#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:31:35 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181247 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/25/2232543.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232543_Fobs loop_ _publ_author_name 'Zhu, Xiao-Hong' 'Cheng, Xiao-Chun' _publ_section_title ; Poly[tetra-n-butylammonium [(\m~5~-benzene-1,3,5-tricarboxylato)(\m~4~-benzene-1,3,5-tricarboxylato)-\m~3~-hydroxido-trizincate] 0.25-hydrate] ; _journal_coeditor_code ZS2153 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1641 _journal_volume 67 _journal_year 2011 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.2950 _cell_length_b 16.2950 _cell_length_c 28.9460 _exptl_crystal_F_000 3624.00 _reflns_d_resolution_high 0.7458 _cod_data_source_file zs2153Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2110424B_0m in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 584.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 149779.25 139197.39 1346.28 o 4 0 0 85428.18 92312.13 4122.98 o 6 0 0 15573.25 15494.96 451.26 o 8 0 0 1265.63 1366.66 177.45 o 10 0 0 96950.70 98132.70 1210.94 o 12 0 0 88343.25 84404.23 2933.77 o 14 0 0 9052.98 7999.15 722.81 o 16 0 0 3608.44 3991.72 943.52 o 18 0 0 3098.49 2104.68 798.79 o 20 0 0 1340.72 1639.09 810.01 o 2 1 0 15086.37 10447.80 179.28 o 4 1 0 246173.95 249647.23 3527.53 o 6 1 0 173504.77 169303.63 1753.97 o 8 1 0 14343.13 12752.79 384.56 o 10 1 0 54601.95 57814.80 956.37 o 12 1 0 3185.20 3524.47 338.45 o 14 1 0 5398.45 5356.60 452.92 o 16 1 0 18234.82 17261.72 1101.40 o 18 1 0 24445.39 25063.49 1692.38 o 20 1 0 2449.79 2420.57 649.26 o 2 2 0 187297.88 178317.47 2135.88 o 4 2 0 7277.81 6662.84 214.02 o 6 2 0 4221.91 3301.40 196.13 o 8 2 0 18813.95 19126.08 523.85 o 10 2 0 83309.30 84311.34 1234.26 o 12 2 0 97512.19 95606.16 1568.11 o 14 2 0 100.00 203.80 210.13 o 16 2 0 1259.92 1514.12 369.03 o 18 2 0 340.71 209.41 351.22 o 20 2 0 58.57 441.66 422.29 o 2 3 0 68145.69 60247.85 708.69 o 4 3 0 56045.72 58204.55 721.07 o 6 3 0 41896.15 37358.48 656.74 o 8 3 0 148.98 221.08 103.48 o 10 3 0 12793.67 12523.58 454.85 o 12 3 0 3474.71 3204.99 313.98 o 14 3 0 1040.87 684.38 417.35 o 16 3 0 5447.49 6310.89 648.70 o 18 3 0 4068.98 4719.37 769.90 o 20 3 0 98.05 222.82 394.14 o 0 4 0 4095.88 2756.51 300.67 o 2 4 0 13682.21 13051.76 343.70 o 4 4 0 140411.41 142397.30 890.51 o 6 4 0 2470.84 3039.62 213.27 o 8 4 0 2431.39 2112.53 216.36 o 10 4 0 12153.27 11925.39 452.44 o 12 4 0 15406.79 14230.97 663.81 o 14 4 0 4527.11 4160.25 630.65 o 16 4 0 11901.42 12557.46 983.17 o 18 4 0 336.12 294.18 364.83 o 20 4 0 506.46 311.92 406.87 o 2 5 0 9818.62 8450.10 375.22 o 4 5 0 7775.00 8232.87 274.31 o 6 5 0 17229.51 18611.66 324.70 o 8 5 0 4414.71 4146.41 277.54 o 10 5 0 26045.67 25920.50 662.30 o 12 5 0 373.81 53.05 170.50 o 14 5 0 4413.63 3677.73 604.84 o 16 5 0 336.26 690.45 406.13 o 18 5 0 223.59 48.96 281.35 o 20 5 0 3822.94 3883.10 780.55 o 0 6 0 33275.71 36371.97 1185.85 o 2 6 0 32075.89 30053.86 754.31 o 4 6 0 72541.40 73855.36 904.77 o 6 6 0 10.54 12.47 75.12 o 8 6 0 11263.63 11843.58 451.56 o 10 6 0 5310.80 5883.62 497.22 o 12 6 0 224.65 146.99 190.41 o 14 6 0 6235.13 5604.14 732.23 o 16 6 0 19127.61 19195.69 1205.71 o 18 6 0 88.80 50.41 282.43 o 20 6 0 1043.62 1154.23 556.99 o 2 7 0 44935.16 47833.75 1032.33 