#------------------------------------------------------------------------------
#$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $
#$Revision: 31968 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/24/2232469.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2232469_Fobs
loop_
_publ_author_name
'Shahverdizadeh, Gholam Hossein'
'Ng, Seik Weng'
'Tiekink, Edward R. T.'
'Mirtamizdoust, Babak'
_publ_section_title
;
 <i>catena</i>-Poly[[lead(II)-\m-(2-oxidobenzaldehyde
 isonicotinoylhydrazonato)] methanol monosolvate]
;
_journal_coeditor_code           SU2329
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1583
_journal_volume                  67
_journal_year                    2011
_space_group_IT_number           148
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   28.6702
_cell_length_b                   28.6702
_cell_length_c                   9.0146
_exptl_crystal_F_000             4032.00
_reflns_d_resolution_high        0.7966
_[local]_cod_data_source_file    su2329Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  R-3'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1246.33
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 3 0 230733.48 155798.84 30802.63 o
-2 4 0 1553335.88 1480501.50 10761.75 o
-4 5 0 172220.92 176446.27 1412.27 o
-1 5 0 171285.70 174426.59 1537.75 o
-3 6 0 151867.64 150503.56 1055.14 o
0 6 0 509333.59 497331.22 2774.43 o
-5 7 0 283714.44 288710.41 2057.48 o
-2 7 0 26034.26 24995.77 447.01 o
-7 8 0 317612.09 315807.00 1872.48 o
-4 8 0 1045026.06 1029789.31 5549.48 o
-1 8 0 17467.37 16301.12 348.15 o
-6 9 0 34497.04 36457.53 528.41 o
-3 9 0 161547.69 160904.02 1632.49 o
0 9 0 15317.15 17134.72 539.03 o
-8 10 0 722196.94 721304.31 3622.22 o
-5 10 0 109468.71 113052.89 1007.47 o
-2 10 0 644314.06 632856.38 3625.79 o
-10 11 0 13498.31 15733.60 388.82 o
-7 11 0 251280.50 258022.13 2842.94 o
-4 11 0 325.92 571.69 114.99 o
-1 11 0 148845.03 142390.45 1376.25 o
-9 12 0 349174.13 353101.81 2121.93 o
-6 12 0 571829.38 576505.56 4062.55 o
-3 12 0 4058.73 3774.65 199.68 o
0 12 0 399557.03 394002.59 2490.05 o
-11 13 0 74599.42 79012.42 769.36 o
-8 13 0 1405.04 2250.45 181.30 o
-5 13 0 272396.41 276424.88 2274.49 o
-2 13 0 17219.69 18977.49 495.01 o
-13 14 0 133460.19 127805.09 1091.46 o
-10 14 0 466246.72 458692.41 2683.71 o
-7 14 0 57631.34 59346.36 1170.22 o
-4 14 0 321661.41 319107.31 2421.21 o
-1 14 0 85125.11 89694.48 1088.24 o
-12 15 0 45189.77 36678.41 4347.91 o
-9 15 0 225515.11 229344.89 2256.66 o
-6 15 0 19360.87 19796.49 443.09 o
-3 15 0 301043.44 303618.00 2461.42 o
0 15 0 71806.63 76675.96 1051.73 o
-14 16 0 77759.23 73240.03 954.79 o
-11 16 0 146438.69 147210.31 1549.17 o
-8 16 0 161477.09 161338.47 1510.46 o
-5 16 0 2955.02 4260.25 275.86 o
-2 16 0 189398.67 192749.66 1933.63 o
-16 17 0 53211.05 54284.98 891.94 o
-13 17 0 60387.84 60080.35 822.09 o
-10 17 0 51943.41 53160.59 1025.49 o
