#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/24/2232457.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232457_Fobs loop_ _publ_author_name 'Wang, Qian' 'Shu, Youqin' 'Hou, Xuehui' _publ_section_title ; (Furan-2-yl)[(furan-2-yl)carbonyldisulfanyl]methanone ; _journal_coeditor_code RZ2653 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3055 _journal_volume 67 _journal_year 2011 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.6900 _cell_length_b 7.9611 _cell_length_c 9.9042 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file rz2653Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 100210h in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 150.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 518.36 531.18 5.66 o 4 0 0 509.26 463.75 5.98 o 6 0 0 18108.88 18580.51 221.16 o 8 0 0 244.62 177.55 4.64 o 10 0 0 441.10 416.15 13.03 o 12 0 0 9.71 -0.86 3.13 o 14 0 0 978.40 839.81 23.03 o 16 0 0 71.54 55.71 8.87 o 1 1 0 6675.49 6799.92 74.80 o 3 1 0 5372.13 5601.05 76.88 o 5 1 0 3209.47 3178.89 24.61 o 7 1 0 5133.88 5247.60 36.55 o 9 1 0 1589.06 1574.31 20.82 o 11 1 0 869.46 863.07 20.73 o 13 1 0 107.34 108.74 6.12 o 15 1 0 136.21 128.53 7.22 o 0 2 0 22363.15 18630.75 219.99 o 2 2 0 149.24 174.71 2.74 o 4 2 0 905.51 908.15 7.15 o 6 2 0 2456.69 2473.00 26.42 o 8 2 0 0.79 -1.87 1.25 o 10 2 0 13.51 6.66 1.97 o 12 2 0 89.37 98.45 5.62 o 14 2 0 382.56 380.92 13.63 o 1 3 0 154.32 163.11 3.08 o 3 3 0 508.26 488.67 5.90 o 5 3 0 507.21 502.46 5.25 o 7 3 0 920.96 955.89 10.92 o 9 3 0 378.08 350.21 6.83 o 11 3 0 351.04 358.30 7.56 o 13 3 0 187.53 193.38 10.16 o 15 3 0 74.05 80.42 6.99 o 0 4 0 2080.01 1968.72 29.86 o 2 4 0 403.89 422.28 5.96 o 4 4 0 99.40 104.09 3.12 o 6 4 0 1218.50 1191.06 12.52 o 8 4 0 604.28 603.51 10.52 o 10 4 0 314.68 320.40 10.50 o 12 4 0 301.39 311.08 9.75 o 14 4 0 156.53 177.30 12.31 o 1 5 0 857.97 824.70 21.35 o 3 5 0 1257.26 1322.74 13.44 o 5 5 0 996.85 1025.91 9.58 o 7 5 0 192.33 185.87 6.78 o 9 5 0 1308.45 1284.97 19.77 o 11 5 0 137.25 143.76 10.89 o 13 5 0 13.28 10.88 3.98 o 0 6 0 709.51 673.05 17.21 o 2 6 0 5.65 0.96 2.32 o 4 6 0 73.47 73.60 4.38 o 6 6 0 220.20 196.97 7.02 o 8 6 0 86.75 92.21 5.53 