#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/25/2232546.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232546_Fobs loop_ _publ_author_name 'Mohamed, Shaaban K.' 'Horton, Peter N.' 'El-Remaily, Mahmoud A.A.' 'Ng, Seik Weng' _publ_section_title ; 2-(1,3-Benzothiazol-2-yl)guanidinium chloride ; _journal_coeditor_code ZS2157 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3132 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 3.8857 _cell_length_b 11.0349 _cell_length_c 22.1860 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file zs2157Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P212121 839 Friedel pairs' _shelx_refln_list_code 4 _shelx_f_calc_maximum 129.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1931.20 2169.42 22.22 o 4 0 0 43.35 39.45 7.56 o 1 1 0 62.99 72.77 2.31 o 2 1 0 823.48 842.93 8.87 o 3 1 0 172.58 196.20 3.45 o 4 1 0 877.33 975.98 26.39 o 1 2 0 1021.49 964.40 6.73 o 2 2 0 1655.26 1818.59 13.47 o 3 2 0 365.43 367.31 5.26 o 4 2 0 5.15 3.71 1.13 o 1 3 0 163.88 150.80 2.07 o 2 3 0 5286.47 5465.55 21.94 o 3 3 0 599.64 623.98 7.12 o 4 3 0 37.79 31.83 2.52 o 0 4 0 1575.07 1565.42 9.73 o 1 4 0 415.61 401.10 4.15 o 2 4 0 3089.85 3285.72 13.56 o 3 4 0 586.77 596.20 5.14 o 4 4 0 114.98 84.91 9.26 o 1 5 0 83.83 92.25 2.06 o 2 5 0 0.49 1.54 0.74 o 3 5 0 566.17 561.26 7.55 o 4 5 0 796.99 856.33 29.23 o 0 6 0 209.19 157.51 3.17 o 1 6 0 1489.73 1466.95 7.19 o 2 6 0 2.07 3.47 0.90 o 3 6 0 206.69 213.14 6.06 o 4 6 0 128.30 111.50 9.58 o 1 7 0 605.14 581.53 6.80 o 2 7 0 501.60 523.19 6.20 o 3 7 0 7.72 6.59 0.99 o 4 7 0 10.83 12.44 3.71 o 0 8 0 378.36 389.19 7.67 o 1 8 0 904.72 883.95 7.17 o 2 8 0 1141.58 1200.37 11.99 o 3 8 0 0.61 1.87 1.33 o 4 8 0 0.03 0.49 2.90 o 1 9 0 193.40 189.62 5.71 o 2 9 0 340.11 335.67 8.88 o 3 9 0 41.47 30.13 3.49 o 0 10 0 128.65 159.13 13.41 o 1 10 0 1549.96 1597.84 13.31 o 2 10 0 372.90 391.20 10.73 o 3 10 0 35.95 30.47 3.29 o 1 11 0 282.96 284.64 13.24 o 2 11 0 191.02 190.05 12.40 o 3 11 0 181.65 167.76 19.80 o 0 12 0 108.87 113.40 12.94 o 1 12 0 0.32 0.34 2.06 o 2 12 0 26.19 24.46 3.41 o 1 13 0 65.80 57.08 5.39 o 2 13 0 66.65 65.30 6.71 o 0 14 0 328.62 322.70 31.11 o 1 14 0 361.91 373.40 39.09 o 1 0 1 14.40 23.34 0.86 o 2 0 1 51.79 43.31 2.13 o 3 0 1 37.42 37.58 3.53 o 4 