#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/23/2232345.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232345_Fobs loop_ _publ_author_name 'Srinivasan, T.' 'Suhitha, S.' 'Priya, M. Gnana Ruba' 'Girija, K.' 'Chandran, N. Ravi' 'Velmurugan, D.' _publ_section_title ; 3-(4-Bromophenyl)quinazolin-4(3H)-one ; _journal_coeditor_code IM2320 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2928 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.168 _cell_angle_gamma 90.000 _cell_length_a 16.9610 _cell_length_b 3.9530 _cell_length_c 17.6984 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.7496 _[local]_cod_data_source_file im2320Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ssmmm_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 234.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3071.88 3162.40 88.59 o 4 0 0 10174.03 10144.48 325.65 o 6 0 0 4498.47 4391.12 135.92 o 8 0 0 2530.13 2509.50 73.87 o 10 0 0 799.11 828.86 26.53 o 12 0 0 5.37 14.14 7.89 o 14 0 0 194.74 143.33 16.47 o 16 0 0 50.35 12.57 13.91 o 18 0 0 167.30 139.38 21.35 o 20 0 0 36.56 45.87 20.90 o 22 0 0 3.75 30.25 38.51 o 1 1 0 11075.98 11284.11 221.85 o 2 1 0 1556.39 1658.72 31.82 o 3 1 0 3418.81 3508.06 66.74 o 4 1 0 1569.91 1613.21 30.46 o 5 1 0 874.21 869.31 17.92 o 6 1 0 7739.29 7979.45 141.77 o 7 1 0 1182.94 1232.66 25.19 o 8 1 0 3897.25 4068.58 76.47 o 9 1 0 1235.78 1324.41 28.82 o 10 1 0 2544.77 2533.32 53.01 o 11 1 0 852.79 894.60 20.91 o 12 1 0 1224.39 1240.29 37.90 o 13 1 0 4.13 12.41 10.93 o 14 1 0 506.80 524.55 28.45 o 15 1 0 7.13 -11.43 12.59 o 16 1 0 74.67 86.72 12.15 o 17 1 0 0.90 -3.48 10.43 o 18 1 0 106.83 110.46 13.49 o 19 1 0 1.22 2.25 11.90 o 20 1 0 25.81 29.59 13.24 o 21 1 0 17.59 38.40 15.06 o 0 2 0 1656.03 1578.60 52.68 o 1 2 0 10.87 16.37 2.72 o 2 2 0 1394.46 1354.33 30.80 o 3 2 0 238.51 249.13 7.76 o 4 2 0 1292.98 1212.92 26.72 o 5 2 0 5660.81 5982.17 132.58 o 6 2 0 651.64 643.11 15.85 o 7 2 0 1459.38 1482.24 35.53 o 8 2 0 203.98 216.41 7.89 o 9 2 0 654.50 613.69 15.65 o 10 2 0 29.98 29.60 6.15 o 11 2 0 371.07 411.98 22.91 o 12 2 0 427.21 441.37 24.40 o 13 2 0 1258.74 1082.06 102.59 o 14 2 0 4.71 -4.38 16.89 o 15 2 0 139.58 142.53 23.14 o 16 2 0 17.65 27.72 20.28 o 17 2 0 46.71 48.32 21.92 o 18 2 0 7.19 -2.25 22.06 o 19 2 0 0.43 -15.93 18.81 o 20 2 0 104.27 83.97 32.33 o 1 3 0 1356.67 1404.65 42.60 o 2 3 0 173.52 195.67 11.10 o 3 3 0 1636.99 1681.16 50.15 o 4 3 0 38.18 36.96 7.74 o 5 3 0 1191.30 1187.43 44.04 o 6 3 0 191.38 204.18 12.00 o 7 3 0 821.76 772.21 26.63 o 8 3 0 60.01 56.46 9.23 o 9 3 0 381.66 434.15 20.74 o 10 3 0 185.70 188.45 16.10 o 11 3 0 205.83 205.11 31.35 o 12 3 0 12.62 14.41 16.36 o 13 3 0 63.74 85.06 19.16 o 14 3 0 3.16 -2.75 28.60 o 15 3 0 1.01 9.90 31.90 o 16 3 0 2.87 2.20 33.55 o 17 3 0 0.81 4.40 35.76 o 18 3 0 0.05 -9.35 39.06 o 0 4 0 533.18 450.27 32.03 o 1 4 0 75.45 75.19 13.11 o 2 4 0 9.85 4.02 11.68 o 3 4 0 51.59 33.88 12.86 o 4 4 0 34.47 36.18 12.14 o 5 4 0 62.94 57.04 14.33 o 6 4 0 13.30 0.88 13.54 o 7 4 0 10.78 -15.40 23.93 o 8 4 0 143.12 162.24 22.31 o 9 4 0 28.26 24.75 25.30 o 10 4 0 0.42 -23.10 23.10 o 12 4 0 0.29 -26.95 28.60 o 13 4 0 89.38 116.07 35.21 o 14 4 0 1.13 -20.35 30.80 o 1 5 0 0.94 -21.78 21.78 o 2 5 0 0.07 -17.37 22.52 o 3 5 0 26.89 7.46 24.48 o 4 5 0 7.07 0.00 30.80 o -21 0 1 1.36 -2.72 19.74 o -19 0 1 12.44 16.78 19.30 o -17 0 1 56.73 84.74 42.08 o -15 0 1 163.06 200.48 48.96 o -13 0 1 16.44 14.89 9.64 o -11 0 1 1130.51 1109.10 34.60 o -9 0 1 4439.41 4425.97 131.10 o -7 0 1 6396.83 6450.32 176.98 o -5 0 1 18178.09 18144.27 456.08 o -3 0 1 54768.06 51770.35 1148.65 o -1 0 1 4112.43 4517.84 116.72 o 1 0 1 64.99 48.81 3.33 o 3 0 1 556.59 591.98 19.26 o 5 0 1 2017.83 2104.26 60.86 o 7 0 1 1994.73 2083.53 55.67 o 9 0 1 5916.01 6628.42 239.89 o 11 0 1 801.94 784.73 40.65 o 13 0 1 611.42 552.03 24.09 o 15 0 1 222.82 198.85 45.11 o 17 0 1 173.50 157.07 35.21 o 19 0 1 13.64 7.84 16.48 o 21 0 1 99.91 129.79 24.30 o -22 1 1 10.81 44.01 29.70 o -21 1 1 12.88 27.27 15.85 o -20 1 1 2.75 7.40 12.66 o -19 1 1 87.34 89.36 14.03 o -18 1 1 0.07 -9.99 11.02 o -17 1 1 100.58 115.17 12.88 o -16 1 1 0.86 1.64 9.73 o -15 1 1 586.88 618.33 29.85 o -14 1 1 30.18 8.27 8.99 o -13 1 1 868.81 850.83 45.25 o -12 1 1 876.09 825.97 26.24 o -11 1 1 656.67 680.92 21.48 o -10 1 1 588.77 646.22 14.99 o -9 1 1 29.71 34.37 3.76 o -8 1 1 815.27 802.72 15.79 o -7 1 1 1192.18 1296.90 26.06 o -6 1 1 846.08 835.67 16.02 o -5 1 1 1026.51 1033.92 21.18 o -4 1 1 773.46 764.32 15.01 o -3 1 1 2089.05 2150.19 41.67 o -2 1 1 26326.38 27252.21 489.17 o -1 1 1 624.78 637.28 14.14 o 