o 10 6 0 110.05 109.98 6.47 o 12 6 0 42.38 43.25 5.60 o 1 7 0 3.83 -0.80 2.73 o 3 7 0 89.61 84.95 5.27 o 5 7 0 129.77 116.14 9.33 o 7 7 0 4.73 -3.06 4.01 o 9 7 0 43.77 44.08 5.39 o 0 8 0 103.62 90.76 8.28 o 2 8 0 6.46 1.45 3.33 o 4 8 0 50.39 51.84 8.50 o 6 8 0 1.12 -6.28 4.28 o 8 8 0 19.38 14.53 7.03 o 1 9 0 5.99 -0.73 5.33 o 3 9 0 0.02 5.07 5.77 o 5 9 0 0.12 1.68 5.81 o 1 1 1 1881.07 1914.85 9.85 o 2 1 1 293.50 300.27 2.41 o 3 1 1 206.02 204.19 2.13 o 4 1 1 2051.63 2141.85 17.76 o 5 1 1 50.76 54.14 1.29 o 6 1 1 291.55 292.05 2.65 o 7 1 1 5.76 2.63 0.68 o 8 1 1 2.82 0.19 0.64 o 9 1 1 19.76 19.46 1.40 o 10 1 1 159.08 147.20 3.10 o 11 1 1 63.74 52.35 2.73 o 12 1 1 1.81 1.45 1.88 o 13 1 1 26.52 21.70 2.89 o 14 1 1 12.06 24.44 3.36 o 15 1 1 8.16 2.99 2.81 o 16 1 1 0.53 -1.96 2.42 o 1 2 1 7826.35 7818.73 73.53 o 2 2 1 202.24 217.39 1.94 o 3 2 1 527.31 531.48 6.51 o 4 2 1 230.27 243.81 4.60 o 5 2 1 385.17 401.08 5.65 o 6 2 1 16.92 11.90 0.98 o 7 2 1 151.04 155.52 2.40 o 8 2 1 52.47 62.48 1.76 o 9 2 1 2.59 0.93 1.23 o 10 2 1 282.38 267.46 5.04 o 11 2 1 15.11 17.82 1.86 o 12 2 1 23.44 24.78 2.45 o 13 2 1 125.90 109.77 4.36 o 14 2 1 1.10 -0.46 2.49 o 15 2 1 0.43 0.42 2.72 o 1 3 1 7.03 10.11 1.67 o 2 3 1 22.95 25.28 1.18 o 3 3 1 925.55 898.83 5.62 o 4 3 1 158.40 185.18 2.29 o 5 3 1 1427.96 1517.03 8.64 o 6 3 1 94.18 100.12 2.00 o 7 3 1 99.10 92.03 2.02 o 8 3 1 205.02 202.99 3.51 o 9 3 1 173.18 177.13 3.54 o 10 3 1 3.39 3.68 1.68 o 11 3 1 618.42 587.92 6.96 o 12 3 1 0.14 -0.24 1.60 o 13 3 1 1.17 -1.64 1.90 o 14 3 1 21.79 29.81 4.08 o 15 3 1 9.75 5.28 3.44 o 1 4 1 22.61 24.74 1.89 o 2 4 1 507.59 473.39 4.53 o 3 4 1 45.12 48.32 1.65 o 4 4 1 2519.08 2626.20 13.64 o 5 4 1 318.12 326.05 3.40 o 6 4 1 59.76 58.73 1.80 o 7 4 1 45.85 45.46 2.08 o 8 4 1 11.09 9.48 1.51 o 9 4 1 9.30 16.44 2.11 o 10 4 1 651.85 637.03 10.67 o 11 4 1 24.78 29.01 2.70 o 12 4 1 44.45 51.12 3.35 o 13 4 1 0.05 -2.92 1.95 o 14 4 1 12.20 13.05 3.62 o 1 5 1 719.91 718.37 8.18 o 2 5 1 143.78 152.91 3.11 o 3 5 1 575.08 548.32 5.49 o 4 5 1 0.05 -0.10 1.04 o 5 5 1 536.85 544.67 6.38 o 6 5 1 103.20 107.63 3.62 o 7 5 1 38.74 33.51 2.36 o 8 5 1 64.10 69.49 3.07 o 9 5 1 103.23 99.48 4.17 o 10 5 1 