#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/24/2232484.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232484_Fobs loop_ _publ_author_name 'Yeo, Chien Ing' 'Tiekink, Edward R. T.' _publ_section_title ; 1,3-Bis(2-chlorophenyl)thiourea: a monoclinic polymorph ; _journal_coeditor_code VM2125 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2965 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.509 _cell_angle_gamma 90.000 _cell_length_a 11.9999 _cell_length_b 14.6811 _cell_length_c 8.0806 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file vm2125Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Tu in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9667.88 9302.55 94.13 o 3 0 0 9976.65 9604.37 99.51 o 4 0 0 4678.75 4568.27 53.14 o 5 0 0 465.69 538.69 15.15 o 6 0 0 1445.23 1465.28 28.93 o 7 0 0 2830.42 2605.61 46.91 o 8 0 0 2121.20 1965.99 41.11 o 9 0 0 377.14 447.23 34.77 o 10 0 0 73.82 41.61 17.93 o 11 0 0 968.84 922.62 76.19 o 12 0 0 223.59 224.52 69.50 o 13 0 0 668.78 645.20 51.88 o 14 0 0 76.12 73.86 26.84 o 1 1 0 3127.29 3113.38 28.40 o 2 1 0 424.92 422.25 8.94 o 3 1 0 33.63 24.54 3.37 o 4 1 0 401.15 387.13 8.47 o 5 1 0 296.44 262.45 7.92 o 6 1 0 348.72 411.46 10.32 o 7 1 0 601.57 548.46 13.09 o 8 1 0 1068.60 1079.47 21.74 o 9 1 0 188.92 195.01 17.51 o 10 1 0 1629.67 1559.65 60.67 o 11 1 0 677.28 697.89 32.40 o 12 1 0 81.34 89.92 16.17 o 13 1 0 374.76 390.39 30.99 o 14 1 0 703.63 692.73 41.49 o 0 2 0 6659.40 6186.91 130.48 o 1 2 0 1077.78 1052.54 10.38 o 2 2 0 438.81 430.94 6.74 o 3 2 0 6367.15 6093.28 61.75 o 4 2 0 2371.29 2269.15 30.23 o 5 2 0 1085.65 1062.35 20.32 o 6 2 0 794.84 765.90 22.22 o 7 2 0 331.17 320.00 13.55 o 8 2 0 1703.02 1570.40 27.74 o 9 2 0 34.17 31.88 7.97 o 10 2 0 2211.92 2247.80 50.02 o 11 2 0 232.08 228.86 21.01 o 12 2 0 485.53 472.86 29.94 o 13 2 0 49.55 32.85 15.18 o 14 2 0 0.02 -10.23 13.26 o 1 3 0 1976.58 2105.01 18.06 o 2 3 0 1262.26 1266.66 15.10 o 3 3 0 852.38 888.56 13.48 o 4 3 0 899.12 914.87 18.60 o 5 3 0 304.08 329.04 13.38 o 6 3 0 10398.51 10455.19 98.95 o 7 3 0 1075.23 1027.67 21.78 o 8 3 0 290.56 295.57 14.64 o 9 3 0 574.74 581.71 20.17 o 10 3 0 2.93 5.77 10.40 o 11 3 0 33.18 35.39 13.25 o 12 3 0 237.20 220.21 22.21 o 13 3 0 288.52 326.30 