0 1 1 12.85 13.84 1.46 o 1 1 1 19462.75 19427.89 345.32 o 2 1 1 66.59 68.79 2.68 o 3 1 1 25204.86 25260.24 530.91 o 4 1 1 4.18 2.92 2.18 o 5 1 1 6441.34 6382.95 139.16 o 6 1 1 27.52 25.79 3.05 o 7 1 1 4646.06 4408.06 91.07 o 8 1 1 521.97 567.61 12.31 o 9 1 1 737.18 697.54 14.64 o 10 1 1 183.79 224.88 7.68 o 11 1 1 2170.97 2356.61 52.79 o 12 1 1 75.62 96.57 12.79 o 13 1 1 517.50 500.72 26.21 o 14 1 1 8.33 14.44 8.95 o 15 1 1 210.29 234.56 14.34 o 16 1 1 117.52 88.80 11.21 o 17 1 1 29.44 26.85 10.56 o 18 1 1 1.06 21.33 11.15 o 19 1 1 29.42 30.66 12.49 o 20 1 1 22.16 22.74 16.12 o 21 1 1 28.94 22.56 14.13 o -20 2 1 31.42 5.45 16.46 o -19 2 1 3.27 -5.03 20.08 o -18 2 1 84.44 110.42 43.46 o -17 2 1 0.55 -4.54 19.96 o -16 2 1 41.14 49.06 20.91 o -15 2 1 47.51 39.54 19.80 o -14 2 1 277.84 302.42 43.18 o -13 2 1 13.68 1.02 10.46 o -12 2 1 69.24 69.78 12.40 o -11 2 1 50.55 71.75 12.08 o -10 2 1 1742.59 1672.49 51.38 o -9 2 1 685.11 706.39 16.87 o -8 2 1 433.62 444.46 12.24 o -7 2 1 843.54 831.31 18.56 o -6 2 1 4.18 7.96 3.96 o -5 2 1 1481.09 1450.98 36.58 o -4 2 1 1528.41 1503.62 34.79 o -3 2 1 661.19 641.26 16.27 o -2 2 1 3082.71 3199.90 75.69 o -1 2 1 514.14 498.81 11.74 o 0 2 1 553.35 556.58 12.25 o 1 2 1 1214.23 1169.27 26.76 o 2 2 1 3023.33 3158.13 69.28 o 3 2 1 1186.36 1109.61 27.37 o 4 2 1 6934.85 6995.52 144.83 o 5 2 1 324.44 300.63 8.66 o 6 2 1 1621.26 1586.05 34.87 o 7 2 1 35.48 36.06 4.24 o 8 2 1 905.27 849.48 20.22 o 9 2 1 3.53 -0.69 4.17 o 10 2 1 2019.73 1997.59 49.70 o 11 2 1 30.15 45.47 9.96 o 12 2 1 69.99 77.37 15.25 o 13 2 1 251.67 297.64 26.37 o 14 2 1 36.92 30.41 18.84 o 15 2 1 151.16 161.74 26.95 o 16 2 1 42.56 55.31 36.58 o 17 2 1 180.87 203.92 26.63 o 18 2 1 19.19 15.77 23.93 o 19 2 1 8.31 -7.58 14.35 o 20 2 1 9.03 -12.01 14.72 o -18 3 1 0.03 -30.80 35.76 o -17 3 1 1.41 31.90 36.31 o -16 3 1 8.88 -13.75 31.90 o -15 3 1 11.69 68.21 33.00 o -14 3 1 30.11 52.81 30.80 o -13 3 1 42.94 42.32 17.44 o -12 3 1 115.62 120.72 19.80 o -11 3 1 29.79 4.80 14.79 o -10 3 1 639.39 670.67 39.83 o -9 3 1 2.00 -9.33 9.33 o -8 3 1 554.29 527.09 20.53 o -7 3 1 2.95 11.47 8.16 o -6 3 1 599.76 666.95 23.64 o -5 3 1 118.74 117.80 12.82 o -4 3 1 675.14 665.90 26.53 o -3 3 1 230.14 267.41 14.25 o -2 3 1 2262.92 2269.79 66.52 o -1 3 1 166.66 185.33 10.48 o 0 3 1 