0.23 5.54 2.30 o 11 5 1 159.54 154.17 5.37 o 12 5 1 57.58 59.53 4.25 o 13 5 1 10.87 8.76 2.88 o 1 6 1 14.76 13.65 2.01 o 2 6 1 347.44 345.45 7.30 o 3 6 1 126.11 121.74 3.71 o 4 6 1 439.98 447.68 6.97 o 5 6 1 220.88 216.04 5.00 o 6 6 1 1.74 -1.47 1.72 o 7 6 1 32.27 37.98 3.12 o 8 6 1 116.34 100.10 4.63 o 9 6 1 41.55 48.06 5.18 o 10 6 1 151.93 161.42 5.34 o 11 6 1 73.51 85.73 4.66 o 12 6 1 0.99 -3.55 2.42 o 1 7 1 536.20 551.68 8.31 o 2 7 1 32.64 31.74 2.94 o 3 7 1 322.02 314.68 7.47 o 4 7 1 130.69 130.93 6.80 o 5 7 1 145.82 149.67 7.20 o 6 7 1 1.76 -0.56 2.36 o 7 7 1 78.64 84.88 4.72 o 8 7 1 31.71 28.48 3.84 o 9 7 1 62.84 71.26 5.35 o 10 7 1 36.70 39.17 4.46 o 1 8 1 12.10 9.66 2.50 o 2 8 1 254.94 254.74 7.27 o 3 8 1 0.10 4.18 4.61 o 4 8 1 223.85 224.94 9.03 o 5 8 1 14.16 13.85 4.17 o 6 8 1 50.12 47.83 5.93 o 7 8 1 5.86 9.08 4.26 o 8 8 1 66.55 67.02 6.92 o 1 9 1 147.11 151.40 6.23 o 2 9 1 1.25 3.76 3.91 o 3 9 1 62.11 64.44 6.87 o 4 9 1 6.81 7.99 4.48 o 0 0 2 10323.52 10594.18 121.34 o 1 0 2 598.55 502.34 14.23 o 2 0 2 613.30 626.89 5.93 o 3 0 2 850.87 948.86 8.30 o 4 0 2 148.70 146.09 2.37 o 5 0 2 469.33 481.92 9.54 o 6 0 2 2968.84 3153.02 20.58 o 7 0 2 30.22 46.59 1.92 o 8 0 2 388.94 361.46 5.00 o 9 0 2 7.84 4.92 2.02 o 10 0 2 6.55 2.78 1.60 o 11 0 2 11.32 12.44 3.17 o 12 0 2 242.85 276.26 23.22 o 13 0 2 294.63 320.66 19.28 o 14 0 2 163.86 151.23 7.42 o 15 0 2 76.83 84.26 6.55 o 16 0 2 11.54 9.72 4.46 o 0 1 2 9706.23 9592.12 425.94 o 1 1 2 5698.98 5982.50 85.13 o 2 1 2 5781.08 6091.19 31.79 o 3 1 2 231.23 235.58 2.45 o 4 1 2 56.07 56.31 1.11 o 5 1 2 2831.78 2901.22 15.33 o 6 1 2 141.41 142.60 1.93 o 7 1 2 1021.45 1058.91 6.47 o 8 1 2 2120.96 2192.34 12.52 o 9 1 2 421.07 430.03 4.61 o 10 1 2 1.08 -0.11 1.16 o 11 1 2 234.20 216.81 4.50 o 12 1 2 568.81 545.03 8.48 o 13 1 2 63.81 76.74 3.93 o 14 1 2 14.36 19.99 3.28 o 15 1 2 149.41 150.24 5.48 o 0 2 2 22714.23 21511.25 1162.04 o 1 2 2 8175.17 8028.03 99.08 o 2 2 2 57.84 57.57 1.30 o 3 2 2 35.04 41.22 1.16 o 4 2 2 209.00 224.73 2.45 o 5 2 2 1458.28 1507.56 9.71 o 6 2 2 4174.57 4403.83 39.23 o 7 2 2 818.20 750.93 5.98 o 8 2 2 320.37 303.90 3.73 o 9 2 2 492.30 484.38 5.63 o 10 2 2 136.96 125.30 3.17 o 11 2 