0 1 85.79 72.86 10.38 o -4 1 1 86.68 67.99 9.25 o -3 1 1 513.26 513.61 5.33 o -2 1 1 112.98 124.46 2.51 o -1 1 1 15884.07 16081.57 52.62 o 0 1 1 224.38 199.81 11.15 o 1 1 1 15998.57 16016.17 133.41 o 2 1 1 114.80 121.41 1.53 o 3 1 1 513.07 519.61 4.45 o 4 1 1 85.91 64.59 10.42 o -4 2 1 62.05 47.19 5.15 o -3 2 1 467.50 502.03 6.64 o -2 2 1 87.03 93.89 3.16 o -1 2 1 16717.17 16579.57 47.38 o 0 2 1 3.56 11.11 0.93 o 1 2 1 16795.00 16626.97 36.26 o 2 2 1 92.80 99.29 2.61 o 3 2 1 474.23 514.80 7.56 o 4 2 1 60.94 47.28 3.70 o -4 3 1 553.81 578.37 12.51 o -3 3 1 1370.60 1458.58 13.84 o -2 3 1 785.61 794.67 8.15 o -1 3 1 1154.81 1182.53 7.67 o 0 3 1 6.09 4.61 0.85 o 1 3 1 1145.47 1162.14 8.90 o 2 3 1 762.77 762.24 7.50 o 3 3 1 1346.54 1427.87 11.81 o 4 3 1 544.67 564.73 11.52 o -4 4 1 109.11 87.46 9.30 o -3 4 1 396.38 409.00 5.28 o -2 4 1 3014.64 3133.92 14.44 o -1 4 1 78.96 98.88 2.09 o 0 4 1 4308.40 4337.67 23.58 o 1 4 1 73.70 94.63 1.79 o 2 4 1 3055.98 3144.86 16.03 o 3 4 1 401.14 415.19 3.97 o 4 4 1 107.60 106.01 7.49 o -4 5 1 276.26 255.72 11.30 o -3 5 1 520.18 535.84 8.04 o -2 5 1 329.98 327.73 3.03 o -1 5 1 419.54 414.66 4.33 o 0 5 1 575.57 506.36 4.62 o 1 5 1 420.63 420.96 4.03 o 2 5 1 341.25 330.72 3.64 o 3 5 1 514.23 535.19 5.76 o 4 5 1 296.17 281.54 8.77 o -4 6 1 56.96 36.45 4.67 o -3 6 1 493.78 513.45 6.26 o -2 6 1 646.30 622.96 5.62 o -1 6 1 825.70 806.63 7.41 o 0 6 1 30.02 19.85 1.20 o 1 6 1 828.63 809.93 6.84 o 2 6 1 630.27 608.27 5.46 o 3 6 1 490.59 512.50 5.81 o 4 6 1 59.71 50.60 11.49 o -4 7 1 290.59 310.76 16.55 o -3 7 1 249.70 252.74 8.43 o -2 7 1 699.24 694.54 6.63 o -1 7 1 437.11 432.69 5.37 o 0 7 1 7.22 9.74 1.04 o 1 7 1 421.70 410.13 5.44 o 2 7 1 698.55 705.90 6.44 o 3 7 1 251.18 260.51 5.19 o 4 7 1 287.54 284.61 26.19 o -4 8 1 52.45 48.28 7.09 o -3 8 1 59.48 52.11 4.97 o -2 8 1 793.85 814.77 8.43 o -1 8 1 367.43 364.25 3.13 o 0 8 1 35.64 36.87 1.95 o 1 8 1 366.22 361.26 3.76 o 2 8 1 811.12 829.57 9.66 o 3 8 1 57.43 50.14 4.52 o 4 8 1 54.78 36.11 5.69 o -3 9 1 146.91 137.48 7.30 o -2 9 1 98.13 108.24 6.02 o -1 9 1 10.55 12.95 1.03 o 0 9 1 1212.67 1179.74 9.95 o 1 9 1 10.80 12.43 1.29 o 2 9 1 92.83 96.47 6.44 o 3 9 1 145.80 133.03 6.22 o -3 10 1 111.47 109.53 11.60 o -2 10 1 51.84 49.26 3.53 o -1 10 1 593.59 593.00 7.62 o 0 