#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/25/2232551.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232551_Fobs loop_ _publ_author_name 'Herbst, Leandra' 'Visser, Hendrik G.' 'Roodt, Andreas' 'Muller, Theunis J.' _publ_section_title ; cyclo-Tetra-\m-oxido-tetrakis[(acetylacetonato-\k^2^O,O')bis(ethanolato-\kO)niobium(V)] ; _journal_coeditor_code BG2426 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1669 _journal_page_last m1670 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 136.982 _cell_angle_gamma 90.000 _cell_length_a 13.9070 _cell_length_b 12.6620 _cell_length_c 21.3543 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file bg2426Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 11Tlh2_0ma in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 450.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7926.77 7969.68 74.07 o 3 0 0 1994.75 1958.68 23.79 o 4 0 0 2551.34 2391.47 32.77 o 5 0 0 15698.71 15808.44 182.09 o 6 0 0 26693.26 26315.88 326.53 o 7 0 0 519.51 663.37 28.14 o 8 0 0 7639.87 7849.17 116.04 o 9 0 0 31.66 16.73 9.86 o 10 0 0 34.74 19.91 14.72 o 11 0 0 4687.65 4646.70 144.84 o 12 0 0 2036.48 2184.47 97.00 o 2 1 0 2204.92 2197.51 43.17 o 3 1 0 29219.24 27791.17 200.00 o 4 1 0 1761.79 1595.44 18.77 o 5 1 0 2563.86 2750.82 28.39 o 6 1 0 1458.82 1536.06 23.15 o 7 1 0 30.35 33.05 6.98 o 8 1 0 3353.25 3486.37 44.49 o 9 1 0 2423.93 2592.39 40.85 o 10 1 0 39.73 35.02 9.98 o 11 1 0 875.62 914.87 38.70 o 12 1 0 16.17 1.12 17.04 o 0 2 0 12186.02 9152.74 663.70 o 1 2 0 345.94 354.69 7.99 o 2 2 0 3.63 6.14 1.59 o 3 2 0 51.53 27.49 2.90 o 4 2 0 3675.76 3711.83 85.50 o 5 2 0 359.77 423.47 10.16 o 6 2 0 1115.05 1131.47 18.30 o 7 2 0 309.02 300.31 11.93 o 8 2 0 61.17 59.88 7.84 o 9 2 0 32.40 21.83 7.86 o 10 2 0 1.15 -8.80 8.80 o 11 2 0 1349.27 1329.57 39.97 o 12 2 0 486.73 476.11 32.85 o 1 3 0 113.95 169.94 3.85 o 2 3 0 14381.25 14632.50 97.94 o 3 3 0 18213.36 17380.33 124.21 o 4 3 0 2749.12 2982.25 42.83 o 5 3 0 521.76 519.91 10.76 o 6 3 0 2.42 7.53 4.16 o 7 3 0 413.71 444.10 13.63 o 8 3 0 3111.29 3326.08 48.73 o 9 3 0 6409.18 6602.15 79.75 o 10 3 0 262.42 207.50 17.16 o 11 3 0 1313.04 1242.91 39.06 o 12 3 0 37.74 43.66 17.01 o 0 4 0 25617.79 25228.26 205.08 o 1 4 0 1987.58 1752.43 14.39 o 2 4 0 132.04 182.75 5.36 o 3 4 0 313.53 412.17 7.52 o 4 4 0 1899.96 1665.15 21.88 