2 46.90 51.01 2.60 o 12 2 2 133.90 142.14 4.35 o 13 2 2 149.15 139.02 5.14 o 14 2 2 271.20 257.22 6.57 o 15 2 2 124.54 125.28 5.43 o 0 3 2 3755.82 3938.53 49.08 o 1 3 2 831.16 831.61 7.60 o 2 3 2 1736.44 1806.09 11.62 o 3 3 2 1835.06 1975.73 11.59 o 4 3 2 6.18 4.60 0.68 o 5 3 2 1533.15 1601.07 9.08 o 6 3 2 1240.74 1277.50 10.83 o 7 3 2 468.61 450.45 4.51 o 8 3 2 1012.55 1041.80 9.30 o 9 3 2 1199.98 1211.78 9.87 o 10 3 2 5.61 5.88 1.60 o 11 3 2 388.92 379.37 5.60 o 12 3 2 20.66 24.69 2.59 o 13 3 2 25.43 26.19 3.13 o 14 3 2 45.70 45.61 6.68 o 15 3 2 100.54 118.49 6.05 o 0 4 2 4640.96 4576.93 51.04 o 1 4 2 950.65 963.00 8.03 o 2 4 2 23.83 24.30 2.93 o 3 4 2 203.23 214.98 3.07 o 4 4 2 8.83 12.27 1.23 o 5 4 2 104.30 84.62 2.08 o 6 4 2 742.07 755.39 7.57 o 7 4 2 289.45 277.19 5.22 o 8 4 2 60.97 61.59 3.59 o 9 4 2 39.41 38.37 2.72 o 10 4 2 92.35 80.13 3.33 o 11 4 2 7.49 9.53 2.17 o 12 4 2 21.14 24.21 2.82 o 13 4 2 37.37 39.08 3.33 o 14 4 2 156.76 151.37 6.65 o 0 5 2 197.06 199.89 6.00 o 1 5 2 1.31 -0.58 1.20 o 2 5 2 0.08 -1.04 0.96 o 3 5 2 316.70 319.11 4.48 o 4 5 2 163.50 153.87 2.98 o 5 5 2 50.31 47.66 2.60 o 6 5 2 79.33 76.88 3.70 o 7 5 2 189.63 183.28 4.79 o 8 5 2 0.58 -1.81 1.53 o 9 5 2 198.96 201.22 4.96 o 10 5 2 127.08 127.63 4.43 o 11 5 2 104.00 102.34 3.94 o 12 5 2 0.63 -1.48 2.23 o 13 5 2 28.42 28.27 3.63 o 0 6 2 260.05 237.95 12.35 o 1 6 2 213.69 214.92 5.37 o 2 6 2 7.11 4.14 1.74 o 3 6 2 134.23 134.94 3.96 o 4 6 2 16.08 15.18 2.64 o 5 6 2 1.84 1.12 1.81 o 6 6 2 63.62 67.38 4.12 o 7 6 2 198.11 188.76 5.14 o 8 6 2 1.53 0.00 2.05 o 9 6 2 50.76 53.64 3.88 o 10 6 2 17.67 17.89 3.08 o 11 6 2 23.39 23.64 3.44 o 12 6 2 8.32 9.84 3.33 o 0 7 2 83.96 77.04 4.99 o 1 7 2 21.38 12.95 2.50 o 2 7 2 67.95 66.00 3.41 o 3 7 2 22.68 15.04 3.01 o 4 7 2 2.96 2.32 3.29 o 5 7 2 18.29 16.43 4.03 o 6 7 2 75.57 80.67 6.72 o 7 7 2 26.33 27.57 3.81 o 8 7 2 80.78 82.88 5.11 o 9 7 2 28.91 32.99 4.21 o 10 7 2 0.02 2.67 3.53 o 0 8 2 104.90 95.97 5.84 o 1 8 2 33.97 32.80 3.22 o 2 8 2 4.88 3.99 2.82 o 3 8 2 0.63 1.03 3.60 o 4 8 2 2.76 -0.09 3.60 o 5 8 2 0.17 0.05 3.61 o 6 8 2 28.32 21.14 4.89 o 7 8 2 4.63 1.51 3.81 o 8 8 2 0.92 0.67 3.98 o 0 9 2 55.57 70.92 9.67 o 1 9 2 0.54 