#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/23/2232333.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232333_Fobs loop_ _publ_author_name 'Kadi, Adnan A.' 'Alanzi, Amer M.' 'El-Emam, Ali A.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; N'-(Adamantan-2-ylidene)thiophene-2-carbohydrazide ; _journal_coeditor_code HG5127 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3127 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.473 _cell_angle_gamma 90.000 _cell_length_a 16.7262 _cell_length_b 12.5663 _cell_length_c 13.5562 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.7929 _[local]_cod_data_source_file hg5127Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 194.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5723.01 4979.00 30.42 o 4 0 0 240.43 192.19 8.77 o 6 0 0 10563.32 9470.46 76.37 o 8 0 0 6601.35 6061.02 73.51 o 10 0 0 27.27 24.97 6.50 o 12 0 0 5286.33 5318.10 90.87 o 14 0 0 15994.07 15635.20 183.55 o 16 0 0 821.67 883.62 29.26 o 18 0 0 3.71 3.09 3.59 o 20 0 0 121.42 108.46 6.63 o 1 1 0 1713.83 1639.52 9.94 o 3 1 0 1759.93 1763.56 16.09 o 5 1 0 1187.74 1026.20 16.17 o 7 1 0 18.13 8.85 2.40 o 9 1 0 165.50 162.29 9.51 o 11 1 0 716.91 689.31 22.02 o 13 1 0 14.53 17.69 3.82 o 15 1 0 5207.21 5200.03 59.31 o 17 1 0 3247.49 3262.42 37.62 o 19 1 0 62.27 55.52 3.91 o 0 2 0 10063.99 8326.45 42.85 o 4 2 0 490.68 420.84 10.34 o 6 2 0 726.09 599.83 14.00 o 8 2 0 474.12 388.75 13.48 o 10 2 0 305.53 309.51 14.08 o 12 2 0 3021.03 2922.27 65.64 o 14 2 0 1988.99 2040.90 31.92 o 16 2 0 1122.20 1185.73 27.73 o 18 2 0 53.51 59.26 4.37 o 20 2 0 296.34 303.55 9.42 o 1 3 0 4485.38 4039.83 26.90 o 3 3 0 1127.22 1230.08 14.66 o 5 3 0 5397.79 5493.06 41.54 o 7 3 0 469.93 526.01 19.62 o 9 3 0 31.77 35.08 6.50 o 11 3 0 4166.12 4168.61 73.90 o 13 3 0 2993.68 2913.36 31.73 o 15 3 0 656.96 673.71 18.58 o 17 3 0 22.61 24.41 3.72 o 19 3 0 241.85 220.02 7.89 o 0 4 0 2798.78 2965.88 37.77 o 2 4 0 418.47 358.00 6.96 o 4 4 0 13.39 21.62 2.22 o 6 4 0 6669.07 6911.34 65.41 o 8 4 0 3659.42 3585.51 54.74 o 10 4 0 2276.30 2239.86 49.92 o 12 4 0 594.09 543.45 15.04 o 14 4 0 29.40 36.40 4.64 o 16 4 0 64.09 52.92 5.40 o 18 4 0 299.46 299.92 10.42 o 1 5 0 5676.64 5806.95 49.14 o 3 5 0 1744.59 