o 5 4 0 7735.65 7795.41 73.67 o 6 4 0 11871.21 12417.68 228.88 o 7 4 0 1735.50 1822.79 43.22 o 8 4 0 946.74 1036.02 26.31 o 9 4 0 1.45 1.10 8.51 o 10 4 0 469.58 465.54 25.11 o 11 4 0 1195.91 1194.01 38.48 o 12 4 0 673.58 655.94 38.65 o 1 5 0 6182.15 5557.02 39.85 o 2 5 0 179.82 122.43 4.67 o 3 5 0 813.79 906.67 14.31 o 4 5 0 170.50 85.97 6.19 o 5 5 0 10039.31 9706.11 89.69 o 6 5 0 483.76 551.32 14.91 o 7 5 0 2049.18 2101.92 59.56 o 8 5 0 550.07 507.49 21.62 o 9 5 0 1242.55 1509.97 46.60 o 10 5 0 644.84 620.97 28.11 o 11 5 0 272.33 310.82 22.69 o 0 6 0 20660.90 21507.29 208.73 o 1 6 0 940.14 948.56 12.16 o 2 6 0 11709.22 12148.69 90.46 o 3 6 0 216.08 184.34 7.35 o 4 6 0 1151.52 1040.24 16.91 o 5 6 0 8598.99 9032.78 89.77 o 6 6 0 11599.80 11483.66 106.67 o 7 6 0 34.63 20.11 8.93 o 8 6 0 2028.69 2223.49 43.75 o 9 6 0 10.82 9.72 12.08 o 10 6 0 150.13 175.92 17.79 o 11 6 0 822.73 862.08 40.75 o 1 7 0 4030.22 3986.53 35.52 o 2 7 0 5657.03 5758.29 48.02 o 3 7 0 8268.27 8064.76 66.57 o 4 7 0 954.42 855.71 17.66 o 5 7 0 7.23 12.21 5.77 o 6 7 0 783.79 869.23 31.25 o 7 7 0 864.19 935.70 35.37 o 8 7 0 2451.92 2503.42 47.32 o 9 7 0 449.85 431.07 30.94 o 10 7 0 0.39 -6.45 17.54 o 11 7 0 136.02 175.08 25.14 o 0 8 0 6.26 6.52 6.96 o 1 8 0 4023.44 3743.93 35.89 o 2 8 0 7035.28 6849.99 61.04 o 3 8 0 554.36 561.50 13.53 o 4 8 0 11193.18 11290.54 130.94 o 5 8 0 623.52 590.20 16.56 o 6 8 0 24.30 30.57 10.93 o 7 8 0 956.61 881.13 26.55 o 8 8 0 294.10 257.69 17.68 o 9 8 0 1598.81 1729.35 51.90 o 10 8 0 2588.78 2829.11 66.17 o 11 8 0 110.84 104.15 20.31 o 1 9 0 11892.28 11864.55 98.27 o 2 9 0 1139.64 1100.41 19.14 o 3 9 0 3581.24 3966.19 105.31 o 4 9 0 58.55 42.45 6.56 o 5 9 0 1930.46 2119.08 92.38 o 6 9 0 151.19 162.31 12.73 o 7 9 0 2535.65 2754.31 101.82 o 8 9 0 33.17 37.26 12.89 o 9 9 0 1549.45 1546.65 58.26 o 10 9 0 192.00 182.52 23.31 o 0 10 0 2481.22 2395.28 41.42 o 1 10 0 7669.41 7735.21 71.50 o 2 10 0 9.62 25.31 10.06 o 3 10 0 27.60 53.39 14.27 o 4 10 0 22.58 21.43 8.53 o 5 10 0 893.10 881.60 25.36 o 6 10 0 2480.35 2471.53 50.22 o 7 10 0 83.87 97.01 15.53 o 8 10 0 1.00 28.69 13.56 o 9 10 0 194.97 183.24 22.46 o 10 10 0 226.66 186.32 24.58 o 1 11 0 4195.10 4652.49 126.42 o 2 11 0 2510.08 2406.61 42.15 o 3 11 0 39.17 73.26 25.12 o 4 11 0 487.72 498.50 24.14 o 5 11 0 784.91 738.45 29.80 o 6 11 0 239.67 255.27 20.49 o 7 11 