982.22 215.25 o 6 12 0 5385.28 4990.90 283.45 o 7 12 0 2778.60 2827.56 219.80 o 8 12 0 587.53 587.95 103.40 o 9 12 0 450.85 489.49 109.83 o 10 12 0 262.37 272.74 86.38 o 11 12 0 266.13 105.80 53.98 o 12 12 0 876.32 838.21 135.48 o 13 12 0 430.98 576.40 130.41 o -7 13 0 1.00 0.00 68.04 o -6 13 0 110.51 145.23 52.19 o -5 13 0 211.20 217.23 86.29 o -4 13 0 3826.68 3825.54 188.25 o -3 13 0 260.32 211.74 58.70 o -2 13 0 385.74 352.29 46.01 o -1 13 0 1222.26 1287.27 80.73 o 0 13 0 56.62 137.62 44.86 o 1 13 0 490.30 493.14 86.89 o 2 13 0 1831.62 1483.53 147.08 o 3 13 0 41.71 24.60 43.15 o 4 13 0 7.67 0.00 40.84 o 5 13 0 2449.92 2417.51 200.18 o 6 13 0 23.15 45.06 50.82 o 7 13 0 6504.09 6506.73 341.66 o 8 13 0 595.79 429.91 96.23 o 9 13 0 288.87 202.79 74.11 o 10 13 0 534.32 401.21 103.22 o 11 13 0 479.22 522.59 115.70 o 12 13 0 289.39 240.31 88.33 o -5 14 0 928.15 1019.76 109.66 o -4 14 0 3.63 110.20 56.83 o -3 14 0 1515.30 1617.17 167.30 o -2 14 0 348.77 329.94 66.13 o -1 14 0 2.11 52.32 33.17 o 0 14 0 4951.57 4810.31 190.79 o 1 14 0 608.72 625.08 102.46 o 2 14 0 806.68 847.43 118.21 o 3 14 0 295.08 258.69 74.53 o 4 14 0 68.42 53.78 53.20 o 5 14 0 339.36 345.90 91.04 o 6 14 0 456.94 648.72 114.86 o 7 14 0 67.38 66.92 67.71 o 8 14 0 1409.05 1393.20 174.40 o 9 14 0 488.84 672.29 133.17 o 10 14 0 533.56 434.43 107.52 o 11 14 0 1225.70 1111.97 164.39 o -4 15 0 990.05 1260.03 177.41 o -3 15 0 1.35 81.62 83.84 o -2 15 0 399.55 456.57 78.73 o -1 15 0 292.28 260.37 78.45 o 0 15 0 29.89 4.68 39.92 o 1 15 0 5450.45 5202.26 281.50 o 2 15 0 5.24 25.07 48.55 o 3 15 0 350.51 297.35 77.73 o 4 15 0 41.71 77.99 60.41 o 5 15 0 356.95 211.51 74.47 o 6 15 0 3.41 0.00 48.79 o 7 15 0 1683.15 1576.51 182.93 o 8 15 0 82.04 0.00 62.76 o 9 15 0 32.57 15.58 62.48 o -1 16 0 5.56 0.00 94.02 o 0 16 0 4285.82 4540.90 310.02 o 1 16 0 2.48 22.77 47.60 o 2 16 0 2192.86 2497.83 212.20 o 3 16 0 381.64 319.44 84.21 o 4 16 0 251.97 379.94 95.10 o 5 16 0 1472.83 1754.92 193.07 o 6 16 0 908.42 1037.13 153.13 o 7 16 0 223.24 329.13 96.71 o -7 -16 1 1064.18 1102.65 166.86 o -6 -16 1 316.37 388.17 106.70 o -5 -16 1 1156.60 1226.63 167.28 o -4 -16 1 29.72 218.87 77.29 o -3 -16 1 957.56 995.82 143.16 o -2 -16 1 2.63 34.87 50.97 o -1 -16 1 3223.71 3390.56 239.76 o 0 -16 1 10.00 94.83 65.17 o 1 -16 1 857.89 821.55 148.79 o -9 -15 1 66.58 122.45 83.10 o -8 -15 1 617.11 723.29 130.74 o -7 -15 1 238.93 195.28 83.18 o -6 -15 1 3116.53 3131.75 253.94 o -5 -15 1 40.86 0.00 61.02 o -4 -15 1 29.72 0.00 44.97 o -3 -15 1 484.94 430.44 96.16 o -2 -15 1 491.43 412.48 90.12 o -1 -15 1 133.21 164.33 63.15 o 0 -15 1 1892.56 2236.02 137.37 o 1 -15 1 146.44 238.80 66.77 o 2 -15 1 389.63 314.98 73.97 o 3 -15 1 662.46 887.11 135.73 o -10 -14 1 1234.08 1704.36 199.63 o -9 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