#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232273.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232273_Fobs loop_ _publ_author_name 'van Rooyen, Jason' 'Betz, Richard' 'van Brecht, Bernardus J. A. M.' _publ_section_title ; 1,3-Bis(2-methoxyphenyl)thiourea ; _journal_coeditor_code HB6427 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2889 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.790 _cell_angle_gamma 90.000 _cell_length_a 14.3187 _cell_length_b 12.8628 _cell_length_c 16.1168 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.7504 _[local]_cod_data_source_file hb6427Isup3.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 5m_hs1_s in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 342.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2049.37 1890.36 113.54 o 4 0 0 35924.66 34449.68 1110.90 o 6 0 0 3092.07 3403.34 125.18 o 8 0 0 19067.96 20022.73 1082.96 o 10 0 0 3385.29 3283.91 53.73 o 12 0 0 35.86 48.54 19.50 o 14 0 0 90.83 51.64 22.43 o 16 0 0 18.22 6.06 23.01 o 18 0 0 854.62 874.05 64.63 o 1 1 0 141.67 105.49 33.19 o 3 1 0 1035.96 1054.25 38.49 o 5 1 0 702.46 773.65 20.59 o 7 1 0 12729.87 12930.51 458.34 o 9 1 0 0.27 2.49 8.90 o 11 1 0 510.10 514.95 21.46 o 13 1 0 92.59 108.91 15.29 o 15 1 0 290.52 305.28 21.60 o 17 1 0 1.03 8.44 18.76 o 0 2 0 84143.10 74426.31 4160.94 o 2 2 0 1076.57 1287.22 43.78 o 4 2 0 602.04 616.49 18.82 o 6 2 0 2.46 18.32 6.46 o 8 2 0 14216.77 14587.07 557.26 o 10 2 0 349.55 377.50 19.05 o 12 2 0 404.41 353.58 24.20 o 14 2 0 67.10 81.11 16.04 o 16 2 0 268.17 282.35 30.34 o 18 2 0 307.34 312.64 33.36 o 1 3 0 4247.73 4585.15 186.73 o 3 3 0 21119.71 20356.29 632.14 o 5 3 0 751.63 879.92 71.39 o 7 3 0 3218.85 3538.66 98.66 o 9 3 0 282.08 213.58 13.23 o 11 3 0 838.13 878.41 34.79 o 13 3 0 2173.69 2109.38 64.96 o 15 3 0 102.47 88.95 17.68 o 17 3 0 0.07 -15.26 19.36 o 0 4 0 13259.06 12725.56 586.31 o 2 4 0 2449.01 2683.70 96.73 o 4 4 0 790.39 813.13 23.46 o 6 4 0 1041.02 1106.58 35.97 o 8 4 0 227.93 206.42 12.57 o 10 4 0 23.21 21.33 11.10 o 12 4 0 332.40 374.22 24.58 o 14 4 0 47.61 60.14 16.40 o 16 4 0 20.30 25.37 18.55 o 18 4 0 30.51 26.27 32.74 o 1 5 0 32.43 26.25 4.91 o 3 5 0 11688.61 11622.53 295.25 o 5 5 0 14883.29 15566.66 531.97 o 7 5 0 88.47 129.68 10.43 o 9 5 0 1358.25 1272.15 38.15 o 11 5 0 727.99 733.00 30.25 o 13 5 0 137.76 140.81 17.15 o 15 5 0 248.75 249.60 21.57 o 17 5 0 14.41 -19.66 19.66 o 0 6 0 8840.29 9005.20 435.80 o 2 6 0 621.58 680.66 21.01 o 4 6 0 1262.67 1280.02 43.09 o 6 6 0 1309.14 1348.91 30.53 o 8 6 0 351.13 391.03 18.96 o 10 6 0 205.51 235.97 15.61 o 12 6 0 38.51 24.35 