#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:31:35 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181247 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/25/2232535.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232535_Fobs loop_ _publ_author_name 'Walha, Sondra' 'Na\"ili, Houcine' 'Yahyaoui, Samia' 'Mhiri, Tahar' _publ_section_title ; 1-Methylpiperazine-1,4-diium tetrachloridozincate hemihydrate ; _journal_coeditor_code ZQ2122 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1605 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.821 _cell_angle_gamma 90.000 _cell_length_a 14.3210 _cell_length_b 12.7590 _cell_length_c 13.7970 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.6706 _cod_data_source_file zq2122Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound A1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 357.36 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 0 0 2247.58 2254.54 68.67 o 10 0 0 91.40 106.56 181.65 o 12 0 0 5890.33 5648.93 153.77 o 14 0 0 7376.99 6878.46 211.75 o 16 0 0 526.12 274.87 87.29 o 18 0 0 78.07 63.58 65.94 o 20 0 0 4.04 14.32 61.45 o 3 1 0 169.54 192.62 11.77 o 5 1 0 6456.16 6463.48 60.08 o 7 1 0 6481.83 6464.18 83.35 o 9 1 0 212.54 219.05 41.30 o 11 1 0 4668.88 4776.37 90.76 o 13 1 0 41.01 81.77 26.97 o 15 1 0 101.06 25.54 34.55 o 17 1 0 25.57 -23.14 129.28 o 19 1 0 433.13 286.99 55.66 o 2 2 0 117921.17 108263.16 920.35 o 4 2 0 14242.61 13017.42 118.81 o 6 2 0 6277.87 5833.21 77.94 o 8 2 0 7210.09 6974.16 90.68 o 10 2 0 6293.24 6209.93 105.58 o 12 2 0 3999.27 3903.19 86.67 o 14 2 0 781.85 734.98 55.66 o 16 2 0 264.15 422.13 56.78 o 18 2 0 94.40 -27.38 36.44 o 20 2 0 41.48 37.31 87.38 o 1 3 0 3860.68 3789.44 40.25 o 3 3 0 5887.29 5732.13 59.63 o 5 3 0 4771.88 4498.88 59.70 o 7 3 0 5396.27 5326.10 136.21 o 9 3 0 5801.70 5776.09 88.49 o 11 3 0 4807.83 4580.22 95.49 o 13 3 0 639.78 623.05 40.36 o 15 3 0 729.47 785.69 52.21 o 17 3 0 545.13 560.47 74.95 o 19 3 0 55.20 264.41 345.01 o 0 4 0 249.87 140.33 14.68 o 2 4 0 14997.44 14009.24 129.71 o 4 4 0 14345.89 13589.56 122.59 o 6 4 0 36379.30 35500.17 291.09 o 8 4 0 26763.30 25079.60 232.27 o 10 4 0 19239.72 18296.47 198.70 o 12 4 0 1752.92 1750.38 62.89 o 14 4 0 639.49 680.65 47.93 o 16 4 0 232.14 354.84 52.66 o 18 4 0 104.16 410.27 80.02 o 20 4 0 141.16 101.48 56.64 o 1 5 0 467.52 413.70 16.32 o 3 5 0 96.40 128.07 16.46 o 5 5 0 199.03 