o 4 7 0 4175.58 4438.59 308.73 o 6 7 0 25336.68 24506.08 598.16 o 8 7 0 3653.42 3318.17 379.83 o 10 7 0 9528.22 8964.63 560.52 o 12 7 0 5488.29 6158.36 572.12 o 14 7 0 5965.10 6522.06 637.88 o 16 7 0 1311.53 1474.07 488.26 o 18 7 0 7326.01 7647.49 1182.48 o 20 7 0 3816.04 3319.59 756.81 o 0 8 0 47806.50 50860.18 1633.49 o 2 8 0 10890.91 11337.67 569.93 o 4 8 0 25754.37 27442.59 708.17 o 6 8 0 288.47 523.39 140.11 o 8 8 0 16209.69 16151.88 700.36 o 10 8 0 348.21 552.68 237.25 o 12 8 0 6287.43 6637.03 625.38 o 14 8 0 599.61 352.46 263.24 o 16 8 0 8919.89 8895.80 1510.64 o 18 8 0 104.33 195.61 382.75 o 20 8 0 929.34 921.32 441.34 o 2 9 0 3435.71 3154.40 394.85 o 4 9 0 18287.45 19184.96 640.67 o 6 9 0 81306.09 81250.35 1146.64 o 8 9 0 3045.02 3438.48 417.36 o 10 9 0 8213.46 8759.34 592.15 o 12 9 0 1248.47 1234.87 326.94 o 14 9 0 920.30 1293.74 362.36 o 16 9 0 3387.35 3778.84 718.08 o 18 9 0 2053.30 2022.88 599.61 o 0 10 0 39812.52 36695.07 1584.12 o 2 10 0 14846.37 15554.59 751.36 o 4 10 0 13245.67 13564.23 585.80 o 6 10 0 613.43 497.58 187.27 o 8 10 0 1023.25 892.30 268.54 o 10 10 0 24276.57 23590.81 951.74 o 12 10 0 24975.59 25992.62 1057.96 o 14 10 0 1747.93 1016.37 355.96 o 16 10 0 1434.46 1449.16 510.90 o 18 10 0 185.42 440.93 433.49 o 2 11 0 5385.11 7752.04 596.27 o 4 11 0 14176.90 15861.77 666.50 o 6 11 0 56674.92 57390.13 1205.82 o 8 11 0 466.93 595.17 321.49 o 10 11 0 2047.29 2578.44 433.61 o 12 11 0 1399.34 1170.04 348.41 o 14 11 0 952.47 983.77 372.73 o 16 11 0 3396.44 3047.22 942.96 o 18 11 0 2890.00 2818.59 719.91 o 0 12 0 21598.97 22528.86 1410.23 o 2 12 0 459.09 274.42 231.76 o 4 12 0 15688.02 16670.67 719.46 o 6 12 0 289.39 494.31 284.65 o 8 12 0 7349.28 7990.47 845.86 o 10 12 0 2802.82 3010.98 583.93 o 12 12 0 17705.83 16875.78 924.89 o 14 12 0 2793.36 2948.83 528.76 o 16 12 0 1809.27 1473.47 446.44 o 18 12 0 3227.33 2682.46 1027.66 o 2 13 0 14989.06 14929.41 875.61 o 4 13 0 166.91 178.31 205.40 o 6 13 0 8886.84 8396.09 799.16 o 8 13 0 3940.67 4212.13 663.18 o 10 13 0 218.81 -98.63 276.76 o 12 13 0 1974.36 2577.86 591.98 o 14 13 0 6429.42 7489.20 798.23 o 16 13 0 75.05 164.24 341.08 o 0 14 0 14.16 -131.26 302.91 o 2 14 0 2737.26 2947.87 517.54 o 4 14 0 15291.78 16453.35 791.89 o 6 14 0 101.33 154.58 285.73 o 8 14 0 19591.61 19275.04 1175.04 o 10 14 0 2719.57 2311.36 561.64 o 12 14 0 13.47 -60.14 340.11 o 14 14 0 1749.95 2220.45 635.41 o 16 14 0 3186.63 3456.09 637.23 o 2 15 0 26610.97 27818.23 1264.98 o 4 15 0 16547.52 15047.25 984.30 o 6 15 0 2999.64 2899.70 594.17 o 8 15 0 10756.87 11074.14 956.95 o 10 15 0 6364.93 5099.70 800.27 o 12 15 0 1670.52 1693.63 570.60 o 14 15 0 7956.74 7755.34 1042.99 o 0 16 0 10330.62 9993.88 1234.09 o 2 16 0 18029.61 18365.61 1094.72 o 4 16 0 14547.25 14713.85 1055.78 o 6 16 0 4730.66 4415.64 733.49 o 8 16 0 21669.34 21760.01 1336.16 o 10 16 0 8254.70 8504.33 1027.59 o 12 16 0 2998.91 2387.65 662.80 o 14 16 0 3318.60 3535.12 787.75 o 2 17 0 21840.70 24050.66 1287.97 o 4 17 0 20166.98 20581.52 1279.59 o 6 17 0 5112.36 4989.48 902.01 o 8 17 0 4197.77 3576.81 707.48 o 10 17 0 13282.46 12800.43 1319.91 o 12 17 0 21.13 -4.70 411.15 o 0 18 0 291.42 272.62 551.97 o 2 18 0 6745.71 7288.13 902.02 o 4 18 0 11974.09 11695.49 1182.42 o 6 18 0 190.37 560.80 430.59 o 8 18 0 19650.96 18503.62 1329.05 o 10 18 0 6777.50 4578.16 857.02 o 