13.77 o 14 6 0 8.84 -10.53 16.06 o 16 6 0 23.37 31.18 19.85 o 1 7 0 256.78 344.88 13.15 o 3 7 0 11837.95 11715.50 287.92 o 5 7 0 10149.00 10630.66 265.34 o 7 7 0 138.35 156.63 10.23 o 9 7 0 139.78 119.62 13.26 o 11 7 0 265.37 243.96 24.03 o 13 7 0 60.70 79.42 16.63 o 15 7 0 20.80 5.83 18.36 o 0 8 0 7133.38 7054.36 60.51 o 2 8 0 266.72 240.53 12.88 o 4 8 0 3342.82 3395.54 32.42 o 6 8 0 761.42 861.55 19.96 o 8 8 0 3216.21 3085.11 70.63 o 10 8 0 945.65 981.93 37.29 o 12 8 0 432.96 456.65 34.29 o 14 8 0 378.37 367.89 23.98 o 16 8 0 393.45 348.23 26.89 o 1 9 0 8.44 9.09 8.31 o 3 9 0 53.06 57.60 9.69 o 5 9 0 4418.70 4401.45 134.80 o 7 9 0 1056.65 1059.42 27.33 o 9 9 0 721.81 737.25 26.49 o 11 9 0 273.89 291.96 16.59 o 13 9 0 136.50 128.14 16.35 o 15 9 0 105.05 109.32 20.78 o 0 10 0 2684.90 2574.64 71.61 o 2 10 0 1923.16 1994.99 34.26 o 4 10 0 4229.47 4250.43 103.45 o 6 10 0 4.54 5.54 13.58 o 8 10 0 522.77 548.58 25.30 o 10 10 0 170.24 171.36 16.54 o 12 10 0 729.62 828.12 29.24 o 14 10 0 425.72 424.52 25.09 o 1 11 0 3.93 -8.78 24.74 o 3 11 0 0.63 24.44 17.46 o 5 11 0 1252.76 1222.23 89.08 o 7 11 0 234.65 227.85 32.90 o 9 11 0 166.37 179.33 38.43 o 11 11 0 229.20 262.90 49.62 o 13 11 0 2.71 -14.91 20.25 o 0 12 0 981.52 985.14 57.06 o 2 12 0 69.39 76.20 34.06 o 4 12 0 1108.57 1073.33 43.01 o 6 12 0 251.35 257.98 28.56 o 8 12 0 3508.20 3556.61 194.47 o 10 12 0 254.12 180.18 31.22 o 12 12 0 1.01 -4.16 23.97 o 1 13 0 2684.84 2594.32 98.11 o 3 13 0 181.82 156.90 25.49 o 5 13 0 5.14 22.96 21.40 o 7 13 0 43.19 27.28 24.61 o 9 13 0 714.50 802.10 48.04 o 11 13 0 124.95 148.18 32.61 o 0 14 0 2446.97 2208.42 83.26 o 2 14 0 44.22 49.78 23.87 o 4 14 0 123.04 120.83 27.38 o 6 14 0 114.62 102.16 40.76 o 8 14 0 27.96 22.58 28.81 o 10 14 0 11.15 7.57 31.29 o 1 15 0 583.31 547.44 43.42 o 3 15 0 59.68 33.44 26.95 o 5 15 0 959.04 1051.52 52.08 o 7 15 0 77.94 102.96 31.16 o 0 16 0 235.22 250.94 48.91 o 2 16 0 88.20 112.07 30.57 o 4 16 0 17.65 17.05 29.01 o 6 16 0 195.43 221.17 36.20 o 1 17 0 327.01 381.30 39.11 o -17 1 1 234.81 233.21 23.20 o -15 1 1 717.18 671.76 51.68 o -13 1 1 1070.32 996.96 28.66 o -11 1 1 196.50 171.14 14.08 o -9 1 1 3177.69 2991.85 81.77 o -7 1 1 19392.63 18766.98 574.23 o -5 1 1 41229.14 41672.77 1467.56 o -3 1 1 23658.32 22603.63 542.89 o -1 1 1 16.71 11.46 3.06 o 1 1 1 12358.40 11789.52 448.79 o 3 1 1 65397.23 62836.79 1392.35 o 5 1 1 1537.22 1577.88 60.00 o 7 1 1 2977.92 3287.92 85.55 o 9 1 1 446.74 431.30 22.61 o 11 1 1 96.46 85.15 12.70 o 13 1 1 994.79 937.52 28.25 o 15 1 1 3.14 4.53 15.92 o 17 1 1 1187.92 1264.15 88.07 o -18 2 1 99.53 86.89 22.97 o -16 2 1 186.31 