1840.08 18.06 o 5 5 0 1235.36 1346.54 20.46 o 7 5 0 134.14 147.86 18.00 o 9 5 0 627.33 729.86 30.96 o 11 5 0 163.11 132.38 6.99 o 13 5 0 2425.48 2430.10 34.60 o 15 5 0 159.77 158.75 9.02 o 17 5 0 5.29 3.30 4.95 o 19 5 0 115.16 96.79 4.64 o 0 6 0 22407.26 21749.12 132.60 o 2 6 0 31.77 41.63 27.29 o 4 6 0 5025.82 5670.09 51.07 o 6 6 0 1551.67 1605.60 28.60 o 8 6 0 3183.95 3284.79 67.12 o 10 6 0 46.38 77.87 7.19 o 12 6 0 1.44 3.38 4.90 o 14 6 0 1716.23 1595.67 33.33 o 16 6 0 43.44 44.93 6.98 o 18 6 0 194.02 217.43 9.95 o 1 7 0 705.58 807.01 23.31 o 3 7 0 78.96 150.87 9.14 o 5 7 0 3577.94 3555.41 48.40 o 7 7 0 22.56 20.62 6.19 o 9 7 0 134.82 158.15 10.49 o 11 7 0 9.18 9.22 4.18 o 13 7 0 216.06 204.18 12.44 o 15 7 0 3.07 1.15 3.00 o 17 7 0 9.10 7.74 3.31 o 0 8 0 3601.33 4168.61 71.30 o 2 8 0 576.46 622.68 19.84 o 4 8 0 76.80 62.39 6.89 o 6 8 0 1.67 4.81 4.88 o 8 8 0 1367.31 1455.42 33.50 o 10 8 0 4159.06 3907.87 65.12 o 12 8 0 356.23 318.86 15.30 o 14 8 0 332.02 305.87 13.61 o 16 8 0 10.19 5.46 2.82 o 1 9 0 2545.83 2545.40 43.09 o 3 9 0 1441.78 1511.32 33.45 o 5 9 0 312.66 287.50 15.75 o 7 9 0 127.07 158.29 9.72 o 9 9 0 1017.70 987.33 22.15 o 11 9 0 175.83 167.94 11.10 o 13 9 0 301.98 321.53 13.69 o 15 9 0 1369.47 1405.52 28.85 o 0 10 0 2391.24 2614.46 65.11 o 2 10 0 2566.26 2770.89 41.70 o 4 10 0 844.58 829.46 61.84 o 6 10 0 78.83 105.69 10.14 o 8 10 0 367.72 364.03 18.10 o 10 10 0 2355.31 2327.40 32.42 o 12 10 0 2181.03 2000.83 32.01 o 14 10 0 893.32 840.30 40.45 o 1 11 0 826.65 769.83 27.34 o 3 11 0 3231.31 3389.97 55.69 o 5 11 0 462.05 454.04 30.91 o 7 11 0 46.52 44.70 6.80 o 9 11 0 184.36 171.50 10.32 o 11 11 0 368.85 342.30 16.39 o 13 11 0 228.41 245.89 11.30 o 0 12 0 2380.81 2328.87 66.92 o 2 12 0 311.67 334.94 17.99 o 4 12 0 37.20 55.14 7.58 o 6 12 0 67.23 85.70 13.38 o 8 12 0 20.02 11.78 8.40 o 10 12 0 1040.98 980.82 24.42 o 12 12 0 973.07 932.55 41.25 o 1 13 0 3113.79 3058.86 51.09 o 3 13 0 2373.62 2577.93 44.88 o 5 13 0 2901.86 2953.57 70.47 o 7 13 0 35.29 33.49 6.57 o 9 13 0 929.13 939.91 37.59 o 11 13 0 474.16 495.51 19.91 o 0 14 0 117.26 133.77 14.03 o 2 14 0 33.30 36.35 5.53 o 4 14 0 143.14 160.50 15.53 o 6 14 0 1424.97 1425.51 31.03 o 8 14 0 91.44 81.83 10.36 o 1 15 0 743.08 