281.18 22.23 o 7 5 0 294.98 316.90 25.76 o 9 5 0 481.09 491.19 32.69 o 11 5 0 2429.02 2354.63 76.17 o 13 5 0 1441.06 1540.38 107.73 o 15 5 0 386.91 595.36 85.26 o 17 5 0 191.27 77.44 79.66 o 19 5 0 0.99 34.54 105.38 o 0 6 0 12035.67 11483.65 170.95 o 2 6 0 24737.53 22652.16 199.73 o 4 6 0 66305.77 65120.84 616.51 o 6 6 0 2009.24 1754.72 57.84 o 8 6 0 7240.46 7218.71 130.79 o 10 6 0 10600.21 10294.12 151.14 o 12 6 0 2127.28 2105.37 70.72 o 14 6 0 2.00 8.75 30.40 o 16 6 0 33.39 116.78 81.59 o 18 6 0 80.95 157.55 59.27 o 1 7 0 10446.17 9610.95 123.09 o 3 7 0 1036.30 973.53 39.06 o 5 7 0 8035.05 7638.98 127.56 o 7 7 0 316.76 271.49 33.93 o 9 7 0 1715.23 1540.82 64.45 o 11 7 0 1492.45 1370.61 66.01 o 13 7 0 359.51 323.63 54.49 o 15 7 0 451.44 345.54 62.52 o 17 7 0 84.00 489.62 184.61 o 19 7 0 253.36 284.48 127.24 o 0 8 0 29522.68 29316.23 394.65 o 2 8 0 22780.34 21632.75 229.25 o 4 8 0 8460.49 8040.09 145.48 o 6 8 0 8265.87 7978.59 137.06 o 8 8 0 99.27 145.73 31.66 o 10 8 0 888.17 893.21 55.15 o 12 8 0 442.12 304.65 42.63 o 14 8 0 160.33 135.40 44.36 o 16 8 0 710.26 744.60 82.29 o 18 8 0 0.63 -26.77 95.75 o 1 9 0 7585.60 7565.87 127.36 o 3 9 0 1620.05 1554.79 59.13 o 5 9 0 2102.64 1949.45 75.61 o 7 9 0 1364.85 1213.57 62.99 o 9 9 0 43.87 28.10 47.69 o 11 9 0 14.40 69.38 42.41 o 13 9 0 2147.07 2358.72 192.90 o 15 9 0 112.24 21.75 48.40 o 17 9 0 16.61 3.10 56.94 o 0 10 0 6066.96 5791.36 149.29 o 2 10 0 7523.98 7483.04 137.70 o 4 10 0 7235.89 7074.30 145.35 o 6 10 0 12452.30 11961.43 190.92 o 8 10 0 8140.65 7823.84 166.66 o 10 10 0 13.53 -8.81 50.99 o 12 10 0 132.53 -56.82 67.45 o 14 10 0 730.41 1086.00 105.39 o 16 10 0 49.61 178.56 102.51 o 1 11 0 1199.49 1182.48 58.07 o 3 11 0 283.17 415.42 53.33 o 5 11 0 338.23 167.16 52.97 o 7 11 0 1203.93 1046.98 65.81 o 9 11 0 447.14 421.61 103.28 o 11 11 0 492.42 581.91 93.37 o 13 11 0 10.44 98.24 63.91 o 15 11 0 105.10 197.78 123.44 o 0 12 0 4406.20 4389.18 147.63 o 2 12 0 1304.04 1233.09 63.34 o 4 12 0 5941.42 5780.62 150.63 o 6 12 0 10548.38 10414.53 216.65 o 8 12 0 4279.69 4096.67 136.14 o 10 12 0 8.45 42.53 43.83 o 12 12 0 197.33 137.89 70.65 o 14 12 0 215.09 56.73 91.73 o 16 12 0 51.43 20.59 67.96 o 1 13 0 2962.94 2987.72 101.97 o 3 13 0 35.68 34.18 30.69 o 5 13 0 1015.21 859.67 72.24 o 7 13 0 2.60 1.01 38.12 o 9 13 0 46.14 -27.34 44.65 o 11 13 0 105.93 71.32 44.54 o 13 13 0 796.02 771.85 107.32 o 15 13 0 133.94 521.78 141.00 o 