#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/23/2232312.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232312_Fobs loop_ _publ_author_name 'Pansuriya, Pramod B.' 'Friedrich, Holger B.' 'Maguire, Glenn E. M.' _publ_section_title ; 4,10,16,22-Tetrakis(2-chloroacetoxy)-6,12,18,24-tetramethoxy-2,8,14,20-tetrapentylresorcin[4]arene ; _journal_coeditor_code HG5096 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2907 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.407 _cell_angle_gamma 90.000 _cell_length_a 12.4190 _cell_length_b 26.1925 _cell_length_c 19.1638 _exptl_crystal_F_000 2400.00 _reflns_d_resolution_high 0.7684 _[local]_cod_data_source_file hg5096Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' c5tmtcoc in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 350.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13619.06 13432.96 197.36 o 4 0 0 2074.82 2734.01 56.07 o 6 0 0 224.27 153.57 16.55 o 8 0 0 398.83 582.08 32.89 o 10 0 0 21.01 26.22 19.51 o 12 0 0 1882.25 1724.78 182.68 o 14 0 0 661.66 605.02 52.87 o 1 1 0 5308.01 5662.18 70.66 o 2 1 0 279.03 246.46 6.20 o 3 1 0 84222.14 81694.98 927.32 o 4 1 0 4306.15 4526.53 61.82 o 5 1 0 10845.24 9605.26 125.55 o 6 1 0 8.90 -8.18 9.75 o 7 1 0 244.84 237.11 14.35 o 8 1 0 89.57 134.28 17.30 o 9 1 0 134.92 153.04 13.76 o 10 1 0 1422.80 1396.65 30.30 o 11 1 0 3.20 25.42 14.60 o 12 1 0 21.56 21.25 15.97 o 13 1 0 95.55 97.42 21.68 o 14 1 0 39.36 12.30 26.54 o 15 1 0 468.92 489.28 37.79 o 0 2 0 2568.25 1730.77 191.49 o 1 2 0 1.75 -2.95 2.95 o 2 2 0 1.69 -2.30 3.86 o 3 2 0 2680.76 3611.83 40.81 o 4 2 0 8294.77 8244.11 96.45 o 5 2 0 194.04 102.19 9.66 o 6 2 0 3725.59 3588.44 52.09 o 7 2 0 913.51 851.94 20.97 o 8 2 0 1271.71 1032.65 23.68 o 9 2 0 916.96 919.88 39.68 o 10 2 0 519.48 546.12 43.58 o 11 2 0 759.91 681.15 23.64 o 12 2 0 467.90 436.58 25.39 o 13 2 0 63.39 33.63 19.86 o 14 2 0 258.28 197.45 30.60 o 15 2 0 89.71 151.01 36.42 o 1 3 0 801.43 837.71 13.71 o 2 3 0 4951.98 4950.84 58.29 o 3 3 0 39.61 62.13 6.15 o 4 3 0 20175.12 22145.47 229.48 o 5 3 0 796.43 602.54 16.17 o 6 3 0 426.51 341.79 18.48 o 7 3 0 30.80 38.31 10.15 o 8 3 0 93.39 30.60 17.30 o 9 3 0 880.62 824.04 22.19 o 10 3 0 165.51 150.80 17.30 o 11 3 0 177.06 191.35 18.14 o 12 3 0 255.43 249.72 22.56 o 13 3 0 388.27 367.73 35.72 o 14 3 0 297.98 251.96 32.62 o 15 3 0 37.88 