794.76 29.42 o 3 15 0 2555.47 2569.84 48.18 o 5 15 0 508.78 514.89 23.20 o -19 1 1 2.80 4.12 1.85 o -17 1 1 123.21 112.60 7.42 o -15 1 1 233.62 232.15 11.02 o -13 1 1 2420.74 2504.39 32.65 o -11 1 1 10.39 16.59 3.63 o -9 1 1 36.51 55.40 5.67 o -7 1 1 2913.64 3163.65 33.47 o -5 1 1 637.31 616.02 12.22 o -3 1 1 20458.64 15964.62 270.36 o -1 1 1 3.90 12.84 0.94 o 1 1 1 862.60 855.53 8.82 o 3 1 1 33175.56 25293.26 449.10 o 5 1 1 92.90 98.10 5.56 o 7 1 1 193.53 208.11 19.20 o 9 1 1 608.29 601.67 18.49 o 11 1 1 2078.66 2101.32 39.19 o 13 1 1 1362.94 1444.73 23.44 o 15 1 1 1402.48 1436.42 31.56 o 17 1 1 464.58 492.05 14.69 o 19 1 1 228.39 225.97 7.66 o -20 2 1 8.22 9.34 2.37 o -18 2 1 19.79 19.14 2.87 o -16 2 1 0.21 3.05 2.79 o -14 2 1 16992.56 15933.79 76.11 o -12 2 1 1966.31 1929.03 52.21 o -10 2 1 158.98 170.23 13.82 o -8 2 1 77.23 110.13 5.99 o -6 2 1 1288.34 1224.15 49.74 o -4 2 1 321.24 387.07 9.64 o -2 2 1 4578.82 4071.83 21.59 o 0 2 1 7333.50 6602.78 44.02 o 2 2 1 357.03 395.41 11.61 o 4 2 1 2510.27 2406.98 24.14 o 6 2 1 351.73 346.68 11.26 o 8 2 1 6.53 6.46 4.31 o 10 2 1 96.41 111.21 15.68 o 12 2 1 1195.59 1267.14 17.62 o 14 2 1 1274.89 1295.72 25.56 o 16 2 1 43.60 46.93 5.17 o 18 2 1 77.91 75.47 7.29 o 20 2 1 44.05 49.14 5.47 o -19 3 1 189.89 170.65 7.32 o -17 3 1 383.25 414.59 15.32 o -15 3 1 137.88 117.90 8.07 o -13 3 1 482.16 520.73 13.87 o -11 3 1 7486.55 7699.90 91.24 o -9 3 1 1309.63 1317.00 34.51 o -7 3 1 1197.68 1177.79 27.13 o -5 3 1 1367.30 1381.18 25.59 o -3 3 1 59.44 56.94 3.44 o -1 3 1 58.46 79.12 1.89 o 1 3 1 12022.67 10878.78 26.92 o 3 3 1 28276.10 23840.17 69.89 o 5 3 1 4017.25 3966.43 53.03 o 7 3 1 23.45 45.51 5.54 o 9 3 1 2095.67 2005.63 40.41 o 11 3 1 103.13 118.42 13.19 o 13 3 1 2260.35 2243.01 45.51 o 15 3 1 1155.77 1244.56 28.39 o 17 3 1 778.43 844.47 20.02 o 19 3 1 683.14 742.65 17.89 o -20 4 1 34.92 21.60 4.31 o -18 4 1 15.95 13.36 3.00 o -16 4 1 733.44 750.47 18.33 o -14 4 1 1807.57 1766.84 40.70 o -12 4 1 2809.12 2820.14 47.53 o -10 4 1 6298.46 6852.06 76.87 o -8 4 1 6.59 24.35 3.63 o -6 4 1 321.56 379.42 10.73 o -4 4 1 776.09 769.32 10.33 o -2 4 1 6350.68 5840.34 28.21 o 0 4 1 49.89 52.88 2.61 o 2 4 1 2402.50 2379.69 20.00 o 4 4 1 260.69 292.92 14.72 o 6 4 1 193.61 