0 14 0 1412.21 1233.90 126.77 o 2 14 0 2620.08 2339.20 131.41 o 4 14 0 2044.62 2106.41 148.89 o 6 14 0 1982.53 2185.34 176.57 o 8 14 0 450.78 455.70 96.24 o 10 14 0 462.15 667.47 139.69 o 12 14 0 207.77 142.20 78.15 o 1 15 0 55.76 79.69 46.48 o 3 15 0 373.16 186.57 129.79 o 5 15 0 11.14 -5.03 66.55 o 7 15 0 380.70 837.18 153.48 o 9 15 0 0.12 -35.59 80.13 o 11 15 0 220.78 190.58 166.90 o 0 16 0 626.15 578.44 193.69 o 2 16 0 1430.00 1649.38 163.66 o 4 16 0 2324.90 2554.94 201.85 o 6 16 0 713.46 726.35 215.14 o 10 16 0 743.32 887.08 136.13 o 1 17 0 1.72 -89.61 125.00 o 3 17 0 4.51 427.00 125.59 o 5 17 0 69.91 968.71 248.43 o 7 17 0 1.80 92.39 132.65 o 9 17 0 109.33 506.02 136.48 o 0 18 0 294.97 492.78 199.74 o 2 18 0 830.54 944.18 173.34 o 4 18 0 1041.32 1304.74 180.77 o 6 18 0 248.27 475.39 134.11 o 1 19 0 114.18 382.74 144.41 o -21 1 1 261.28 233.58 111.28 o -19 1 1 827.33 650.85 102.16 o -17 1 1 9495.59 9129.72 205.23 o -15 1 1 7420.55 7333.02 151.26 o -13 1 1 1590.65 1509.21 72.08 o -11 1 1 1631.11 1526.75 49.81 o -9 1 1 8215.49 7962.37 112.14 o -7 1 1 1054.02 962.91 34.14 o -5 1 1 126.74 146.46 14.53 o -3 1 1 1497.23 1420.29 22.11 o 3 1 1 494.93 349.44 14.90 o 5 1 1 2128.84 2373.13 32.12 o 7 1 1 31806.71 31548.41 206.56 o 9 1 1 31563.56 30623.87 254.53 o 11 1 1 9168.97 9081.05 130.81 o 13 1 1 7870.97 7452.65 127.22 o 15 1 1 4869.62 4727.42 123.18 o 17 1 1 1110.32 1113.16 66.47 o 19 1 1 411.07 563.95 80.54 o -20 2 1 196.31 79.59 56.54 o -18 2 1 71.38 -46.67 59.18 o -16 2 1 838.01 696.24 88.40 o -14 2 1 14.95 33.24 23.83 o -12 2 1 1333.44 1236.58 50.82 o -10 2 1 3884.80 3708.41 78.78 o -8 2 1 786.59 929.95 40.30 o -6 2 1 37491.10 37134.95 260.15 o -4 2 1 23244.24 23198.28 143.97 o -2 2 1 340.96 367.76 10.22 o 0 2 1 5.66 6.05 3.82 o 2 2 1 120.81 140.03 8.53 o 4 2 1 46813.77 47699.45 440.38 o 6 2 1 1718.90 1811.12 40.31 o 8 2 1 8633.11 8259.67 99.40 o 10 2 1 2960.84 2975.63 70.34 o 12 2 1 657.41 770.14 41.03 o 14 2 1 3712.72 3686.90 99.16 o 16 2 1 12.41 34.02 37.20 o 18 2 1 593.63 729.26 63.98 o 20 2 1 595.05 787.73 117.93 o -19 3 1 2304.60 2061.04 129.16 o -17 3 1 235.75 374.31 109.81 o -15 3 1 1862.37 1778.86 74.72 o -13 3 1 1424.91 1354.61 56.39 o -11 3 1 10168.46 9745.70 142.67 o -9 3 1 17985.03 17366.08 184.85 o -7 3 1 27355.03 26207.93 247.35 o -5 3 1 12602.89 11800.20 107.46 o -3 3 1 3482.28 3541.05 43.21 o -1 3 1 22558.99 22891.79 131.80 o 1 3 1 10030.70 9792.03 