0.13 2.84 o 2 9 2 1.54 -2.05 3.58 o 3 9 2 0.85 1.48 3.71 o 4 9 2 23.13 22.33 5.31 o 1 1 3 3687.74 3953.49 48.65 o 2 1 3 2841.22 2975.21 34.04 o 3 1 3 822.58 855.53 8.71 o 4 1 3 74.71 56.16 1.30 o 5 1 3 1156.29 1238.55 10.94 o 6 1 3 192.50 198.89 2.41 o 7 1 3 1.23 2.74 0.76 o 8 1 3 268.38 283.17 3.72 o 9 1 3 2.18 1.23 1.11 o 10 1 3 48.95 47.62 2.32 o 11 1 3 40.30 35.93 2.54 o 12 1 3 45.83 47.90 3.08 o 13 1 3 104.96 105.64 4.46 o 14 1 3 0.85 -3.62 2.41 o 15 1 3 0.40 0.66 2.79 o 1 2 3 291.10 313.91 3.45 o 2 2 3 16.93 14.45 1.02 o 3 2 3 994.28 1018.95 7.91 o 4 2 3 1011.27 1073.13 9.02 o 5 2 3 74.31 69.74 1.86 o 6 2 3 529.17 570.83 4.54 o 7 2 3 20.63 20.87 1.41 o 8 2 3 5.57 9.49 1.30 o 9 2 3 131.74 125.15 3.34 o 10 2 3 273.52 259.28 4.39 o 11 2 3 6.65 3.25 1.68 o 12 2 3 12.56 18.41 2.34 o 13 2 3 5.77 2.30 2.09 o 14 2 3 0.18 -4.04 2.69 o 15 2 3 0.26 4.41 3.47 o 1 3 3 1095.90 1166.60 13.34 o 2 3 3 2013.08 2083.96 13.33 o 3 3 3 20.45 21.25 1.33 o 4 3 3 30.51 15.62 1.14 o 5 3 3 0.37 0.46 0.71 o 6 3 3 4.31 4.44 1.05 o 7 3 3 169.48 165.69 5.04 o 8 3 3 418.10 418.26 5.62 o 9 3 3 1.35 -1.82 1.21 o 10 3 3 13.87 8.62 1.85 o 11 3 3 0.17 0.35 1.66 o 12 3 3 27.62 27.03 3.16 o 13 3 3 22.48 28.49 3.25 o 14 3 3 0.04 2.26 3.22 o 1 4 3 386.78 374.38 6.22 o 2 4 3 0.34 0.38 0.88 o 3 4 3 114.71 113.19 2.74 o 4 4 3 16.68 23.99 1.49 o 5 4 3 191.62 173.67 3.50 o 6 4 3 44.98 55.47 2.96 o 7 4 3 31.92 42.35 7.42 o 8 4 3 148.01 134.35 3.70 o 9 4 3 165.32 150.80 4.04 o 10 4 3 32.24 25.31 2.55 o 11 4 3 11.02 16.67 2.36 o 12 4 3 9.69 9.51 2.33 o 13 4 3 10.87 7.82 2.91 o 14 4 3 26.58 23.94 3.53 o 1 5 3 67.60 56.87 2.61 o 2 5 3 262.87 252.58 4.84 o 3 5 3 311.96 290.64 5.16 o 4 5 3 351.35 349.06 5.62 o 5 5 3 160.98 153.22 3.61 o 6 5 3 83.47 75.10 2.84 o 7 5 3 14.85 10.86 2.14 o 8 5 3 33.85 37.25 2.84 o 9 5 3 82.56 77.95 3.53 o 10 5 3 112.94 108.80 3.96 o 11 5 3 69.88 77.91 3.89 o 12 5 3 66.94 67.28 4.22 o 13 5 3 0.18 -3.69 2.46 o 1 6 3 1.84 1.22 1.69 o 2 6 3 373.81 371.35 6.39 o 3 6 3 417.67 420.92 8.17 o 4 6 3 543.50 546.51 9.49 o 5 6 3 179.65 194.01 5.83 o 6 6 3 20.51 17.15 4.02 o 7 6 3 60.46 58.14 4.48 o 8 6 3 0.57 -1.22 2.49 o 9 6 3 96.75 96.42 6.41 o 10 6 3 138.13 143.38 6.25 o 