176.28 20.21 o -14 2 1 334.53 316.60 20.72 o -12 2 1 4103.53 3889.61 139.08 o -10 2 1 451.80 450.31 20.00 o -8 2 1 913.18 1010.56 21.50 o -6 2 1 164.89 191.88 10.43 o -4 2 1 30479.98 30579.44 716.43 o -2 2 1 16252.65 16456.26 458.63 o 0 2 1 10988.14 9830.92 692.23 o 2 2 1 2942.00 3056.71 95.13 o 4 2 1 39.37 64.13 6.06 o 6 2 1 157.75 189.35 10.22 o 8 2 1 2.64 7.92 8.13 o 10 2 1 116.26 109.32 12.57 o 12 2 1 549.07 536.29 40.76 o 14 2 1 3655.19 3455.83 63.79 o 16 2 1 46.92 33.66 17.74 o 18 2 1 79.07 93.01 24.22 o -17 3 1 14.93 6.33 19.19 o -15 3 1 720.20 614.63 28.81 o -13 3 1 521.18 506.07 24.26 o -11 3 1 231.21 218.16 15.55 o -9 3 1 561.02 439.59 18.25 o -7 3 1 7773.30 8355.27 189.17 o -5 3 1 647.99 689.45 25.38 o -3 3 1 1893.95 1729.67 78.20 o -1 3 1 10246.30 10302.92 230.89 o 1 3 1 15346.73 15166.21 526.37 o 3 3 1 802.99 843.34 20.09 o 5 3 1 12996.59 13544.48 219.16 o 7 3 1 4549.72 4847.26 126.06 o 9 3 1 11.72 10.77 9.43 o 11 3 1 65.36 74.67 12.93 o 13 3 1 1559.48 1599.82 64.16 o 15 3 1 20.88 -10.18 15.98 o 17 3 1 179.28 206.10 23.59 o -18 4 1 0.92 -10.56 21.29 o -16 4 1 646.69 622.69 31.76 o -14 4 1 750.06 772.48 43.53 o -12 4 1 1579.82 1527.27 68.49 o -10 4 1 1676.77 1676.61 91.18 o -8 4 1 4265.47 3969.68 136.90 o -6 4 1 1341.78 1358.33 36.14 o -4 4 1 14697.10 15013.01 361.79 o -2 4 1 2729.53 2718.14 92.02 o 0 4 1 1283.03 1296.00 45.71 o 2 4 1 369.70 402.32 19.27 o 4 4 1 6317.87 6133.71 217.87 o 6 4 1 145.80 142.70 10.94 o 8 4 1 65.27 59.72 10.16 o 10 4 1 2046.17 2095.83 41.68 o 12 4 1 72.08 30.54 13.63 o 14 4 1 1980.96 1914.86 59.95 o 16 4 1 109.10 128.31 20.84 o -17 5 1 15.21 -5.72 19.48 o -15 5 1 539.26 479.85 29.02 o -13 5 1 128.33 103.37 18.15 o -11 5 1 22.57 12.71 11.17 o -9 5 1 646.93 599.38 24.37 o -7 5 1 26.91 26.02 8.20 o -5 5 1 171.50 187.22 11.18 o -3 5 1 2073.43 2071.73 39.97 o -1 5 1 72.72 64.59 5.47 o 1 5 1 7929.53 7942.04 262.31 o 3 5 1 338.59 400.11 12.28 o 5 5 1 1119.65 1276.34 35.40 o 7 5 1 86.52 129.78 11.00 o 9 5 1 239.93 245.22 22.21 o 11 5 1 50.78 32.70 12.68 o 13 5 1 341.30 279.83 28.40 o 15 5 1 30.33 8.01 17.43 o 17 5 1 13.79 21.88 21.07 o -16 6 1 567.15 575.65 31.74 o -14 6 1 418.53 439.17 30.39 o -12 6 1 2389.51 2316.62 82.61 o -10 6 1 2627.27 2585.50 105.22 o -8 6 1 554.81 505.96 32.69 o -6 6 1 546.85 504.13 15.02 o -4 6 1 7999.66 7896.55 177.32 o -2 6 1 22331.30 22721.51 293.46 o 0 6 1 67.09 91.58 6.88 o 2 6 1 2580.09 2863.20 83.55 o 4 6 1 4339.97 4392.22 101.85 o 6 6 1 1071.79 1191.42 29.77 o 8 6 1 85.05 108.36 11.93 o 10 6 1 1784.71 1787.52 58.74 o 12 6 1 19.54 -0.53 14.15 o 14 6 1 714.14 685.05 34.12 o 16 6 1 515.73 469.79 28.69 o -17 