45.66 28.43 o 0 4 0 15222.22 17577.79 260.45 o 1 4 0 185.71 116.49 7.18 o 2 4 0 49183.25 53503.31 608.15 o 3 4 0 47964.13 47267.63 457.04 o 4 4 0 11058.87 11666.85 122.84 o 5 4 0 1514.91 1463.25 22.47 o 6 4 0 0.72 13.64 9.30 o 7 4 0 5709.30 5953.28 121.59 o 8 4 0 7.45 48.97 11.34 o 9 4 0 523.02 574.11 18.81 o 10 4 0 53.72 19.28 13.67 o 11 4 0 681.26 631.39 55.50 o 12 4 0 86.54 55.69 20.20 o 13 4 0 51.51 71.52 28.83 o 14 4 0 151.15 123.82 23.40 o 15 4 0 46.97 20.40 28.21 o 1 5 0 110.16 77.04 7.23 o 2 5 0 62053.04 61658.33 649.27 o 3 5 0 5344.78 6229.73 73.29 o 4 5 0 15169.25 14612.80 153.21 o 5 5 0 5985.53 5941.84 71.29 o 6 5 0 4029.11 3953.74 50.10 o 7 5 0 6461.23 6563.75 89.77 o 8 5 0 566.63 553.84 27.98 o 9 5 0 55.56 72.20 12.35 o 10 5 0 48.02 46.37 13.00 o 11 5 0 126.78 166.67 20.52 o 12 5 0 273.54 297.60 23.20 o 13 5 0 375.96 425.49 26.75 o 14 5 0 139.59 216.12 25.79 o 15 5 0 6.90 -1.94 25.92 o 0 6 0 4365.62 4698.47 71.20 o 1 6 0 66273.71 66716.83 884.92 o 2 6 0 6306.64 7022.82 92.35 o 3 6 0 12998.06 13574.14 155.38 o 4 6 0 4416.63 4291.48 52.86 o 5 6 0 331.33 300.65 14.72 o 6 6 0 599.70 544.17 13.34 o 7 6 0 14.99 40.88 8.04 o 8 6 0 191.86 214.70 12.44 o 9 6 0 3.16 -0.29 11.18 o 10 6 0 1291.29 1210.41 35.37 o 11 6 0 75.18 93.57 19.38 o 12 6 0 9.08 1.34 18.49 o 13 6 0 21.14 -2.91 20.05 o 14 6 0 4.23 27.00 21.87 o 15 6 0 28.53 21.15 27.94 o 1 7 0 413.08 483.02 16.82 o 2 7 0 12130.40 12317.45 158.73 o 3 7 0 3138.55 2920.21 46.44 o 4 7 0 2534.47 2162.57 45.13 o 5 7 0 1241.45 1474.28 25.54 o 6 7 0 1422.98 1809.83 35.27 o 7 7 0 1160.89 1202.43 20.52 o 8 7 0 513.86 518.20 16.17 o 9 7 0 846.22 700.15 29.85 o 10 7 0 56.49 56.28 17.40 o 11 7 0 1671.94 1547.17 40.86 o 12 7 0 395.64 375.36 25.11 o 13 7 0 2.92 18.17 20.03 o 14 7 0 0.06 9.45 22.42 o 15 7 0 0.02 21.18 23.35 o 0 8 0 40300.66 40264.45 590.75 o 1 8 0 139.41 152.17 12.28 o 2 8 0 1773.01 2613.38 38.09 o 3 8 0 204.35 186.22 9.48 o 4 8 0 1687.98 2059.41 31.24 o 5 8 0 870.70 832.73 17.97 o 6 8 0 0.16 -6.41 8.85 o 7 8 0 8.89 9.94 10.02 o 8 8 0 7.49 30.11 11.19 o 9 8 0 904.68 938.23 29.91 o 10 8 0 12.74 -1.96 16.72 o 11 8 0 44.39 43.45 19.94 o 12 8 0 9.73 5.82 19.18 o 13 8 0 62.46 62.35 21.59 o 14 8 0 64.08 44.10 22.33 o 1 9 0 62.47 75.81 7.66 o 2 9 0 983.63 1118.54 21.23 o 3 9 0 11520.44 11656.25 151.82 o 4 9 0 5943.75 6033.71 118.78 o 5 9 0 48.66 140.14 8.24 o 6 9 0 