73.25 o 3 3 1 12660.01 12912.03 89.76 o 5 3 1 3661.52 3512.19 50.83 o 7 3 1 4494.00 4146.44 73.53 o 9 3 1 16723.68 16665.35 165.50 o 11 3 1 12641.46 12277.80 165.52 o 13 3 1 3251.96 3148.36 84.10 o 15 3 1 1337.93 1363.22 68.02 o 17 3 1 617.07 584.17 61.53 o 19 3 1 1170.64 1032.09 121.94 o -20 4 1 198.67 8.09 54.72 o -18 4 1 9.73 30.99 49.43 o -16 4 1 574.00 593.36 74.20 o -14 4 1 914.51 727.75 67.37 o -12 4 1 0.22 173.10 59.43 o -10 4 1 1292.71 1258.37 41.71 o -8 4 1 1985.50 2068.86 61.15 o -6 4 1 7106.18 6695.81 98.90 o -4 4 1 1039.39 1106.27 32.94 o -2 4 1 37522.44 37566.13 217.01 o 0 4 1 4583.03 4592.16 50.02 o 2 4 1 44.26 29.45 15.91 o 4 4 1 275.93 227.24 17.11 o 6 4 1 1437.75 1388.08 44.22 o 8 4 1 221.95 219.19 22.44 o 10 4 1 2422.68 2299.41 58.16 o 12 4 1 168.28 111.11 34.10 o 14 4 1 367.36 476.91 44.91 o 16 4 1 293.83 371.37 57.45 o 18 4 1 429.97 472.42 75.65 o 20 4 1 9.65 10.04 119.90 o -19 5 1 961.39 1079.85 117.88 o -17 5 1 480.34 340.58 69.21 o -15 5 1 161.76 233.31 54.05 o -13 5 1 3298.21 3166.95 94.63 o -11 5 1 619.33 733.24 43.63 o -9 5 1 5601.86 5507.93 109.11 o -7 5 1 28409.81 28201.24 259.13 o -5 5 1 10314.87 9707.88 121.89 o -3 5 1 2863.64 3010.13 50.09 o -1 5 1 9840.77 10029.19 85.64 o 1 5 1 47.19 25.04 16.39 o 3 5 1 31770.60 31623.71 234.00 o 5 5 1 21873.12 20811.81 179.84 o 7 5 1 3706.63 3550.90 77.73 o 9 5 1 4597.53 4452.57 90.92 o 11 5 1 9427.33 9225.50 141.43 o 13 5 1 1947.23 1835.44 73.77 o 15 5 1 228.38 396.05 69.46 o 17 5 1 2728.43 2704.13 141.31 o 19 5 1 2382.30 2449.83 144.50 o -18 6 1 186.03 248.58 85.73 o -16 6 1 129.23 190.22 53.23 o -14 6 1 235.85 39.69 39.47 o -12 6 1 266.16 298.27 36.44 o -10 6 1 1217.44 1177.09 58.23 o -8 6 1 260.46 173.48 24.53 o -6 6 1 259.90 309.22 23.91 o -4 6 1 12013.29 11591.35 145.25 o -2 6 1 10905.27 10727.48 114.60 o 0 6 1 901.08 746.88 30.15 o 2 6 1 11962.29 11541.74 130.33 o 4 6 1 34027.00 32884.60 293.29 o 6 6 1 4167.28 4157.33 90.51 o 8 6 1 1536.25 1414.14 56.37 o 10 6 1 4454.65 4330.45 95.77 o 12 6 1 1581.52 1520.48 60.56 o 14 6 1 4.53 120.56 47.52 o 16 6 1 697.14 755.84 78.64 o 18 6 1 348.66 686.86 90.18 o -19 7 1 1512.92 1422.10 115.68 o -17 7 1 1863.85 2210.13 142.93 o -15 7 1 1829.24 1748.09 96.62 o -13 7 1 6167.27 6233.55 167.38 o -11 7 1 1957.53 2008.23 79.57 o -9 7 1 690.48 638.93 43.12 o -7 7 1 479.39 461.74 34.68 o -5 7 1 11545.54 11711.82 157.95 o -3 7 1 1585.32 1587.18 51.00 o -1 7 1 