#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/23/2232331.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232331_Fobs loop_ _publ_author_name 'Fairuz, Zainal Abidin' 'Abdullah, Zanariah' 'Nasir, Shah Bakhtiar' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; Tetra-\m-acetato-\k^8^O:O'-bis[(2-phenoxypyrimidine-\kN^1^)copper(II)](Cu---Cu) ; _journal_coeditor_code HG5123 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1637 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.579 _cell_angle_gamma 90.000 _cell_length_a 11.0738 _cell_length_b 7.5002 _cell_length_c 18.0539 _exptl_crystal_F_000 724.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file hg5123Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 187.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5874.26 6313.84 338.89 o 4 0 0 2977.63 2778.60 67.65 o 6 0 0 9851.88 9253.67 272.31 o 8 0 0 1630.62 1500.50 56.88 o 10 0 0 835.50 781.63 35.18 o 12 0 0 1387.68 1329.55 53.98 o 1 1 0 5081.80 4858.22 88.76 o 2 1 0 202.75 171.19 6.09 o 3 1 0 0.23 -0.87 1.47 o 4 1 0 967.37 809.18 42.55 o 5 1 0 5155.89 4680.72 80.00 o 6 1 0 314.35 323.42 8.35 o 7 1 0 2983.96 3074.03 126.49 o 8 1 0 2010.12 1877.13 45.45 o 9 1 0 138.52 175.58 26.15 o 10 1 0 2.75 2.11 6.73 o 11 1 0 1079.27 1107.18 32.89 o 12 1 0 0.28 6.10 8.18 o 0 2 0 1476.75 1850.77 45.70 o 1 2 0 502.60 441.05 9.23 o 2 2 0 695.47 814.91 15.52 o 3 2 0 2865.02 2579.14 44.86 o 4 2 0 1324.70 1426.59 26.27 o 5 2 0 453.56 445.33 12.02 o 6 2 0 26.00 32.02 3.16 o 7 2 0 1373.04 1277.93 41.64 o 8 2 0 121.28 120.86 9.51 o 9 2 0 878.40 1013.66 28.98 o 10 2 0 724.08 652.17 22.86 o 11 2 0 1.36 69.98 9.68 o 12 2 0 29.16 1.57 9.48 o 1 3 0 309.41 257.76 7.78 o 2 3 0 4317.07 5495.35 174.33 o 3 3 0 1.95 3.82 2.75 o 4 3 0 2270.91 2197.54 94.83 o 5 3 0 1.31 4.88 3.04 o 6 3 0 534.46 558.33 13.38 o 7 3 0 25.96 22.42 4.08 o 8 3 0 1111.71 1048.01 25.25 o 9 3 0 6.04 11.43 6.71 o 10 3 0 485.47 369.04 21.34 o 11 3 0 26.39 32.33 10.23 o 12 3 0 33.90 29.65 10.99 o 0 4 0 458.43 681.46 21.03 o 1 4 0 131.21 114.94 5.58 o 3 4 0 3221.77 2926.23 52.16 o 4 4 0 387.69 455.75 20.61 o 5 4 0 4.16 3.91 5.49 o 6 4 0 413.94 412.63 16.38 o 7 4 0 144.30 114.42 10.83 o 8 4 0 0.82 -3.32 5.66 o 9 4 0 344.82 327.69 19.64 o 10 4 0 331.54 306.32 20.56 o 11 4 0 12.69 106.47 