27.16 o 14 3 0 113.98 121.81 23.44 o 1 4 0 2347.56 2329.77 28.66 o 2 4 0 8803.02 8749.70 69.09 o 3 4 0 15.42 7.89 4.15 o 4 4 0 2011.88 1991.01 40.79 o 5 4 0 4204.16 4071.76 51.04 o 6 4 0 129.58 109.91 9.98 o 7 4 0 0.57 4.18 6.73 o 8 4 0 912.37 912.35 22.77 o 9 4 0 120.09 120.60 11.67 o 10 4 0 26.74 18.96 8.26 o 11 4 0 52.67 68.35 14.99 o 12 4 0 275.66 282.75 24.47 o 13 4 0 274.37 285.00 29.59 o 14 4 0 18.04 14.21 15.99 o 1 5 0 39.21 38.08 6.52 o 2 5 0 1968.41 1983.08 20.98 o 3 5 0 5347.40 5234.33 46.31 o 4 5 0 7559.51 7945.06 74.77 o 5 5 0 1477.31 1373.54 23.66 o 6 5 0 23.07 40.84 9.30 o 7 5 0 259.85 210.93 14.41 o 8 5 0 0.13 2.94 7.56 o 9 5 0 1243.46 1285.61 28.76 o 10 5 0 8.52 -5.11 7.93 o 11 5 0 14.74 13.14 11.84 o 12 5 0 1039.70 1124.71 40.44 o 13 5 0 36.57 51.99 16.95 o 14 5 0 181.98 212.94 25.52 o 1 6 0 2.47 -0.42 3.78 o 2 6 0 3406.07 3435.10 32.87 o 3 6 0 130.76 103.87 7.78 o 4 6 0 217.46 196.18 8.56 o 5 6 0 224.90 216.74 11.58 o 6 6 0 499.58 489.53 15.23 o 7 6 0 419.37 420.79 22.46 o 8 6 0 141.21 168.23 16.44 o 9 6 0 5.00 -9.65 8.33 o 10 6 0 287.20 281.01 19.37 o 11 6 0 29.73 33.03 17.16 o 12 6 0 5.33 7.97 16.16 o 13 6 0 31.31 43.83 25.24 o 1 7 0 399.06 388.12 11.79 o 2 7 0 170.62 197.96 8.00 o 3 7 0 109.71 173.29 7.14 o 4 7 0 3125.58 2886.64 43.12 o 5 7 0 11.58 10.69 5.10 o 6 7 0 126.66 148.60 9.53 o 7 7 0 254.40 241.50 21.60 o 8 7 0 1803.47 1698.75 41.58 o 9 7 0 453.37 459.83 26.00 o 10 7 0 527.25 536.03 35.24 o 11 7 0 701.86 741.66 44.61 o 12 7 0 35.49 40.82 18.40 o 13 7 0 141.10 146.35 29.48 o 0 8 0 1289.99 1336.98 33.53 o 1 8 0 2920.60 2989.61 38.84 o 2 8 0 506.47 600.02 13.36 o 3 8 0 4495.01 4270.18 41.22 o 4 8 0 27.80 17.24 6.01 o 5 8 0 19.99 21.30 6.09 o 6 8 0 2041.19 1982.97 38.89 o 7 8 0 26.26 34.05 12.17 o 8 8 0 368.17 384.34 28.45 o 9 8 0 445.81 424.97 26.06 o 10 8 0 886.04 939.20 33.75 o 11 8 0 465.39 479.58 27.67 o 12 8 0 7.92 -15.99 15.26 o 13 8 0 10.79 3.54 18.02 o 1 9 0 571.49 573.33 15.51 o 2 9 0 28.48 43.83 6.41 o 3 9 0 689.66 704.65 15.10 o 4 9 0 348.83 345.40 16.93 o 5 9 0 62.75 57.53 9.38 o 6 9 0 53.94 31.32 13.54 o 7 9 0 308.91 272.72 23.66 o 8 9 0 2734.96 2505.55 54.24 o 9 9 0 13.52 30.56 14.53 o 10 9 0 630.56 587.54 34.07 o 11 9 0 270.71 247.40 20.79 o 12 9 0 34.55 11.56 21.87 o 0 