#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/24/2232490.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232490_Fobs loop_ _publ_author_name 'Zhao, Dan' _publ_section_title ; Heptasodium tetraaluminium tetrakis(diphosphate) orthophosphate, Na~7~Al~4~(P~2~O~7~)~4~(PO~4~) ; _journal_coeditor_code WM2530 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i64 _journal_volume 67 _journal_year 2011 _space_group_IT_number 114 _symmetry_space_group_name_Hall 'P -4 2n' _symmetry_space_group_name_H-M 'P -4 21 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.0543 _cell_length_b 14.0543 _cell_length_c 6.1718 _exptl_crystal_F_000 1040.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file wm2530Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P-42(1)c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 213.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'y, -x, -z' '-x, -y, z' '-y, x, -z' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 2 0 644.25 655.03 5.77 o 2 2 0 4300.48 4348.92 73.15 o 1 3 0 169.10 194.61 4.39 o 2 3 0 18744.40 18636.46 183.31 o 0 4 0 8448.93 8114.93 75.15 o 1 4 0 1295.13 1395.79 24.90 o 3 4 0 12478.61 12343.96 140.31 o 4 4 0 503.39 606.63 11.83 o 1 5 0 1155.37 1092.67 11.11 o 2 5 0 1695.82 1780.73 26.57 o 3 5 0 115.90 138.06 4.97 o 4 5 0 4962.29 5457.04 47.30 o 0 6 0 794.66 891.41 17.20 o 1 6 0 7268.29 6750.36 48.03 o 2 6 0 902.23 715.01 10.73 o 3 6 0 86.00 124.20 5.22 o 4 6 0 3092.02 3001.37 27.86 o 5 6 0 227.02 313.10 7.39 o 6 6 0 9109.10 9102.91 178.50 o 1 7 0 2690.73 2639.24 76.90 o 2 7 0 10277.53 11194.23 100.42 o 3 7 0 1426.81 1470.95 15.81 o 4 7 0 25.07 39.38 10.64 o 5 7 0 6348.55 6824.43 69.07 o 6 7 0 181.06 159.38 6.80 o 7 7 0 364.18 344.33 10.67 o 0 8 0 2040.79 1928.45 31.25 o 1 8 0 15.11 15.12 4.79 o 2 8 0 603.87 637.04 10.91 o 3 8 0 1610.12 1580.14 32.77 o 4 8 0 3297.10 3270.55 39.97 o 5 8 0 6351.39 6309.81 94.24 o 6 8 0 2436.57 2319.56 20.22 o 7 8 0 572.87 577.58 10.56 o 8 8 0 6516.85 6233.28 215.01 o 1 9 0 740.85 781.85 15.46 o 2 9 0 2234.63 2263.47 34.18 o 3 9 0 3062.10 3106.52 38.01 o 4 9 0 1875.38 1805.96 18.95 o 5 9 0 4600.37 4555.95 55.54 o 6 9 0 376.84 393.49 9.73 o 7 9 0 15.18 10.39 4.05 o 8 9 0 2103.52 2122.62 29.70 o 9 9 0 397.70 402.84 15.31 o 0 10 0 1166.20 1190.54 24.63 o 1 10 0 9703.49 9693.46 68.36 o 2 10 0 1457.18 1433.55 19.51 o 3 10 0 122.05 141.75 8.28 o 4 10 0 8482.96 8500.47 70.27 o 5 10 0 1.22 