10 1 265.79 267.21 8.03 o 1 10 1 600.15 609.94 10.35 o 2 10 1 51.09 46.36 4.37 o 3 10 1 115.34 115.32 9.06 o -3 11 1 322.83 353.66 25.01 o -2 11 1 216.15 224.88 6.68 o -1 11 1 32.13 36.00 3.59 o 0 11 1 446.02 457.51 11.66 o 1 11 1 31.66 34.44 3.24 o 2 11 1 222.34 220.95 15.91 o 3 11 1 321.67 359.13 21.18 o -2 12 1 458.36 472.25 16.34 o -1 12 1 293.05 320.56 10.82 o 0 12 1 413.30 435.24 11.89 o 1 12 1 295.38 330.51 14.36 o 2 12 1 456.30 466.48 24.02 o -2 13 1 276.72 232.16 23.08 o -1 13 1 88.55 78.16 5.44 o 0 13 1 71.08 67.34 4.67 o 1 13 1 85.34 72.08 6.69 o 2 13 1 269.59 284.08 22.29 o -1 14 1 246.49 240.29 21.44 o 0 14 1 196.08 164.29 15.68 o 1 14 1 253.22 270.18 28.99 o 1 0 2 777.06 770.36 5.98 o 2 0 2 2408.30 2328.98 15.39 o 3 0 2 19.12 12.63 2.35 o 4 0 2 271.41 300.04 18.41 o -4 1 2 36.24 21.92 4.02 o -3 1 2 332.85 345.96 3.13 o -2 1 2 2766.16 2880.72 20.63 o -1 1 2 811.71 823.67 6.29 o 0 1 2 1224.12 1098.23 30.48 o 1 1 2 793.44 806.31 5.69 o 2 1 2 2735.47 2868.53 20.50 o 3 1 2 335.23 322.61 5.57 o 4 1 2 35.18 27.56 4.90 o -4 2 2 58.47 56.59 5.37 o -3 2 2 23.15 26.55 1.94 o -2 2 2 373.53 359.06 3.00 o -1 2 2 4567.24 4427.97 22.47 o 0 2 2 3647.29 3723.33 25.40 o 1 2 2 4618.99 4498.60 13.28 o 2 2 2 373.30 357.68 3.80 o 3 2 2 26.68 31.23 1.66 o 4 2 2 61.74 57.23 5.92 o -4 3 2 131.89 112.46 9.03 o -3 3 2 478.58 490.03 7.78 o -2 3 2 931.46 1036.48 5.45 o -1 3 2 628.66 578.28 4.12 o 0 3 2 356.21 348.47 3.69 o 1 3 2 648.70 597.58 3.84 o 2 3 2 928.07 1033.71 6.73 o 3 3 2 461.84 469.55 5.76 o 4 3 2 133.72 110.39 8.05 o -4 4 2 275.55 245.95 11.82 o -3 4 2 650.74 678.98 9.77 o -2 4 2 394.39 379.55 5.17 o -1 4 2 760.56 691.13 6.44 o 0 4 2 3191.03 3138.31 8.48 o 1 4 2 765.39 689.38 6.22 o 2 4 2 397.87 385.96 5.18 o 3 4 2 637.60 656.52 7.20 o 4 4 2 274.68 254.74 8.09 o -4 5 2 354.34 325.25 32.75 o -3 5 2 463.90 493.57 5.97 o -2 5 2 78.33 68.82 2.05 o -1 5 2 448.69 448.26 4.87 o 0 5 2 1860.45 1916.94 12.50 o 1 5 2 464.62 463.77 4.19 o 2 5 2 81.94 76.81 2.15 o 3 5 2 471.76 493.02 4.22 o 4 5 2 352.52 349.35 24.06 o -4 6 2 40.11 36.49 6.15 o -3 6 2 1662.14 1807.63 16.95 o -2 6 2 71.13 68.28 3.39 o -1 6 2 396.88 393.95 3.52 o 0 6 2 318.85 347.81 3.63 o 1 6 2 393.23 386.31 3.00 o 2 6 2 74.28 71.19 3.00 o 3 6 2 1700.53 1832.34 15.93 o 4 6 2 41.49 23.75 6.48 