181.92 11.83 o 8 4 1 427.30 443.82 20.99 o 10 4 1 157.13 160.89 14.32 o 12 4 1 9.89 16.44 2.49 o 14 4 1 3621.09 3649.58 38.66 o 16 4 1 1031.26 1045.69 23.51 o 18 4 1 419.54 414.42 12.05 o -19 5 1 905.87 891.23 18.63 o -17 5 1 316.91 325.17 14.88 o -15 5 1 369.67 379.71 20.12 o -13 5 1 1209.02 1240.97 26.37 o -11 5 1 1443.20 1418.82 24.32 o -9 5 1 12965.52 12980.41 127.18 o -7 5 1 234.61 235.21 15.95 o -5 5 1 763.50 671.56 15.67 o -3 5 1 23679.20 22144.42 85.80 o -1 5 1 1364.72 1261.01 20.91 o 1 5 1 1.30 5.25 3.45 o 3 5 1 3037.36 2932.25 25.48 o 5 5 1 14203.40 14534.55 108.47 o 7 5 1 6.81 17.41 3.60 o 9 5 1 170.47 173.15 20.90 o 11 5 1 5376.98 5452.92 54.78 o 13 5 1 346.09 340.91 11.88 o 15 5 1 925.56 893.43 23.48 o 17 5 1 1087.26 1097.56 37.11 o 19 5 1 17.03 19.87 2.71 o -18 6 1 572.84 544.66 23.63 o -16 6 1 3.18 7.30 4.61 o -14 6 1 1739.28 1805.98 43.48 o -12 6 1 1331.97 1318.01 38.01 o -10 6 1 51.74 61.51 6.78 o -8 6 1 1399.60 1512.26 44.77 o -6 6 1 4548.17 4797.94 46.81 o -4 6 1 642.08 641.98 16.72 o -2 6 1 4625.70 4575.39 43.28 o 0 6 1 60.07 62.97 5.39 o 2 6 1 60.82 53.92 3.80 o 4 6 1 4548.25 4728.78 42.28 o 6 6 1 5646.54 5925.37 84.16 o 8 6 1 498.58 499.79 26.91 o 10 6 1 739.44 798.01 19.07 o 12 6 1 1441.50 1406.90 37.16 o 14 6 1 1593.87 1529.94 32.27 o 16 6 1 413.73 458.01 26.36 o 18 6 1 52.29 54.88 3.93 o -17 7 1 1552.35 1568.38 43.13 o -15 7 1 873.84 916.73 27.76 o -13 7 1 1952.47 1957.51 37.37 o -11 7 1 2228.75 2282.36 89.31 o -9 7 1 519.01 605.19 19.79 o -7 7 1 706.22 638.01 30.27 o -5 7 1 4170.83 4529.94 48.98 o -3 7 1 643.36 533.83 16.64 o -1 7 1 1423.79 1496.00 27.50 o 1 7 1 4449.91 4557.91 76.62 o 3 7 1 3170.60 3474.75 50.68 o 5 7 1 795.17 841.45 23.46 o 7 7 1 29.50 10.74 5.26 o 9 7 1 5863.60 5952.09 81.64 o 11 7 1 5245.29 5232.09 61.49 o 13 7 1 250.95 224.93 12.75 o 15 7 1 1766.26 1679.49 30.51 o 17 7 1 77.34 67.69 6.48 o -18 8 1 52.65 49.63 5.23 o -16 8 1 1079.69 1012.30 18.93 o -14 8 1 3817.81 3673.31 51.43 o -12 8 1 279.17 304.72 15.06 o -10 8 1 36.47 51.99 6.88 o -8 8 1 712.44 685.83 16.93 o -6 8 1 2781.49 2928.69 67.36 o -4 8 1 1870.49 1952.81 34.70 o -2 8 1 1103.34 1156.52 26.67 o 0 8 1 7246.73 7288.82 67.35 o 2 8 1 598.15 661.11 20.71 o 4 8 1 104.94 100.61 9.37 o 6 8 1 