0 4018.20 4102.82 80.03 o 8 11 0 251.48 250.39 22.14 o 9 11 0 16.44 20.44 15.05 o 0 12 0 1297.66 1294.71 47.71 o 1 12 0 36.77 94.12 20.54 o 2 12 0 2607.44 2682.16 55.93 o 3 12 0 375.32 417.59 23.40 o 4 12 0 2004.22 2151.07 49.96 o 5 12 0 17.71 26.10 11.64 o 6 12 0 199.31 115.52 17.01 o 7 12 0 467.14 475.20 39.29 o 8 12 0 613.03 490.46 30.23 o 1 13 0 99.25 93.72 14.85 o 2 13 0 265.76 200.02 18.63 o 3 13 0 363.54 264.48 20.60 o 4 13 0 64.02 9.75 11.93 o 5 13 0 9.77 -10.61 10.61 o 6 13 0 60.93 59.98 14.06 o 7 13 0 8.76 6.80 13.56 o 0 14 0 112.43 117.50 21.23 o 1 14 0 1127.50 1167.13 37.54 o 2 14 0 1969.33 1988.86 68.44 o 3 14 0 370.04 382.56 25.10 o 4 14 0 3070.77 3135.78 67.25 o 5 14 0 569.06 588.76 45.85 o 6 14 0 0.04 0.92 12.92 o 1 15 0 1717.20 1757.64 54.02 o 2 15 0 442.27 453.67 34.95 o 3 15 0 0.72 -0.34 13.24 o 4 15 0 660.06 774.94 40.17 o 5 15 0 596.70 641.96 72.66 o 0 16 0 128.53 308.32 39.11 o 1 16 0 31.54 56.88 16.20 o 2 16 0 75.27 33.83 15.61 o 3 16 0 1.79 -11.83 11.83 o -12 1 1 3743.66 3784.52 83.59 o -11 1 1 977.60 995.02 29.34 o -10 1 1 574.58 602.00 19.43 o -9 1 1 17.65 8.78 6.76 o -8 1 1 363.73 339.09 12.95 o -7 1 1 4128.50 4283.24 48.83 o -6 1 1 14674.00 14072.14 122.33 o -5 1 1 390.61 484.40 9.64 o -4 1 1 4131.44 4263.21 37.57 o -3 1 1 10465.41 10415.99 73.02 o -2 1 1 3661.91 3493.18 81.00 o 1 1 1 8685.03 9283.95 73.59 o 2 1 1 7545.08 7059.03 73.18 o 3 1 1 399.80 388.49 9.55 o 4 1 1 84.54 93.78 4.75 o 5 1 1 19762.87 20769.38 232.10 o 6 1 1 3301.17 3524.37 41.70 o 7 1 1 5644.74 5567.62 65.57 o 8 1 1 3056.67 3139.72 48.42 o 9 1 1 96.82 107.44 11.89 o 10 1 1 391.99 342.23 23.68 o 11 1 1 2474.54 2664.79 67.76 o 12 1 1 14.46 30.48 18.97 o -12 2 1 5.42 2.66 14.92 o -11 2 1 322.75 274.54 19.03 o -10 2 1 2751.44 2933.27 45.88 o -9 2 1 7578.73 7910.50 84.12 o -8 2 1 635.25 558.71 16.71 o -7 2 1 6359.48 6646.29 69.01 o -6 2 1 1122.19 1061.44 16.61 o -5 2 1 46.18 15.15 3.50 o -4 2 1 14052.29 14212.66 305.21 o -3 2 1 27833.46 28123.38 497.57 o -2 2 1 706.25 743.48 8.12 o -1 2 1 28047.99 25463.60 517.67 o 0 2 1 6559.03 5646.79 100.84 o 1 2 1 104.51 47.82 2.04 o 2 2 1 7908.58 7802.19 52.88 o 3 2 1 6949.66 7456.78 131.47 o 4 2 1 7311.79 7223.70 105.25 o 5 2 1 14987.24 14799.21 196.71 o 6 2 1 618.11 533.22 15.37 o 7 2 1 672.71 673.11 18.65 o 8 2 1 5515.59 5792.76 70.32 o 9 2 1 558.50 568.48 21.36 o 10 2 1 