o -4 7 2 421.94 460.24 14.67 o -3 7 2 145.23 139.81 9.08 o -2 7 2 91.46 92.94 4.30 o -1 7 2 974.46 945.19 6.33 o 0 7 2 124.05 140.63 2.45 o 1 7 2 982.66 950.24 5.61 o 2 7 2 90.52 81.77 4.08 o 3 7 2 149.28 142.48 7.41 o 4 7 2 418.11 420.33 34.91 o -4 8 2 81.55 51.14 8.43 o -3 8 2 142.75 135.35 13.67 o -2 8 2 234.90 229.97 3.87 o -1 8 2 516.05 510.05 4.17 o 0 8 2 2606.37 2566.37 9.27 o 1 8 2 511.80 496.32 3.66 o 2 8 2 228.82 212.14 6.25 o 3 8 2 138.32 136.64 8.44 o 4 8 2 81.18 62.45 8.79 o -3 9 2 30.11 21.71 3.66 o -2 9 2 87.77 94.03 5.45 o -1 9 2 663.25 664.38 7.55 o 0 9 2 21.02 23.92 1.41 o 1 9 2 667.50 670.18 7.46 o 2 9 2 88.07 90.78 6.16 o 3 9 2 31.84 24.44 3.06 o -3 10 2 338.74 365.21 21.11 o -2 10 2 78.61 75.57 5.18 o -1 10 2 23.66 26.03 1.84 o 0 10 2 961.30 998.96 14.20 o 1 10 2 23.09 21.57 1.79 o 2 10 2 80.47 72.28 6.32 o 3 10 2 342.55 382.98 15.29 o -3 11 2 15.78 18.54 3.78 o -2 11 2 148.40 148.44 8.57 o -1 11 2 241.28 268.47 11.46 o 0 11 2 24.73 23.74 2.16 o 1 11 2 230.09 238.02 12.85 o 2 11 2 143.12 137.86 10.78 o 3 11 2 15.26 13.29 3.88 o -2 12 2 291.63 319.64 17.27 o -1 12 2 200.99 203.94 10.57 o 0 12 2 83.54 85.48 6.10 o 1 12 2 193.07 205.69 12.85 o 2 12 2 289.15 307.60 13.28 o -2 13 2 318.22 321.25 26.52 o -1 13 2 31.67 27.10 2.81 o 0 13 2 41.06 35.30 3.17 o 1 13 2 32.53 23.65 2.96 o 2 13 2 326.99 329.21 20.17 o -1 14 2 354.81 341.52 31.92 o 0 14 2 191.49 179.26 12.87 o 1 14 2 350.53 269.76 23.54 o 1 0 3 584.40 602.49 4.77 o 2 0 3 877.26 872.16 7.18 o 3 0 3 28.94 29.90 2.57 o 4 0 3 20.45 20.93 3.66 o -4 1 3 46.50 34.37 5.92 o -3 1 3 657.50 695.48 11.09 o -2 1 3 1344.97 1286.77 9.23 o -1 1 3 151.37 147.85 2.37 o 0 1 3 654.35 515.85 10.54 o 1 1 3 160.93 157.70 2.45 o 2 1 3 1355.70 1273.42 10.26 o 3 1 3 672.79 716.09 6.96 o 4 1 3 48.70 36.65 6.44 o -4 2 3 29.92 20.25 2.71 o -3 2 3 38.21 37.19 2.45 o -2 2 3 1638.73 1687.74 8.00 o -1 2 3 1946.72 1938.09 8.43 o 0 2 3 304.19 245.00 3.62 o 1 2 3 1965.83 1978.25 8.86 o 2 2 3 1633.68 1678.25 8.08 o 3 2 3 34.26 31.98 1.81 o 4 2 3 26.73 20.62 3.13 o -4 3 3 35.65 28.60 2.98 o -3 3 3 92.06 92.99 3.16 o -2 3 3 601.94 578.39 5.79 o -1 3 3 2041.33 2007.87 6.64 o 0 3 3 892.63 900.66 7.48 o 1 3 3 2006.31 1978.67 6.54 o 2 3 3 609.30 572.92 5.90 o 3 3 3 87.44 91.40 2.89 o 4 3 3 37.06 27.91 2.33 o -4 4 3 257.13 250.00 19.93 o -3 4 3 503.93 528.37 10.31 o -2 4 3 956.60 923.26 4.67 o -1 4 3 710.49 770.43 7.45 o 0 4 3 1682.42 1625.74 6.23 o 1 4 3 703.89 758.55 6.61 o 2 4 3 966.75 933.86 5.51 o 3 4 3 505.37 547.28 4.44 o 4 4 3 263.34 273.71 9.18 o -4 5 3 1085.99 1122.87 46.77 o -3 5 3 176.89 171.73 5.25 o -2 5 3 687.36 689.66 5.40 o -1 5 3 83.25 90.58 2.23 o 0 5 3 1464.11 1470.42 9.91 o 1 5 3 91.74 94.72 3.09 o 2 5 3 688.85 687.46 4.70 o 3 5 3 175.91 178.18 3.18 o 4 5 3 1083.15 1134.05 36.19 o -4 6 3 24.90 15.15 4.20 o -3 6 3 73.94 68.82 4.27 o -2 6 3 169.51 164.42 2.86 o -1 6 3 2087.28 2098.80 11.12 o 0 6 3 2083.98 2000.58 9.22 o 1 6 3 2117.19 2146.35 10.22 o 2 6 3 179.79 178.01 3.97 o 3 6 3 78.00 76.66 4.15 o 4 6 3 25.24 14.75 2.79 o -4 7 3 81.48 78.22 10.59 o -3 7 3 396.50 423.20 18.62 o -2 7 3 450.31 441.31 6.16 o -1 7 3 127.83 128.24 4.13 o 0 7 3 559.87 555.18 6.46 o 1 7 3 136.85 133.25 4.35 o 2 7 3 447.23 437.07 5.28 o 3 7 3 402.89 432.46 9.57 o 4 7 3 85.80 80.06 13.01 o -4 8 3 284.22 308.03 35.09 o -3 8 3 91.71 82.78 11.01 o -2 8 3 89.03 92.63 5.08 o -1 8 3 90.75 88.86 3.80 o 0 8 3 628.17 578.94 4.50 o 1 8 3 81.01 76.74 3.91 o 2 8 3 90.74 91.72 5.04 o 3 8 3 82.78 66.07 4.86 o 4 8 3 288.13 262.70 33.23 o -3 9 3 282.21 297.06 19.96 o -2 9 3 97.54 95.47 6.13 o -1 9 3 509.73 510.21 6.98 o 0 9 3 165.15 156.79 4.43 o 1 9 3 496.45 498.44 6.23 o 2 9 3 99.44 93.22 5.68 o 3 9 3 280.96 273.64 8.45 o -3 10 3 439.44 464.69 16.09 o -2 10 3 28.56 27.57 2.91 o -1 10 3 879.10 897.32 9.71 o 0 10 3 836.14 856.94 11.54 o 1 10 3 882.85 911.24 10.67 o 2 10 3 28.50 28.42 3.67 o 3 10 3 433.67 474.37 15.78 o -3 11 3 274.67 294.88 18.92 o -2 11 3 231.58 244.37 13.57 o -1 11 3 172.39 165.44 9.86 o 0 11 3 562.83 554.02 13.46 o 1 11 3 175.36 176.70 10.60 o 2 11 3 232.55 264.55 7.23 o 3 11 3 268.59 293.38 19.24 o -2 12 3 77.28 81.18 7.01 o -1 12 3 304.04 342.11 16.10 o 0 12 3 599.54 607.82 16.53 o 1 12 3 315.15 368.80 15.42 o 2 12 3 79.38 85.76 7.04 o -2 13 3 97.58 88.03 7.53 o -1 13 3 186.54 159.20 10.75 o 0 13 3 149.00 134.64 8.00 o 1 13 3 189.22 172.67 12.60 o 2 13 3 89.18 67.62 6.52 o 0 14 3 0.38 6.07 2.02 o 0 0 4 1555.17 1582.90 11.90 o 1 0 4 1601.50 1522.96 8.39 o 2 0 4 397.66 364.78 5.65 o 3 0 4 1353.98 1420.61 36.04 o 4 0 4 58.07 43.98 7.12 o -4 1 4 