10 0 1364.87 1359.49 59.38 o 1 10 0 84.54 110.48 8.90 o 2 10 0 5732.63 5581.86 70.67 o 3 10 0 678.99 733.00 32.85 o 4 10 0 299.27 293.11 16.74 o 5 10 0 1094.84 1042.40 26.35 o 6 10 0 40.02 39.39 14.03 o 7 10 0 258.94 220.63 22.94 o 8 10 0 270.28 212.48 22.74 o 9 10 0 107.36 141.55 19.84 o 10 10 0 302.79 338.45 29.44 o 11 10 0 635.44 683.85 49.83 o 12 10 0 45.09 29.23 23.79 o 1 11 0 148.72 154.85 12.47 o 2 11 0 22.29 16.03 12.84 o 3 11 0 1565.71 1513.27 33.31 o 4 11 0 529.09 551.26 23.34 o 5 11 0 1230.48 1176.43 28.81 o 6 11 0 461.90 462.78 31.04 o 7 11 0 8.75 1.75 11.78 o 8 11 0 83.72 64.16 19.58 o 9 11 0 336.74 335.29 29.31 o 10 11 0 7.24 -3.90 13.17 o 11 11 0 1.14 7.02 16.41 o 12 11 0 636.32 618.13 66.76 o 0 12 0 834.78 777.72 41.40 o 1 12 0 1336.97 1280.96 38.50 o 2 12 0 1727.00 1813.43 59.89 o 3 12 0 35.35 19.76 10.00 o 4 12 0 355.46 393.80 20.84 o 5 12 0 1405.71 1371.09 46.08 o 6 12 0 169.86 138.99 20.00 o 7 12 0 415.36 350.56 29.00 o 8 12 0 678.93 665.09 39.95 o 9 12 0 202.13 190.32 23.48 o 10 12 0 4.17 17.59 14.71 o 11 12 0 4.39 12.34 16.39 o 1 13 0 0.41 15.90 10.45 o 2 13 0 23.55 7.40 9.48 o 3 13 0 258.10 285.89 19.12 o 4 13 0 357.99 354.92 20.78 o 5 13 0 200.89 207.34 26.69 o 6 13 0 796.98 784.38 40.84 o 7 13 0 145.69 140.68 21.40 o 8 13 0 182.04 200.85 29.23 o 9 13 0 10.45 -5.25 13.27 o 10 13 0 84.25 75.02 19.90 o 0 14 0 416.69 509.86 40.32 o 1 14 0 17.60 2.07 11.78 o 2 14 0 157.27 193.64 20.15 o 3 14 0 167.42 186.93 17.15 o 4 14 0 4.64 -8.31 9.20 o 5 14 0 42.15 20.19 15.20 o 6 14 0 42.04 57.49 17.54 o 7 14 0 233.61 232.69 26.68 o 8 14 0 8.57 20.46 17.62 o 9 14 0 5.12 8.27 15.84 o 1 15 0 2235.63 2281.06 53.67 o 2 15 0 369.93 363.01 23.00 o 3 15 0 168.96 177.20 17.51 o 4 15 0 122.99 103.27 19.92 o 5 15 0 290.02 287.88 47.49 o 6 15 0 693.05 722.52 44.27 o 7 15 0 1062.97 1131.18 76.78 o 8 15 0 5.51 17.17 16.66 o 9 15 0 20.48 7.26 16.91 o 0 16 0 3289.76 3326.06 97.21 o 1 16 0 236.29 246.95 20.53 o 2 16 0 29.55 46.27 12.69 o 3 16 0 294.55 319.74 22.68 o 4 16 0 72.14 55.63 25.67 o 5 16 0 5.18 16.37 20.09 o 6 16 0 36.36 9.90 16.87 o 7 16 0 275.89 326.12 33.21 o 8 16 0 151.68 101.54 22.79 o 1 17 0 19.93 -4.89 10.44 o 2 17 0 1.79 9.08 11.83 o 3 17 0 104.04 97.57 19.87 o 4 17 0 139.33 141.08 24.57 o 5 17 0 1.20 