2 19 0 11698.60 11989.74 1729.97 o 4 19 0 1273.22 1705.28 561.09 o 6 19 0 149.75 142.10 402.15 o 8 19 0 1377.07 1110.56 551.92 o 0 20 0 2675.33 3449.84 1048.98 o 2 20 0 395.71 540.76 696.70 o 4 20 0 1813.40 2179.98 643.32 o 6 20 0 60.21 -274.31 391.51 o 2 21 0 2368.46 1901.97 627.50 o 4 21 0 32.22 -69.56 647.34 o 1 1 1 73546.16 66573.48 399.30 o 2 1 1 19971.78 16108.85 178.48 o 3 1 1 8994.36 7363.08 128.84 o 4 1 1 37706.97 38748.18 354.13 o 5 1 1 2129.82 2369.16 93.46 o 6 1 1 2344.08 2215.83 91.72 o 7 1 1 50.70 58.59 40.77 o 8 1 1 520.83 536.68 67.22 o 9 1 1 7368.44 7641.32 182.65 o 10 1 1 9.84 7.57 65.32 o 11 1 1 2579.28 3158.69 191.25 o 12 1 1 617.64 572.45 125.83 o 13 1 1 2075.72 1854.34 193.73 o 14 1 1 523.56 411.15 146.39 o 15 1 1 1373.92 1030.53 212.05 o 16 1 1 1.42 116.92 180.59 o 17 1 1 10.78 90.71 212.39 o 18 1 1 114.07 179.82 235.62 o 19 1 1 312.15 345.15 269.60 o 20 1 1 129.07 -101.31 247.34 o 21 1 1 62.47 2.33 273.26 o 0 2 1 1274.24 200.00 55.10 o 1 2 1 12223.06 8269.52 299.55 o 2 2 1 385.60 318.23 41.96 o 3 2 1 24774.24 26883.83 360.67 o 4 2 1 21845.71 21461.18 257.48 o 5 2 1 4472.67 4126.21 142.68 o 6 2 1 2161.55 2077.82 122.90 o 7 2 1 4628.28 4270.09 165.94 o 8 2 1 9553.41 9339.74 244.04 o 9 2 1 1755.13 2327.54 160.73 o 10 2 1 119.55 159.72 83.64 o 11 2 1 1131.44 1206.87 140.64 o 12 2 1 69.41 114.29 113.76 o 13 2 1 0.39 -11.24 119.99 o 14 2 1 1016.82 736.43 186.88 o 15 2 1 1401.23 1374.14 233.49 o 16 2 1 2638.00 2568.02 340.30 o 17 2 1 331.78 511.56 256.09 o 18 2 1 6.01 126.78 227.77 o 19 2 1 2515.67 2917.02 472.30 o 20 2 1 59.49 -85.30 253.18 o 21 2 1 861.41 740.23 345.46 o 1 3 1 51169.59 52289.90 1311.00 o 2 3 1 3116.76 3878.47 113.84 o 3 3 1 11986.00 14204.20 188.09 o 4 3 1 5642.12 6682.28 160.49 o 5 3 1 9985.59 9628.56 204.36 o 6 3 1 1065.42 1039.72 93.91 o 7 3 1 1696.66 1727.64 126.33 o 8 3 1 3159.86 3434.54 180.29 o 9 3 1 277.09 212.96 77.92 o 10 3 1 278.88 227.45 87.98 o 11 3 1 10921.84 11076.99 321.47 o 12 3 1 3715.76 3879.31 265.26 o 13 3 1 8584.19 9191.84 526.12 o 14 3 1 258.75 206.56 163.35 o 15 3 1 6723.78 7163.07 514.27 o 16 3 1 18.20 -14.29 155.71 o 17 3 1 1116.15 1086.51 275.48 o 18 3 1 1048.53 1062.33 320.68 o 19 3 1 17.40 63.13 250.57 o 20 3 1 449.99 482.18 311.20 o 21 3 1 34.30 11.20 291.06 o 0 4 1 6143.83 6648.38 497.56 o 1 4 1 61810.64 65890.00 725.28 o 2 4 1 651.23 1263.64 98.63 o 3 4 1 489.10 1075.82 81.42 o 4 4 1 3131.66 3357.00 113.44 o 5 4 1 37.01 89.24 41.87 o 6 4 1 1632.39 1316.35 109.42 o 7 4 1 906.06 1101.62 108.67 o 8 4 1 3552.34 3136.78 176.65 o 9 4 1 220.83 255.13 84.02 o 10 4 1 3632.03 3682.96 218.36 o 11 4 1 331.20 312.43 104.66 o 12 4 1 45.27 151.34 109.96 o 13 4 1 289.70 566.43 208.20 o 14 4 1 894.70 919.39 252.47 o 15 4 1 1358.70 1452.61 308.99 o 16 4 1 1897.63 1915.31 318.17 o 17 4 1 56.26 214.50 189.86 o 18 4 1 857.43 966.21 287.27 o 19 4 1 1286.59 1368.64 372.01 o 20 4 1 1144.91 1212.85 369.61 o 21 4 1 862.84 1199.30 397.91 o 1 5 1 4298.67 5380.57 221.30 o 2 5 1 4566.54 3996.03 194.13 o 3 5 1 6267.43 7196.09 186.31 o 4 5 1 4432.99 4145.01 146.62 o 5 5 1 178.72 183.82 51.65 o 6 5 1 10733.41 11518.31 185.66 o 7 5 1 598.83 772.22 99.84 o 8 5 1 2789.93 2591.17 173.02 o 9 5 1 5440.84 5344.51 235.59 o 10 5 1 4823.78 4773.71 241.38 o 11 5 1 1550.65 1665.24 189.78 o 12 5 1 1248.45 1430.68 209.92 o 13 5 1 105.72 74.61 