13.98 o 1 5 0 1412.15 1162.32 23.80 o 2 5 0 347.11 405.65 12.60 o 3 5 0 291.99 294.05 11.32 o 4 5 0 109.03 127.52 8.16 o 5 5 0 613.45 591.67 20.48 o 6 5 0 272.05 268.71 12.26 o 7 5 0 1046.44 1045.14 43.64 o 8 5 0 2039.27 1871.77 46.76 o 9 5 0 2.33 5.03 8.31 o 10 5 0 19.33 21.87 9.83 o 0 6 0 4779.86 5646.00 139.62 o 1 6 0 17.84 35.03 5.42 o 2 6 0 543.46 720.92 18.92 o 3 6 0 424.45 381.89 13.36 o 4 6 0 111.01 110.44 8.51 o 5 6 0 258.14 243.74 13.50 o 6 6 0 1910.28 1754.32 39.37 o 7 6 0 242.56 227.61 14.30 o 8 6 0 426.16 385.96 18.89 o 9 6 0 49.82 46.00 11.05 o 1 7 0 1121.54 1047.95 24.19 o 2 7 0 795.15 834.03 20.64 o 3 7 0 72.02 71.67 10.48 o 4 7 0 219.17 209.64 11.90 o 5 7 0 579.14 552.80 22.77 o 6 7 0 125.25 106.04 9.88 o 7 7 0 130.53 124.57 18.41 o 8 7 0 410.55 395.99 20.49 o 0 8 0 462.21 464.16 28.21 o 1 8 0 13.57 12.16 6.69 o 2 8 0 12.59 9.08 6.58 o 3 8 0 994.87 907.52 25.44 o 4 8 0 13.50 19.82 7.28 o 5 8 0 78.35 82.17 9.62 o -13 0 1 283.90 262.94 24.88 o -11 0 1 796.86 744.07 36.38 o -9 0 1 1995.65 1937.71 67.11 o -7 0 1 2335.25 2091.01 87.28 o -5 0 1 310.23 289.50 32.18 o -3 0 1 181.02 421.23 22.40 o -1 0 1 4434.63 5099.33 261.02 o 1 0 1 23504.17 21137.55 1279.87 o 3 0 1 2054.39 2193.31 53.74 o 5 0 1 5877.21 5393.08 129.82 o 7 0 1 6607.81 6408.42 154.85 o 9 0 1 44.02 45.89 11.24 o 11 0 1 25.16 45.09 28.70 o -12 1 1 462.00 643.68 24.26 o -11 1 1 61.03 59.07 9.90 o -10 1 1 608.55 610.27 21.54 o -9 1 1 1116.14 1009.00 28.95 o -8 1 1 369.20 360.67 16.35 o -7 1 1 2802.73 2744.89 54.30 o -6 1 1 2193.55 2046.90 41.02 o -5 1 1 249.07 229.93 7.14 o -4 1 1 12671.78 11553.01 192.98 o -3 1 1 2473.69 2212.66 67.47 o -2 1 1 4015.09 3858.38 65.22 o -1 1 1 5774.35 7095.67 118.16 o 0 1 1 19506.28 17786.34 425.94 o 1 1 1 328.90 355.04 7.01 o 2 1 1 5711.08 5252.72 96.72 o 3 1 1 8227.97 8111.31 148.59 o 4 1 1 213.59 199.36 6.62 o 5 1 1 1297.66 1272.36 23.85 o 6 1 1 997.35 848.11 20.66 o 7 1 1 1033.09 959.82 19.59 o 8 1 1 1329.02 1860.56 88.86 o 9 1 1 767.82 659.25 21.87 o 10 1 1 660.23 645.73 22.45 o 11 1 1 51.10 45.65 9.32 o 12 1 1 691.06 673.02 25.25 o -12 2 1 63.99 89.05 13.69 o -11 2 1 285.78 247.25 15.79 o -10 2 1 326.50 334.38 16.81 o -9 2 1 56.98 53.65 8.10 o -8 2 1 3562.09 3366.27 75.45 o -7 2 1 673.06 716.95 15.86 o -6 2 1 650.99 613.04 15.17 o -5 2 1 