275.73 295.22 17.14 o -3 1 4 103.76 105.73 3.82 o -2 1 4 299.91 296.51 2.17 o -1 1 4 2390.00 2351.83 7.06 o 0 1 4 1068.32 985.89 9.87 o 1 1 4 2373.26 2341.05 11.70 o 2 1 4 301.83 295.73 4.39 o 3 1 4 99.58 100.96 2.12 o 4 1 4 270.58 232.19 25.66 o -4 2 4 101.43 87.08 8.65 o -3 2 4 846.89 900.04 9.70 o -2 2 4 823.77 822.30 7.95 o -1 2 4 1349.95 1318.74 11.25 o 0 2 4 1453.14 1430.33 12.04 o 1 2 4 1366.23 1335.01 9.32 o 2 2 4 800.28 805.30 7.72 o 3 2 4 857.24 897.70 8.40 o 4 2 4 102.32 91.22 8.10 o -4 3 4 165.42 146.09 10.51 o -3 3 4 200.38 201.12 4.46 o -2 3 4 523.18 525.16 5.16 o -1 3 4 1795.76 1841.86 12.87 o 0 3 4 997.31 963.14 7.23 o 1 3 4 1790.80 1824.59 7.79 o 2 3 4 535.89 545.64 5.37 o 3 3 4 201.85 203.49 3.34 o 4 3 4 166.23 135.15 14.41 o -4 4 4 279.82 274.16 20.81 o -3 4 4 119.60 126.15 3.66 o -2 4 4 498.20 515.47 7.08 o -1 4 4 1398.30 1422.62 12.71 o 0 4 4 676.23 657.73 5.51 o 1 4 4 1342.66 1356.64 9.67 o 2 4 4 520.19 530.73 6.19 o 3 4 4 127.47 131.46 2.53 o 4 4 4 284.68 285.85 8.14 o -4 5 4 227.35 194.68 24.19 o -3 5 4 776.67 795.96 9.12 o -2 5 4 19.06 18.97 1.42 o -1 5 4 188.40 177.82 3.46 o 0 5 4 673.20 581.92 5.65 o 1 5 4 187.41 177.51 3.66 o 2 5 4 21.98 23.38 1.44 o 3 5 4 789.30 830.50 9.25 o 4 5 4 223.00 230.81 17.08 o -4 6 4 285.61 291.76 50.23 o -3 6 4 18.71 15.32 1.62 o -2 6 4 141.03 145.28 4.05 o -1 6 4 2353.55 2374.28 15.58 o 0 6 4 144.04 172.84 2.95 o 1 6 4 2333.56 2364.70 11.36 o 2 6 4 145.15 145.97 3.24 o 3 6 4 17.85 17.08 1.34 o 4 6 4 275.92 319.10 19.01 o -4 7 4 3.85 10.88 8.42 o -3 7 4 238.92 246.55 5.68 o -2 7 4 227.96 235.92 4.20 o -1 7 4 423.41 413.95 4.70 o 0 7 4 2175.14 2160.70 11.51 o 1 7 4 425.87 423.01 3.33 o 2 7 4 241.18 251.41 5.32 o 3 7 4 238.40 252.72 8.92 o 4 7 4 4.86 5.99 2.03 o -4 8 4 34.23 24.19 4.74 o -3 8 4 66.89 64.31 5.36 o -2 8 4 1630.00 1663.51 25.63 o -1 8 4 716.86 719.03 8.00 o 0 8 4 858.98 849.46 7.59 o 1 8 4 737.22 743.68 6.75 o 2 8 4 1627.69 1669.89 19.34 o 3 8 4 69.62 60.59 4.88 o 4 8 4 35.87 22.98 5.26 o -3 9 4 498.03 529.93 12.13 o -2 9 4 589.01 619.08 12.03 o -1 9 4 0.57 3.93 2.29 o 0 9 4 166.01 156.40 6.64 o 1 9 4 0.21 3.89 1.55 o 2 9 4 578.67 590.15 10.11 o 3 9 4 495.65 535.48 10.68 o -3 10 4 153.39 148.80 7.97 o -2 10 4 67.54 64.59 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