137.37 o 14 5 1 906.64 785.92 244.57 o 15 5 1 42.45 -115.14 184.57 o 16 5 1 168.74 58.16 218.58 o 17 5 1 2021.19 1997.29 338.72 o 18 5 1 123.35 152.26 223.88 o 19 5 1 100.63 54.29 256.80 o 20 5 1 566.34 659.36 332.52 o 21 5 1 427.84 376.93 332.87 o 0 6 1 2271.37 2264.50 272.48 o 1 6 1 6995.64 8019.69 347.99 o 2 6 1 3899.17 3145.69 206.04 o 3 6 1 17874.06 18025.85 350.76 o 4 6 1 3129.37 3109.49 156.90 o 5 6 1 5638.77 4791.56 174.97 o 6 6 1 15.90 164.34 61.58 o 7 6 1 9397.26 9890.67 252.35 o 8 6 1 12976.67 13244.62 321.31 o 9 6 1 10066.15 9875.53 295.83 o 10 6 1 21464.25 21243.25 489.66 o 11 6 1 425.06 455.20 149.14 o 12 6 1 6413.22 6316.24 390.21 o 13 6 1 359.44 208.52 151.67 o 14 6 1 2268.41 2485.30 369.10 o 15 6 1 1461.21 1718.32 348.24 o 16 6 1 7.78 -39.25 202.39 o 17 6 1 2765.44 3003.64 454.84 o 18 6 1 3944.67 4006.88 463.25 o 19 6 1 28.90 12.59 230.08 o 20 6 1 5545.09 5833.95 661.97 o 1 7 1 3029.95 2972.19 233.69 o 2 7 1 33953.19 36304.52 639.34 o 3 7 1 56109.00 58752.45 729.91 o 4 7 1 24949.18 25606.89 423.14 o 5 7 1 2786.22 2552.98 161.19 o 6 7 1 22887.44 22232.03 367.32 o 7 7 1 5398.83 4572.96 191.19 o 8 7 1 28121.33 29803.42 625.99 o 9 7 1 25930.05 26736.75 543.15 o 10 7 1 5691.44 5025.47 347.12 o 11 7 1 14199.61 14154.00 499.70 o 12 7 1 298.57 338.78 155.90 o 13 7 1 5315.66 5531.10 399.92 o 14 7 1 7432.23 7420.74 471.91 o 15 7 1 1608.37 1642.78 338.41 o 16 7 1 6188.75 6527.10 620.67 o 17 7 1 1263.50 1095.30 335.32 o 18 7 1 684.26 823.71 319.01 o 19 7 1 2196.63 2210.66 402.53 o 20 7 1 174.09 155.31 303.96 o 0 8 1 8858.61 6969.78 470.41 o 1 8 1 33137.55 34208.36 674.35 o 2 8 1 23563.28 24070.19 568.52 o 3 8 1 27765.65 28438.31 609.04 o 4 8 1 8390.63 8439.14 295.46 o 5 8 1 25388.17 26006.19 458.35 o 6 8 1 1945.26 2108.88 158.53 o 7 8 1 20514.20 19753.84 372.68 o 8 8 1 39373.54 41319.13 765.70 o 9 8 1 13127.81 13511.64 471.60 o 10 8 1 49974.00 49819.57 892.41 o 11 8 1 2022.33 1945.94 251.67 o 12 8 1 5943.45 5834.28 412.37 o 13 8 1 6479.15 6927.63 458.08 o 14 8 1 3149.36 2826.35 326.67 o 15 8 1 7870.47 8099.00 657.78 o 16 8 1 9.47 14.20 222.58 o 17 8 1 3700.92 3885.53 511.19 o 18 8 1 2052.29 1943.66 416.42 o 19 8 1 1085.78 1040.01 335.91 o 20 8 1 2325.83 2725.21 509.75 o 1 9 1 59189.05 60922.08 952.82 o 2 9 1 5638.20 4638.52 323.06 o 3 9 1 32820.00 34229.88 712.60 o 4 9 1 6505.17 7198.09 294.31 o 5 9 1 3605.05 3610.60 246.04 o 6 9 1 28332.72 27757.44 504.14 o 7 9 1 5439.99 6253.48 359.18 o 8 9 1 19898.82 18992.80 554.26 o 9 9 1 48158.91 49212.85 894.00 o 10 9 1 1124.11 1295.95 214.18 o 11 9 1 3555.31 4087.87 351.64 o 12 9 1 2136.50 2547.50 294.98 o 13 9 1 7104.59 7331.16 480.13 o 14 9 1 7267.73 8225.53 525.11 o 15 9 1 4108.74 3954.75 395.77 o 16 9 1 8523.91 8934.39 728.08 o 17 9 1 505.31 395.93 291.66 o 18 9 1 3069.01 3302.15 511.42 o 19 9 1 3114.00 2581.48 489.36 o 0 10 1 865.37 786.03 259.25 o 1 10 1 82.01 40.26 116.84 o 2 10 1 24059.88 24481.04 653.94 o 3 10 1 5650.10 5220.19 362.75 o 4 10 1 13308.97 14592.52 428.74 o 5 10 1 14323.53 15238.87 436.93 o 6 10 1 51.76 3.88 98.56 o 7 10 1 9900.15 9646.58 457.62 o 8 10 1 10660.04 11379.24 459.54 o 9 10 1 548.77 627.66 175.96 o 10 10 1 2651.57 2268.47 273.65 o 11 10 1 102.12 -18.36 140.31 o 12 10 1 5863.05 5574.58 430.64 o 13 10 1 2200.22 2176.13 303.25 o 14 10 1 5051.10 4722.47 422.82 o 15 10 1 2197.16 2371.37 339.27 