#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:29:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181244 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/22/2232280.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232280_Fobs loop_ _publ_author_name 'Jiang, Yu-Hang' 'Cui, Li-Na' 'Huang, Xu' 'Jin, Qiong-Hua' 'Zhang, Cun-Lin' _publ_section_title ; Tris(3-amino-5,6-dimethyl-1,2,4-triazine-\kN^2^)silver(I) trifluromethanesulfonate--3-amino-5,6-dimethyl-1,2,4-triazine (1/1) ; _journal_coeditor_code HB6434 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1526 _journal_page_last m1527 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 76.735 _cell_angle_beta 72.565 _cell_angle_gamma 81.201 _cell_length_a 13.9357 _cell_length_b 15.1693 _cell_length_c 16.2257 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.8403 _cod_data_source_file hb6434Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 101028g in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 720.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 240.38 287.00 22.15 o 3 0 0 950.32 1002.02 45.73 o 4 0 0 902.17 605.17 38.85 o 5 0 0 364.06 540.13 84.36 o 6 0 0 1027.14 1021.95 122.86 o 7 0 0 614.86 719.05 111.54 o 8 0 0 1847.80 1740.43 140.98 o 9 0 0 1451.46 1585.87 190.24 o 10 0 0 743.63 1106.31 176.08 o 11 0 0 0.03 17.55 85.49 o 12 0 0 2334.91 2166.77 198.16 o 13 0 0 395.38 632.42 166.46 o 15 0 0 1.89 19.82 170.42 o -15 1 0 6.44 31.71 181.74 o -14 1 0 65.92 167.59 191.37 o -13 1 0 293.57 267.24 197.03 o -12 1 0 216.68 201.03 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