1386.02 1382.88 41.96 o 1 3 1 102.49 116.07 10.64 o 2 3 1 587.52 568.32 20.22 o 3 3 1 33.03 27.83 7.40 o 4 3 1 294.45 298.14 13.73 o 5 3 1 20.21 21.59 8.21 o 6 3 1 106.75 127.59 12.09 o 7 3 1 240.59 251.25 13.96 o 8 3 1 490.91 459.04 21.03 o 9 3 1 236.64 249.13 15.28 o 10 3 1 59.60 72.65 12.86 o 11 3 1 82.21 75.50 13.34 o 12 3 1 61.30 26.20 16.39 o 13 3 1 50.30 42.22 23.65 o 14 3 1 93.04 74.26 32.45 o 15 3 1 1.78 -6.05 31.35 o 16 3 1 159.02 126.52 40.16 o 17 3 1 12.60 44.56 37.41 o 18 3 1 60.06 19.25 40.16 o -14 4 1 9.25 45.11 34.10 o -13 4 1 0.58 8.80 31.35 o -12 4 1 18.89 -25.85 28.05 o -11 4 1 17.40 15.95 28.60 o -10 4 1 25.39 21.45 28.05 o -9 4 1 32.16 -8.25 25.30 o -8 4 1 4.20 1.00 17.93 o -7 4 1 8.28 -9.08 20.08 o -6 4 1 30.23 27.23 14.18 o -5 4 1 23.25 24.09 13.80 o -4 4 1 0.63 -11.43 13.20 o -3 4 1 134.32 114.65 14.03 o -2 4 1 81.13 81.87 12.86 o -1 4 1 7.71 18.66 11.93 o 0 4 1 148.18 148.67 14.37 o 1 4 1 3.93 17.14 11.60 o 2 4 1 46.81 31.87 11.93 o 3 4 1 0.28 -11.03 11.03 o 4 4 1 86.65 103.60 16.11 o 5 4 1 71.91 64.48 15.05 o 6 4 1 211.78 226.71 24.27 o 7 4 1 9.19 2.62 17.45 o 8 4 1 296.22 281.07 26.68 o 9 4 1 125.37 84.16 26.40 o 10 4 1 436.74 335.55 38.51 o 11 4 1 11.17 -1.10 25.85 o 13 4 1 0.54 34.10 31.90 o 14 4 1 0.79 25.85 34.10 o -5 5 1 0.30 -21.45 33.00 o -4 5 1 3.80 -17.05 32.45 o -3 5 1 7.00 18.00 50.33 o -2 5 1 5.54 7.92 22.24 o -1 5 1 1.75 12.57 22.47 o 0 5 1 54.25 18.79 21.20 o 1 5 1 26.68 0.68 22.52 o 2 5 1 39.94 54.02 24.25 o 3 5 1 22.95 -26.95 30.25 o 4 5 1 12.75 42.91 31.90 o -22 0 2 1.62 13.79 22.04 o -20 0 2 0.17 27.40 20.59 o -18 0 2 9.47 -15.84 15.84 o -16 0 2 37.33 75.25 15.99 o -14 0 2 202.68 185.84 18.23 o -12 0 2 2125.11 2090.72 69.94 o -10 0 2 2876.44 2791.13 88.52 o -8 0 2 3505.61 3357.78 87.26 o -6 0 2 1914.73 1917.76 43.92 o -4 0 2 9248.06 9557.23 212.69 o -2 0 2 1675.31 1749.62 45.62 o 0 0 2 5279.69 5370.67 129.38 o 2 0 2 54.00 81.89 3.26 o 4 0 2 1042.48 1082.17 62.57 o 6 0 2 4534.53 4859.84 138.34 o 8 0 2 5468.38 5719.73 209.37 o 10 0 2 64.33 49.48 4.77 o 12 0 2 931.21 932.43 50.56 o 14 0 2 721.32 705.12 44.83 o 16 0 2 386.44 380.21 28.33 o 18 0 2 329.76 359.15 28.29 o 20 0 2 190.76 165.23 23.07 o 22 0 2 14.94 -14.85 40.71 o -22 1 2 70.11 128.72 34.65 o -21 1 2 31.54 30.27 20.36 o -20 1 2 34.52 50.60 17.63 o -19 1 