#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:29:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181244 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232278.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232278_Fobs loop_ _publ_author_name 'Yin, Bang-Shao' 'Li, Tian-Bao' 'Yang, Ming-Sheng' _publ_section_title ; \m-Propane-1,3-dithiolato-\k^4^S,S':S,S'-bis[dicarbonyl(triphenylphosphane-\kP)iron(II)](Fe---Fe) ; _journal_coeditor_code HB6432 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1502 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 77.773 _cell_angle_beta 89.496 _cell_angle_gamma 71.187 _cell_length_a 9.1393 _cell_length_b 13.4796 _cell_length_c 16.7861 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8402 _cod_data_source_file hb6432Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelx in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6861.04 7065.45 327.25 o 2 0 0 7328.10 8144.56 314.38 o 3 0 0 851.51 733.20 56.06 o 4 0 0 2413.69 2435.14 147.51 o 5 0 0 945.05 625.49 103.68 o 6 0 0 76.18 47.48 35.34 o 7 0 0 44.04 46.57 40.36 o 8 0 0 116.54 112.99 91.26 o 9 0 0 13.98 13.15 26.64 o 10 0 0 75.78 136.23 122.91 o -10 1 0 39.00 36.07 58.98 o -9 1 0 0.57 16.39 66.29 o -8 1 0 32.04 60.91 48.19 o -7 1 0 148.66 116.24 53.43 o -6 1 0 935.88 769.44 128.64 o -5 1 0 1526.91 1109.18 96.74 o -4 1 0 3315.41 2054.46 244.83 o -3 1 0 13584.27 13507.56 946.35 o -2 1 0 14082.89 13468.86 840.91 o -1 1 0 1482.72 1246.22 69.20 o 0 1 0 9321.79 7970.74 1116.80 o 1 1 0 30542.47 33461.52 817.02 o 2 1 0 4253.60 4396.46 185.86 o 3 1 0 2516.69 1815.81 236.65 o 4 1 0 3016.78 3157.38 133.47 o 5 1 0 5636.39 5131.69 1012.69 o 6 1 0 1424.90 1461.99 316.11 o 7 1 0 138.19 190.44 122.75 o 8 1 0 487.05 508.01 134.78 o 9 1 0 440.16 503.50 196.82 o 10 1 0 238.85 223.60 183.29 o -9 2 0 76.73 108.08 78.19 o -8 2 0 69.78 139.53 156.52 o -7 2 0 45.63 78.95 56.91 o -6 2 0 1037.46 862.04 128.58 o -5 2 0 892.08 674.10 60.63 o -4 2 0 3668.44 3312.75 385.61 o -3 2 0 5562.55 4536.15 450.61 o -2 2 0 17098.11 18134.17 807.21 o -1 2 0 1961.88 1586.12 149.19 o 0 2 0 827.27 714.05 42.09 o 1 2 0 9451.80 7849.98 813.39 o 2 2 0 1165.12 1040.43 89.96 o 3 2 0 1321.29 1099.62 108.18 o 4 2 0 2531.48 2151.93 244.22 o 5 2 0 2628.92 2190.60 282.31 o 6 2 0 315.75 221.39 127.22 o 7 2 0 346.74 491.07 309.54 o 8 2 0 611.54 605.18 118.02 o 9 2 0 82.84 104.91 78.19 o 10 