-7 17 0 244925.58 246650.55 1980.18 o
-4 17 0 198.86 793.91 153.72 o
-1 17 0 104673.45 104403.77 1189.23 o
-15 18 0 81361.03 81029.63 1026.01 o
-12 18 0 81439.23 83611.46 1029.71 o
-9 18 0 17736.88 17348.05 462.33 o
-6 18 0 52426.07 51179.58 952.53 o
-3 18 0 45994.98 40608.31 3971.12 o
0 18 0 5403.38 6026.97 381.77 o
-17 19 0 28039.08 27239.87 602.72 o
-14 19 0 117264.08 117216.96 1304.21 o
-11 19 0 98022.48 96555.77 1083.63 o
-8 19 0 72116.76 71970.02 980.75 o
-5 19 0 196404.38 198747.88 1524.37 o
-2 19 0 1873.74 2228.39 242.88 o
-19 20 0 154793.64 158038.94 2334.68 o
-16 20 0 2394.55 2218.70 300.59 o
-13 20 0 73240.28 74251.23 1060.88 o
-10 20 0 14941.17 15618.05 546.83 o
-7 20 0 507.16 1021.69 217.96 o
-4 20 0 5648.00 5943.30 353.56 o
-1 20 0 87397.08 89259.97 1536.45 o
-18 21 0 211659.20 210149.75 2234.03 o
-15 21 0 74027.84 72053.34 1057.36 o
-12 21 0 209671.61 212060.63 2052.36 o
-9 21 0 77022.59 75420.46 1163.49 o
-6 21 0 44676.30 44922.42 958.21 o
-3 21 0 149993.75 148547.63 1984.09 o
0 21 0 140.69 798.47 255.44 o
-20 22 0 122.91 157.65 204.95 o
-17 22 0 60681.02 60590.88 1260.89 o
-14 22 0 6660.03 7229.70 401.42 o
-11 22 0 21670.05 23625.16 804.83 o
-8 22 0 64.82 398.33 176.20 o
-5 22 0 24253.95 24458.66 708.96 o
-2 22 0 192.06 689.17 190.28 o
-22 23 0 395090.56 392756.97 3793.58 o
-19 23 0 20708.29 21868.92 750.79 o
-16 23 0 225842.75 229238.73 3150.92 o
-13 23 0 73225.09 74703.63 1128.78 o
-10 23 0 228213.95 228305.38 2160.71 o
-7 23 0 243209.45 247198.69 2693.09 o
-4 23 0 38721.54 39337.98 834.41 o
-1 23 0 143430.78 144365.25 2001.39 o
-21 24 0 165334.55 164748.25 2607.98 o
-18 24 0 2516.23 2669.15 494.47 o
-15 24 0 22478.48 25344.92 1016.15 o
-12 24 0 155.56 1344.37 238.86 o
-9 24 0 541.16 826.97 195.00 o
-6 24 0 363.31 984.76 286.38 o
-3 24 0 174960.28 168125.94 2596.30 o
0 24 0 38618.82 38738.53 1106.63 o
-23 25 0 37485.58 37780.06 1124.13 o
-20 25 0 477210.97 474461.63 4726.69 o
-17 25 0 24929.18 24654.70 811.85 o
-14 25 0 203084.63 203577.30 2172.18 o
-11 25 0 175919.70 174178.81 2386.70 o
-8 25 0 124494.56 121720.59 1821.80 o
-5 25 0 78534.84 78548.49 1354.96 o
-2 25 0 918.75 670.82 257.99 o
-25 26 0 55572.90 54932.02 1841.04 o
-22 26 0 34830.21 35705.26 970.51 o
-19 26 0 92527.60 91505.51 3008.88 o
-16 26 0 13342.45 13709.59 676.85 o
-13 26 0 1396.17 2704.59 440.47 o
-10 26 0 21509.22 21790.23 778.73 o
-7 26 0 52315.29 51966.59 1148.21 o
-4 26 0 15447.83 16792.96 618.35 o
-1 26 0 172273.41 164863.42 3289.48 o
-24 27 0 306034.16 308103.94 4730.85 o
-21 27 0 52296.30 52812.40 1260.20 o
-18 27 0 311915.75 311654.03 3913.72 o
-15 27 0 59730.92 58714.90 1294.27 o
-12 27 0 212623.73 211652.61 3389.30 o
-9 27 0 98079.63 97374.64 1825.42 o
-6 27 0 39445.64 39975.88 981.24 o
-3 27 0 54643.04 53833.82 1819.13 o
0 27 0 4025.83 4025.97 799.25 o
-26 28 0 29072.14 27393.10 1352.23 o
-23 28 0 87839.70 87528.75 2756.21 o
-20 28 0 30955.25 32948.11 1862.86 o