3483.25 3568.43 63.41 o 11 2 1 1785.33 1819.58 54.93 o -12 3 1 12.12 9.91 12.44 o -11 3 1 127.42 94.03 13.83 o -10 3 1 6.22 1.12 8.57 o -9 3 1 96.46 88.68 9.04 o -8 3 1 757.30 780.91 18.18 o -7 3 1 8213.23 8380.39 111.07 o -6 3 1 506.59 435.60 12.10 o -5 3 1 521.67 451.46 15.91 o -4 3 1 752.37 839.37 12.21 o -3 3 1 35.44 19.86 3.11 o -2 3 1 124.64 139.46 4.23 o -1 3 1 1363.91 917.21 8.19 o 0 3 1 1739.66 1643.78 12.99 o 1 3 1 3976.96 4374.20 31.18 o 2 3 1 1031.42 1133.81 12.80 o 3 3 1 286.75 149.43 5.51 o 4 3 1 6737.76 6930.85 65.08 o 5 3 1 1009.69 1026.56 24.77 o 6 3 1 370.85 372.13 16.42 o 7 3 1 1316.94 1351.43 27.30 o 8 3 1 2383.45 2443.84 39.30 o 9 3 1 268.08 225.52 16.73 o 10 3 1 180.40 173.74 21.69 o 11 3 1 0.79 17.46 15.32 o -12 4 1 74.48 50.90 14.48 o -11 4 1 1101.96 1078.31 36.19 o -10 4 1 918.35 949.94 32.94 o -9 4 1 2547.48 2593.32 46.89 o -8 4 1 56.93 57.42 8.69 o -7 4 1 7697.47 8301.24 205.61 o -6 4 1 56.80 57.77 5.94 o -5 4 1 1783.23 1661.33 22.56 o -4 4 1 3138.99 3110.66 33.40 o -3 4 1 10234.62 10115.82 77.88 o -2 4 1 2.67 9.73 2.34 o -1 4 1 2577.77 2832.63 20.15 o 0 4 1 208.92 163.44 3.75 o 1 4 1 2875.98 2580.07 19.91 o 2 4 1 12.18 8.19 2.23 o 3 4 1 5511.54 5430.02 52.49 o 4 4 1 1379.78 1250.07 18.81 o 5 4 1 3124.70 3219.05 37.16 o 6 4 1 1131.27 1062.76 31.53 o 7 4 1 16.87 7.91 6.55 o 8 4 1 1041.26 1167.82 34.35 o 9 4 1 651.08 680.72 25.94 o 10 4 1 2587.85 2632.10 56.42 o 11 4 1 340.67 365.77 28.56 o -12 5 1 2263.64 2499.48 72.38 o -11 5 1 694.38 758.17 29.92 o -10 5 1 261.38 243.31 17.46 o -9 5 1 83.23 118.99 17.36 o -8 5 1 0.22 4.20 6.60 o -7 5 1 6581.00 6821.45 97.55 o -6 5 1 15875.03 15837.85 139.55 o -5 5 1 1297.55 1130.66 18.48 o -4 5 1 7339.16 7830.17 75.87 o -3 5 1 1019.41 984.13 15.22 o -2 5 1 662.96 569.00 8.48 o -1 5 1 12870.34 12585.96 85.61 o 0 5 1 11413.57 11042.45 71.43 o 1 5 1 2005.01 1922.41 17.98 o 2 5 1 11521.71 10913.33 87.51 o 3 5 1 1525.61 1383.17 18.71 o 4 5 1 5336.62 5436.78 57.45 o 5 5 1 12581.31 12971.77 116.55 o 6 5 1 2662.08 2829.55 37.55 o 7 5 1 3809.21 3744.83 51.14 o 8 5 1 2229.92 2380.12 109.70 o 9 5 1 147.56 144.77 18.76 o 10 5 1 424.63 425.46 25.61 o 11 5 1 1253.94 1389.04 74.21 o -12 6 1 55.74 52.93 18.97 o -11 6 1 1087.13 1112.87 39.73 o -10 6 1 321.59 333.48 20.32 o -9 6 1 1253.06 1199.67 31.60 o -8 6 1 1098.17 1106.57 27.05 o -7 6 1 83.60 90.44 9.13 o -6 6 1 4373.44 4443.39 49.22 o -5 6 1 6465.78 6037.92 56.94 o -4 6 1 452.07 337.64 10.79 o -3 6 1 1111.55 1078.98 15.03 o -2 6 1 4249.96 3929.78 34.11 o -1 6 1 6.60 1.12 2.67 o 0 6 1 7983.80 7622.92 56.57 o 1 6 1 3173.68 2822.63 27.73 o 2 6 1 1744.83 1585.50 20.40 o 3 6 1 67.55 38.78 4.86 o 4 6 1 1520.70 1513.66 22.45 o 5 6 1 271.77 263.67 11.84 o 6 6 1 6939.16 6787.21 77.13 o 7 6 1 1965.52 1826.22 53.62 o 8 6 1 20.49 14.71 13.43 o 9 6 1 611.50 654.56 38.21 o 10 6 1 11.68 4.71 12.51 o 11 6 1 399.75 419.94 34.18 o -11 7 1 300.72 296.56 24.07 o -10 7 1 1258.88 1376.61 36.45 o -9 7 1 64.63 41.15 10.86 o -8 7 1 1629.39 1827.59 98.52 o -7 7 1 186.81 199.60 16.71 o -6 7 1 6967.25 7085.16 75.22 o -5 7 1 152.16 109.32 7.90 o -4 7 1 8964.26 9254.27 78.55 o -3 7 1 6136.42 5989.57 53.37 o -2 7 1 8378.83 7729.22 63.40 o -1 7 1 1587.21 1866.30 20.18 o 0 7 1 2547.25 2818.37 27.70 o 1 7 1 1210.67 1047.96 16.15 o 2 7 1 5215.05 5893.31 57.40 o 3 7 1 8961.33 8778.30 97.98 o 4 7 1 3546.87 3251.75 39.63 o 5 7 1 3759.81 3755.06 44.08 o 6 7 1 406.66 414.25 23.14 o 7 7 1 3707.22 3916.85 118.41 o 8 7 1 52.73 83.34 12.95 o 9 7 1 1245.97 1368.26 45.04 o 10 7 1 630.69 661.54 34.29 o -11 8 1 82.86 108.09 26.63 o -10 8 1 473.13 473.51 35.33 o -9 8 1 2536.51 2741.73 52.54 o -8 8 1 1.62 7.94 9.45 o -7 8 1 508.94 507.85 21.10 o -6 8 1 41.30 28.52 9.22 o -5 8 1 29.63 37.66 9.11 o -4 8 1 4300.56 4324.87 55.04 o -3 8 1 4266.38 4325.97 61.26 o -2 8 1 3814.45 3859.64 38.23 o -1 8 1 5591.08 5594.18 49.22 o 0 8 1 396.58 433.69 9.93 o 1 8 1 12.37 12.75 4.18 o 2 8 1 7395.13 7464.94 67.97 o 3 8 1 2599.95 2693.70 34.89 o 4 8 1 2481.57 2489.54 37.90 o 5 8 1 3864.12 4067.06 140.16 o 6 8 1 18.95 15.77 9.30 o 7 8 1 24.54 24.62 13.75 o 8 8 1 1051.26 1022.00 35.98 o 9 8 1 22.39 20.43 13.05 o 10 8 1 1214.98 1405.65 46.33 o -11 9 1 499.83 483.83 34.42 o -10 9 1 522.52 540.17 34.42 o -9 9 1 47.21 12.79 13.65 o -8 9 1 1881.05 1882.88 45.42 o -7 9 1 1718.15 1693.12 36.92 o -6 9 1 325.20 369.87 21.83 o -5 9 1 993.39 1107.14 51.71 o -4 9 1 1036.05 1325.02 67.68 o -3 9 1 1874.25 1823.06 25.08 o -2 9 1 13630.88 13437.31 109.77 o -1 9 1 7951.24 7820.00 68.06 o 0 9 1 1206.65 1160.65 21.85 o 1 9 1 936.90 978.58 20.04 o 2 9 1 58.58 37.56 8.40 o 3 9 1 3750.95 3977.82 85.41 o 4 9 1 4165.84 4106.79 55.12 o 5 9 1 594.55 553.97 26.93 o 6 9 1 89.74 59.27 16.57 o 7 9 1 9.91 