163.08 232.22 17.52 o 7 9 0 226.11 330.84 16.62 o 8 9 0 2763.21 2921.37 46.04 o 9 9 0 307.19 309.77 20.10 o 10 9 0 676.05 648.66 26.72 o 11 9 0 382.40 336.09 23.08 o 12 9 0 108.79 134.89 21.21 o 13 9 0 91.02 114.73 22.45 o 14 9 0 18.30 31.85 21.85 o 0 10 0 2144.63 2119.99 55.80 o 1 10 0 43.23 58.62 7.89 o 2 10 0 2524.73 2180.02 33.97 o 3 10 0 17372.58 18927.95 280.99 o 4 10 0 185.08 275.99 20.34 o 5 10 0 184.88 294.13 31.13 o 6 10 0 1897.24 1914.98 48.84 o 7 10 0 3305.59 3536.73 52.02 o 8 10 0 0.08 22.69 10.22 o 9 10 0 169.82 235.16 18.44 o 10 10 0 9.59 18.70 20.75 o 11 10 0 170.89 194.50 20.77 o 12 10 0 18.68 1.39 36.50 o 13 10 0 146.62 144.94 22.59 o 14 10 0 0.00 -19.52 19.52 o 1 11 0 1825.46 1527.86 30.65 o 2 11 0 8420.68 9779.45 148.50 o 3 11 0 3679.15 3854.53 63.53 o 4 11 0 49.73 62.42 17.39 o 5 11 0 493.95 431.01 24.09 o 6 11 0 2600.06 3171.15 73.49 o 7 11 0 1422.20 1474.08 26.22 o 8 11 0 945.98 999.72 27.46 o 9 11 0 411.79 471.48 22.48 o 10 11 0 199.83 219.99 18.80 o 11 11 0 4.26 -16.25 16.25 o 12 11 0 22.80 5.36 18.21 o 13 11 0 265.16 196.52 25.55 o 14 11 0 39.39 57.62 21.03 o 0 12 0 3351.27 3334.98 67.61 o 1 12 0 1567.55 1708.04 34.01 o 2 12 0 1546.29 1352.18 29.60 o 3 12 0 2859.38 3301.61 79.92 o 4 12 0 3269.63 2907.81 66.41 o 5 12 0 56.57 -0.34 18.68 o 6 12 0 671.15 740.27 41.12 o 7 12 0 641.53 683.89 38.18 o 8 12 0 1090.43 1151.43 22.33 o 9 12 0 22.85 15.93 12.82 o 10 12 0 289.65 255.43 39.71 o 11 12 0 13.85 31.50 15.86 o 12 12 0 294.79 277.55 20.76 o 13 12 0 83.81 37.86 17.86 o 14 12 0 0.07 -17.80 17.80 o 1 13 0 1165.46 1550.59 31.78 o 2 13 0 389.28 625.64 20.22 o 3 13 0 271.87 313.96 14.33 o 4 13 0 726.69 952.77 22.95 o 5 13 0 5392.36 5434.54 112.50 o 6 13 0 1097.07 959.25 76.36 o 7 13 0 0.20 12.50 22.00 o 8 13 0 1.54 4.72 32.31 o 9 13 0 40.53 -20.58 24.88 o 10 13 0 57.52 38.03 26.54 o 11 13 0 225.03 240.55 15.72 o 12 13 0 26.57 13.54 13.56 o 13 13 0 11.60 26.34 35.24 o 14 13 0 29.28 26.66 32.80 o 0 14 0 180.07 123.74 22.32 o 1 14 0 91.89 176.79 10.85 o 2 14 0 58.01 40.24 11.97 o 3 14 0 94.67 79.81 11.83 o 4 14 0 1260.18 1347.08 29.19 o 5 14 0 1307.24 1274.61 42.27 o 6 14 0 578.57 587.57 90.46 o 7 14 0 19.19 23.47 21.17 o 8 14 0 189.36 139.90 56.98 o 9 14 0 253.60 226.68 30.70 o 10 14 0 24.30 11.71 27.38 o 11 14 0 159.59 223.78 33.20 o 12 14 0 39.75 64.71 30.70 o 13 14 0 2.09 10.94 30.31 o 14 14 0 7.59 