o 16 10 1 178.27 85.26 248.09 o 17 10 1 2115.98 2173.21 429.57 o 18 10 1 1289.05 1290.49 387.68 o 19 10 1 161.60 25.59 291.14 o 1 11 1 3895.51 3672.52 341.07 o 2 11 1 665.27 618.77 182.67 o 3 11 1 9648.81 9095.84 445.94 o 4 11 1 5759.78 5700.72 335.85 o 5 11 1 401.61 389.66 136.76 o 6 11 1 4891.25 5257.90 321.03 o 7 11 1 1362.37 1024.92 247.13 o 8 11 1 18.58 97.52 164.11 o 9 11 1 992.66 1015.82 210.98 o 10 11 1 1018.09 1096.55 223.03 o 11 11 1 350.35 402.71 189.15 o 12 11 1 2930.77 2801.93 330.86 o 13 11 1 1211.36 1656.38 289.94 o 14 11 1 4661.86 4575.19 430.46 o 15 11 1 906.13 1005.65 269.56 o 16 11 1 1841.37 1686.51 391.61 o 17 11 1 363.37 244.90 293.40 o 18 11 1 926.86 992.60 371.93 o 0 12 1 3197.05 3009.27 474.31 o 1 12 1 565.09 675.67 204.81 o 2 12 1 5701.72 5475.04 427.86 o 3 12 1 544.35 441.40 190.82 o 4 12 1 4214.59 4188.09 317.44 o 5 12 1 564.26 875.03 183.62 o 6 12 1 319.58 370.33 201.43 o 7 12 1 141.72 293.14 197.07 o 8 12 1 3316.55 3586.48 416.79 o 9 12 1 311.93 553.83 230.81 o 10 12 1 238.35 247.71 195.44 o 11 12 1 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345.21 o 0 8 27 506.79 293.53 374.43 o 1 8 27 727.49 883.46 323.38 o 2 8 27 540.26 916.45 319.69 o 3 8 27 245.63 91.10 250.52 o 4 8 27 839.63 792.60 270.40 o 5 8 27 1132.43 1083.67 289.29 o 6 8 27 334.75 30.63 244.74 o 7 8 27 651.60 499.93 294.55 o 8 8 27 8.09 77.84 273.87 o 9 8 27 6.08 -108.54 308.14 o 10 8 27 54.83 50.78 320.10 o 11 8 27 1342.74 1053.69 373.35 o 12 8 27 253.16 235.01 305.40 o 13 8 27 210.81 124.63 426.45 o 1 9 27 920.84 999.91 336.96 o 2 9 27 2072.43 2257.50 417.28 o 3 9 27 120.75 216.65 271.44 o 4 9 27 69.70 -42.77 242.75 o 5 9 27 339.48 343.10 251.08 o 6 9 27 21.31 44.67 255.00 o 7 9 27 1439.73 1350.35 367.35 o 8 9 27 1030.99 544.28 356.82 o 9 9 27 1012.97 890.94 412.70 o 10 9 27 1671.98 1837.01 496.00 o 11 9 27 840.46 1203.14 469.63 o 12 9 27 3.99 69.11 352.05 o 0 10 27 1390.42 1425.92 531.11 o 1 10 27 396.95 237.32 284.56 o 2 10 27 81.67 207.98 278.98 o 3 10 27 1676.21 1620.65 390.37 o 4 10 27 576.63 510.27 304.14 o 5 10 27 1095.77 1058.47 411.19 o 6 10 27 242.02 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1 28 1072.86 1106.21 253.52 o 7 1 28 1128.36 1361.39 273.72 o 8 1 28 1.21 20.25 190.46 o 9 1 28 4391.08 4134.59 463.89 o 10 1 28 90.20 -0.28 261.91 o 11 1 28 911.78 1015.16 352.26 o 12 1 28 119.11 -6.69 302.35 o 13 1 28 216.47 106.00 399.26 o 14 1 28 116.23 148.29 426.42 o 0 2 28 802.18 985.19 323.95 o 1 2 28 6293.37 6325.49 447.90 o 2 2 28 51.79 40.35 167.97 o 3 2 28 3907.51 3667.59 366.90 o 4 2 28 2828.00 3076.50 350.60 o 5 2 28 643.51 503.34 219.93 o 6 2 28 110.63 156.88 190.84 o 7 2 28 183.40 200.43 202.20 o 8 2 28 123.55 -105.51 189.50 o 9 2 28 2479.00 2511.30 391.40 o 10 2 28 12.00 18.49 229.86 o 11 2 28 1.36 -111.25 239.95 o 12 2 28 84.99 235.94 333.00 o 13 2 28 8377.76 8798.77 911.27 o 14 2 28 278.55 256.47 452.22 o 1 3 28 1855.20 1909.53 315.06 o 2 3 28 2763.78 2450.37 350.36 o 3 3 28 9223.94 9038.36 532.02 o 4 3 28 123.00 171.30 188.24 o 5 3 28 3454.93 3431.73 372.14 o 6 3 28 3922.50 3621.86 377.47 o 7 3 28 7500.81 8147.91 544.50 o 8 3 28 381.72 235.99 211.86 o 9 3 28 8055.89 8038.83 615.08 o 10 3 28 1702.80 1499.43 343.46 o 11 3 28 395.92 483.95 356.26 o 12 3 28 55.24 10.50 317.50 o 13 3 28 733.60 765.65 418.75 o 14 3 28 511.16 641.49 519.93 o 0 4 