8.87 16.95 o 6 17 0 66.46 46.05 19.72 o 0 18 0 0.71 1.74 18.00 o 1 18 0 403.94 424.76 36.31 o 2 18 0 6.13 0.50 12.95 o 3 18 0 140.44 118.16 23.98 o 4 18 0 2.92 17.17 17.86 o 1 19 0 106.75 81.52 16.27 o -15 1 1 17.00 17.81 15.98 o -14 1 1 37.64 32.86 14.69 o -13 1 1 137.02 176.37 20.88 o -12 1 1 769.33 790.65 35.27 o -11 1 1 0.34 1.38 10.31 o -10 1 1 318.10 313.59 21.47 o -9 1 1 0.33 -9.35 7.41 o -8 1 1 88.80 85.08 8.17 o -7 1 1 0.44 -7.64 5.09 o -6 1 1 346.98 346.03 24.23 o -5 1 1 7351.69 7157.58 73.93 o -4 1 1 5326.17 5166.79 54.18 o -3 1 1 19.85 8.75 3.94 o -2 1 1 1053.20 1045.36 12.77 o -1 1 1 1551.77 1536.29 30.11 o 0 1 1 624.86 629.51 7.97 o 1 1 1 4057.99 3933.99 43.50 o 2 1 1 124.48 112.61 6.74 o 3 1 1 8160.39 7917.57 65.57 o 4 1 1 1181.09 1093.94 17.91 o 5 1 1 1172.46 1244.58 17.57 o 6 1 1 12.01 24.07 4.46 o 7 1 1 177.13 188.80 8.63 o 8 1 1 966.54 898.08 26.34 o 9 1 1 74.57 63.25 13.14 o 10 1 1 75.93 83.92 15.19 o 11 1 1 187.49 238.27 22.24 o 12 1 1 78.51 69.96 16.35 o 13 1 1 0.85 -3.73 14.38 o 14 1 1 109.26 119.08 21.08 o -15 2 1 0.32 6.94 14.86 o -14 2 1 247.52 249.71 25.01 o -13 2 1 7.08 1.68 11.91 o -12 2 1 237.91 218.96 21.61 o -11 2 1 4206.40 4138.16 72.52 o -10 2 1 60.49 55.32 10.61 o -9 2 1 201.07 206.62 16.18 o -8 2 1 255.33 263.80 14.99 o -7 2 1 122.77 92.38 8.12 o -6 2 1 1143.81 994.82 26.91 o -5 2 1 147.26 152.86 8.15 o -4 2 1 2702.29 2631.25 32.41 o -3 2 1 3000.58 3066.05 31.48 o -2 2 1 123.64 150.46 6.54 o -1 2 1 2803.57 2780.31 44.87 o 0 2 1 1686.21 1739.21 17.64 o 1 2 1 9987.43 9662.94 241.72 o 2 2 1 11892.92 12002.32 123.10 o 3 2 1 1445.58 1443.68 27.48 o 4 2 1 918.46 890.41 18.30 o 5 2 1 184.18 153.05 10.08 o 6 2 1 15.75 5.90 5.64 o 7 2 1 1698.35 1762.24 29.20 o 8 2 1 24.47 28.08 7.96 o 9 2 1 705.89 752.97 41.80 o 10 2 1 689.04 735.94 32.56 o 11 2 1 656.06 650.78 40.64 o 12 2 1 33.80 17.75 13.42 o 13 2 1 97.48 111.21 19.78 o 14 2 1 52.80 27.58 17.52 o -14 3 1 106.81 124.85 21.16 o -13 3 1 2.14 34.44 14.37 o -12 3 1 8.72 0.39 11.30 o -11 3 1 46.93 60.66 15.63 o -10 3 1 435.57 457.62 22.01 o -9 3 1 247.00 263.39 14.61 o -8 3 1 569.42 559.21 18.03 o -7 3 1 2372.10 2463.99 34.65 o -6 3 1 3.90 8.18 5.09 o -5 3 1 365.12 407.45 14.62 o -4 3 1 277.79 291.34 9.71 o -3 3 1 852.65 846.39 14.21 o -2 3 