15.99 32.80 o 1 15 0 0.06 -0.47 9.38 o 2 15 0 53.70 102.39 11.02 o 3 15 0 520.86 576.34 20.36 o 4 15 0 7.58 1.55 10.37 o 5 15 0 295.90 216.80 28.78 o 6 15 0 16.28 10.04 28.19 o 7 15 0 30.23 23.39 23.66 o 8 15 0 49.38 40.32 24.41 o 9 15 0 182.13 86.61 27.38 o 10 15 0 24.62 -5.87 26.58 o 11 15 0 588.78 641.59 43.61 o 12 15 0 96.35 152.68 34.03 o 13 15 0 0.00 -22.00 34.66 o 0 16 0 1652.77 1401.40 37.63 o 1 16 0 65.56 37.52 9.72 o 2 16 0 78.49 116.77 19.49 o 3 16 0 2398.24 2677.14 49.79 o 4 16 0 1226.69 1328.45 30.47 o 5 16 0 49.30 49.98 20.57 o 6 16 0 8.67 3.52 20.72 o 7 16 0 77.42 52.28 25.75 o 8 16 0 48.83 149.27 27.74 o 9 16 0 115.41 142.43 29.87 o 10 16 0 17.96 -11.25 28.21 o 11 16 0 23.15 4.77 36.42 o 12 16 0 51.98 22.17 31.78 o 13 16 0 20.06 29.09 57.56 o 1 17 0 0.01 -5.49 12.04 o 2 17 0 5436.13 5334.86 87.43 o 3 17 0 0.14 -2.04 12.61 o 4 17 0 1235.35 1279.16 30.44 o 5 17 0 1354.14 1286.21 33.83 o 6 17 0 480.76 563.03 33.10 o 7 17 0 142.56 195.46 37.59 o 8 17 0 13.23 19.97 24.92 o 9 17 0 123.00 125.87 33.48 o 10 17 0 1.89 -1.39 83.41 o 11 17 0 51.70 66.22 31.72 o 12 17 0 12.55 4.21 32.80 o 13 17 0 2.76 -32.27 32.27 o 0 18 0 4334.89 4140.51 85.45 o 1 18 0 1094.07 1265.65 26.10 o 2 18 0 2090.90 2276.21 54.42 o 3 18 0 136.68 71.08 13.60 o 4 18 0 0.12 -10.41 11.95 o 5 18 0 534.71 481.08 37.01 o 6 18 0 1319.91 1262.21 48.16 o 7 18 0 1.68 -23.26 23.26 o 8 18 0 31.71 -15.21 25.24 o 9 18 0 38.86 26.35 29.04 o 10 18 0 2.94 -14.26 41.71 o 11 18 0 3.04 -1.77 30.24 o 12 18 0 245.35 373.71 44.64 o 13 18 0 214.70 256.17 82.24 o 1 19 0 190.79 209.96 13.54 o 2 19 0 2699.56 2839.72 53.54 o 3 19 0 965.09 983.10 28.65 o 4 19 0 579.13 485.75 20.62 o 5 19 0 127.67 158.97 24.76 o 6 19 0 418.65 371.89 30.60 o 7 19 0 86.98 35.17 36.42 o 8 19 0 26.61 -15.75 25.59 o 9 19 0 215.58 195.98 30.94 o 10 19 0 31.97 6.95 28.58 o 11 19 0 108.42 116.45 45.82 o 12 19 0 40.79 82.26 34.47 o 0 20 0 163.12 144.50 30.54 o 1 20 0 965.89 849.08 27.02 o 2 20 0 420.91 372.46 20.09 o 3 20 0 12.03 27.31 14.54 o 4 20 0 18.10 22.62 23.47 o 5 20 0 253.03 325.58 57.56 o 6 20 0 450.30 516.64 34.41 o 7 20 0 14.19 0.74 47.58 o 8 20 0 130.41 199.16 79.89 o 9 20 0 4.86 -7.92 28.58 o 10 20 0 117.86 123.06 38.77 o 11 20 0 143.15 83.55 33.79 o 12 20 0 1.47 24.25 62.26 o 1 21 0 29.50 28.37 19.51 o 2 21 0 904.90 683.38 31.33 o 3 21 0 412.53 447.07 37.53 o 4 21 0 314.96 