10.10 18.48 6.01 o 8 8 1 3898.34 3760.97 79.38 o 10 8 1 483.78 495.81 19.03 o 12 8 1 1300.21 1227.95 28.93 o 14 8 1 84.06 77.31 5.73 o 16 8 1 46.13 43.11 5.34 o -17 9 1 315.14 316.97 13.26 o -15 9 1 297.22 273.67 10.56 o -13 9 1 1017.60 1006.32 24.29 o -11 9 1 1171.65 1193.15 28.91 o -9 9 1 2380.69 2338.29 33.89 o -7 9 1 244.60 253.59 10.71 o -5 9 1 13.29 5.87 10.89 o -3 9 1 1925.13 1988.36 37.54 o -1 9 1 168.76 188.19 14.34 o 1 9 1 1344.01 1326.82 31.23 o 3 9 1 4200.74 4472.17 58.25 o 5 9 1 260.69 251.10 10.12 o 7 9 1 344.44 302.09 13.42 o 9 9 1 427.83 477.68 23.28 o 11 9 1 10.13 8.52 4.15 o 13 9 1 592.05 594.54 17.68 o 15 9 1 1242.90 1165.65 35.47 o -16 10 1 3.14 5.87 2.40 o -14 10 1 23.79 26.40 3.73 o -12 10 1 681.59 623.48 18.49 o -10 10 1 55.02 65.65 7.27 o -8 10 1 414.09 456.76 16.37 o -6 10 1 40.08 21.02 7.63 o -4 10 1 125.28 150.78 12.05 o -2 10 1 285.81 290.26 15.91 o 0 10 1 903.51 994.78 23.57 o 2 10 1 1237.65 1328.87 27.56 o 4 10 1 199.72 194.27 22.28 o 6 10 1 2077.47 2127.14 43.53 o 8 10 1 65.70 62.28 7.37 o 10 10 1 282.32 274.70 17.40 o 12 10 1 48.37 39.95 12.33 o 14 10 1 348.19 308.03 13.10 o -13 11 1 225.71 207.02 7.94 o -11 11 1 580.86 598.57 16.61 o -9 11 1 1133.48 1118.40 25.13 o -7 11 1 94.74 108.83 15.30 o -5 11 1 209.61 232.64 22.53 o -3 11 1 8.74 18.05 4.73 o -1 11 1 3354.56 3188.38 76.58 o 1 11 1 1335.91 1298.29 51.11 o 3 11 1 1035.05 991.49 45.30 o 5 11 1 1295.16 1317.00 33.31 o 7 11 1 17.99 26.56 14.64 o 9 11 1 67.35 67.89 9.03 o 11 11 1 189.62 174.96 11.83 o 13 11 1 53.09 64.61 7.94 o -12 12 1 80.08 71.75 6.53 o -10 12 1 694.99 714.45 35.69 o -8 12 1 1363.70 1236.42 34.51 o -6 12 1 3.55 13.61 7.62 o -4 12 1 1051.99 1164.35 31.22 o -2 12 1 5.87 5.38 4.41 o 0 12 1 29.75 32.92 7.18 o 2 12 1 48.20 42.41 7.33 o 4 12 1 1573.72 1620.70 37.07 o 6 12 1 1430.04 1440.18 52.17 o 8 12 1 3.42 3.29 3.89 o 10 12 1 248.85 265.76 12.90 o 12 12 1 119.71 115.95 9.92 o -11 13 1 5.66 13.03 4.81 o -9 13 1 12.05 11.34 6.37 o -7 13 1 20.15 22.70 5.88 o -5 13 1 677.28 715.33 34.82 o -3 13 1 2860.17 2943.73 47.72 o -1 13 1 7.74 17.31 5.27 o 1 13 1 96.68 89.42 9.44 o 3 13 1 558.63 582.50 21.52 o 5 13 1 39.28 28.56 8.53 o 7 13 1 216.86 193.61 21.20 o 9 13 1 843.11 792.92 33.41 o 11 13 1 362.44 