7 1 796.59 713.30 36.19 o -15 7 1 343.34 319.93 23.70 o -13 7 1 0.82 -14.12 14.12 o -11 7 1 0.77 -5.14 13.95 o -9 7 1 1317.55 1357.16 40.84 o -7 7 1 623.13 741.15 17.19 o -5 7 1 3297.75 3214.14 113.40 o -3 7 1 1082.65 1147.83 35.38 o -1 7 1 1061.69 976.89 21.26 o 1 7 1 2845.29 3040.26 36.64 o 3 7 1 473.41 536.84 54.03 o 5 7 1 2669.04 2709.14 66.66 o 7 7 1 42.96 33.76 8.46 o 9 7 1 855.65 949.73 28.77 o 11 7 1 424.36 427.41 24.54 o 13 7 1 0.27 -14.63 15.20 o 15 7 1 5.00 18.66 18.58 o -16 8 1 265.05 248.64 28.58 o -14 8 1 797.84 860.55 38.41 o -12 8 1 258.29 263.42 19.76 o -10 8 1 128.75 129.35 12.48 o -8 8 1 296.09 285.40 13.43 o -6 8 1 626.64 538.55 60.46 o -4 8 1 2518.04 2505.70 75.87 o -2 8 1 1609.48 1524.36 24.62 o 0 8 1 1237.04 1434.71 22.77 o 2 8 1 1819.13 2046.96 31.18 o 4 8 1 1934.04 1836.11 65.79 o 6 8 1 80.17 75.31 9.94 o 8 8 1 5.36 10.23 9.31 o 10 8 1 38.68 41.36 11.01 o 12 8 1 35.17 51.60 15.87 o 14 8 1 174.37 151.85 20.30 o 16 8 1 423.81 411.45 28.93 o -15 9 1 739.78 736.47 28.72 o -13 9 1 5.16 8.17 14.39 o -11 9 1 34.47 32.29 12.44 o -9 9 1 2187.21 2206.67 55.55 o -7 9 1 5991.38 6063.38 221.95 o -5 9 1 2806.10 2773.84 89.25 o -3 9 1 10.35 19.64 8.98 o -1 9 1 880.15 889.82 19.32 o 1 9 1 398.65 364.38 15.52 o 3 9 1 1959.28 1938.61 39.16 o 5 9 1 3.93 4.78 9.49 o 7 9 1 2196.03 2135.35 76.13 o 9 9 1 2777.86 2928.77 84.19 o 11 9 1 577.01 592.94 27.34 o 13 9 1 232.59 239.98 20.60 o 15 9 1 19.61 8.82 19.46 o -14 10 1 0.92 -15.12 17.71 o -12 10 1 69.39 52.72 16.20 o -10 10 1 1.97 -11.58 11.58 o -8 10 1 144.53 127.56 13.19 o -6 10 1 39.82 27.58 11.44 o -4 10 1 203.07 216.83 16.53 o -2 10 1 223.36 217.44 16.19 o 0 10 1 575.27 587.48 23.81 o 2 10 1 16.28 16.79 16.03 o 4 10 1 2655.18 2634.08 58.34 o 6 10 1 171.30 178.76 18.14 o 8 10 1 703.76 684.75 37.23 o 10 10 1 2.69 -10.04 13.52 o 12 10 1 101.46 102.42 18.14 o 14 10 1 9.86 -6.28 18.78 o -13 11 1 244.62 263.97 25.03 o -11 11 1 329.48 317.67 40.02 o -9 11 1 297.95 302.04 31.08 o -7 11 1 1490.67 1502.64 83.84 o -5 11 1 1756.56 1732.44 47.95 o -3 11 1 1412.01 1382.96 43.23 o -1 11 1 1507.58 1426.54 42.99 o 1 11 1 48.87 37.55 18.11 o 3 11 1 135.94 169.84 22.54 o 5 11 1 646.63 621.23 28.22 o 7 11 1 2867.83 2794.42 104.64 o 9 11 1 698.76 800.94 34.82 o 11 11 1 62.31 50.24 18.44 o 13 11 1 821.60 910.99 35.19 o -12 12 1 100.39 73.36 25.57 o -10 12 1 123.10 108.55 28.37 o -8 12 1 577.91 609.90 63.75 o -6 12 1 822.12 777.66 40.55 o -4 12 1 11.03 8.71 18.70 o -2 12 1 84.20 58.77 20.57 o 0 12 1 1004.65 928.41 39.52 o 2 12 1 189.26 178.76 24.08 o 4 12 1 385.67 353.63 29.38 o 6 12 1 229.06 275.48 29.61 o 8 12 1 0.74 -19.35 23.67 