362.74 19.13 o 5 21 0 447.44 377.89 31.14 o 6 21 0 10.76 46.13 26.23 o 7 21 0 24.68 13.85 27.38 o 8 21 0 135.86 226.40 31.91 o 9 21 0 1.24 -19.95 27.60 o 10 21 0 95.06 177.52 34.06 o 11 21 0 58.00 59.91 36.42 o 12 21 0 3.47 28.73 34.86 o 0 22 0 1742.21 1557.77 68.14 o 1 22 0 1599.77 1415.45 44.77 o 2 22 0 66.90 70.82 20.32 o 3 22 0 761.90 839.24 35.64 o 4 22 0 71.47 79.77 16.02 o 5 22 0 83.91 55.45 24.76 o 6 22 0 3.59 -25.71 25.71 o 7 22 0 334.51 290.17 33.64 o 8 22 0 1.69 87.24 30.60 o 9 22 0 106.30 188.56 34.89 o 10 22 0 140.37 147.40 35.69 o 11 22 0 16.48 34.00 34.86 o 1 23 0 852.66 762.86 42.29 o 2 23 0 50.92 66.16 20.88 o 3 23 0 317.46 303.57 23.90 o 4 23 0 113.45 50.52 37.59 o 5 23 0 26.82 -15.27 39.94 o 6 23 0 90.64 139.80 43.47 o 7 23 0 137.11 163.67 33.20 o 8 23 0 47.51 34.05 30.11 o 9 23 0 72.56 53.29 32.37 o 10 23 0 0.45 -32.40 32.40 o 11 23 0 178.44 246.57 41.89 o 0 24 0 469.68 414.70 39.94 o 1 24 0 4.80 14.24 21.07 o 2 24 0 25.17 14.91 19.47 o 3 24 0 639.80 583.33 31.01 o 4 24 0 1001.07 941.01 65.79 o 5 24 0 129.40 151.55 43.47 o 6 24 0 173.80 163.30 44.64 o 7 24 0 1058.12 1174.79 79.89 o 8 24 0 62.22 91.63 46.99 o 9 24 0 44.61 101.92 34.47 o 10 24 0 9.78 47.41 38.18 o 1 25 0 90.87 87.46 25.26 o 2 25 0 160.17 110.54 23.14 o 3 25 0 124.78 120.62 23.03 o 4 25 0 8.81 -38.77 38.77 o 5 25 0 527.02 456.99 56.39 o 6 25 0 174.61 239.66 49.34 o 7 25 0 231.47 277.25 51.69 o 8 25 0 31.44 8.22 48.17 o 9 25 0 1.07 -27.02 44.64 o 10 25 0 102.42 90.46 52.87 o 0 26 0 522.44 529.83 45.82 o 1 26 0 81.59 57.56 24.55 o 2 26 0 741.72 897.46 39.46 o 3 26 0 0.05 -19.55 19.55 o 4 26 0 0.02 -39.94 39.94 o 5 26 0 52.06 -22.32 37.59 o 6 26 0 266.25 260.80 50.52 o 7 26 0 0.06 25.85 48.17 o 8 26 0 106.26 192.67 52.87 o 9 26 0 5.95 3.52 50.52 o 1 27 0 540.76 409.62 31.27 o 2 27 0 341.18 378.08 29.54 o 3 27 0 161.63 138.63 42.29 o 4 27 0 43.54 79.89 42.29 o 5 27 0 260.33 307.80 51.69 o 6 27 0 141.27 153.90 46.99 o 7 27 0 13.99 -8.22 45.82 o 8 27 0 78.13 58.74 49.34 o 9 27 0 0.04 9.40 46.99 o 0 28 0 38.21 52.87 34.07 o 1 28 0 66.57 68.96 24.55 o 2 28 0 22.03 -16.53 23.03 o 3 28 0 1.74 -9.40 37.59 o 4 28 0 32.32 24.67 42.29 o 5 28 0 228.28 226.73 49.34 o 6 28 0 32.06 52.87 46.99 o 7 28 0 16.05 -4.70 49.34 o 8 28 0 0.20 75.19 54.04 o 1 29 0 90.75 82.25 45.23 o 2 29 0 143.71 109.26 32.89 o 3 29 0 46.73 105.73 41.12 o 4 29 0 36.56 21.15 