2 0 48.47 51.41 48.16 o -9 3 0 195.99 256.20 217.31 o -8 3 0 620.53 714.50 258.51 o -7 3 0 297.46 471.45 134.58 o -6 3 0 85.06 61.58 35.83 o -5 3 0 1245.71 1332.41 160.12 o -4 3 0 3228.42 3822.00 216.68 o -3 3 0 58.79 15.92 23.57 o -2 3 0 2687.97 2700.13 114.65 o -1 3 0 648.89 659.70 50.68 o 0 3 0 522.02 518.49 51.51 o 1 3 0 1521.56 1439.20 82.25 o 2 3 0 6399.31 4271.97 591.77 o 3 3 0 939.30 849.79 80.23 o 4 3 0 1226.97 1158.29 73.20 o 5 3 0 2820.14 3499.58 287.82 o 6 3 0 18.44 20.69 43.52 o 7 3 0 371.17 420.50 172.29 o 8 3 0 388.14 623.74 374.64 o 9 3 0 10.69 92.33 80.80 o 10 3 0 302.55 385.47 249.55 o -9 4 0 28.85 23.91 65.51 o -8 4 0 43.61 23.68 49.57 o -7 4 0 2.49 23.74 59.68 o -6 4 0 655.82 728.58 182.41 o -5 4 0 189.47 159.00 117.89 o -4 4 0 447.38 339.53 95.42 o -3 4 0 3827.24 4189.42 230.81 o -2 4 0 1575.58 1620.75 100.80 o -1 4 0 6135.37 6674.22 237.34 o 0 4 0 728.25 661.56 56.39 o 1 4 0 3048.48 2317.75 304.17 o 2 4 0 453.28 384.49 45.94 o 3 4 0 1373.86 1307.63 70.81 o 4 4 0 69.00 28.97 29.60 o 5 4 0 1359.35 1161.95 167.62 o 6 4 0 371.20 272.28 77.34 o 7 4 0 731.79 617.74 204.33 o 8 4 0 327.95 485.94 158.53 o 9 4 0 317.27 475.57 145.03 o 10 4 0 4.48 8.19 56.93 o -8 5 0 148.58 205.23 213.78 o -7 5 0 19.10 27.93 66.58 o -6 5 0 101.14 133.95 95.09 o -5 5 0 368.40 451.40 243.06 o -4 5 0 272.22 328.89 195.92 o -3 5 0 2309.00 2972.36 221.08 o -2 5 0 125.65 91.98 27.53 o -1 5 0 4573.03 4509.76 158.09 o 0 5 0 1374.73 1302.48 47.34 o 1 5 0 3108.00 3189.21 126.00 o 2 5 0 1.05 4.25 7.13 o 3 5 0 1203.18 1086.17 51.61 o 4 5 0 36.98 16.55 17.43 o 5 5 0 263.29 186.96 91.89 o 6 5 0 62.52 109.16 80.16 o 7 5 0 118.15 234.61 126.87 o 8 5 0 96.94 130.24 62.96 o 9 5 0 209.16 268.81 194.50 o 10 5 0 168.08 260.71 157.36 o -8 6 0 6.92 49.08 59.27 o -7 6 0 0.16 -15.70 89.86 o -6 6 0 220.36 282.07 221.04 o -5 6 0 245.41 234.59 128.43 o -4 6 0 391.97 468.66 272.59 o -3 6 0 2729.79 3431.03 512.25 o -2 6 0 5265.68 4400.85 651.08 o -1 6 0 724.80 729.48 68.73 o 0 6 0 4300.92 4290.02 163.34 o 1 6 0 2356.25 2099.36 137.85 o 2 6 0 717.15 757.13 112.60 o 3 6 0 492.15 376.50 65.99 o 4 6 0 3044.29 2781.60 269.01 o 5 6 0 62.94 58.64 29.83 o 6 6 0 22.93 51.04 50.50 o 7 6 0 42.27 77.55 77.08 o 8 6 0 162.11 274.70 187.09 o 9 6 0 13.61 38.62 46.86 o 10 6 0 15.97 33.08 75.26 o -7 7 0 0.40 17.90 52.56 o -6 7 0 432.59 452.66 340.03 o -5 7 0 267.73 261.29 170.26 o -4 7 0 56.13 171.54 93.75 