28 1028.31 708.77 405.19 o 1 4 28 13300.12 13248.88 618.68 o 2 4 28 809.95 1003.73 271.62 o 3 4 28 27266.44 26601.95 856.95 o 4 4 28 656.95 564.13 222.83 o 5 4 28 1183.34 1073.21 256.58 o 6 4 28 2269.71 2150.51 319.23 o 7 4 28 1275.40 1316.12 279.76 o 8 4 28 1010.50 702.93 268.61 o 9 4 28 7103.26 7101.76 590.56 o 10 4 28 88.49 153.35 250.20 o 11 4 28 373.24 134.72 272.74 o 12 4 28 188.93 -30.51 310.14 o 13 4 28 7522.91 7371.28 852.31 o 1 5 28 5031.26 4973.55 535.80 o 2 5 28 680.01 848.78 263.36 o 3 5 28 16594.67 16094.17 691.17 o 4 5 28 715.85 969.22 278.01 o 5 5 28 4588.32 4394.99 414.52 o 6 5 28 7.73 -116.22 176.26 o 7 5 28 8078.39 7818.32 542.11 o 8 5 28 34.78 58.61 225.99 o 9 5 28 14681.37 15545.84 738.25 o 10 5 28 878.89 1048.49 356.64 o 11 5 28 1498.72 1429.09 387.09 o 12 5 28 63.80 42.97 339.30 o 13 5 28 426.03 371.25 384.49 o 14 5 28 985.60 1089.36 815.62 o 0 6 28 1446.49 1473.65 499.89 o 1 6 28 5263.77 5387.09 559.19 o 2 6 28 5.37 -160.35 220.62 o 3 6 28 17632.69 17259.04 718.96 o 4 6 28 25.80 25.43 204.90 o 5 6 28 4456.34 4600.52 471.72 o 6 6 28 1030.21 610.17 264.96 o 7 6 28 3120.79 3199.00 427.76 o 8 6 28 808.31 857.46 290.30 o 9 6 28 11571.97 12260.78 724.42 o 10 6 28 2.26 -51.52 258.55 o 11 6 28 1682.25 1511.82 406.49 o 12 6 28 19.94 -132.74 304.66 o 13 6 28 3427.04 3665.50 658.65 o 1 7 28 184.87 190.31 260.78 o 2 7 28 1345.56 1420.28 349.85 o 3 7 28 11172.58 11813.73 620.25 o 4 7 28 843.33 662.97 259.48 o 5 7 28 834.82 740.18 268.48 o 6 7 28 720.35 529.36 261.37 o 7 7 28 6178.94 6637.08 634.23 o 8 7 28 468.34 261.67 292.07 o 9 7 28 5399.52 5718.73 628.64 o 10 7 28 132.18 -15.82 280.21 o 11 7 28 5.47 30.84 283.59 o 12 7 28 0.82 47.21 311.42 o 13 7 28 53.38 117.80 670.90 o 0 8 28 1020.29 1250.24 501.74 o 1 8 28 4035.68 4277.75 529.74 o 2 8 28 3.37 -13.53 245.36 o 3 8 28 6422.11 6496.59 624.48 o 4 8 28 48.34 -157.73 215.66 o 5 8 28 57.31 40.87 226.18 o 6 8 28 40.35 -15.67 245.96 o 7 8 28 46.12 68.99 260.02 o 8 8 28 25.81 202.20 294.66 o 9 8 28 3392.52 3672.21 600.86 o 10 8 28 272.94 36.10 342.58 o 11 8 28 1680.00 1814.98 452.87 o 12 8 28 83.75 198.58 331.98 o 1 9 28 5708.20 5562.40 597.82 o 2 9 28 684.89 722.91 318.75 o 3 9 28 10.59 -5.96 263.90 o 4 9 28 74.87 172.54 277.26 o 5 9 28 412.32 315.93 261.16 o 6 9 28 1876.98 1516.15 395.02 o 7 9 28 4415.37 3841.14 532.15 o 8 9 28 101.55 34.68 305.26 o 9 9 28 105.32 33.02 332.85 o 10 9 28 273.94 240.98 360.63 o 11 9 28 2647.90 3334.36 617.54 o 12 9 28 158.22 369.10 753.92 o 0 10 28 19.93 164.50 392.28 o 1 10 28 438.91 414.81 295.13 o 2 10 28 116.95 145.89 281.16 o 3 10 28 521.49 386.75 302.10 o 4 10 28 36.29 -84.04 267.29 o 5 10 28 5557.89 6387.67 771.17 o 6 10 28 39.20 47.26 277.97 o 7 10 28 6606.99 6445.65 664.20 o 8 10 28 174.00 179.79 346.40 o 9 10 28 6.37 -242.82 311.63 o 10 10 28 80.59 166.14 365.27 o 11 10 28 821.15 738.78 537.03 o 1 11 28 12160.60 13116.78 825.24 o 2 11 28 1225.25 1253.87 383.61 o 3 11 28 75.00 163.85 289.52 o 4 11 28 493.20 572.77 392.71 o 5 11 28 244.51 160.12 361.67 o 6 11 28 915.99 1038.17 450.57 o 7 11 28 1555.71 1283.31 453.53 o 8 11 28 3.57 115.44 353.55 o 9 11 28 451.56 290.35 382.97 o 10 11 28 895.29 783.09 741.58 o 0 12 28 1174.44 1012.02 559.11 o 1 12 28 70.79 166.53 302.77 o 2 12 28 82.87 -53.32 289.05 o 3 12 28 242.24 289.68 328.07 o 4 12 28 330.26 423.52 382.79 o 5 12 28 