5.89 10.49 o 8 9 1 568.89 579.88 33.68 o 9 9 1 1584.30 1562.28 51.71 o 10 9 1 689.45 650.20 38.94 o -10 10 1 113.46 109.16 19.62 o -9 10 1 453.49 456.74 30.68 o -8 10 1 941.83 918.04 35.36 o -7 10 1 1673.63 1778.34 54.98 o -6 10 1 1505.12 1534.28 33.00 o -5 10 1 5246.47 5448.78 72.08 o -4 10 1 0.21 5.87 7.02 o -3 10 1 273.35 302.96 11.30 o -2 10 1 6124.09 6379.69 92.97 o -1 10 1 1863.08 1924.83 37.49 o 0 10 1 4089.53 4295.09 57.50 o 1 10 1 11784.89 12048.88 110.17 o 2 10 1 74.99 75.60 9.61 o 3 10 1 247.25 253.44 19.35 o 4 10 1 1186.80 1254.60 32.04 o 5 10 1 131.99 115.55 15.77 o 6 10 1 4367.08 4454.43 75.03 o 7 10 1 2587.36 2586.76 58.60 o 8 10 1 409.47 363.81 27.54 o 9 10 1 191.01 151.33 21.35 o -9 11 1 21.58 12.90 13.89 o -8 11 1 335.59 335.20 24.90 o -7 11 1 121.91 72.26 14.66 o -6 11 1 1264.26 1300.06 38.43 o -5 11 1 31.29 15.17 10.11 o -4 11 1 1649.00 1579.92 40.44 o -3 11 1 663.77 846.15 26.22 o -2 11 1 675.15 748.68 32.02 o -1 11 1 795.88 781.25 38.55 o 0 11 1 1279.38 1204.49 31.48 o 1 11 1 23.49 41.88 10.58 o 2 11 1 1190.86 1212.51 44.87 o 3 11 1 429.77 487.73 22.23 o 4 11 1 185.26 207.23 16.82 o 5 11 1 1222.98 1134.38 35.44 o 6 11 1 364.25 310.45 23.23 o 7 11 1 329.07 314.28 23.94 o 8 11 1 98.33 116.78 17.63 o -9 12 1 84.65 89.05 24.10 o -8 12 1 78.86 90.85 16.66 o -7 12 1 128.25 173.36 19.59 o -6 12 1 806.90 680.87 30.27 o -5 12 1 1074.35 1084.39 35.22 o -4 12 1 582.63 519.46 26.88 o -3 12 1 84.22 83.77 15.36 o -2 12 1 752.13 828.39 49.08 o -1 12 1 141.57 162.10 23.59 o 0 12 1 882.15 926.01 38.50 o 1 12 1 2976.51 2890.75 57.91 o 2 12 1 175.35 120.11 14.42 o 3 12 1 10.39 38.37 11.51 o 4 12 1 35.81 32.28 12.19 o 5 12 1 37.57 21.29 12.26 o 6 12 1 1256.06 1176.10 39.46 o 7 12 1 759.65 732.46 33.61 o 8 12 1 31.16 -11.27 13.29 o -8 13 1 2872.97 3093.32 71.37 o -7 13 1 371.46 415.13 27.17 o -6 13 1 4.76 -8.65 11.94 o -5 13 1 492.47 510.27 28.00 o -4 13 1 908.07 1010.59 31.40 o -3 13 1 1433.06 1459.09 40.83 o -2 13 1 5390.26 5515.52 94.05 o -1 13 1 137.01 152.50 20.02 o 0 13 1 386.00 360.17 25.95 o 1 13 1 1448.90 1584.15 72.68 o 2 13 1 161.98 139.51 20.12 o 3 13 1 3250.46 3393.84 70.93 o 4 13 1 2350.36 2522.61 57.82 o 5 13 1 1.04 -7.27 11.29 o 6 13 1 81.84 72.28 15.93 o 7 13 1 297.35 318.43 25.54 o -7 14 1 136.58 87.19 18.04 o -6 14 1 45.84 59.89 15.68 o -5 14 1 764.35 854.46 35.86 o -4 14 1 2.00 22.41 