42.29 o 5 29 0 390.42 425.27 59.91 o 6 29 0 13.19 -15.27 48.17 o 7 29 0 89.63 112.78 50.52 o 8 29 0 58.95 32.89 51.69 o 0 30 0 40.55 39.94 36.42 o 1 30 0 31.98 28.61 42.29 o 2 30 0 80.95 89.28 44.64 o 3 30 0 36.28 50.52 41.12 o 4 30 0 24.39 -34.07 41.12 o 5 30 0 54.46 17.62 49.34 o 6 30 0 14.31 -14.10 49.34 o 7 30 0 40.09 -16.45 48.17 o 1 31 0 41.83 56.62 27.26 o 2 31 0 0.00 -41.12 41.12 o 3 31 0 32.72 45.82 43.47 o 4 31 0 40.66 8.22 43.47 o 5 31 0 68.28 130.40 48.17 o 6 31 0 21.50 -24.67 46.99 o 0 32 0 25.55 42.29 38.77 o 1 32 0 1.06 -21.41 28.78 o 2 32 0 2.91 56.39 41.12 o 3 32 0 48.63 38.77 43.47 o 4 32 0 16.76 16.45 44.64 o 5 32 0 28.06 54.04 48.17 o 1 33 0 158.36 184.44 46.99 o 2 33 0 29.71 -24.67 44.64 o 3 33 0 12.59 -45.82 45.82 o 0 34 0 18.97 -34.07 37.59 o -15 0 1 266.80 287.82 48.17 o -13 0 1 40.48 27.02 35.24 o -11 0 1 1609.73 1527.97 47.00 o -9 0 1 756.94 740.80 30.70 o -7 0 1 127.23 182.94 35.83 o -5 0 1 411.67 179.88 13.81 o -3 0 1 48530.58 41114.16 605.66 o -1 0 1 5735.20 5873.11 87.04 o 1 0 1 5302.47 5161.24 97.60 o 3 0 1 6100.68 7175.94 132.50 o 5 0 1 706.49 1297.89 34.03 o 7 0 1 1.88 0.00 21.73 o 9 0 1 5794.35 5356.34 110.01 o 11 0 1 576.12 553.95 85.76 o 13 0 1 6.12 -32.89 32.89 o 15 0 1 432.03 346.56 51.69 o -15 1 1 243.99 303.65 34.06 o -14 1 1 14.37 28.78 26.58 o -13 1 1 354.11 344.93 25.02 o -12 1 1 4.21 9.72 15.38 o -11 1 1 46.64 55.93 15.22 o -10 1 1 439.06 430.54 21.53 o -9 1 1 382.37 369.08 21.48 o -8 1 1 434.78 466.64 16.43 o -7 1 1 1774.89 1851.24 32.73 o -6 1 1 27039.83 26558.11 275.76 o -5 1 1 22.31 32.17 7.62 o -4 1 1 3048.58 2751.01 32.52 o -3 1 1 992.16 797.96 12.97 o -2 1 1 707.85 586.70 10.42 o -1 1 1 545.69 699.74 9.42 o 1 1 1 16.26 -3.56 3.56 o 2 1 1 38381.85 44695.20 571.93 o 3 1 1 30272.63 32021.14 404.83 o 4 1 1 15.87 -1.10 9.50 o 5 1 1 790.25 684.81 29.84 o 6 1 1 9869.70 10225.01 134.80 o 7 1 1 468.66 463.56 16.42 o 8 1 1 1135.89 989.25 23.39 o 9 1 1 8.63 7.79 12.54 o 10 1 1 189.75 246.35 16.55 o 11 1 1 306.44 350.04 24.93 o 12 1 1 389.03 459.10 21.50 o 13 1 1 187.30 126.46 29.37 o 14 1 1 7.26 -2.01 26.91 o 15 1 1 2.62 10.57 29.07 o -15 2 1 22.38 77.40 27.82 o -14 2 1 335.46 292.34 32.74 o -13 2 1 51.65 80.05 45.93 o -12 2 1 0.61 -17.85 17.85 o -11 2 1 208.41 233.87 16.87 o -10 2 1 488.71 462.69 18.72 o -9 2 1 4262.63 4075.65 61.03 o -8 2 1 3008.18 2956.29 46.31 o -7 2 1 