#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:30:32 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181245 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/23/2232340.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232340_Fobs loop_ _publ_author_name 'Deng, Yi-Fang' 'Chen, Man-Sheng' 'Zhang, Chun-Hua' 'Nie, Xue' _publ_section_title ; Poly[[tetraaquatetrakis[\m~3~-5-(pyridine-4-carboxamido)isophthalato]cobalt(II)diholmium(III)] tetrahydrate] ; _journal_coeditor_code HY2478 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1574 _journal_page_last m1575 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.141 _cell_angle_beta 78.801 _cell_angle_gamma 86.578 _cell_length_a 10.0597 _cell_length_b 10.7824 _cell_length_c 13.7261 _exptl_crystal_F_000 825.00 _reflns_d_resolution_high 0.8402 _cod_data_source_file hy2478Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 351.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 173.80 226.37 12.79 o 2 0 0 6450.00 6984.35 106.15 o 3 0 0 123524.16 134714.52 896.55 o 4 0 0 126.97 158.59 24.30 o 5 0 0 8833.07 10020.58 196.96 o 7 0 0 112.76 107.43 28.14 o 8 0 0 4049.13 4102.88 159.87 o 9 0 0 6241.50 6228.49 213.58 o 10 0 0 1572.31 1443.94 108.71 o 11 0 0 980.29 928.52 90.81 o -11 1 0 3034.69 2923.68 168.82 o -10 1 0 66.53 136.85 40.93 o -9 1 0 556.98 679.12 71.62 o -8 1 0 2448.60 2456.87 127.90 o -7 1 0 1552.02 1436.26 90.81 o -6 1 0 328.43 289.04 42.21 o -5 1 0 3625.40 3584.90 121.50 o -4 1 0 4128.82 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