o -3 7 0 736.78 800.88 269.96 o -2 7 0 5556.57 5616.75 793.67 o -1 7 0 36.00 24.61 19.42 o 0 7 0 2333.67 2481.64 81.04 o 1 7 0 5790.32 5613.30 322.40 o 2 7 0 2772.91 2939.99 173.32 o 3 7 0 1680.96 1393.60 199.28 o 4 7 0 1265.72 1109.55 172.94 o 5 7 0 686.76 558.06 107.03 o 6 7 0 605.62 565.64 170.51 o 7 7 0 896.84 868.96 123.26 o 8 7 0 369.14 452.03 307.78 o 9 7 0 2.36 19.78 74.51 o 10 7 0 704.67 723.32 147.09 o -7 8 0 139.25 321.21 298.94 o -6 8 0 142.28 229.66 187.55 o -5 8 0 191.14 325.61 228.37 o -4 8 0 5.86 24.21 54.09 o -3 8 0 1325.62 1362.09 371.83 o -2 8 0 391.90 284.50 55.76 o -1 8 0 3319.10 3425.79 240.58 o 0 8 0 8.92 12.67 12.62 o 1 8 0 509.64 409.75 51.24 o 2 8 0 1425.12 1559.74 147.01 o 3 8 0 1360.06 1652.83 415.96 o 4 8 0 292.42 314.97 42.35 o 5 8 0 136.35 119.87 51.02 o 6 8 0 2.72 14.80 13.60 o 7 8 0 586.14 643.88 108.69 o 8 8 0 0.59 23.75 40.89 o 9 8 0 1.06 43.84 62.88 o 10 8 0 6.21 34.62 61.65 o -6 9 0 6.31 65.20 87.72 o -5 9 0 75.58 107.22 96.37 o -4 9 0 26.36 40.60 45.92 o -3 9 0 1233.04 1505.23 327.08 o -2 9 0 1427.13 1245.92 143.04 o -1 9 0 185.39 191.49 52.93 o 0 9 0 753.49 689.02 82.60 o 1 9 0 33.40 32.13 16.51 o 2 9 0 2.62 12.46 56.68 o 3 9 0 753.14 550.75 179.34 o 4 9 0 2141.09 1909.52 302.47 o 5 9 0 621.88 649.31 122.52 o 6 9 0 126.02 104.11 47.89 o 7 9 0 10.64 25.79 33.52 o 8 9 0 362.93 469.30 115.13 o 9 9 0 1.87 8.15 53.34 o 10 9 0 5.46 49.69 66.87 o -5 10 0 255.44 410.96 198.24 o -4 10 0 81.65 131.06 87.46 o -3 10 0 90.84 151.91 156.38 o -2 10 0 1073.59 1175.41 166.72 o -1 10 0 666.23 656.19 73.36 o 0 10 0 124.33 113.95 39.67 o 1 10 0 107.15 122.00 72.30 o 2 10 0 151.53 220.82 176.36 o 3 10 0 4.21 79.27 99.33 o 4 10 0 83.36 149.00 177.22 o 5 10 0 2864.21 2971.93 213.24 o 6 10 0 510.66 636.81 89.09 o 7 10 0 50.32 133.58 70.77 o 8 10 0 21.38 -0.24 47.12 o 9 10 0 169.95 366.49 240.72 o 10 10 0 142.29 366.17 304.43 o -4 11 0 32.20 46.55 65.13 o -3 11 0 209.58 219.70 118.45 o -2 11 0 458.40 441.15 98.89 o -1 11 0 140.05 140.10 95.95 o 0 11 0 556.94 591.54 59.39 o 1 11 0 2735.83 3452.01 644.57 o 2 11 0 108.53 117.48 91.45 o 3 11 0 214.50 254.63 185.52 o 4 11 0 747.16 754.52 160.41 o 5 11 0 1204.71 1400.33 332.56 o 6 11 0 539.41 886.07 265.49 o 7 11 0 243.38 337.06 70.05 o 8 11 0 24.68 62.99 90.63 o 9 11 0 31.07 127.11 151.50 o -3 12 0 0.67 7.58 34.22 o -2 12 0 495.66 515.47 81.75 o -1 12 0 236.48 326.81 268.49 o 0 12 0 296.82 