873.92 535.98 20.26 o -6 2 1 99.83 41.82 8.56 o -5 2 1 66.09 143.49 8.41 o -4 2 1 14740.35 15222.66 146.78 o -3 2 1 9662.87 10879.74 105.16 o -2 2 1 26407.90 26316.08 272.95 o -1 2 1 2525.27 3110.64 47.93 o 0 2 1 1738.47 1913.96 26.73 o 1 2 1 208.59 291.29 9.62 o 2 2 1 6847.60 6968.31 90.60 o 3 2 1 3381.28 3856.63 52.84 o 4 2 1 1070.72 1031.96 20.25 o 5 2 1 60.80 6.53 9.13 o 6 2 1 2380.62 2563.33 40.04 o 7 2 1 1608.35 1541.09 36.97 o 8 2 1 651.58 681.03 21.03 o 9 2 1 177.00 164.05 14.47 o 10 2 1 2.43 5.75 13.28 o 11 2 1 2915.00 2904.93 50.33 o 12 2 1 127.18 107.43 20.36 o 13 2 1 18.74 13.22 19.86 o 14 2 1 372.05 313.32 32.80 o 15 2 1 33.48 8.02 45.23 o -15 3 1 185.87 303.89 67.55 o -14 3 1 655.27 626.36 38.30 o -13 3 1 35.58 60.66 20.52 o -12 3 1 687.22 761.77 32.00 o -11 3 1 4.78 -0.10 13.40 o -10 3 1 592.10 507.07 26.62 o -9 3 1 185.86 239.21 14.44 o -8 3 1 69.89 71.61 11.45 o -7 3 1 557.71 589.49 17.52 o -6 3 1 14.73 2.91 8.53 o -5 3 1 138.28 136.21 11.78 o -4 3 1 25830.14 27665.37 264.74 o -3 3 1 6256.72 5679.34 56.37 o -2 3 1 28152.83 28980.82 302.40 o -1 3 1 8404.38 9218.47 118.94 o 0 3 1 12850.94 14078.07 181.64 o 1 3 1 37.51 64.47 6.99 o 2 3 1 25204.38 27068.76 395.63 o 3 3 1 1759.98 2378.60 34.72 o 4 3 1 1351.76 1121.67 21.30 o 5 3 1 77.06 25.28 9.56 o 6 3 1 1218.41 959.12 30.83 o 7 3 1 490.65 437.14 18.48 o 8 3 1 180.70 186.34 14.62 o 9 3 1 140.63 109.02 13.84 o 10 3 1 2620.41 2556.97 44.78 o 11 3 1 645.76 614.74 27.81 o 12 3 1 486.30 420.85 26.57 o 13 3 1 60.51 63.49 29.62 o 14 3 1 657.99 731.97 58.74 o 15 3 1 210.99 257.05 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18 2 808.06 686.86 19.99 o 2 18 2 6.04 0.18 10.60 o 3 18 2 122.17 130.99 14.24 o 4 18 2 35.36 8.30 12.71 o 5 18 2 27.63 62.41 22.74 o 6 18 2 10.58 -1.37 22.74 o 7 18 2 66.75 61.15 26.08 o 8 18 2 6.36 -15.27 35.24 o 9 18 2 371.21 427.14 37.27 o 10 18 2 40.78 84.87 32.31 o 11 18 2 10.49 38.31 32.62 o 12 18 2 6.68 35.55 31.97 o -13 19 2 49.60 72.07 39.36 o -12 19 2 0.10 34.56 35.69 o -11 19 2 214.64 157.08 34.86 o -10 19 2 39.75 32.96 38.77 o -9 19 2 130.25 123.07 40.53 o -8 19 2 0.42 -24.05 24.05 o -7 19 2 195.73 188.77 28.21 o -6 19 2 158.16 144.88 26.23 o -5 19 2 95.63 93.61 26.50 o -4 19 2 183.01 142.52 28.88 o -3 19 2 114.04 145.16 13.64 o -2 19 2 1568.66 1418.41 29.28 o -1 19 2 10.12 16.30 12.55 o 0 19 2 927.87 891.76 22.68 o 1 