1 267.01 270.89 8.43 o -1 3 1 8179.15 8193.53 77.80 o 0 3 1 1259.72 1348.12 14.42 o 1 3 1 2657.80 2572.80 50.66 o 2 3 1 834.52 799.53 21.31 o 3 3 1 763.93 802.29 17.15 o 4 3 1 223.44 252.18 11.98 o 5 3 1 1551.91 1544.51 27.15 o 6 3 1 1640.34 1612.04 27.22 o 7 3 1 449.75 492.29 19.93 o 8 3 1 15.57 4.52 7.25 o 9 3 1 392.34 422.97 25.93 o 10 3 1 13.78 12.35 11.07 o 11 3 1 324.60 275.94 23.54 o 12 3 1 3.69 -14.61 12.20 o 13 3 1 208.49 190.02 22.83 o -14 4 1 89.46 121.02 20.07 o -13 4 1 84.66 84.08 16.75 o -12 4 1 17.09 34.82 13.59 o -11 4 1 2.53 -8.25 10.23 o -10 4 1 215.13 242.54 15.11 o -9 4 1 1269.41 1186.64 26.22 o -8 4 1 1949.31 1972.33 32.75 o -7 4 1 91.62 86.33 7.32 o -6 4 1 675.99 658.90 14.19 o -5 4 1 309.14 318.34 10.61 o -4 4 1 267.72 256.20 8.96 o -3 4 1 243.93 229.67 9.35 o -2 4 1 48.85 48.97 6.24 o -1 4 1 2377.79 2527.29 33.98 o 0 4 1 6114.99 6151.10 60.23 o 1 4 1 2638.18 2539.63 35.67 o 2 4 1 1714.42 1691.06 23.86 o 3 4 1 382.93 439.99 12.43 o 4 4 1 219.53 218.16 8.67 o 5 4 1 7.04 11.53 6.29 o 6 4 1 57.92 63.90 9.16 o 7 4 1 277.29 310.05 15.49 o 8 4 1 57.44 73.98 10.36 o 9 4 1 1757.48 1818.83 34.17 o 10 4 1 238.58 244.92 21.74 o 11 4 1 2.02 10.32 12.27 o 12 4 1 13.05 1.10 13.09 o 13 4 1 26.94 26.43 15.44 o -14 5 1 21.04 19.07 14.75 o -13 5 1 202.96 218.61 22.85 o -12 5 1 54.85 40.31 18.44 o -11 5 1 190.52 205.43 15.28 o -10 5 1 443.10 497.75 21.45 o -9 5 1 96.01 90.05 11.21 o -8 5 1 237.56 236.11 14.34 o -7 5 1 138.40 126.61 10.52 o -6 5 1 74.87 90.82 7.19 o -5 5 1 3640.02 3699.62 38.60 o -4 5 1 267.54 272.30 10.12 o -3 5 1 1764.74 1834.04 22.00 o -2 5 1 4156.70 4154.04 41.88 o -1 5 1 0.42 5.71 5.42 o 0 5 1 2025.33 2107.43 28.61 o 1 5 1 297.13 300.90 11.51 o 2 5 1 213.52 198.55 14.10 o 3 5 1 93.99 131.87 8.03 o 4 5 1 36.29 36.94 5.96 o 5 5 1 7.05 -5.79 7.27 o 6 5 1 0.08 11.53 8.72 o 7 5 1 116.68 114.07 12.12 o 8 5 1 1340.53 1345.18 29.18 o 9 5 1 32.97 45.94 10.07 o 10 5 1 126.17 110.15 16.38 o 11 5 1 310.48 317.87 25.73 o 12 5 1 4.60 -6.77 12.43 o 13 5 1 65.40 79.59 18.70 o -14 6 1 83.31 95.99 28.35 o -13 6 1 16.38 57.83 20.07 o -12 6 1 9.87 -3.12 15.90 o -11 6 1 0.20 10.31 12.60 o -10 6 1 71.35 57.51 11.50 o -9 6 1 125.39 127.89 14.83 o -8 6 1 402.32 377.62 20.42 o -7 6 1 62.42 70.46 8.98 o -6 6 1 