11 6 3 128.85 146.17 6.40 o 1 7 3 67.14 58.10 3.43 o 2 7 3 27.76 35.04 3.58 o 3 7 3 80.49 72.70 6.58 o 4 7 3 148.44 150.50 5.63 o 5 7 3 289.90 279.37 9.61 o 6 7 3 93.59 102.59 8.78 o 7 7 3 0.02 -0.91 4.66 o 8 7 3 2.97 -1.91 2.73 o 9 7 3 37.19 45.62 4.80 o 10 7 3 82.84 94.95 6.73 o 1 8 3 44.96 42.09 5.11 o 2 8 3 28.02 25.82 3.69 o 3 8 3 184.55 199.08 6.83 o 4 8 3 109.15 102.37 6.85 o 5 8 3 13.47 11.45 4.34 o 6 8 3 20.34 8.96 5.12 o 7 8 3 11.91 10.14 4.40 o 1 9 3 2.60 -0.52 2.93 o 2 9 3 31.27 45.17 6.15 o 0 0 4 231.93 229.87 7.11 o 1 0 4 3985.39 3873.20 99.46 o 2 0 4 324.27 317.34 29.25 o 3 0 4 1034.83 1132.93 21.38 o 4 0 4 480.27 485.37 6.46 o 5 0 4 693.88 690.12 14.69 o 6 0 4 256.92 294.44 5.21 o 7 0 4 2731.31 2769.30 53.43 o 8 0 4 4.17 11.86 1.73 o 9 0 4 1260.50 1263.30 14.39 o 10 0 4 0.03 -0.93 2.21 o 11 0 4 7.31 6.51 2.21 o 12 0 4 255.33 266.87 19.27 o 13 0 4 589.47 588.72 13.68 o 14 0 4 3.99 5.95 4.02 o 15 0 4 128.28 135.32 7.75 o 0 1 4 1151.41 1192.37 46.18 o 1 1 4 8.84 7.11 1.24 o 2 1 4 3899.11 4033.80 46.92 o 3 1 4 222.84 255.84 3.87 o 4 1 4 235.01 206.46 3.84 o 5 1 4 880.50 898.80 6.35 o 6 1 4 1091.18 1077.23 7.94 o 7 1 4 188.74 207.62 4.94 o 8 1 4 1939.79 2013.34 16.50 o 9 1 4 398.38 405.60 4.83 o 10 1 4 36.60 36.25 3.14 o 11 1 4 142.89 127.74 3.79 o 12 1 4 201.36 196.94 4.85 o 13 1 4 3.03 9.96 2.80 o 14 1 4 192.83 222.22 7.41 o 15 1 4 46.92 57.78 4.59 o 0 2 4 1215.10 1255.01 30.75 o 1 2 4 2292.43 2269.76 20.23 o 2 2 4 425.73 473.10 5.43 o 3 2 4 79.55 77.89 2.53 o 4 2 4 108.93 112.09 2.24 o 5 2 4 179.72 136.17 2.26 o 6 2 4 705.58 737.86 6.49 o 7 2 4 1303.75 1319.29 9.76 o 8 2 4 340.52 357.88 5.44 o 9 2 4 27.08 23.65 1.75 o 10 2 4 46.08 43.25 2.40 o 11 2 4 19.48 13.30 2.20 o 12 2 4 57.69 61.52 5.87 o 13 2 4 415.81 415.20 8.21 o 14 2 4 11.01 8.03 3.51 o 0 3 4 97.17 97.00 3.73 o 1 3 4 1173.65 1232.70 11.91 o 2 3 4 2441.41 2502.62 15.94 o 3 3 4 6.93 6.00 1.10 o 4 3 4 474.01 459.44 5.70 o 5 3 4 261.91 260.08 3.15 o 6 3 4 326.32 318.67 6.11 o 7 3 4 102.86 104.26 3.02 o 8 3 4 863.91 844.02 9.01 o 9 3 4 78.82 76.62 3.08 o 10 3 4 51.73 44.43 2.88 o 11 3 4 0.27 -1.56 1.66 o 12 3 4 174.69 176.39 6.36 o 13 3 4 1.32 -0.33 2.41 o 14 3 4 13.77 15.29 