2282.89 2547.55 77.86 o -4 2 1 8974.07 8616.75 144.94 o -3 2 1 2465.97 2994.52 164.37 o -2 2 1 919.97 704.04 13.74 o -1 2 1 4701.89 6051.17 111.73 o 0 2 1 2188.14 2258.53 39.10 o 1 2 1 200.58 182.31 13.16 o 2 2 1 1780.99 1622.75 28.84 o 3 2 1 560.28 663.43 28.94 o 4 2 1 7448.27 6998.21 129.85 o 5 2 1 281.91 277.53 8.15 o 6 2 1 3136.87 3244.34 57.30 o 7 2 1 208.34 171.95 12.06 o 8 2 1 1451.15 1511.04 33.12 o 9 2 1 77.80 66.38 8.37 o 10 2 1 572.65 693.73 23.57 o 11 2 1 350.28 320.24 21.53 o 12 2 1 76.64 79.20 13.28 o -12 3 1 2.02 10.55 16.82 o -11 3 1 61.18 48.33 10.98 o -10 3 1 75.35 68.43 9.06 o -9 3 1 81.19 62.93 8.47 o -8 3 1 58.77 47.13 7.31 o -7 3 1 820.57 767.42 19.52 o -6 3 1 30.11 34.30 4.01 o -5 3 1 135.84 128.33 5.92 o -4 3 1 475.91 485.47 13.90 o -3 3 1 3373.16 3794.91 90.05 o -2 3 1 35.38 26.83 2.94 o -1 3 1 220.75 208.06 6.31 o 0 3 1 497.97 480.47 10.79 o 1 3 1 10.49 10.14 5.23 o 2 3 1 29.42 23.38 2.77 o 3 3 1 7272.25 6763.58 114.68 o 4 3 1 55.23 74.94 4.49 o 5 3 1 367.13 248.45 8.49 o 6 3 1 2.82 2.73 2.70 o 7 3 1 813.08 825.78 20.17 o 8 3 1 203.82 219.47 10.53 o 9 3 1 828.20 754.68 41.41 o 10 3 1 7.42 9.78 8.54 o 11 3 1 206.38 187.89 16.71 o 12 3 1 26.87 29.16 11.22 o -11 4 1 756.16 635.25 27.93 o -10 4 1 82.57 112.71 13.25 o -9 4 1 11.58 0.85 7.64 o -8 4 1 584.35 594.15 28.16 o -7 4 1 671.10 679.25 16.59 o -6 4 1 1644.92 1641.54 32.02 o -5 4 1 919.52 998.96 43.40 o -4 4 1 1097.59 974.86 20.26 o -3 4 1 1358.68 1939.61 35.86 o -2 4 1 408.14 334.62 9.48 o -1 4 1 1240.59 1546.35 29.10 o 0 4 1 114.11 117.52 5.58 o 1 4 1 600.37 549.57 12.70 o 2 4 1 2222.80 1889.39 42.93 o 3 4 1 38.22 44.61 4.16 o 4 4 1 1945.79 1905.12 35.49 o 5 4 1 265.87 264.54 11.43 o 6 4 1 473.12 464.83 12.65 o 7 4 1 175.25 178.65 9.45 o 8 4 1 963.03 997.33 30.43 o 9 4 1 38.64 43.85 9.75 o 10 4 1 685.89 819.42 31.63 o 11 4 1 447.60 410.91 25.47 o -10 5 1 720.63 750.01 30.55 o -9 5 1 16.27 2.98 7.98 o -8 5 1 237.04 206.43 13.05 o -7 5 1 783.10 760.25 20.72 o -6 5 1 3525.10 3182.60 63.96 o -5 5 1 114.99 114.54 6.95 o -4 5 1 763.02 746.15 17.51 o -3 5 1 333.00 355.08 11.00 o -2 5 1 186.79 178.90 7.98 o -1 5 1 1338.33 1627.89 31.51 o 0 5 1 3006.41 2706.54 49.22 o 1 5 1 154.83 172.75 9.63 o 2 5 1 1147.08 1040.70 21.99 o 3 5 1 77.91 76.12 10.25 o 4 5 1 381.25 378.43 12.11 o 