2.48 3.67 o 6 10 0 198.37 197.61 7.46 o 7 10 0 1366.08 1321.49 20.80 o 8 10 0 184.65 196.40 9.99 o 9 10 0 1920.96 1869.54 28.95 o 10 10 0 2.62 7.65 6.70 o 1 11 0 23.91 22.82 8.49 o 2 11 0 1381.89 1358.94 20.72 o 3 11 0 508.64 502.91 14.45 o 4 11 0 134.71 159.16 13.29 o 5 11 0 178.07 149.44 8.58 o 6 11 0 76.58 101.19 10.57 o 7 11 0 67.05 62.31 11.76 o 8 11 0 3562.88 3507.43 43.12 o 9 11 0 1062.99 1004.38 16.31 o 10 11 0 468.37 464.59 11.52 o 11 11 0 1216.06 1289.43 24.75 o 0 12 0 2.83 7.51 8.37 o 1 12 0 33.70 25.16 9.17 o 2 12 0 8321.59 8375.15 113.74 o 3 12 0 447.85 441.62 13.44 o 4 12 0 1938.02 1926.83 42.25 o 5 12 0 30.04 25.40 7.42 o 6 12 0 2.31 8.41 3.05 o 7 12 0 67.93 72.63 10.04 o 8 12 0 11861.96 12137.25 70.92 o 9 12 0 3.27 6.35 3.36 o 10 12 0 149.84 148.42 8.71 o 11 12 0 23.41 23.83 9.50 o 12 12 0 2.14 11.23 7.65 o 1 13 0 876.57 824.22 19.54 o 2 13 0 2660.81 2663.81 48.83 o 3 13 0 94.23 81.07 9.20 o 4 13 0 1.02 6.11 5.42 o 5 13 0 1329.99 1325.47 23.15 o 6 13 0 714.31 650.48 15.01 o 7 13 0 6.00 14.53 7.97 o 8 13 0 1039.13 1041.06 19.47 o 9 13 0 119.83 108.21 9.31 o 10 13 0 3226.65 3303.52 37.81 o 11 13 0 704.50 685.37 16.87 o 12 13 0 23.52 21.85 12.52 o 0 14 0 1790.95 1667.76 39.39 o 1 14 0 2726.00 2681.00 48.04 o 2 14 0 733.93 732.12 17.78 o 3 14 0 438.90 413.95 13.61 o 4 14 0 4883.29 5062.47 55.36 o 5 14 0 376.31 375.43 16.46 o 6 14 0 4.22 6.13 3.49 o 7 14 0 345.95 366.68 12.45 o 8 14 0 183.99 191.97 11.37 o 9 14 0 23.62 14.72 5.92 o 10 14 0 463.97 472.37 15.99 o 11 14 0 1597.16 1674.39 45.17 o 1 15 0 73.00 62.05 12.14 o 2 15 0 365.66 358.67 13.35 o 3 15 0 3.48 6.25 4.06 o 4 15 0 220.55 232.75 13.56 o 5 15 0 1293.32 1272.34 22.59 o 6 15 0 2279.84 2276.75 32.22 o 7 15 0 1320.22 1371.07 25.37 o 8 15 0 12.72 8.07 5.95 o 9 15 0 275.45 266.52 18.55 o 10 15 0 1987.94 1927.38 32.28 o 0 16 0 9533.33 9876.54 112.75 o 1 16 0 1308.39 1314.97 31.48 o 2 16 0 627.78 647.21 19.56 o 3 16 0 310.23 290.79 14.76 o 4 16 0 218.98 189.27 23.41 o 5 16 0 1043.81 1050.61 25.38 o 6 16 0 70.01 56.76 12.59 o 7 16 0 1042.36 1047.66 27.83 o 8 16 0 3529.10 3674.79 49.54 o 1 17 0 3268.05 3324.95 60.37 o 2 17 0 169.19 215.29 17.27 o 3 17 0 1380.21 1383.09 32.57 o 4 17 0 116.79 127.58 13.44 o 5 17 0 161.69 145.69 14.48 o 6 17 0 2.24 4.68 7.85 o 0 18 0 647.60 661.96 41.09 o 1 18 0 200.72 193.94 40.85 o 2 18 0 42.42 56.75 32.70 o 0 1 1 4333.12 4532.90 32.76 o -1 2 1 120.37 149.68 2.98 o 0 2 1 5741.62 