3.21 o 0 4 4 542.71 588.03 10.36 o 1 4 4 2795.94 2882.88 21.19 o 2 4 4 207.31 197.71 3.42 o 3 4 4 360.76 380.24 4.88 o 4 4 4 56.70 59.17 2.29 o 5 4 4 442.61 417.50 6.29 o 6 4 4 177.62 190.62 4.01 o 7 4 4 507.73 513.47 6.73 o 8 4 4 9.96 6.78 2.04 o 9 4 4 14.67 11.71 2.09 o 10 4 4 20.66 20.77 2.48 o 11 4 4 60.40 50.83 3.30 o 12 4 4 0.00 -2.34 2.10 o 13 4 4 108.87 99.47 4.66 o 0 5 4 499.13 470.30 11.85 o 1 5 4 1.24 1.16 1.43 o 2 5 4 525.77 532.53 9.11 o 3 5 4 106.08 109.95 3.50 o 4 5 4 2.74 1.84 1.96 o 5 5 4 9.47 9.81 2.66 o 6 5 4 535.17 502.39 15.94 o 7 5 4 7.01 8.07 2.16 o 8 5 4 473.34 493.80 10.20 o 9 5 4 43.31 47.21 3.61 o 10 5 4 9.01 9.50 2.33 o 11 5 4 4.02 5.66 2.42 o 12 5 4 48.48 56.23 3.90 o 0 6 4 256.07 245.75 7.58 o 1 6 4 576.45 571.33 8.24 o 2 6 4 165.89 167.43 4.57 o 3 6 4 21.86 21.45 3.03 o 4 6 4 60.27 56.67 4.44 o 5 6 4 182.65 183.94 5.86 o 6 6 4 67.56 66.97 5.85 o 7 6 4 44.33 45.41 5.15 o 8 6 4 3.87 0.88 2.61 o 9 6 4 1.88 -0.23 2.25 o 10 6 4 11.38 15.28 3.81 o 11 6 4 9.71 14.83 3.82 o 0 7 4 3.28 0.31 2.72 o 1 7 4 14.83 11.82 2.27 o 2 7 4 18.93 16.19 3.01 o 3 7 4 0.88 -0.12 2.24 o 4 7 4 1.56 -0.63 2.54 o 5 7 4 1.26 -0.67 3.22 o 6 7 4 13.58 9.92 3.82 o 7 7 4 0.79 -3.40 3.23 o 8 7 4 52.74 70.13 6.81 o 9 7 4 7.13 6.31 4.21 o 0 8 4 0.00 -2.59 2.93 o 1 8 4 0.45 -3.69 2.46 o 2 8 4 1.63 -1.29 2.74 o 3 8 4 1.56 -0.77 3.00 o 4 8 4 24.05 20.68 4.49 o 5 8 4 4.06 1.79 3.72 o 6 8 4 0.52 -5.11 3.41 o 1 1 5 5.06 3.66 1.03 o 2 1 5 2.80 1.40 0.91 o 3 1 5 74.39 79.18 2.48 o 4 1 5 70.79 76.13 2.42 o 5 1 5 1.18 -0.49 0.85 o 6 1 5 318.06 315.55 3.80 o 7 1 5 0.00 5.77 1.64 o 8 1 5 10.63 10.13 1.63 o 9 1 5 17.84 17.20 1.81 o 10 1 5 1.70 -0.08 1.29 o 11 1 5 11.42 7.66 2.17 o 12 1 5 15.05 16.58 2.47 o 13 1 5 1.20 11.51 3.04 o 14 1 5 2.76 -0.18 4.38 o 1 2 5 51.31 49.84 2.20 o 2 2 5 1250.24 1340.21 28.11 o 3 2 5 152.86 151.94 2.99 o 4 2 5 93.83 106.96 2.59 o 5 2 5 0.02 -1.06 0.90 o 6 2 5 0.18 -1.56 1.04 o 7 2 5 8.94 8.22 1.42 o 8 2 5 218.33 222.65 3.72 o 9 2 5 112.84 96.63 2.67 o 10 2 5 223.35 221.13 5.52 o 11 2 5 14.33 12.72 2.65 o 12 2 5 9.89 3.87 2.91 o 13 2 5 12.29 10.18 2.89 o 14 2 5 1.87 -0.73 3.14 o 1 3 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