-17 28 0 29071.06 28924.74 927.44 o
-14 28 0 42608.51 42707.27 1108.26 o
-11 28 0 4024.33 4458.34 503.02 o
-8 28 0 44804.29 45302.11 1112.03 o
-5 28 0 75574.27 75530.13 1495.26 o
-2 28 0 43957.95 42320.20 1668.09 o
-28 29 0 215926.28 212584.06 4032.69 o
-25 29 0 11582.06 10842.17 1052.06 o
-22 29 0 336537.31 337118.38 5890.49 o
-19 29 0 61568.94 63400.63 1920.67 o
-16 29 0 212033.02 216296.63 3001.74 o
-13 29 0 40586.04 43284.25 1276.23 o
-10 29 0 85024.49 86410.09 1689.08 o
-7 29 0 47122.02 48528.78 1223.57 o
-4 29 0 7687.55 8140.66 689.68 o
-1 29 0 22809.46 23488.76 1316.23 o
-27 30 0 36991.77 35081.00 1851.74 o
-24 30 0 26194.67 28946.19 1661.50 o
-21 30 0 22468.06 23345.13 1470.69 o
-18 30 0 32642.05 31097.01 1104.30 o
-15 30 0 9642.27 10979.10 694.49 o
-12 30 0 43558.43 42559.43 1390.59 o
-9 30 0 21241.46 22675.49 1051.66 o
-6 30 0 83222.80 82138.45 2205.03 o
-3 30 0 77225.45 76306.53 1992.52 o
0 30 0 31546.06 32221.03 1573.59 o
-29 31 0 5843.83 5713.97 880.48 o
-26 31 0 234963.52 244468.88 7787.21 o
-23 31 0 18481.05 20398.83 2008.35 o
-20 31 0 261202.52 263249.81 3792.00 o
-17 31 0 46004.46 49263.71 1839.14 o
-14 31 0 227099.75 232001.88 3241.99 o
-11 31 0 24999.58 26448.90 1130.79 o
-8 31 0 74788.72 76782.69 2099.16 o
-5 31 0 8290.95 8893.61 740.29 o
-2 31 0 1547.47 1559.25 457.49 o
-28 32 0 28922.38 30276.25 1790.05 o
-25 32 0 62099.32 60464.63 2463.10 o
-22 32 0 14988.92 16744.44 1989.55 o
-19 32 0 14989.65 15071.08 871.91 o
-16 32 0 49511.61 51830.48 1503.73 o
-13 32 0 44.27 525.08 388.88 o
-10 32 0 47176.28 49540.18 1579.94 o
-7 32 0 24767.06 25182.51 1167.99 o
-4 32 0 74542.20 72442.48 2003.54 o
-27 33 0 7548.32 7708.84 974.28 o
-24 33 0 243556.77 250002.64 5620.78 o
-21 33 0 22371.60 23178.46 1093.54 o
-18 33 0 255056.63 256660.17 3885.65 o
-15 33 0 23075.07 26382.07 1089.00 o
-12 33 0 80965.33 82552.33 2226.36 o
-9 33 0 9527.82 10933.07 1129.32 o
-6 33 0 10952.64 11420.14 1262.36 o
-26 34 0 24372.48 25257.79 1672.33 o
-23 34 0 19904.89 20779.36 1497.27 o
-20 34 0 36323.13 37468.18 1403.67 o
-17 34 0 21981.24 24084.98 1050.59 o
-14 34 0 35395.74 36292.66 1286.73 o
-11 34 0 941.69 995.11 485.90 o
-8 34 0 44631.51 43399.86 1816.39 o
-22 35 0 238461.08 238998.70 6622.21 o
-19 35 0 16628.29 18832.35 1439.26 o
-16 35 0 214436.63 220488.70 3333.40 o
-13 35 0 219.27 468.32 405.39 o
-1 1 1 30122.64 31541.03 497.20 o
-3 2 1 99618.77 102298.88 903.87 o
0 2 1 3253.88 4441.93 241.16 o
-5 3 1 5895.72 7264.15 139.31 o
-2 3 1 62657.99 67607.34 803.47 o
1 3 1 294909.78 296270.63 1963.72 o
-7 4 1 52887.33 53180.83 525.53 o
-4 4 1 50358.09 52207.01 619.27 o
-1 4 1 18769.32 20318.12 308.29 o
2 4 1 11052.11 12310.33 269.58 o
-9 5 1 18728.57 20485.11 355.45 o
-6 5 1 171405.61 176512.44 1519.20 o
-3 5 1 181253.16 190280.02 1636.23 o
0 5 1 6963.37 7332.33 210.52 o
3 5 1 278832.00 276098.75 1977.13 o
-11 6 1 311247.00 308610.47 2047.74 o
-8 6 1 44365.13 45009.58 512.72 o