351.40 15.98 o -8 14 1 148.05 149.27 13.53 o -6 14 1 313.75 298.15 14.59 o -4 14 1 393.93 421.61 24.29 o -2 14 1 53.70 68.14 7.88 o 0 14 1 45.28 43.39 5.98 o 2 14 1 505.75 536.92 18.58 o 4 14 1 1.89 4.95 5.33 o 6 14 1 1603.06 1693.76 51.42 o 8 14 1 429.01 422.49 20.85 o -5 15 1 0.15 -5.22 5.22 o -3 15 1 39.10 57.85 7.90 o -1 15 1 8.55 8.19 4.32 o 1 15 1 17.53 19.04 4.64 o 3 15 1 154.60 127.10 13.61 o 5 15 1 287.48 234.92 15.19 o -20 0 2 972.09 981.08 31.38 o -18 0 2 771.57 792.05 25.82 o -16 0 2 5795.18 5671.00 71.85 o -14 0 2 1387.47 1541.32 38.61 o -12 0 2 2162.15 2095.15 49.42 o -10 0 2 3289.63 3602.88 58.58 o -4 0 2 2121.31 1980.31 26.98 o 2 0 2 24137.36 18893.60 79.64 o 4 0 2 272.83 316.72 13.28 o 6 0 2 366.81 494.42 19.87 o 8 0 2 1927.73 1848.22 44.14 o 10 0 2 670.43 678.55 30.52 o 12 0 2 1103.75 1201.18 32.86 o 14 0 2 259.11 242.62 23.83 o 16 0 2 413.27 444.18 20.75 o 18 0 2 5.40 7.36 3.39 o -19 1 2 20.46 14.81 3.09 o -17 1 2 69.07 64.12 5.64 o -15 1 2 40.89 53.64 5.74 o -13 1 2 229.60 213.61 8.66 o -11 1 2 1782.18 1882.98 31.34 o -9 1 2 250.81 274.33 10.80 o -7 1 2 827.43 923.24 34.25 o -5 1 2 1889.09 1993.04 30.09 o -3 1 2 521.65 737.00 9.63 o -1 1 2 1750.56 1447.84 16.96 o 1 1 2 5741.36 5283.65 61.68 o 3 1 2 270.78 243.33 13.62 o 5 1 2 3649.85 3816.96 35.68 o 7 1 2 751.04 949.87 25.08 o 9 1 2 650.68 612.86 19.31 o 11 1 2 340.81 315.75 15.82 o 13 1 2 1157.44 1239.91 24.52 o 15 1 2 1380.29 1390.86 30.81 o 17 1 2 971.54 966.17 19.04 o 19 1 2 665.92 660.84 16.38 o -20 2 2 869.44 917.28 28.32 o -18 2 2 4.73 5.35 2.45 o -16 2 2 524.88 494.05 15.52 o -14 2 2 3602.81 3379.08 34.73 o -12 2 2 1822.65 1864.92 51.30 o -10 2 2 19.41 9.08 2.49 o -8 2 2 2559.78 2416.06 40.07 o -6 2 2 9265.14 8464.19 38.99 o -4 2 2 2777.82 2494.94 31.83 o -2 2 2 1054.48 970.29 9.30 o 2 2 2 26821.32 21795.75 83.22 o 4 2 2 3945.28 3734.44 128.52 o 6 2 2 22286.52 21248.21 92.10 o 8 2 2 6464.78 6192.17 57.98 o 10 2 2 0.25 0.73 2.57 o 12 2 2 4308.16 4366.16 34.38 o 14 2 2 5193.75 5272.06 50.12 o 16 2 2 2216.29 2131.47 34.03 o 18 2 2 99.69 99.79 6.61 o -19 3 2 60.78 60.35 5.42 o -17 3 2 3013.20 2960.78 37.92 o -15 3 2 6629.99 6600.54 56.10 o -13 3 2 412.99 435.16 11.32 o -11 3 2 62.30 38.60 6.96 o -9 3 2 3621.67 4169.06 