11.41 o -3 14 1 79.07 65.13 15.24 o -2 14 1 23.06 27.00 15.96 o -1 14 1 87.23 67.05 14.73 o 0 14 1 555.68 692.65 36.21 o 1 14 1 556.01 643.74 40.50 o 2 14 1 28.02 53.18 14.42 o 3 14 1 1.26 -1.32 12.90 o 4 14 1 543.46 580.27 31.59 o 5 14 1 4.84 -3.25 12.69 o 6 14 1 442.80 561.92 32.07 o -6 15 1 0.95 -11.73 13.92 o -5 15 1 262.89 288.56 24.54 o -4 15 1 606.31 631.65 33.12 o -3 15 1 415.49 372.48 25.94 o -2 15 1 1107.00 1076.35 37.77 o -1 15 1 3.74 -11.60 11.60 o 0 15 1 84.89 95.08 16.80 o 1 15 1 224.68 192.06 20.35 o 2 15 1 21.21 26.15 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2897.26 2992.62 52.05 o -4 11 2 759.35 709.74 24.53 o -3 11 2 211.20 203.24 19.30 o -2 11 2 37.51 24.74 11.86 o -1 11 2 971.30 928.38 24.15 o 0 11 2 5504.03 5795.83 72.92 o 1 11 2 901.46 843.51 38.23 o 2 11 2 1060.59 1013.70 55.70 o 3 11 2 619.18 711.10 39.86 o 4 11 2 38.92 25.31 10.31 o 5 11 2 516.14 543.06 35.64 o 6 11 2 3242.21 3186.03 67.44 o 7 11 2 91.23 54.26 15.40 o 8 11 2 727.63 752.87 37.15 o -9 12 2 1632.83 1691.27 50.61 o -8 12 2 1434.40 1650.29 49.39 o -7 12 2 239.04 150.59 17.98 o -6 12 2 328.89 328.43 22.81 o -5 12 2 550.12 467.16 25.74 o -4 12 2 285.46 251.76 19.04 o -3 12 2 3295.50 3537.94 89.25 o -2 12 2 898.17 1029.42 32.49 o -1 12 2 1959.14 2006.72 50.20 o 0 12 2 1419.11 1425.18 60.92 o 1 12 2 1226.90 1188.53 34.99 o 2 12 2 88.62 108.34 14.45 o 3 12 2 2199.68 2277.70 51.78 o 4 12 2 23.95 30.18 11.43 o 5 12 2 1943.41 1916.30 51.87 o 6 12 2 258.39 249.84 25.15 o 7 12 2 76.69 35.37 15.18 o -8 13 2 19.94 21.62 14.59 o -7 13 2 210.36 152.63 18.77 o -6 13 2 89.67 61.89 16.37 o -5 13 2 77.98 75.09 14.46 o -4 13 2 179.49 214.11 19.56 o -3 13 2 41.16 34.35 13.16 o -2 13 2 160.41 99.19 15.22 o -1 13 2 215.72 184.52 16.80 o 0 13 2 546.48 502.59 33.11 o 1 13 2 29.38 0.55 10.93 o 2 13 2 43.06 71.45 13.64 o 3 13 2 182.25 175.84 21.71 o 4 13 2 562.54 527.72 28.67 o 5 13 2 83.78 67.22 15.08 o 6 13 2 0.23 -0.02 13.67 o -7 14 2 25.19 -1.39 12.99 o -6 14 2 124.60 113.95 17.89 o -5 14 2 154.85 193.22 19.99 o -4 14 2 177.42 162.22 18.29 o -3 14 2 3695.59 3876.67 75.84 o -2 14 2 2305.21 2291.52 54.26 o -1 14 2 430.20 383.77 30.64 o 0 14 2 167.60 185.59 19.64 o 1 14 2 223.26 252.32 21.15 o 2 14 2 860.71 850.67 34.06 o 3 14 2 2859.71 2987.97 65.37 o 4 14 2 147.86 115.62 19.37 o 5 14 2 647.31 594.52 32.38 o -6 15 2 1678.25 1827.07 