2 14.25 -4.60 11.92 o -18 1 2 49.48 37.38 12.04 o -17 1 2 10.10 5.01 10.87 o -16 1 2 269.03 242.70 15.96 o -15 1 2 85.69 83.05 11.42 o -14 1 2 95.84 85.67 11.07 o -13 1 2 57.05 57.57 11.90 o -12 1 2 570.35 564.72 22.63 o -11 1 2 4.75 3.79 4.24 o -10 1 2 61.00 67.54 4.63 o -9 1 2 537.15 510.68 12.61 o -8 1 2 29.83 31.83 3.17 o -7 1 2 1503.23 1566.00 33.37 o -6 1 2 1257.39 1314.30 25.32 o -5 1 2 1579.64 1593.19 30.32 o -4 1 2 1302.72 1260.41 22.97 o -3 1 2 1607.14 1726.67 32.18 o -2 1 2 22794.10 22892.34 411.89 o -1 1 2 6714.13 6892.83 136.18 o 0 1 2 1133.58 1076.58 21.96 o 1 1 2 8.78 7.53 1.57 o 2 1 2 14830.93 14734.39 346.54 o 3 1 2 85.50 88.88 3.93 o 4 1 2 889.41 809.24 19.87 o 5 1 2 73.52 85.17 4.08 o 6 1 2 2133.19 2002.03 44.60 o 7 1 2 1609.78 1736.73 39.16 o 8 1 2 4030.05 4201.21 92.24 o 9 1 2 90.73 90.48 4.02 o 10 1 2 797.41 782.08 17.31 o 11 1 2 261.42 251.50 9.59 o 12 1 2 4.45 6.87 5.25 o 13 1 2 24.15 8.55 11.14 o 14 1 2 38.83 35.90 9.68 o 15 1 2 30.90 15.73 8.83 o 16 1 2 1.61 1.01 9.24 o 17 1 2 39.87 46.87 12.74 o 18 1 2 79.57 44.07 11.57 o 19 1 2 102.52 89.01 17.99 o 20 1 2 0.86 1.81 12.87 o 21 1 2 17.08 15.14 14.28 o -20 2 2 5.97 12.10 37.96 o -19 2 2 4.53 -0.11 26.42 o -18 2 2 7.87 9.35 22.69 o -17 2 2 22.88 19.03 20.48 o -16 2 2 35.49 57.54 21.95 o -15 2 2 23.45 19.59 18.17 o -14 2 2 7.22 -3.38 17.10 o -13 2 2 868.41 725.94 33.83 o -12 2 2 971.29 998.81 78.41 o -11 2 2 156.10 185.50 15.54 o -10 2 2 234.38 263.91 15.96 o -9 2 2 11.37 11.55 5.42 o -8 2 2 578.46 615.92 15.11 o -7 2 2 671.02 691.73 18.44 o -6 2 2 309.28 323.28 9.75 o -5 2 2 1452.05 1520.58 35.65 o -4 2 2 392.03 377.19 11.01 o -3 2 2 331.19 356.53 11.05 o -2 2 2 1211.13 1179.53 26.01 o -1 2 2 4420.97 4608.98 100.81 o 0 2 2 764.98 764.72 17.07 o 1 2 2 5098.50 5161.93 112.43 o 2 2 2 366.99 362.85 9.97 o 3 2 2 2226.40 2137.80 47.55 o 4 2 2 206.03 215.66 6.98 o 5 2 2 524.89 464.97 11.87 o 6 2 2 468.93 460.19 11.38 o 7 2 2 629.23 607.38 15.16 o 8 2 2 241.47 251.79 8.27 o 9 2 2 184.42 192.44 8.01 o 10 2 2 617.38 640.43 18.25 o 11 2 2 244.26 275.82 17.02 o 12 2 2 300.75 292.40 19.61 o 13 2 2 38.64 13.33 21.88 o 14 2 2 231.63 210.20 25.58 o 15 2 2 50.59 65.49 20.83 o 16 2 2 91.48 121.37 23.13 o 17 2 2 8.22 -7.82 20.44 o 18 2 2 0.84 -13.88 13.88 o 19 2 2 10.13 -13.89 13.89 o 20 2 2 87.77 