7696.64 7849.38 864.83 o 6 12 28 175.79 171.14 388.31 o 7 12 28 6875.16 5689.15 1370.96 o 8 12 28 114.91 73.86 419.44 o 9 12 28 2.03 149.21 603.58 o 1 13 28 2602.41 2610.98 495.71 o 2 13 28 294.86 428.15 347.90 o 3 13 28 250.66 328.12 404.26 o 4 13 28 149.85 81.22 366.82 o 5 13 28 656.99 192.86 408.65 o 0 14 28 176.14 217.14 482.52 o 1 14 28 1350.68 1486.42 452.06 o 2 14 28 136.46 119.62 326.31 o 3 14 28 463.22 506.38 419.02 o 4 14 28 830.95 1572.90 921.08 o 5 14 28 4194.29 5884.36 1359.74 o 1 15 28 235.13 564.32 775.23 o 1 1 29 141.05 140.58 163.54 o 2 1 29 802.34 983.75 237.81 o 3 1 29 32.23 215.50 188.96 o 4 1 29 2260.47 2449.61 322.17 o 5 1 29 3.98 60.50 186.52 o 6 1 29 459.23 522.08 219.95 o 7 1 29 439.38 467.45 233.17 o 8 1 29 1684.83 1419.07 293.01 o 9 1 29 472.06 413.39 252.16 o 10 1 29 65.25 7.20 247.76 o 11 1 29 1160.39 882.52 347.13 o 12 1 29 45.92 193.24 336.27 o 13 1 29 299.49 135.62 439.36 o 0 2 29 3008.26 3225.19 489.23 o 1 2 29 46.27 59.41 193.69 o 2 2 29 1199.13 1672.82 285.19 o 3 2 29 635.43 789.68 236.41 o 4 2 29 741.13 848.21 238.47 o 5 2 29 4965.39 5500.48 458.00 o 6 2 29 1072.11 955.95 258.83 o 7 2 29 4228.22 3809.81 398.18 o 8 2 29 800.12 865.89 258.34 o 9 2 29 1333.88 1392.86 335.10 o 10 2 29 2182.28 2415.67 397.63 o 11 2 29 103.77 166.14 272.83 o 12 2 29 1366.55 1493.73 594.09 o 13 2 29 77.17 -129.01 362.25 o 1 3 29 4934.39 5382.84 484.99 o 2 3 29 2547.21 2774.76 370.69 o 3 3 29 49.91 16.67 178.71 o 4 3 29 2797.67 2993.63 357.68 o 5 3 29 2.71 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277.38 o 11 5 29 1552.20 2015.19 441.18 o 12 5 29 1.39 23.84 356.63 o 13 5 29 208.81 483.54 761.77 o 0 6 29 3.50 148.67 353.22 o 1 6 29 23.19 143.48 253.64 o 2 6 29 511.14 343.07 280.08 o 3 6 29 723.28 663.98 269.92 o 4 6 29 7.80 -34.46 214.84 o 5 6 29 3626.36 3385.62 425.98 o 6 6 29 81.34 186.73 236.52 o 7 6 29 307.72 278.83 257.53 o 8 6 29 442.38 415.58 267.28 o 9 6 29 21.76 86.56 243.45 o 10 6 29 509.37 454.26 320.85 o 11 6 29 292.47 156.56 292.37 o 12 6 29 25.90 38.15 348.33 o 1 7 29 960.76 940.12 336.70 o 2 7 29 555.59 407.71 292.55 o 3 7 29 174.25 122.22 266.50 o 4 7 29 213.04 215.69 240.32 o 5 7 29 252.48 118.79 233.92 o 6 7 29 284.46 413.12 294.07 o 7 7 29 1291.62 907.62 347.93 o 8 7 29 2.63 -61.80 261.73 o 9 7 29 662.53 659.77 337.14 o 10 7 29 167.49 345.92 305.90 o 11 7 29 141.98 241.11 320.58 o 12 7 29 334.66 414.74 412.94 o 0 8 29 52.56 346.71 403.08 o 1 8 29 10.64 2.28 260.57 o 2 8 29 944.64 1121.31 352.06 o 3 8 29 786.77 919.29 343.67 o 4 8 29 217.87 129.03 271.05 o 5 8 29 769.24 836.38 297.14 o 6 8 29 59.53 -72.07 260.29 o 7 8 29 269.58 206.78 293.56 o 8 8 29 60.63 9.51 292.01 o 9 8 29 829.71 593.21 379.13 o 10 8 29 3.33 70.43 337.51 o 11 8 29 413.87 547.00 409.17 o 1 9 29 2223.42 1738.48 403.64 o 2 9 29 244.77 248.87 294.30 o 3 9 29 7.94 56.52 274.62 o 4 9 29 103.85 171.73 280.75 o 5 9 29 707.19 1203.62 441.93 o 6 9 29 379.97 115.51 284.04 o 7 9 29 1773.81 1358.59 395.76 o 8 9 29 282.18 531.96 385.07 o 9 9 29 1046.65 1021.48 440.22 o 10 9 29 527.09 436.21 388.98 o 11 9 29 1092.39 1063.20 549.75 o 0 10 29 285.07 185.70 428.05 o 1 10 29 81.18 108.89 298.03 o 2 10 29 2.07 52.34 290.30 o 3 10 29 1427.79 1296.27 384.22 o 4 10 29 54.77 161.93 302.52 o 5 10 29 3558.86 3333.70 604.60 o 6 10 29 257.69 407.92 395.94 o 7 10 29 1857.25 2029.38 442.00 