70.77 o -5 15 2 1391.57 1556.01 62.72 o -4 15 2 77.17 61.13 16.46 o -3 15 2 128.26 73.94 16.18 o -2 15 2 65.07 48.12 14.59 o -1 15 2 194.47 256.46 21.78 o 0 15 2 2521.70 2792.43 62.38 o 1 15 2 555.86 576.58 30.50 o 2 15 2 483.01 476.35 25.23 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1320.59 1348.75 54.58 o -12 2 3 2.53 -8.78 8.78 o -11 2 3 1505.94 1571.79 30.71 o -10 2 3 1842.57 1790.86 30.36 o -9 2 3 1271.57 1276.07 23.52 o -8 2 3 28986.13 29334.88 273.25 o -7 2 3 2311.90 2139.35 29.45 o -6 2 3 26.27 50.65 4.74 o -5 2 3 5260.69 5301.35 46.46 o -4 2 3 10109.49 9680.36 76.38 o -3 2 3 72536.91 76776.76 606.45 o -2 2 3 31243.94 32920.79 244.20 o -1 2 3 3379.61 3133.22 35.52 o 0 2 3 3701.01 4420.31 33.37 o 1 2 3 867.99 955.26 10.55 o 2 2 3 1746.16 1837.88 19.15 o 3 2 3 32329.10 31817.95 260.79 o 4 2 3 23605.39 24349.06 311.92 o 5 2 3 98.87 96.88 7.41 o 6 2 3 4417.06 4193.35 56.70 o 7 2 3 49.33 54.63 8.80 o 8 2 3 284.38 250.63 16.93 o 9 2 3 4580.67 4701.62 78.04 o 10 2 3 2074.22 2284.07 62.17 o -13 3 3 84.33 89.05 15.30 o -12 3 3 56.10 25.01 10.92 o -11 3 3 11.56 26.40 9.29 o -10 3 3 96.07 90.14 9.28 o -9 3 3 212.69 213.83 12.33 o -8 3 3 1507.02 1510.60 27.32 o -7 3 3 101.21 115.73 7.94 o -6 3 3 2020.02 2056.50 33.69 o -5 3 3 1612.41 1566.45 20.34 o -4 3 3 1762.03 1774.37 19.36 o -3 3 3 6732.96 6341.92 49.39 o -2 3 3 6553.23 6479.45 50.55 o -1 3 3 32.57 2.66 2.24 o 0 3 3 7043.83 6267.77 48.93 o 1 3 3 49.55 121.51 4.20 o 2 3 3 1.09 2.39 2.11 o 3 3 3 1987.92 2157.83 29.18 o 4 3 3 953.88 856.51 19.07 o 5 3 3 3366.50 3325.08 48.52 o 6 3 3 943.56 869.49 22.04 o 7 3 3 1270.02 1196.73 27.50 o 8 3 3 14.62 -2.35 8.59 o 9 3 3 35.31 36.69 13.32 o 10 3 3 17.12 11.19 16.09 o -13 4 3 675.32 606.56 29.27 o -12 4 3 1099.60 1098.00 36.30 o -11 4 3 45.75 27.97 10.11 o -10 4 3 3064.74 3026.61 48.05 o -9 4 3 76.63 70.46 8.63 o -8 4 3 9935.89 10303.13 119.00 o -7 4 3 930.82 939.25 18.54 o -6 4 3 5026.31 4835.20 52.91 o -5 4 3 30.41 40.62 4.30 o -4 4 3 4277.89 3997.44 35.72 o -3 4 3 6806.83 7617.17 53.47 o -2 4 3 12172.37 12802.81 88.65 o -1 4 3 89.86 61.67 3.39 o 0 4 3 940.31 592.51 9.93 o 1 4 3 309.34 445.27 7.21 o 2 4 3 805.69 622.20 11.48 o 3 4 3 5048.69 5132.35 71.86 o 4 4 3 8003.76 7993.01 89.07 o 5 4 3 367.96 324.74 24.78 o 6 4 3 1598.31 1676.55 29.42 o 7 4 3 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