19 2 39.80 42.84 12.03 o 2 19 2 3962.09 3716.65 65.79 o 3 19 2 6.86 -1.69 13.92 o 4 19 2 19.01 -4.59 13.64 o 5 19 2 121.11 100.70 25.33 o 6 19 2 302.29 290.89 30.11 o 7 19 2 269.89 317.85 34.06 o 8 19 2 2.32 3.45 26.43 o 9 19 2 1.33 -27.82 27.82 o 10 19 2 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46.40 o -5 21 2 41.99 62.36 25.33 o -4 21 2 69.14 39.22 14.86 o -3 21 2 5.86 -5.84 14.86 o -2 21 2 261.89 242.56 19.07 o -1 21 2 2938.73 2783.47 67.27 o 0 21 2 31.95 1.07 22.91 o 1 21 2 668.55 608.47 30.94 o 2 21 2 293.08 291.03 23.99 o 3 21 2 160.81 188.87 21.08 o 4 21 2 458.82 558.97 27.64 o 5 21 2 39.04 41.76 24.55 o 6 21 2 4.74 31.32 26.99 o 7 21 2 8.20 -27.38 27.38 o 8 21 2 433.00 512.75 39.45 o 9 21 2 203.71 196.68 34.47 o 10 21 2 178.67 177.24 78.12 o 11 21 2 66.27 58.02 52.28 o -12 22 2 83.74 72.25 40.53 o -11 22 2 3.19 18.85 33.64 o -10 22 2 1.55 70.75 65.79 o -9 22 2 133.08 130.89 54.04 o -8 22 2 29.70 -28.65 28.65 o -7 22 2 27.25 5.24 26.16 o -6 22 2 8.21 41.91 25.71 o -5 22 2 564.78 726.64 62.85 o -4 22 2 26.79 28.80 24.79 o -3 22 2 2.84 -2.76 18.86 o -2 22 2 671.90 575.68 42.88 o -1 22 2 3882.21 4039.61 89.70 o 0 22 2 693.95 761.80 36.96 o 1 22 2 260.01 209.31 72.84 o 2 22 2 419.53 356.82 25.69 o 3 22 2 337.20 335.83 25.41 o 4 22 2 370.78 247.88 42.29 o 5 22 2 157.98 142.15 38.77 o 6 22 2 0.91 -0.29 26.91 o 7 22 2 20.38 36.42 29.07 o 8 22 2 47.63 63.37 30.24 o 9 22 2 104.30 120.97 31.97 o 10 22 2 11.72 60.43 33.94 o 11 22 2 77.82 37.63 35.30 o -11 23 2 101.04 98.68 36.52 o -10 23 2 47.21 -9.76 37.01 o -9 23 2 0.03 24.54 29.90 o -8 23 2 15.19 2.94 29.91 o -7 23 2 101.40 179.02 43.47 o -6 23 2 0.29 -16.59 28.10 o -5 23 2 11.01 -6.56 23.92 o -4 23 2 89.72 113.17 20.09 o -3 23 2 2015.59 1981.11 54.68 o -2 23 2 308.23 330.13 32.31 o -1 23 2 399.59 458.91 43.47 o 0 23 2 1084.77 1028.91 71.66 o 1 23 2 16.37 30.50 42.88 o 2 23 2 86.75 74.34 22.32 o 3 23 2 67.14 127.41 20.81 o 4 23 2 0.16 -1.17 35.24 o 5 23 2 325.14 303.10 46.99 o 6 23 2 57.03 22.32 42.29 o 7 23 2 16.06 -18.80 39.94 o 8 23 2 46.94 20.79 29.77 o 9 23 2 157.21 119.52 36.52 o 10 23 2 6.16 -11.27 36.42 o -11 24 2 129.29 76.55 36.96 o -10 24 2 147.26 203.44 39.02 o -9 24 2 56.68 70.81 66.96 o -8 24 2 14.01 23.43 35.24 o -7 24 2 542.22 675.50 62.26 o -6 24 2 52.30 63.44 41.12 o -5 24 2 234.27 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