5630.48 53.64 o 1 2 1 119.25 139.72 5.42 o -2 3 1 2874.05 2920.67 23.13 o -1 3 1 5964.02 6062.69 40.70 o 0 3 1 5626.31 5655.93 40.64 o 1 3 1 5911.75 6042.10 66.25 o 2 3 1 2876.81 2874.35 21.38 o -3 4 1 5516.32 5404.53 77.78 o -2 4 1 2506.97 2517.82 16.89 o -1 4 1 1290.86 1291.40 9.41 o 0 4 1 2285.80 2365.76 15.86 o 1 4 1 1306.48 1281.21 18.66 o 2 4 1 2472.21 2550.93 34.65 o 3 4 1 5549.18 5433.74 33.57 o -4 5 1 1876.74 1936.12 20.65 o -3 5 1 1174.95 1229.26 12.66 o -2 5 1 6453.82 6541.57 47.95 o -1 5 1 764.83 725.39 9.03 o 0 5 1 1477.03 1553.39 20.94 o 1 5 1 753.89 729.03 12.14 o 2 5 1 6291.59 6562.06 51.31 o 3 5 1 1152.86 1217.48 13.09 o 4 5 1 1854.79 1899.63 27.02 o -5 6 1 3800.68 3952.20 34.59 o -4 6 1 4823.66 5074.94 36.29 o -3 6 1 2655.24 2955.30 30.45 o -2 6 1 2664.10 2807.35 24.07 o -1 6 1 1528.09 1410.76 13.04 o 0 6 1 120.40 89.20 4.78 o 1 6 1 1545.10 1399.98 24.65 o 2 6 1 2644.17 2761.84 34.15 o 3 6 1 2578.71 2921.83 31.93 o 4 6 1 4736.87 5017.65 66.11 o 5 6 1 3813.98 3912.90 30.22 o -6 7 1 4935.03 4835.92 74.18 o -5 7 1 8006.08 8196.96 98.95 o -4 7 1 3150.15 3167.29 26.69 o -3 7 1 1658.18 1720.20 18.79 o -2 7 1 888.35 897.18 11.25 o -1 7 1 665.44 658.63 9.26 o 0 7 1 3893.62 3846.98 34.71 o 1 7 1 672.35 669.37 20.54 o 2 7 1 944.13 960.98 15.62 o 3 7 1 1662.25 1721.12 16.22 o 4 7 1 3125.11 3039.62 26.05 o 5 7 1 7993.79 7966.14 133.15 o 6 7 1 4927.65 4814.78 64.35 o -7 8 1 54.51 53.61 8.70 o -6 8 1 7409.93 7440.54 53.79 o -5 8 1 2425.64 2318.89 32.07 o -4 8 1 11738.17 11756.25 88.99 o -3 8 1 87.47 90.18 13.70 o -2 8 1 51.15 60.92 7.92 o -1 8 1 317.54 302.54 7.95 o 0 8 1 36.62 29.42 6.59 o 1 8 1 336.12 304.15 10.16 o 2 8 1 49.71 49.97 8.08 o 3 8 1 90.49 86.56 4.61 o 4 8 1 11735.52 11919.08 148.20 o 5 8 1 2461.27 2348.75 20.17 o 6 8 1 7375.51 7535.05 46.36 o 7 8 1 51.97 50.77 5.96 o -8 9 1 174.51 149.71 7.21 o -7 9 1 868.09 891.80 15.08 o -6 9 1 159.53 151.45 8.14 o -5 9 1 9331.08 9044.46 104.52 o -4 9 1 680.39 659.44 14.43 o -3 9 1 569.19 576.31 10.38 o -2 9 1 2624.53 2535.91 30.26 o -1 9 1 826.86 782.19 15.65 o 0 9 1 3279.94 3373.45 46.03 o 1 9 1 816.30 773.87 16.39 o 2 9 1 2559.28 2469.89 40.46 o 3 9 1 568.69 560.79 17.27 o 4 9 1 681.42 664.08 9.97 o 5 9 1 9295.97 9117.49 120.50 o 6 9 1 163.48 152.49 9.24 o 7 9 1 851.89 862.12 14.04 o 8 9 1 171.80 156.87 8.47 o -9 10 1 1077.51 1135.21 20.16 o -8 10 1 3228.42 3146.18 39.19 o -7 10 1 307.35 299.88 10.97 o -6 10 1 