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Information card for entry 2232548
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| Coordinates | 2232548.cif |
|---|---|
| Structure factors | 2232548.hkl |
| Original IUCr paper | HTML |
| Common name | Dichloridobis{2-[(dimethylamino)methyl]phenyl}bis{2- [(dimethylazaniumyl)methyl]phenyl}di-μ-hydroxido-di-μ~3~-oxido- tetraphenyltetratin(IV) dichloride deuterochloroform decasolvate |
|---|---|
| Chemical name | bis{2-[2-(dimethylazaniumyl)methyl]phenyl}-2κ<i>C</i>^1^,3κ<i>C</i>^1^- bis{2-[(dimethylamino)methyl]phenyl}-1κ<i>C</i>^1^,4κ<i>C</i>^1^- dichlorido-1κ<i>Cl</i>,4κ<i>Cl</i>- di-μ-hydroxido-1:2κ^2^<i>O</i>:<i>O</i>;3:4κ^2^<i>O</i>:<i>O</i>- di-μ~3~-oxido-1:2:3κ^3^<i>O</i>:<i>O</i>:<i>O</i>;2:3:4κ^3^<i>O</i>: <i>O</i>:<i>O</i>-tetraphenyl- 1κ<i>C</i>^1^,2κ<i>C</i>^1^,3κ<i>C</i>^1^,4κ<i>C</i>^1^-tetratin(IV) dichloride deuterochloroform decasolvate |
| Formula | C70 H72 Cl34 D10 N4 O4 Sn4 |
| Calculated formula | C70 H72 Cl34 D10 N4 O4 Sn4 |
| Title of publication | Dichloridobis{2-[(dimethylamino)methyl]phenyl}bis{2-[(dimethylazaniumyl)methyl]phenyl}di-μ-hydroxido-di-μ~3~-oxido-tetraphenyltetratin(IV) dichloride deuterochloroform decasolvate |
| Authors of publication | Turek, Jan; Padělková, Zdeňka |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2011 |
| Journal volume | 67 |
| Journal issue | 12 |
| Pages of publication | m1890 - m1891 |
| a | 11.9279 ± 0.0005 Å |
| b | 15.408 ± 0.0012 Å |
| c | 15.9651 ± 0.0014 Å |
| α | 83.752 ± 0.007° |
| β | 68.178 ± 0.004° |
| γ | 76.339 ± 0.005° |
| Cell volume | 2646.1 ± 0.3 Å3 |
| Cell temperature | 150 ± 1 K |
| Ambient diffraction temperature | 150 ± 1 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0754 |
| Residual factor for significantly intense reflections | 0.0537 |
| Weighted residual factors for significantly intense reflections | 0.1301 |
| Weighted residual factors for all reflections included in the refinement | 0.1458 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181247 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/25. |
2232548.cif 2232548.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2232548.cif 2232548.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2232548.cif 2232548.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2232548.cif 2232548.hkl |
| 31968 | 2012-01-03 | hkl/ Adding automatically assigned IUCr Fobs data for the rest of the year 2001 structures. |
2232548.cif 2232548.hkl |
| 31417 | 2012-01-02 | ../uploads/cif-deposit/cod/cif Adding structures of 2232548 via cif-deposit CGI script. |
2232548.cif |
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