o 10 12 1 46.93 24.89 27.13 o 12 12 1 72.99 103.60 32.99 o -11 13 1 132.05 152.03 32.91 o -9 13 1 676.46 742.24 75.69 o -7 13 1 37.44 24.40 24.47 o -5 13 1 771.90 787.34 41.58 o -3 13 1 119.98 104.21 23.26 o -1 13 1 584.81 555.00 36.02 o 1 13 1 0.28 21.54 20.17 o 3 13 1 11.22 18.30 20.35 o 5 13 1 41.75 45.15 45.41 o 7 13 1 230.01 236.84 29.98 o 9 13 1 32.26 32.68 27.38 o 11 13 1 306.49 356.73 55.60 o -10 14 1 441.60 400.73 41.16 o -8 14 1 125.31 127.13 31.44 o -6 14 1 900.25 870.34 47.35 o -4 14 1 200.24 194.32 37.55 o -2 14 1 510.24 523.04 69.87 o 0 14 1 94.78 83.25 31.73 o 2 14 1 350.30 352.56 32.90 o 4 14 1 517.11 459.63 51.82 o 6 14 1 68.27 56.74 27.16 o 8 14 1 287.35 261.77 47.74 o 10 14 1 63.23 9.96 31.89 o -9 15 1 46.72 30.32 32.40 o -7 15 1 50.99 17.95 27.99 o -5 15 1 18.46 25.74 27.57 o -3 15 1 49.19 7.59 25.93 o -1 15 1 227.51 222.82 32.32 o 1 15 1 0.02 12.33 24.91 o 3 15 1 41.88 25.59 43.38 o 5 15 1 54.69 25.26 40.47 o 7 15 1 88.93 103.72 31.99 o -6 16 1 89.71 132.54 33.55 o -4 16 1 265.20 328.11 37.77 o -2 16 1 241.26 207.25 33.75 o 0 16 1 355.42 389.71 38.07 o 2 16 1 118.08 103.64 30.88 o 4 16 1 86.08 71.50 30.26 o 6 16 1 169.74 162.29 58.22 o -1 17 1 0.45 20.50 30.05 o 1 17 1 48.65 46.86 31.69 o -18 0 2 1007.81 1045.71 54.11 o -16 0 2 180.44 235.24 30.05 o -14 0 2 1440.51 1298.71 59.10 o -12 0 2 4491.07 4510.61 374.38 o -10 0 2 3426.49 3150.07 164.48 o -8 0 2 644.77 887.52 74.53 o -6 0 2 10.34 21.22 8.67 o -4 0 2 117512.53 111248.93 6519.86 o -2 0 2 16534.35 16465.98 955.74 o 0 0 2 117.18 144.98 8.73 o 2 0 2 12068.35 12188.35 105.97 o 4 0 2 6294.56 5858.90 237.26 o 6 0 2 4770.87 4852.04 326.05 o 8 0 2 203.06 186.11 16.67 o 10 0 2 62.05 30.91 17.18 o 12 0 2 8052.06 7707.82 520.81 o 14 0 2 1738.65 1602.11 93.45 o 16 0 2 367.19 396.59 41.34 o 18 0 2 18.41 56.24 32.22 o -17 1 2 105.59 93.42 20.19 o -15 1 2 5.15 2.10 15.75 o -13 1 2 101.56 110.14 14.89 o -11 1 2 3506.56 3499.43 107.15 o -9 1 2 300.77 291.21 16.47 o -7 1 2 185.50 202.04 14.79 o -5 1 2 1736.33 1769.41 48.07 o -3 1 2 6206.61 6098.17 175.56 o -1 1 2 318.76 278.37 26.12 o 1 1 2 7021.37 6654.63 161.87 o 3 1 2 4286.42 4209.10 35.85 o 5 1 2 835.86 939.09 24.46 o 7 1 2 1590.31 1489.89 46.31 o 9 1 2 1665.88 1737.32 52.44 o 11 1 2 442.25 410.72 37.90 o 13 1 2 1140.30 1125.05 48.91 o 15 1 2 46.65 46.97 16.80 o 17 1 2 62.59 56.89 20.77 o -18 2 2 693.50 724.43 55.67 o -16 2 2 63.82 91.02 18.82 o -14 2 2 245.30 213.07 18.61 o -12 2 2 7194.11 7215.75 232.53 o -10 2 2 3098.75 2923.63 81.60 o -8 2 2 379.61 391.90 16.31 o -6 2 2 3400.70 3514.62 160.51 o -4 2 2 617.95 701.82 31.51 o -2 2 2 1840.66 2080.26 