489.63 483.22 12.54 o -5 10 1 162.16 152.50 8.15 o -4 10 1 5241.94 5183.65 44.29 o -3 10 1 737.45 721.82 12.12 o -2 10 1 3711.86 3693.42 33.46 o -1 10 1 1548.29 1498.44 21.12 o 0 10 1 1682.43 1638.52 21.88 o 1 10 1 1553.05 1494.44 20.00 o 2 10 1 3709.80 3693.69 66.08 o 3 10 1 735.24 706.93 16.36 o 4 10 1 5254.43 5203.23 80.42 o 5 10 1 149.45 142.28 8.21 o 6 10 1 488.13 481.96 10.19 o 7 10 1 323.14 329.09 8.89 o 8 10 1 3249.58 3165.82 37.86 o 9 10 1 1060.37 1092.83 17.22 o -10 11 1 255.64 243.79 12.31 o -9 11 1 216.02 207.34 11.67 o -8 11 1 6718.17 6795.70 72.81 o -7 11 1 1209.90 1127.44 19.09 o -6 11 1 208.79 201.71 10.83 o -5 11 1 565.52 519.68 12.75 o -4 11 1 86.88 96.04 12.20 o -3 11 1 4872.60 4778.04 47.00 o -2 11 1 1567.70 1543.33 26.28 o -1 11 1 4370.06 4219.71 56.54 o 0 11 1 122.25 121.91 8.90 o 1 11 1 4416.85 4271.89 43.86 o 2 11 1 1584.61 1553.77 26.71 o 3 11 1 4833.17 4856.49 67.06 o 4 11 1 84.10 91.67 16.50 o 5 11 1 567.00 505.87 11.86 o 6 11 1 213.85 197.54 8.70 o 7 11 1 1245.98 1200.80 18.05 o 8 11 1 6671.88 6918.93 77.58 o 9 11 1 214.82 211.30 8.49 o 10 11 1 264.75 235.69 9.18 o -11 12 1 180.40 180.80 9.40 o -10 12 1 340.43 334.63 11.57 o -9 12 1 2721.06 2613.51 30.42 o -8 12 1 1569.70 1531.26 26.53 o -7 12 1 203.00 188.76 10.15 o -6 12 1 341.74 332.56 14.36 o -5 12 1 805.03 794.66 14.76 o -4 12 1 491.67 482.82 12.17 o -3 12 1 1039.46 975.95 21.20 o -2 12 1 7851.09 7879.49 159.99 o -1 12 1 2196.80 2126.13 37.88 o 0 12 1 1899.35 1863.04 33.78 o 1 12 1 2193.04 2114.75 37.58 o 2 12 1 7823.78 7680.01 110.02 o 3 12 1 1048.46 1005.68 21.66 o 4 12 1 488.51 491.62 16.35 o 5 12 1 797.03 789.04 25.06 o 6 12 1 333.81 331.25 10.90 o 7 12 1 213.99 215.19 10.08 o 8 12 1 1548.52 1504.25 23.85 o 9 12 1 2738.96 2675.37 30.93 o 10 12 1 345.99 349.65 13.94 o 11 12 1 193.30 184.46 26.89 o -12 13 1 701.90 709.16 16.22 o -11 13 1 1985.57 2105.64 29.01 o -10 13 1 361.41 373.02 15.75 o -9 13 1 1155.71 1214.12 19.48 o -8 13 1 640.74 660.26 14.86 o -7 13 1 1545.17 1524.61 24.99 o -6 13 1 655.37 655.39 13.68 o -5 13 1 2207.41 2124.26 26.28 o -4 13 1 242.89 260.89 14.24 o -3 13 1 969.37 965.41 37.84 o -2 13 1 3729.65 3721.14 55.15 o -1 13 1 894.78 924.59 20.64 o 0 13 1 0.38 9.13 4.88 o 1 13 1 905.37 931.85 21.07 o 2 13 1 3728.76 3704.21 55.60 o 3 13 1 970.26 946.97 21.24 o 4 13 1 225.33 228.32 11.60 o 5 13 1 2227.05 2129.72 36.79 o 6 13 1 659.90 681.16 18.50 o 7 13 1 1550.33 1517.53 29.13 