5 5 1 11.94 17.87 6.02 o 6 5 1 2313.89 2268.74 47.62 o 7 5 1 183.34 172.95 11.92 o 8 5 1 70.66 76.53 9.35 o 9 5 1 54.59 50.85 10.72 o 10 5 1 264.22 285.29 23.64 o -9 6 1 181.56 181.11 16.78 o -8 6 1 173.78 163.64 12.92 o -7 6 1 583.73 584.84 21.41 o -6 6 1 29.39 31.68 6.85 o -5 6 1 2042.07 2029.28 69.17 o -4 6 1 181.84 171.68 8.94 o -3 6 1 384.60 451.56 13.53 o -2 6 1 593.14 611.32 16.04 o -1 6 1 2604.11 3178.54 58.15 o 0 6 1 25.51 45.57 9.51 o 1 6 1 3918.35 4410.41 78.41 o 2 6 1 1.73 -1.32 4.41 o 3 6 1 286.75 290.87 12.71 o 4 6 1 346.67 349.10 14.34 o 5 6 1 833.87 840.26 22.67 o 6 6 1 731.90 677.48 22.62 o 7 6 1 2163.23 1963.28 49.55 o 8 6 1 43.01 51.80 10.67 o 9 6 1 22.33 15.95 10.03 o -8 7 1 79.76 49.43 9.81 o -7 7 1 428.00 380.64 35.59 o -6 7 1 317.38 348.62 15.90 o -5 7 1 273.44 269.77 13.71 o -4 7 1 585.87 516.37 17.70 o -3 7 1 207.64 207.38 11.67 o -2 7 1 516.07 479.39 16.94 o -1 7 1 514.93 570.98 16.28 o 0 7 1 1711.35 1621.62 33.57 o 1 7 1 12.32 24.50 5.63 o 2 7 1 411.96 388.27 15.75 o 3 7 1 90.86 102.52 11.56 o 4 7 1 299.08 279.67 13.89 o 5 7 1 91.47 94.22 9.18 o 6 7 1 242.29 246.99 15.00 o 7 7 1 278.74 255.01 15.89 o -5 8 1 54.14 63.70 9.20 o -4 8 1 296.95 289.56 15.02 o -3 8 1 44.48 40.84 8.74 o -2 8 1 427.17 389.30 16.83 o -1 8 1 10.21 5.90 5.79 o 0 8 1 21.44 22.26 6.92 o 1 8 1 10.72 28.01 14.85 o 2 8 1 396.94 402.22 17.33 o 3 8 1 15.76 13.24 6.91 o 4 8 1 685.49 656.30 21.49 o 5 8 1 10.67 11.51 7.59 o -12 0 2 1411.08 1297.34 53.37 o -10 0 2 746.08 668.67 32.76 o -8 0 2 8.96 36.21 9.50 o -6 0 2 3984.98 4089.59 154.35 o -4 0 2 5947.17 5912.11 173.97 o -2 0 2 2959.07 3484.24 90.13 o 0 0 2 34959.11 26047.34 1098.30 o 2 0 2 13578.80 12805.50 301.51 o 4 0 2 6.77 21.04 7.77 o 6 0 2 4108.44 3562.26 88.01 o 8 0 2 2403.52 2205.30 73.54 o 10 0 2 1581.00 1467.88 55.30 o 12 0 2 343.51 314.91 25.85 o -13 1 2 11.14 23.94 9.88 o -12 1 2 122.97 125.24 12.84 o -11 1 2 2618.02 2627.51 100.88 o -10 1 2 254.82 247.15 14.64 o -9 1 2 443.68 468.29 19.22 o -8 1 2 2655.23 2578.58 59.31 o -7 1 2 1428.22 1289.02 32.42 o -6 1 2 260.79 234.92 8.18 o -5 1 2 3981.49 3402.25 64.89 o -4 1 2 2054.29 2131.54 37.24 o -3 1 2 2088.94 2122.56 38.92 o -2 1 2 4908.30 6463.90 108.29 o -1 1 2 9631.74 8947.08 148.99 o 0 1 2 689.72 679.38 15.18 o 1 1 2 15078.32 13820.84 251.20 o 