121.84 153.39 8.97 o -5 6 1 153.20 218.04 10.13 o -4 6 1 5.66 6.42 4.34 o -3 6 1 166.30 167.53 7.81 o -2 6 1 2305.82 2327.04 28.31 o -1 6 1 2216.29 2059.99 29.33 o 0 6 1 1867.18 1931.93 28.60 o 1 6 1 836.52 985.73 20.01 o 2 6 1 290.64 298.16 12.18 o 3 6 1 1583.43 1569.37 23.99 o 4 6 1 1728.63 1772.68 25.52 o 5 6 1 1435.26 1415.99 26.57 o 6 6 1 320.00 323.19 20.12 o 7 6 1 1382.86 1302.56 34.53 o 8 6 1 214.93 255.83 19.72 o 9 6 1 388.87 417.70 29.79 o 10 6 1 80.52 55.68 13.95 o 11 6 1 33.53 5.66 16.37 o 12 6 1 1318.41 1363.05 54.79 o 13 6 1 26.88 20.99 19.31 o -14 7 1 0.03 -37.77 30.41 o -13 7 1 29.43 54.87 20.93 o -12 7 1 53.87 43.74 18.89 o -11 7 1 225.49 223.06 21.80 o -10 7 1 71.33 55.06 10.71 o -9 7 1 13.22 11.47 9.35 o -8 7 1 832.43 818.52 25.02 o -7 7 1 1276.04 1244.18 48.11 o -6 7 1 654.81 652.88 18.52 o -5 7 1 1.97 4.23 5.40 o -4 7 1 368.01 381.95 11.42 o -3 7 1 3224.74 3557.88 37.05 o -2 7 1 4166.65 4243.25 45.06 o -1 7 1 159.85 201.65 10.72 o 0 7 1 7.59 -3.70 4.97 o 1 7 1 1602.18 1779.95 42.13 o 2 7 1 1.06 3.10 5.63 o 3 7 1 2196.28 2393.57 35.19 o 4 7 1 180.40 166.82 9.97 o 5 7 1 1030.72 1040.46 23.69 o 6 7 1 519.33 513.75 25.43 o 7 7 1 673.98 627.85 27.38 o 8 7 1 10.26 -7.26 15.45 o 9 7 1 40.40 39.42 12.76 o 10 7 1 0.86 6.37 10.13 o 11 7 1 14.81 24.98 19.58 o 12 7 1 4.38 10.87 17.79 o 13 7 1 78.88 91.53 24.24 o -13 8 1 11.54 -8.68 17.63 o -12 8 1 14.10 39.48 18.92 o -11 8 1 19.29 34.76 12.00 o -10 8 1 283.54 325.19 32.22 o -9 8 1 529.22 606.03 30.59 o -8 8 1 1206.38 1175.51 29.94 o -7 8 1 3.62 5.51 9.41 o -6 8 1 36.54 36.15 7.25 o -5 8 1 30.20 40.68 6.34 o -4 8 1 0.85 -0.20 4.76 o -3 8 1 459.21 511.08 17.75 o -2 8 1 496.96 476.40 15.15 o -1 8 1 549.06 605.23 16.92 o 0 8 1 865.11 844.10 19.96 o 1 8 1 0.17 2.69 6.21 o 2 8 1 38.41 38.87 7.71 o 3 8 1 4.75 -8.69 5.80 o 4 8 1 1.36 1.18 6.19 o 5 8 1 182.67 149.49 10.23 o 6 8 1 64.65 56.13 13.65 o 7 8 1 84.35 99.05 15.26 o 8 8 1 263.95 279.39 21.86 o 9 8 1 449.36 474.59 27.77 o 10 8 1 7.20 13.24 11.48 o 11 8 1 77.66 80.16 21.04 o 12 8 1 10.40 13.91 17.62 o -13 9 1 0.67 10.99 18.63 o -12 9 1 57.19 60.43 16.95 o -11 9 1 44.81 28.55 12.50 o -10 9 1 289.99 280.04 25.80 o -9 9 1 27.65 50.68 14.64 o -8 9 1 178.07 194.54 21.23 o -7 9 1 1428.83 1351.03 43.32 o -6 9 1 161.47 