308.92 65.58 o 1 12 0 1365.03 1439.56 178.32 o 2 12 0 1617.56 1593.05 242.42 o 3 12 0 167.26 154.02 113.40 o 4 12 0 57.67 68.99 87.19 o 5 12 0 439.83 671.37 188.19 o 6 12 0 608.33 1115.36 279.85 o 7 12 0 30.17 56.21 117.62 o 8 12 0 10.28 77.50 153.47 o 9 12 0 0.70 29.75 64.96 o -2 13 0 339.17 393.49 401.21 o -1 13 0 112.92 65.94 80.10 o 0 13 0 247.56 310.84 209.48 o 1 13 0 156.79 339.89 165.47 o 2 13 0 1773.68 2373.59 370.85 o 3 13 0 38.88 73.36 71.25 o 4 13 0 44.50 58.71 94.71 o 5 13 0 240.81 467.20 422.06 o 6 13 0 604.77 1117.48 477.58 o 7 13 0 196.88 382.47 560.88 o 8 13 0 45.09 88.32 117.28 o -1 14 0 75.92 102.92 118.46 o 0 14 0 127.74 211.10 214.94 o 1 14 0 76.80 139.22 112.57 o 2 14 0 683.98 791.57 212.24 o 3 14 0 762.93 1253.53 288.55 o 4 14 0 2.74 7.77 52.12 o 5 14 0 2.43 44.35 90.58 o 6 14 0 590.78 985.74 210.42 o 7 14 0 248.39 536.78 807.58 o 1 15 0 196.80 356.41 406.28 o 2 15 0 23.43 54.38 68.74 o 3 15 0 86.69 169.11 181.40 o 4 15 0 123.78 204.37 250.59 o 5 15 0 33.89 28.18 68.45 o 6 15 0 1.96 39.93 99.18 o -5 -15 1 18.37 38.36 75.29 o -4 -15 1 102.55 242.43 131.98 o -3 -15 1 21.28 81.87 84.09 o -2 -15 1 16.02 5.14 37.73 o -1 -15 1 5.27 24.14 63.63 o -7 -14 1 132.90 294.31 364.43 o -6 -14 1 14.14 51.68 93.04 o -5 -14 1 249.28 390.00 407.70 o -4 -14 1 84.56 157.45 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1 16.56 19.71 9.53 o -1 -7 1 9.72 4.22 8.98 o 0 -7 1 406.51 395.23 48.88 o 1 -7 1 104.61 63.47 25.00 o 2 -7 1 3944.38 3538.20 287.73 o 3 -7 1 295.09 345.45 118.07 o 4 -7 1 3035.66 3827.09 1094.71 o 5 -7 1 1820.67 2132.61 627.56 o 6 -7 1 1.26 7.56 77.44 o 7 -7 1 14.49 91.39 106.97 o -10 -6 1 332.50 601.48 201.46 o -9 -6 1 4.82 33.66 51.64 o -8 -6 1 36.19 26.82 40.04 o -7 -6 1 937.37 828.09 137.84 o -6 -6 1 387.96 378.60 111.16 o -5 -6 1 248.33 185.06 91.16 o -4 -6 1 20.62 29.41 24.84 o -3 -6 1 142.04 115.59 50.98 o -2 -6 1 3582.85 2992.04 234.73 o -1 -6 1 3286.39 2836.00 174.18 o 0 -6 1 706.66 658.81 75.27 o 1 -6 1 385.13 362.86 39.41 o 2 -6 1 2208.33 1846.62 271.29 o 3 -6 1 668.49 677.10 205.03 o 4 -6 1 1176.01 1396.08 373.92 o 5 -6 1 601.84 860.43 291.53 o 6 -6 1 8.24 57.64 57.73 o 7 -6 1 33.66 -17.74 89.22 o 8 -6 1 197.73 322.76 406.10 o -10 -5 1 746.55 1235.96 362.01 o -9 -5 1 298.79 451.67 147.19 o -8 -5 1 1315.17 1270.96 244.96 o -7 -5 1 313.22 382.39 199.02 o -6 -5 1 1286.50 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