2 1 2 8642.39 8216.81 168.66 o 3 1 2 3.37 19.28 2.83 o 4 1 2 1418.92 1189.72 24.58 o 5 1 2 3260.15 3192.76 61.32 o 6 1 2 4.87 0.94 2.67 o 7 1 2 2040.51 2210.00 47.10 o 8 1 2 1462.83 1276.71 33.30 o 9 1 2 0.98 30.31 8.81 o 10 1 2 5.32 3.18 6.91 o 11 1 2 275.34 321.21 17.36 o 12 1 2 10.27 28.42 10.97 o -12 2 2 46.18 43.00 10.11 o -11 2 2 7.89 14.12 8.14 o -10 2 2 381.32 327.68 16.68 o -9 2 2 479.72 465.71 18.33 o -8 2 2 621.39 624.91 30.18 o -7 2 2 1639.46 1487.35 28.48 o -6 2 2 1542.93 1475.51 30.67 o -5 2 2 537.71 597.93 13.01 o -4 2 2 6850.93 7584.77 139.68 o -3 2 2 7462.86 6938.77 116.87 o -2 2 2 0.54 -1.08 1.90 o -1 2 2 6966.31 6630.92 111.45 o 0 2 2 5906.64 5486.83 101.17 o 1 2 2 124.61 149.79 4.71 o 2 2 2 2379.97 2302.51 40.06 o 3 2 2 8742.89 7993.57 147.37 o 4 2 2 848.04 1022.59 27.20 o 5 2 2 2366.98 2225.24 44.20 o 6 2 2 46.95 21.95 3.61 o 7 2 2 524.57 593.63 16.10 o 8 2 2 0.80 3.80 4.66 o 9 2 2 1088.84 1179.12 32.36 o 10 2 2 253.82 272.43 18.32 o 11 2 2 296.51 316.47 20.67 o 12 2 2 39.94 31.23 10.93 o -12 3 2 232.10 254.94 21.61 o -11 3 2 17.33 20.37 9.47 o -10 3 2 3.21 0.58 6.60 o -9 3 2 133.29 145.13 11.02 o -8 3 2 1475.38 1317.69 34.46 o -7 3 2 2.11 -1.31 4.58 o -6 3 2 623.83 487.36 12.31 o -5 3 2 129.33 113.29 6.28 o -4 3 2 1787.40 1890.03 34.56 o -3 3 2 625.46 667.23 14.19 o -2 3 2 2953.19 3380.21 58.68 o -1 3 2 1538.32 1534.85 28.15 o 0 3 2 526.23 607.75 12.81 o 1 3 2 722.80 731.89 16.24 o 2 3 2 4310.10 4161.40 71.58 o 3 3 2 1168.04 1251.92 25.27 o 4 3 2 5072.90 4532.61 78.18 o 5 3 2 1.60 3.51 2.89 o 6 3 2 25.01 23.21 3.84 o 7 3 2 1.38 11.44 6.25 o 8 3 2 1299.77 1277.44 33.39 o 9 3 2 23.98 32.92 9.09 o 10 3 2 1414.09 1299.15 52.80 o 11 3 2 8.92 5.32 8.98 o -11 4 2 54.85 60.37 11.61 o -10 4 2 904.03 843.50 32.01 o -9 4 2 225.35 237.16 14.26 o -8 4 2 83.94 81.18 8.86 o -7 4 2 823.90 802.89 18.67 o -6 4 2 791.19 869.02 26.90 o -5 4 2 0.02 4.53 3.59 o -4 4 2 1616.29 1739.25 33.30 o -3 4 2 4278.69 4231.25 73.77 o -2 4 2 408.40 552.50 12.97 o -1 4 2 595.51 445.54 11.10 o 0 4 2 357.73 339.36 14.50 o 1 4 2 213.26 211.68 8.59 o 2 4 2 5073.07 5090.33 96.27 o 3 4 2 1559.71 1525.81 29.10 o 4 4 2 122.21 149.20 7.91 o 5 4 2 206.61 194.50 8.81 o 6 4 2 845.36 822.08 20.89 o 7 4 2 683.97 657.85 25.38 o 8 4 2 345.14 369.55 16.90 o 9 4 2 882.37 859.12 