86.00 o -7 3 2 33.88 38.40 2.95 o -5 3 2 290.81 353.47 6.65 o -3 3 2 4.04 7.44 1.45 o -1 3 2 22178.13 19328.33 59.53 o 1 3 2 9959.66 9070.79 53.47 o 3 3 2 4779.48 4773.50 38.01 o 5 3 2 1207.60 1129.84 19.99 o 7 3 2 2103.18 2226.84 76.84 o 9 3 2 37.35 55.72 6.40 o 11 3 2 416.87 380.48 12.56 o 13 3 2 470.97 480.00 13.92 o 15 3 2 459.33 484.66 15.11 o 17 3 2 496.30 468.47 12.51 o 19 3 2 74.35 65.17 5.19 o -20 4 2 2.50 2.85 2.76 o -18 4 2 1410.06 1485.34 21.33 o -16 4 2 73.26 78.45 6.26 o -14 4 2 414.27 388.17 12.12 o -12 4 2 2262.02 2065.87 23.66 o -10 4 2 2621.47 2984.35 57.92 o -8 4 2 1268.49 1400.47 23.06 o -6 4 2 547.53 492.40 11.47 o -4 4 2 794.52 849.92 14.11 o -2 4 2 429.17 432.09 8.06 o 0 4 2 34658.23 29124.65 63.13 o 2 4 2 8964.14 8309.76 144.58 o 4 4 2 4120.50 4723.61 32.92 o 6 4 2 662.65 597.93 16.33 o 8 4 2 1230.44 1272.08 27.32 o 10 4 2 716.56 634.63 29.67 o 12 4 2 788.18 769.83 16.93 o 14 4 2 6721.66 6410.29 77.67 o 16 4 2 291.79 337.44 16.23 o 18 4 2 105.68 95.23 7.29 o -19 5 2 0.96 -2.11 4.16 o -17 5 2 8.57 12.30 3.32 o -15 5 2 251.95 263.08 11.17 o -13 5 2 665.86 643.93 21.05 o -11 5 2 3.45 6.62 5.33 o -9 5 2 558.48 639.74 27.70 o -7 5 2 1191.66 1340.21 36.94 o -5 5 2 554.88 471.58 12.33 o -3 5 2 12171.00 12673.80 99.92 o -1 5 2 6924.46 6937.04 40.06 o 1 5 2 158.12 157.51 7.71 o 3 5 2 856.08 882.34 20.05 o 5 5 2 356.83 353.14 12.80 o 7 5 2 63.29 47.80 7.73 o 9 5 2 314.31 330.27 20.29 o 11 5 2 634.65 703.78 15.42 o 13 5 2 1.27 -1.18 3.35 o 15 5 2 3.48 2.35 4.98 o 17 5 2 658.07 636.72 18.99 o -18 6 2 33.68 47.21 7.92 o -16 6 2 213.86 173.36 20.96 o -14 6 2 459.61 449.43 21.77 o -12 6 2 151.66 128.13 17.00 o -10 6 2 584.30 593.71 22.41 o -8 6 2 0.78 5.07 3.77 o -6 6 2 5289.54 5585.88 79.29 o -4 6 2 715.26 712.14 16.86 o -2 6 2 245.01 256.02 7.73 o 0 6 2 3129.83 3593.28 38.92 o 2 6 2 1911.62 2158.85 28.79 o 4 6 2 1020.89 1005.09 17.96 o 6 6 2 156.17 128.29 8.53 o 8 6 2 5.22 25.58 7.29 o 10 6 2 248.85 218.47 9.27 o 12 6 2 23.85 22.04 5.22 o 14 6 2 1363.14 1291.39 28.59 o 16 6 2 67.26 55.72 6.51 o 18 6 2 403.35 343.35 19.36 o -17 7 2 448.21 476.16 17.52 o -15 7 2 1057.09 1043.77 24.98 o -13 7 2 1405.34 1387.48 38.69 o -11 7 2 2.93 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