#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:31:14 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181246 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/24/2232493.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232493_Fobs loop_ _publ_author_name 'Deng, Yi-Fang' 'Chen, Man-Sheng' 'Zhang, Chun-Hua' 'Tan, Xiong-Wen' _publ_section_title ; Poly[[tetraaquatetrakis[\m~3~-5-(pyridine-4-carboxamido)isophthalato]cobalt(II)dierbium(III)] tetrahydrate] ; _journal_coeditor_code WM2536 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1478 _journal_page_last m1479 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.174 _cell_angle_beta 78.771 _cell_angle_gamma 86.355 _cell_length_a 10.0816 _cell_length_b 10.7844 _cell_length_c 13.7316 _exptl_crystal_F_000 827.00 _reflns_d_resolution_high 0.8397 _cod_data_source_file wm2536Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 357.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 174.76 200.95 27.03 o 2 0 0 6863.94 8165.75 417.32 o 3 0 0 127699.77 145082.30 10473.67 o 4 0 0 289.88 330.76 21.81 o 5 0 0 10077.31 11840.89 401.56 o 6 0 0 21317.67 24953.23 1363.49 o 7 0 0 238.99 256.66 28.54 o 8 0 0 4676.51 4940.81 114.24 o 9 0 0 5989.14 6203.32 247.80 o 10 0 0 1996.86 2039.21 108.13 o 11 0 0 1120.65 1240.15 107.01 o -10 1 0 8.74 28.16 21.50 o -9 1 0 568.95 634.23 47.71 o -8 1 0 2893.37 3184.47 114.89 o -7 1 0 1235.44 1274.45 55.35 o -6 1 0 309.98 398.27 30.23 o -5 1 0 4511.56 4793.85 127.28 o -4 1 0 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