56.39 o 0 2 2 737.26 768.97 59.10 o 2 2 2 7906.34 7366.55 183.04 o 4 2 2 1806.81 1734.27 59.69 o 6 2 2 9815.10 10034.32 286.07 o 8 2 2 521.06 564.77 18.00 o 10 2 2 848.59 763.24 44.79 o 12 2 2 2655.41 2543.50 39.06 o 14 2 2 793.43 738.57 28.89 o 16 2 2 558.27 577.97 34.32 o -17 3 2 2657.29 2453.92 91.10 o -15 3 2 702.91 616.46 28.71 o -13 3 2 2073.48 2002.97 82.11 o -11 3 2 1653.14 1723.70 81.94 o -9 3 2 2612.91 2684.51 139.34 o -7 3 2 207.47 182.78 10.89 o -5 3 2 1194.73 1147.78 55.30 o -3 3 2 7566.17 7815.77 224.21 o -1 3 2 1646.64 1590.20 62.55 o 1 3 2 21016.01 20644.70 577.51 o 3 3 2 230.56 208.61 12.82 o 5 3 2 1016.03 1130.82 30.29 o 7 3 2 1757.34 1660.86 28.00 o 9 3 2 2415.03 2426.96 75.63 o 11 3 2 364.66 358.66 20.35 o 13 3 2 549.51 611.56 26.16 o 15 3 2 811.39 782.13 31.93 o 17 3 2 978.96 955.94 37.29 o -18 4 2 11.37 56.32 22.09 o -16 4 2 97.13 118.72 19.68 o -14 4 2 1.30 -15.25 15.25 o -12 4 2 241.83 213.94 17.48 o -10 4 2 90.51 62.90 11.67 o -8 4 2 1145.33 1190.27 37.90 o -6 4 2 1837.12 1892.48 49.83 o -4 4 2 368.60 300.45 70.92 o -2 4 2 3694.64 3706.85 89.11 o 0 4 2 7061.35 6909.15 219.63 o 2 4 2 113.12 110.39 6.44 o 4 4 2 2830.00 2949.47 56.10 o 6 4 2 2080.97 2039.31 87.49 o 8 4 2 704.44 678.58 24.71 o 10 4 2 230.07 280.40 16.22 o 12 4 2 0.98 -9.76 12.80 o 14 4 2 541.23 546.30 27.84 o 16 4 2 33.98 32.70 19.26 o -17 5 2 958.22 975.92 42.69 o -15 5 2 846.47 904.19 41.01 o -13 5 2 3151.81 3061.17 78.49 o -11 5 2 299.81 324.83 22.02 o -9 5 2 3886.10 4021.72 163.29 o -7 5 2 264.51 217.81 12.03 o -5 5 2 3101.60 2762.89 194.66 o -3 5 2 1783.73 2030.37 39.60 o -1 5 2 278.83 253.18 19.10 o 1 5 2 1122.62 963.61 38.43 o 3 5 2 583.52 633.53 24.58 o 5 5 2 175.32 254.57 12.84 o 7 5 2 1113.68 1104.36 29.34 o 9 5 2 6343.31 5982.37 258.92 o 11 5 2 853.66 943.39 28.83 o 13 5 2 2581.11 2515.08 75.72 o 15 5 2 709.65 702.46 36.47 o 17 5 2 787.13 823.36 47.29 o -16 6 2 99.08 78.37 20.75 o -14 6 2 357.37 374.69 23.22 o -12 6 2 31.78 44.60 13.29 o -10 6 2 604.75 628.13 22.24 o -8 6 2 288.27 292.29 16.98 o -6 6 2 179.08 240.83 10.86 o -4 6 2 3022.85 3209.12 48.28 o -2 6 2 166.70 166.41 19.19 o 0 6 2 1269.93 1316.03 164.09 o 2 6 2 1538.09 1720.26 38.84 o 4 6 2 3906.15 3947.26 85.71 o 6 6 2 1.62 -2.34 6.76 o 8 6 2 26.47 13.21 10.45 o 10 6 2 71.26 31.77 12.23 o 12 6 2 635.63 628.82 29.92 o 14 6 2 166.65 191.66 20.71 o 16 6 2 0.35 5.77 20.67 o -17 7 2 64.14 80.37 23.02 o -15 7 2 903.15 894.69 53.89 o -13 7 2 1614.11 1607.46 60.00 o -11 7 2 16.58 21.77 13.34 o -9 7 2 3082.51 3130.13 75.97 o -7 7 2 1109.95 1113.19 32.32 o -5 7 2 20.51 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