-5 6 1 1023813.81 1036463.81 5581.06 o
-2 6 1 24354.59 24781.92 316.52 o
1 6 1 414.62 984.77 205.61 o
4 6 1 14653.09 15167.25 290.13 o
-13 7 1 65809.74 70113.29 931.85 o
-10 7 1 255732.48 255871.61 1744.93 o
-7 7 1 975969.88 989911.94 5498.98 o
-4 7 1 38090.61 40244.20 432.66 o
-1 7 1 158649.59 155000.13 1192.51 o
2 7 1 98391.35 100373.60 935.57 o
5 7 1 232567.47 228156.48 1662.61 o
-15 8 1 738458.69 742089.81 4347.11 o
-12 8 1 10610.39 11746.50 339.53 o
-9 8 1 710785.00 717025.94 4012.20 o
-6 8 1 144519.20 156738.88 1175.64 o
-3 8 1 22633.55 22968.70 352.43 o
0 8 1 42849.33 40818.70 538.29 o
3 8 1 431.49 840.78 109.53 o
6 8 1 1217.66 1370.41 134.55 o
-17 9 1 15372.46 15787.17 447.07 o
-14 9 1 151014.67 148337.38 1440.08 o
-11 9 1 194398.31 197720.92 1509.55 o
-8 9 1 193747.97 202226.73 1619.03 o
-5 9 1 186402.53 183572.89 1449.05 o
-2 9 1 71582.53 72970.63 754.87 o
1 9 1 507198.88 500387.34 3095.34 o
4 9 1 409539.78 412411.41 2585.98 o
7 9 1 373069.50 368645.41 2353.67 o
-19 10 1 526846.06 522990.63 3494.14 o
-16 10 1 29356.45 30095.35 581.32 o
-13 10 1 638162.69 637642.19 5241.67 o
-10 10 1 29413.87 33203.72 531.02 o
-7 10 1 369368.38 371636.56 2348.90 o
-4 10 1 37578.58 38730.29 524.67 o
-1 10 1 1629.91 2294.95 143.47 o
2 10 1 10603.99 10536.04 292.24 o
5 10 1 594.42 1415.32 155.40 o
8 10 1 7859.09 9437.21 330.18 o
-21 11 1 24047.30 25066.88 599.13 o
-18 11 1 120395.46 121899.63 1684.37 o
-15 11 1 61561.38 65055.36 893.44 o
-12 11 1 153031.03 161125.56 1329.94 o
-9 11 1 589316.56 596216.63 4034.78 o
-6 11 1 100782.82 106670.15 898.11 o
-3 11 1 679232.31 682603.50 4091.67 o
0 11 1 244792.42 250751.66 1638.92 o
3 11 1 697374.50 695812.31 3796.56 o
6 11 1 411493.03 406355.78 3275.85 o
9 11 1 196845.73 194149.50 1619.13 o
-23 12 1 199941.13 199481.75 2448.52 o
-20 12 1 23932.79 22688.56 658.25 o
-17 12 1 528979.88 524083.31 3895.14 o
-14 12 1 22130.16 22674.02 497.88 o
-11 12 1 396148.41 393392.59 2551.03 o
-8 12 1 70896.91 77407.99 940.61 o
-5 12 1 149064.73 141252.73 1252.92 o
-2 12 1 75058.35 76032.88 844.69 o
1 12 1 55195.21 56244.95 921.79 o
4 12 1 1177.68 1450.72 275.57 o
7 12 1 4741.71 6078.25 380.91 o
10 12 1 3596.56 4157.74 361.52 o
-25 13 1 3578.81 3577.42 317.65 o
-22 13 1 118569.00 118622.82 1348.66 o
-19 13 1 47966.49 39895.99 3995.99 o
-16 13 1 72504.03 71144.98 1171.22 o
-13 13 1 63857.10 59974.35 850.65 o
-10 13 1 16724.42 17044.77 504.95 o
-7 13 1 812621.06 828083.88 4577.31 o
-4 13 1 134640.03 134533.86 1299.17 o
-1 13 1 814119.88 804869.00 4754.29 o
2 13 1 368623.22 372463.69 2653.92 o
5 13 1 465521.75 424939.34 23385.90 o
8 13 1 204961.69 201094.41 1959.12 o
11 13 1 136976.41 139295.41 1616.22 o
-27 14 1 231368.16 236446.92 3336.69 o
-24 14 1 62201.33 62634.99 1160.54 o
-21 14 1 369999.44 371935.66 3098.22 o
-18 14 1 72189.79 71801.84 1007.43 o
-15 14 1 405033.56 390281.66 3609.34 o
-12 14 1 183.11 201.94 134.02 o
-9 14 1 180412.14 171158.17 1341.35 o