170.26 15.68 o -5 9 1 110.83 113.57 8.52 o -4 9 1 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1222.53 37.64 o -4 6 9 517.71 546.70 38.47 o -3 6 9 29.14 1.95 20.31 o -2 6 9 225.28 152.46 29.43 o -1 6 9 53.15 30.48 27.37 o 0 6 9 374.25 338.77 39.83 o 1 6 9 109.58 101.67 28.90 o -9 7 9 0.46 -19.62 13.08 o -8 7 9 140.86 109.07 17.92 o -7 7 9 220.22 194.26 20.02 o -6 7 9 1.12 -5.69 17.65 o -5 7 9 85.16 70.01 21.73 o -4 7 9 35.54 55.27 28.59 o -3 7 9 309.39 278.66 68.59 o -2 7 9 68.85 80.65 26.23 o -1 7 9 2.17 21.22 21.01 o 0 7 9 1.36 14.49 20.46 o -8 8 9 68.21 57.50 21.73 o -7 8 9 0.85 2.85 16.96 o -6 8 9 19.52 -0.56 28.09 o -5 8 9 22.17 2.62 22.81 o -4 8 9 1.62 -4.16 17.99 o -3 8 9 19.03 15.22 19.16 o -2 8 9 63.28 51.60 23.07 o -1 8 9 16.83 -4.15 19.20 o -7 9 9 12.49 -7.56 16.02 o -6 9 9 493.97 464.38 37.83 o -5 9 9 7.45 17.83 21.58 o -4 9 9 101.34 50.22 24.47 o -3 9 9 350.81 303.55 38.71 o -2 9 9 31.22 51.96 24.34 o -9 0 10 327.23 288.45 38.38 o -8 0 10 52.86 99.19 28.31 o -7 0 10 139.27 141.15 29.81 o -6 0 10 202.61 231.34 42.43 o -5 0 10 579.40 616.58 50.41 o -4 0 10 782.94 683.34 61.14 o -3 0 10 8.99 21.90 28.29 o -2 0 10 344.87 340.66 52.32 o -1 0 10 215.92 217.78 68.28 o -9 1 10 102.76 78.10 18.67 o -8 1 10 88.91 126.30 20.57 o -7 1 10 33.37 56.66 17.68 o -6 1 10 158.26 166.37 21.69 o -5 1 10 392.34 365.54 52.13 o -4 1 10 67.66 44.60 24.49 o -3 1 10 82.84 67.93 22.68 o -2 1 10 1.99 -34.02 26.44 o -1 1 10 0.19 -15.06 15.88 o -9 2 10 5.60 6.00 15.50 o -8 2 10 4.76 7.43 14.52 o -7 2 10 47.25 13.52 13.86 o -6 2 10 51.92 64.23 22.83 o -5 2 10 4.89 -8.79 14.02 o -4 2 10 288.64 336.49 31.31 o -3 2 10 11.01 23.47 18.40 o -2 2 10 2.66 -5.14 22.30 o -1 2 10 48.64 60.66 20.60 o -8 3 10 55.96 27.39 16.57 o -7 3 10 606.28 708.76 62.56 o -6 3 10 76.15 82.30 18.73 o -5 3 10 5.66 8.68 14.28 o -4 3 10 183.87 178.72 23.37 o -3 3 10 5.34 -14.75 17.46 o -2 3 10 0.95 -14.17 15.54 o -8 4 10 128.80 126.63 19.41 o -7 4 10 242.38 255.76 23.37 o -6 4 10 11.83 28.38 23.97 o -5 4 10 26.69 -2.85 14.14 o -4 4 10 3.24 -18.28 17.30 o -3 4 10 223.44 264.28 29.74 o -2 4 10 3.03 7.99 22.94 o -7 5 10 229.91 168.37 20.40 o -6 5 10 184.07 142.74 20.02 o -5 5 10 72.04 32.41 17.69 o -4 5 10 2.34 27.21 25.76 o -3 5 10 205.64 154.94 32.87 o