o 8 13 1 633.27 628.83 17.72 o 9 13 1 1167.70 1245.64 21.63 o 10 13 1 350.03 373.30 20.81 o 11 13 1 1983.73 2090.57 50.45 o 12 13 1 713.92 752.60 29.08 o -11 14 1 105.06 90.57 14.26 o -10 14 1 1829.86 1905.21 32.48 o -9 14 1 264.25 253.62 12.47 o -8 14 1 149.12 120.27 9.03 o -7 14 1 402.24 387.09 11.22 o -6 14 1 64.42 63.81 10.13 o -5 14 1 2437.86 2443.32 42.72 o -4 14 1 1535.51 1460.38 28.65 o -3 14 1 313.68 309.10 17.50 o -2 14 1 187.41 198.93 15.29 o -1 14 1 282.11 279.15 17.72 o 0 14 1 11.39 8.93 8.04 o 1 14 1 274.24 264.79 14.38 o 2 14 1 180.13 180.16 12.92 o 3 14 1 310.71 306.59 17.48 o 4 14 1 1546.91 1519.33 24.32 o 5 14 1 2397.71 2392.60 46.96 o 6 14 1 62.51 73.76 9.10 o 7 14 1 398.64 371.62 12.13 o 8 14 1 161.37 167.66 15.07 o 9 14 1 278.64 281.33 22.13 o 10 14 1 1827.45 1871.35 55.31 o 11 14 1 105.04 69.34 46.57 o -10 15 1 518.58 526.52 16.85 o -9 15 1 490.47 496.68 14.36 o -8 15 1 19.50 15.71 5.87 o -7 15 1 448.55 445.62 13.00 o -6 15 1 627.00 638.86 18.76 o -5 15 1 727.55 733.90 18.82 o -4 15 1 189.30 202.41 19.23 o -3 15 1 627.16 591.35 22.04 o -2 15 1 317.39 289.70 18.74 o -1 15 1 1854.03 1968.80 42.53 o 0 15 1 139.52 161.12 18.66 o 1 15 1 1845.71 1869.13 34.41 o 2 15 1 306.66 302.68 14.43 o 3 15 1 624.67 601.47 17.06 o 4 15 1 183.14 218.46 16.65 o 5 15 1 728.67 752.04 17.87 o 6 15 1 636.04 667.03 18.00 o 7 15 1 455.22 465.18 15.73 o 8 15 1 16.56 13.36 8.78 o 9 15 1 501.06 519.59 26.15 o 10 15 1 520.67 522.23 30.55 o -8 16 1 1049.78 1103.54 34.83 o -7 16 1 215.22 225.90 27.24 o -6 16 1 2469.95 2512.15 41.24 o -5 16 1 1935.87 1967.05 42.92 o -4 16 1 101.65 81.86 23.68 o -3 16 1 24.66 16.39 11.93 o -2 16 1 115.21 127.25 15.94 o -1 16 1 703.42 753.20 22.95 o 0 16 1 109.30 105.63 15.13 o 1 16 1 694.07 729.24 25.11 o 2 16 1 121.67 124.82 18.17 o 3 16 1 24.79 12.59 10.24 o 4 16 1 98.62 95.29 14.10 o 5 16 1 1947.16 1979.80 33.48 o 6 16 1 2479.19 2493.96 54.87 o 7 16 1 224.42 226.14 10.93 o 8 16 1 1053.07 981.56 25.21 o -6 17 1 37.61 12.75 13.15 o -5 17 1 223.50 225.62 14.59 o -4 17 1 15.68 20.33 10.76 o -3 17 1 274.99 262.41 19.09 o -2 17 1 633.86 697.41 24.69 o -1 17 1 1278.35 1344.31 32.99 o 0 17 1 1564.61 1615.53 36.60 o 1 17 1 1269.87 1300.31 32.17 o 2 17 1 620.30 677.21 27.45 o 3 17 1 276.95 274.43 20.62 o 4 17 1 17.86 12.24 9.56 o 5 17 1 224.69 208.06 14.46 o 6 17 1 33.09 21.11 14.15 o -1 18 1 256.75 259.58 18.62 o 0 18 1 2.58 5.75 9.48 o 1 18 1 274.91 320.19 