o 8 10 29 200.38 337.61 386.09 o 9 10 29 139.06 46.93 359.25 o 10 10 29 65.24 169.00 463.65 o 1 11 29 7272.09 7205.47 705.47 o 2 11 29 5.34 77.58 296.13 o 3 11 29 666.09 863.49 367.75 o 4 11 29 545.59 680.87 414.85 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2 32 4295.58 4149.91 467.22 o 3 2 32 2866.75 2397.27 347.52 o 4 2 32 878.19 986.29 282.87 o 5 2 32 1137.30 1149.11 286.08 o 6 2 32 16.14 -113.54 201.31 o 7 2 32 1496.64 1416.67 309.11 o 8 2 32 2916.64 2781.91 392.51 o 9 2 32 1713.21 1638.35 368.43 o 10 2 32 4293.88 4800.87 609.02 o 11 2 32 68.31 74.76 307.51 o 1 3 32 1.35 113.32 268.09 o 2 3 32 380.47 517.67 264.28 o 3 3 32 4070.65 4270.23 476.99 o 4 3 32 1657.28 1714.22 313.92 o 5 3 32 1705.36 1617.03 322.48 o 6 3 32 1105.75 955.48 279.86 o 7 3 32 2045.85 2422.53 372.41 o 8 3 32 321.57 223.91 266.95 o 9 3 32 1184.44 897.92 321.60 o 10 3 32 13.02 50.90 260.67 o 11 3 32 519.47 338.19 478.20 o 0 4 32 944.99 988.70 490.80 o 1 4 32 3825.87 4131.90 541.03 o 2 4 32 343.99 467.31 306.44 o 3 4 32 9306.19 8945.91 653.03 o 4 4 32 1211.37 905.35 298.41 o 5 4 32 56.79 106.15 216.47 o 6 4 32 126.92 220.04 231.82 o 7 4 32 451.02 277.91 241.37 o 8 4 32 314.49 357.28 271.12 o 9 4 32 2175.56 2621.64 445.44 o 10 4 32 384.40 242.12 289.17 o 11 4 32 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7.34 300.35 o 3 6 35 2024.77 2102.00 479.57 o 4 6 35 4.07 -25.95 313.33 o 5 6 35 1505.46 1522.84 444.93 o 6 6 35 0.39 157.25 488.27 o 7 6 35 742.16 909.86 755.04 o 1 7 35 5073.70 5164.13 650.92 o 2 7 35 273.13 381.25 356.59 o 3 7 35 1192.33 966.17 408.42 o 4 7 35 1692.70 1796.79 547.11 o 5 7 35 255.08 475.14 520.47 o 6 7 35 2309.20 2795.77 1135.36 o 0 8 35 2109.67 2696.36 759.90 o 1 8 35 1806.82 1654.92 522.82 o 2 8 35 2556.32 2944.49 622.00 o 3 8 35 1950.91 1723.27 650.80 o 4 8 35 221.17 377.36 510.13 o 1 9 35 2527.34 2290.92 1048.98 o 0 0 36 2700.25 2976.40 1050.10 o 1 0 36 168.48 -55.92 444.85 o 2 0 36 8308.68 7085.34 1014.83 o 3 0 36 125.79 160.31 341.15 o 4 0 36 1326.56 920.29 436.40 o 5 0 36 2263.68 2496.75 563.50 o 6 0 36 681.55 186.25 375.69 o 7 0 36 1419.50 1566.02 503.30 o 1 1 36 958.38 1177.53 396.63 o 2 1 36 315.83 552.33 342.95 o 3 1 36 803.09 998.47 305.30 o 4 1 36 3277.31 3765.92 449.45 o 5 1 36 1117.40 1183.81 324.92 o 6 1 36 5004.63 5099.95 520.12 o 7 1 36 125.14 23.27 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36 3556.44 3930.01 1177.99 o 1 7 36 2527.03 3393.74 1153.31 o 2 7 36 67.45 95.36 624.90 o 3 7 36 7.68 -42.63 672.02 o 1 1 37 40.04 -144.35 305.85 o 2 1 37 103.26 -29.65 305.47 o 3 1 37 763.21 565.42 371.33 o 4 1 37 2.82 -3.28 243.20 o 5 1 37 68.03 42.34 300.26 o 6 1 37 22.27 181.04 323.39 o 0 2 37 313.56 429.41 501.48 o 1 2 37 819.11 971.83 397.94 o 2 2 37 196.83 283.71 333.30 o 3 2 37 239.14 103.63 332.86 o 4 2 37 53.71 -55.39 392.22 o 5 2 37 1078.16 1166.50 404.81 o 6 2 37 48.41 34.99 407.23 o 1 3 37 2070.36 2041.72 484.23 o 2 3 37 5.33 38.06 318.29 o 3 3 37 1261.55 1469.54 442.23 o 4 3 37 692.74 590.24 445.02 o 5 3 37 285.69 502.61 737.09 o 0 4 37 688.16 832.19 555.87 o 1 4 37 103.05 190.12 345.20 o 2 4 37 280.38 509.82 508.34 o 3 4 37 332.39 471.20 753.92 o 4 4 37 257.60 53.85 669.77 o 1 5 37 880.96 832.45 833.57 o 2 5 37 687.36 1069.17 821.23 o 3 5 37 645.36 298.43 706.80 o 4 0 38 1698.19 1991.37 921.08 o 4 1 38 731.61 1312.62 807.77 o