918.88 805.05 33.25 o 1 7 1 76.78 85.94 14.78 o 3 7 1 14953.15 14228.84 154.63 o 5 7 1 19374.48 18985.34 229.22 o 7 7 1 7318.62 7182.78 130.48 o 9 7 1 456.51 500.35 43.68 o 11 7 1 2613.75 2724.27 87.30 o 13 7 1 2365.78 2276.84 97.63 o 15 7 1 2283.50 2163.20 121.21 o 17 7 1 3114.41 3369.03 163.33 o 19 7 1 1317.47 1287.54 111.73 o -18 8 1 184.95 -3.36 80.30 o -16 8 1 739.40 392.28 90.86 o -14 8 1 6.01 -45.61 46.21 o -12 8 1 1862.17 2005.47 94.24 o -10 8 1 27.68 -27.82 27.82 o -8 8 1 121.61 152.87 37.15 o -6 8 1 2619.52 2641.73 77.04 o -4 8 1 657.15 660.45 40.70 o -2 8 1 1994.00 1951.19 62.35 o 0 8 1 822.97 870.12 40.07 o 2 8 1 46.39 19.36 13.56 o 4 8 1 6549.81 6504.91 102.27 o 6 8 1 1149.77 1002.56 51.96 o 8 8 1 4617.93 4655.35 138.57 o 10 8 1 11.00 -6.00 33.46 o 12 8 1 532.21 437.87 56.23 o 14 8 1 137.52 224.71 93.20 o 16 8 1 60.17 2.09 47.68 o 18 8 1 280.31 75.70 98.49 o -17 9 1 1266.45 1266.27 115.40 o -15 9 1 5174.80 5121.15 191.59 o -13 9 1 3344.84 3507.03 130.06 o -11 9 1 5171.57 5013.64 147.12 o -9 9 1 1086.87 1157.66 62.63 o -7 9 1 185.59 224.94 38.74 o -5 9 1 1267.53 1342.65 61.44 o -3 9 1 1225.76 1122.55 49.52 o -1 9 1 3768.17 3880.68 87.11 o 1 9 1 62.28 15.94 30.80 o 3 9 1 850.14 856.70 43.18 o 5 9 1 1563.78 1689.78 64.58 o 7 9 1 1608.81 1648.94 70.69 o 9 9 1 4933.79 4962.60 130.97 o 11 9 1 2873.26 3152.59 147.72 o 13 9 1 4001.16 3993.49 179.47 o 15 9 1 3600.24 3719.13 212.83 o 17 9 1 880.05 1121.28 139.19 o -16 10 1 73.18 4.29 52.50 o -14 10 1 172.06 225.29 67.88 o -12 10 1 517.98 709.04 62.19 o -10 10 1 275.77 199.21 51.79 o -8 10 1 9.33 4.06 34.14 o -6 10 1 165.99 225.09 47.73 o -4 10 1 1085.61 1048.92 76.40 o -2 10 1 103.31 98.12 48.53 o 0 10 1 1120.61 1037.20 51.29 o 2 10 1 855.18 786.34 40.48 o 4 10 1 13.10 -3.20 19.04 o 6 10 1 669.48 664.01 46.63 o 8 10 1 31.54 13.39 32.51 o 10 10 1 445.88 577.16 86.49 o 12 10 1 790.75 863.34 89.31 o 14 10 1 23.22 15.09 111.06 o 16 10 1 26.16 66.75 104.04 o -17 11 1 375.54 172.74 108.64 o -15 11 1 568.79 1060.98 262.97 o -13 11 1 1540.10 1442.39 116.42 o -11 11 1 3664.05 3606.83 166.61 o -9 11 1 4389.62 4473.78 152.42 o -7 11 1 330.03 390.24 86.03 o -5 11 1 834.46 865.82 54.03 o -3 11 1 850.04 867.49 49.45 o -1 11 1 86.62 176.36 36.85 o 1 11 1 1196.16 1248.06 52.65 o 3 11 1 77.33 49.39 53.40 o 5 11 1 875.87 877.13 51.96 o 7 11 1 5061.53 4961.64 138.39 o 9 11 1 4252.84 4174.54 189.57 o 11 11 1 1478.53 1429.10 108.09 o 