34.54 o 0 0 2 13.73 31.47 13.36 o 0 1 2 226.23 212.23 4.11 o -2 2 2 1441.86 1673.15 24.47 o -1 2 2 1344.73 1301.17 13.49 o 0 2 2 2024.87 2061.84 17.47 o 1 2 2 1351.75 1354.80 10.00 o 2 2 2 1453.98 1732.55 13.45 o -3 3 2 8408.77 7571.37 83.11 o -2 3 2 12020.59 11665.31 112.72 o -1 3 2 6280.59 6074.92 73.55 o 0 3 2 14.13 21.84 2.59 o 1 3 2 6280.99 6132.48 47.23 o 2 3 2 11843.91 11620.47 120.71 o 3 3 2 8363.75 7527.04 67.98 o -4 4 2 8830.13 9015.08 175.16 o -3 4 2 449.33 426.72 5.81 o -2 4 2 201.71 278.18 8.07 o -1 4 2 1551.72 1536.51 14.02 o 0 4 2 1368.98 1313.62 9.69 o 1 4 2 1554.42 1528.47 21.63 o 2 4 2 193.62 261.32 6.19 o 3 4 2 432.83 414.31 5.58 o 4 4 2 8805.83 8743.94 258.03 o -5 5 2 843.70 804.85 19.30 o -4 5 2 3002.74 3171.29 38.35 o -3 5 2 9132.91 9492.77 68.17 o -2 5 2 1528.69 1578.86 16.10 o -1 5 2 12278.25 12701.13 145.37 o 0 5 2 2599.39 3381.77 32.53 o 1 5 2 12267.29 12784.10 119.18 o 2 5 2 1501.95 1582.57 22.16 o 3 5 2 9131.77 9499.58 95.91 o 4 5 2 2972.70 3160.13 60.87 o 5 5 2 879.09 835.46 18.57 o -6 6 2 13650.36 13482.11 168.01 o -5 6 2 941.61 933.93 15.98 o -4 6 2 4702.31 5096.94 62.66 o -3 6 2 255.47 247.32 5.56 o -2 6 2 2152.50 2141.99 19.95 o -1 6 2 1415.99 1475.40 14.41 o 0 6 2 458.89 468.48 6.88 o 1 6 2 1427.86 1528.60 35.93 o 2 6 2 2122.71 2080.14 23.77 o 3 6 2 250.00 228.22 7.24 o 4 6 2 4716.60 4987.05 54.01 o 5 6 2 934.91 940.36 12.88 o 6 6 2 13581.42 13770.65 107.34 o -7 7 2 4576.11 4742.85 54.92 o -6 7 2 1424.00 1388.35 17.21 o -5 7 2 240.99 251.83 8.66 o -4 7 2 3525.53 3480.61 39.63 o -3 7 2 4193.93 4164.92 38.09 o -2 7 2 56.84 60.07 3.29 o -1 7 2 3916.26 3923.94 36.15 o 0 7 2 13117.58 12541.30 335.44 o 1 7 2 3927.31 3797.55 61.35 o 2 7 2 59.64 63.18 5.97 o 3 7 2 4160.53 4165.72 64.07 o 4 7 2 3531.74 3528.39 47.38 o 5 7 2 243.40 259.26 5.25 o 6 7 2 1398.87 1360.46 18.13 o 7 7 2 4585.77 4980.36 80.13 o -8 8 2 504.04 452.60 17.45 o -7 8 2 2945.90 3025.88 34.99 o -6 8 2 941.73 929.12 16.49 o -5 8 2 145.22 150.38 7.79 o -4 8 2 3039.78 3114.60 35.17 o -3 8 2 3528.70 3511.54 23.95 o -2 8 2 2332.88 2310.64 27.43 o -1 8 2 981.50 990.25 14.91 o 0 8 2 224.90 201.11 7.66 o 1 8 2 975.56 973.50 19.94 o 2 8 2 2361.58 2365.41 37.79 o 3 8 2 3544.32 3565.01 64.10 o 4 8 2 3020.08 3120.24 48.81 o 5 8 2 143.38 147.54 4.72 o 6 8 2 955.05 980.58 11.87 o 7 8 2 2922.04 2972.45 29.21 o 8 8 2 522.32 489.94 14.29 o -9 9 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