31.84 o 10 4 2 19.32 18.98 9.54 o 11 4 2 181.70 275.90 23.90 o -10 5 2 4.32 12.23 9.42 o -9 5 2 220.46 224.75 17.14 o -8 5 2 213.98 209.44 13.08 o -7 5 2 49.58 49.07 5.98 o -6 5 2 25.94 27.92 5.23 o -5 5 2 1575.49 1511.40 30.39 o -4 5 2 3.88 30.53 5.58 o -3 5 2 4080.67 3860.24 68.59 o -2 5 2 48.31 25.90 4.34 o -1 5 2 800.39 650.81 15.49 o 0 5 2 116.98 122.83 6.58 o 1 5 2 1869.13 1789.91 34.22 o 2 5 2 1070.15 1104.37 30.97 o 3 5 2 851.78 738.26 18.60 o 4 5 2 107.11 137.32 8.47 o 5 5 2 258.44 257.90 15.00 o 6 5 2 64.12 49.81 7.56 o 7 5 2 1727.13 1874.35 74.60 o 8 5 2 331.01 325.11 18.45 o 9 5 2 45.47 63.85 13.03 o 10 5 2 1.22 5.14 9.54 o -9 6 2 7.26 10.09 10.08 o -8 6 2 9.36 2.75 7.26 o -7 6 2 17.41 17.81 7.64 o -6 6 2 1479.14 1511.08 34.78 o -5 6 2 434.11 405.55 15.04 o -4 6 2 640.20 689.29 17.57 o -3 6 2 46.97 56.49 5.99 o -2 6 2 65.53 73.30 6.38 o -1 6 2 0.88 1.46 4.47 o 0 6 2 3706.06 4325.44 77.04 o 1 6 2 1.06 6.22 4.60 o 2 6 2 554.88 543.73 21.52 o 3 6 2 161.10 159.48 9.65 o 4 6 2 39.43 34.06 6.38 o 5 6 2 127.77 119.20 9.40 o 6 6 2 976.57 912.51 30.75 o 7 6 2 31.29 28.31 7.07 o 8 6 2 94.20 90.81 10.62 o 9 6 2 19.38 23.63 9.94 o -8 7 2 145.43 144.62 13.31 o -7 7 2 27.98 15.04 9.51 o -6 7 2 27.21 32.49 7.46 o -5 7 2 551.33 530.55 18.00 o -4 7 2 765.22 847.63 23.33 o -3 7 2 183.89 161.01 9.51 o -2 7 2 919.44 978.78 23.07 o -1 7 2 1029.38 900.01 21.73 o 0 7 2 37.89 55.68 6.58 o 1 7 2 609.43 503.18 16.69 o 2 7 2 102.12 93.43 8.50 o 3 7 2 46.53 47.09 7.26 o 4 7 2 207.87 251.83 14.60 o 5 7 2 511.04 444.15 20.80 o 6 7 2 0.12 -2.07 7.31 o 7 7 2 490.42 459.67 21.46 o -5 8 2 183.56 172.46 14.80 o -4 8 2 134.32 135.82 11.01 o -3 8 2 661.41 593.75 20.75 o -2 8 2 1.92 5.14 6.41 o -1 8 2 98.74 97.63 9.46 o 0 8 2 154.03 163.03 11.29 o 1 8 2 30.92 34.03 7.56 o 2 8 2 0.21 3.27 6.32 o 3 8 2 1166.89 1063.08 28.62 o 4 8 2 4.42 12.28 7.36 o 5 8 2 58.28 73.48 10.57 o -13 0 3 11.84 3.14 35.56 o -11 0 3 2178.47 1838.73 67.49 o -9 0 3 3544.64 3135.03 101.18 o -5 0 3 7932.56 8953.69 262.30 o -3 0 3 9289.42 10531.37 377.37 o -1 0 3 5436.60 5524.75 235.91 o 1 0 3 35148.29 28724.85 676.76 o 3 0 3 2512.01 2577.41 63.22 o 5 0 3 4916.83 4724.66 141.51 o 7 0 3 6073.18 5696.60 138.89 o 9 0 3 239.91 202.70 30.90 o 11 0 3 611.15 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