13 11 1 2365.92 2658.63 180.92 o 15 11 1 1903.55 2021.13 172.27 o -16 12 1 302.82 -35.90 88.76 o -14 12 1 1.26 -15.92 92.11 o -12 12 1 11.01 41.38 62.91 o -10 12 1 34.55 86.40 50.91 o -8 12 1 29.99 63.88 40.06 o -6 12 1 1226.73 1057.95 68.78 o -4 12 1 776.81 723.71 66.06 o -2 12 1 237.08 231.93 38.58 o 0 12 1 0.04 -0.35 34.11 o 2 12 1 15.28 7.15 34.33 o 4 12 1 24.24 118.64 55.79 o 6 12 1 269.00 328.95 56.46 o 8 12 1 369.29 380.10 55.59 o 10 12 1 34.99 -35.63 62.02 o 12 12 1 14.62 -7.11 67.55 o 14 12 1 74.16 31.11 62.20 o -15 13 1 474.54 484.69 140.79 o -13 13 1 382.43 241.12 261.32 o -11 13 1 444.39 913.17 155.80 o -9 13 1 1290.05 1424.10 96.98 o -7 13 1 447.05 507.31 52.94 o -5 13 1 438.12 354.57 48.51 o -3 13 1 1446.55 1443.98 92.70 o -1 13 1 838.44 790.47 69.54 o 1 13 1 1217.57 1091.82 74.04 o 3 13 1 4069.73 3754.45 121.77 o 5 13 1 2462.85 2435.94 119.20 o 7 13 1 2739.49 2536.40 138.84 o 9 13 1 318.95 331.79 102.88 o 11 13 1 69.99 105.47 72.45 o 13 13 1 280.71 188.21 82.77 o -14 14 1 20.50 173.43 156.71 o -12 14 1 63.14 237.53 149.11 o -10 14 1 393.08 712.79 203.43 o -8 14 1 138.19 123.70 163.16 o -6 14 1 34.01 224.02 76.22 o -4 14 1 1.00 197.16 88.89 o -2 14 1 390.19 425.16 83.38 o 0 14 1 432.32 459.02 65.96 o 2 14 1 484.86 392.63 69.89 o 4 14 1 337.16 365.06 84.06 o 6 14 1 14.49 -11.89 113.29 o 8 14 1 186.87 77.28 63.82 o 10 14 1 127.23 8.03 79.21 o 12 14 1 94.27 43.73 63.04 o -13 15 1 684.53 634.62 151.69 o -11 15 1 486.95 942.80 167.43 o -9 15 1 7.57 1.18 59.66 o -7 15 1 330.46 595.94 184.22 o -5 15 1 565.40 468.86 94.03 o -3 15 1 276.95 485.57 92.46 o -1 15 1 98.01 205.97 73.14 o 1 15 1 38.46 6.34 79.34 o 3 15 1 1788.31 1727.70 160.52 o 5 15 1 2482.86 2084.59 268.37 o 7 15 1 287.30 631.86 200.66 o 9 15 1 7.56 81.36 98.60 o 11 15 1 168.86 448.83 182.90 o -10 16 1 306.79 143.33 324.81 o -6 16 1 338.58 262.50 71.24 o -4 16 1 35.68 461.20 171.32 o -2 16 1 217.53 351.72 155.14 o 0 16 1 376.72 456.73 122.19 o 2 16 1 30.60 122.55 73.21 o 4 16 1 194.15 54.54 66.33 o 6 16 1 64.37 -70.26 116.06 o 8 16 1 273.82 91.89 114.48 o 10 16 1 6.74 10.63 105.77 o -9 17 1 151.28 290.26 126.91 o -7 17 1 97.14 193.03 150.14 o -5 17 1 8.51 -75.27 75.27 o -3 17 1 277.85 331.59 162.50 o -1 17 1 45.05 -96.30 96.30 o 1 17 1 6.33 71.98 289.22 o 3 17 1 66.11 64.45 118.14 o 5 17 1 312.67 190.55 124.59 o 7 17 1 23.61 68.64 64.79 o 9 17 1 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