110.09 17.72 o -18 3 2 31.50 29.70 37.96 o -17 3 2 20.58 95.71 38.51 o -16 3 2 7.06 14.85 33.00 o -15 3 2 57.42 108.37 35.21 o -14 3 2 10.33 18.70 28.60 o -13 3 2 77.41 97.11 19.55 o -12 3 2 3.34 2.92 15.20 o -11 3 2 146.25 140.84 20.18 o -10 3 2 36.90 27.80 15.33 o -9 3 2 254.46 269.67 19.27 o -8 3 2 0.93 4.59 9.65 o -7 3 2 923.64 953.43 31.46 o -6 3 2 29.21 25.82 8.23 o -5 3 2 567.14 560.83 20.96 o -4 3 2 50.98 63.55 8.65 o -3 3 2 1045.07 1071.28 34.00 o -2 3 2 18.02 11.70 7.34 o -1 3 2 9.06 6.87 7.02 o 0 3 2 85.97 81.35 8.03 o 1 3 2 49.11 47.95 7.37 o 2 3 2 0.99 2.67 6.73 o 3 3 2 0.06 -0.64 7.05 o 4 3 2 460.49 436.84 17.32 o 5 3 2 88.44 97.92 10.29 o 6 3 2 116.12 131.83 10.54 o 7 3 2 449.94 441.83 17.86 o 8 3 2 0.35 -7.50 9.05 o 9 3 2 42.97 45.00 10.22 o 10 3 2 152.15 158.89 27.77 o 11 3 2 795.24 711.81 32.94 o 12 3 2 13.13 5.73 11.88 o 13 3 2 300.29 319.69 28.49 o 14 3 2 2.71 -14.85 29.15 o 15 3 2 148.49 100.66 35.21 o 16 3 2 16.48 1.10 34.65 o 17 3 2 2.60 -18.15 35.21 o 18 3 2 60.99 66.56 42.91 o -14 4 2 2.06 -6.05 33.55 o -13 4 2 7.36 -2.20 30.80 o -12 4 2 9.44 -25.30 28.60 o -11 4 2 0.66 -8.80 27.50 o -10 4 2 1.22 -13.75 25.85 o -8 4 2 0.73 2.75 24.75 o -7 4 2 22.74 16.50 18.27 o -6 4 2 4.11 6.16 14.12 o -5 4 2 46.53 63.92 15.44 o -4 4 2 8.50 9.56 13.79 o -3 4 2 116.53 140.98 20.17 o -2 4 2 0.26 -4.79 11.41 o -1 4 2 82.45 92.56 13.38 o 0 4 2 0.26 20.15 11.47 o 1 4 2 408.87 434.67 22.53 o 2 4 2 2.16 3.31 11.45 o 3 4 2 315.03 318.79 25.17 o 4 4 2 2.78 -12.92 12.92 o 5 4 2 345.56 340.11 22.60 o 6 4 2 108.26 95.52 19.65 o 7 4 2 706.85 832.28 74.26 o 8 4 2 25.68 27.11 18.62 o 9 4 2 4.08 -23.10 23.10 o 10 4 2 2.59 11.00 23.65 o 11 4 2 10.21 13.75 24.75 o 12 4 2 20.12 -19.80 24.20 o 14 4 2 19.33 18.15 33.55 o -5 5 2 16.88 2.20 34.10 o -4 5 2 0.45 3.12 26.40 o -3 5 2 44.45 4.83 41.81 o -2 5 2 34.32 20.53 22.79 o -1 5 2 17.84 -9.99 22.34 o 0 5 2 3.91 1.73 27.50 o 1 5 2 3.12 -21.38 21.38 o 2 5 2 19.72 21.80 37.68 o 3 5 2 1.13 -3.85 29.70 o 4 5 2 20.72 20.90 32.45 o -21 0 3 20.39 10.11 22.07 o -19 0 3 37.26 39.64 28.05 o -17 0 3 131.43 169.37 20.98 o -15 0 3 770.80 785.68 42.53 o -13 0 3 107.12 107.99 14.79 o -11 0 3 2673.28 2632.85 84.25 o -9 0 3 4392.69 4397.19 117.40 o -7 0 3 1688.70 1662.38 40.89 o 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