-6 14 1 15491.88 16479.56 472.77 o
-3 14 1 99366.41 101726.79 1090.61 o
0 14 1 25533.12 23474.74 473.46 o
3 14 1 22912.69 23969.76 561.01 o
6 14 1 5629.64 6651.67 330.43 o
9 14 1 8543.99 8567.80 398.46 o
12 14 1 39134.63 39058.14 973.17 o
-29 15 1 6321.04 6013.17 497.24 o
-26 15 1 20371.43 21580.97 754.29 o
-23 15 1 2745.14 2651.96 243.06 o
-20 15 1 98036.37 98980.00 1808.57 o
-17 15 1 121720.21 121245.79 1284.95 o
-14 15 1 700.58 564.41 140.58 o
-11 15 1 602939.06 624090.06 4151.78 o
-8 15 1 34586.68 34715.82 594.52 o
-5 15 1 908005.69 889421.88 3139.41 o
-2 15 1 118373.57 114950.73 1901.70 o
1 15 1 713248.19 707103.56 2927.11 o
4 15 1 322895.81 320337.94 2480.86 o
7 15 1 199839.94 199849.14 2009.99 o
10 15 1 61707.33 60508.45 1078.63 o
13 15 1 31896.62 33088.16 904.72 o
-31 16 1 95725.16 97447.77 2026.59 o
-28 16 1 115388.41 113410.56 1633.35 o
-25 16 1 366705.25 363159.22 3308.18 o
-22 16 1 141787.67 143795.31 1635.34 o
-19 16 1 437577.31 431746.97 4319.10 o
-16 16 1 12217.36 11048.31 417.75 o
-13 16 1 423875.06 431916.88 3748.33 o
-10 16 1 847.90 939.43 123.63 o
-7 16 1 277193.00 271306.91 1965.35 o
-4 16 1 99651.95 101249.35 1444.23 o
-1 16 1 88682.53 92660.46 1217.80 o
2 16 1 8471.42 8349.40 350.70 o
5 16 1 16489.65 16932.68 500.18 o
8 16 1 419.46 934.02 204.59 o
11 16 1 7438.82 7453.51 445.96 o
14 16 1 74463.36 75367.13 1522.23 o
-33 17 1 10998.08 10587.11 728.44 o
-30 17 1 3046.10 3043.52 457.20 o
-27 17 1 1104.55 1003.27 233.40 o
-24 17 1 6254.36 6191.52 347.07 o
-21 17 1 29565.10 30500.05 689.01 o
-18 17 1 5903.29 6555.80 293.78 o
-15 17 1 126879.63 127020.65 1559.85 o
-12 17 1 1112.73 1472.28 349.17 o
-9 17 1 629974.81 628027.38 3853.17 o
-6 17 1 48831.86 47663.68 823.89 o
-3 17 1 782650.69 767985.88 5707.94 o
0 17 1 138567.36 136226.03 1915.56 o
3 17 1 417569.69 418564.38 2908.98 o
6 17 1 131067.79 133081.86 2193.21 o
9 17 1 107209.14 109169.42 1791.57 o
12 17 1 113538.62 114003.66 1848.39 o
15 17 1 7117.29 7250.10 604.99 o
-35 18 1 34863.92 34896.99 1419.81 o
-32 18 1 129840.73 128679.67 2534.27 o
-29 18 1 191078.58 194913.53 3047.29 o
-26 18 1 138366.06 137819.89 1779.64 o
-23 18 1 391169.25 393247.09 3071.24 o
-20 18 1 62592.36 59970.69 793.08 o
-17 18 1 305491.19 297045.41 2554.46 o
-14 18 1 4475.17 5405.90 321.07 o
-11 18 1 328647.78 326741.25 2382.75 o
-8 18 1 18631.51 20551.19 504.28 o
-5 18 1 162208.36 159088.16 1593.22 o
-2 18 1 53005.20 52208.23 802.19 o
1 18 1 7686.37 8882.08 418.92 o
4 18 1 2190.95 2088.60 262.83 o
7 18 1 57970.30 57434.20 1185.06 o
10 18 1 13730.56 13513.08 610.47 o
13 18 1 6235.74 5869.28 479.17 o
16 18 1 75015.96 75329.94 2045.63 o
-34 19 1 657.22 516.77 413.20 o
-31 19 1 2139.62 2210.23 472.16 o
-28 19 1 3087.69 3424.53 407.93 o
-25 19 1 7699.16 8451.34 401.75 o
-22 19 1 444.78 1186.49 222.57 o
-19 19 1 94746.02 93448.11 1649.37 o
-16 19 1 440.76 944.21 208.63 o
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