#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:31:35 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181247 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/25/2232554.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232554_Fobs loop_ _publ_author_name 'Wang, Hsiao-Fen' 'Zeng, Weng-Feng' 'Lee, Gene-Hsiang' 'Yih, Kuang-Hway' _publ_section_title ; trans-Bromido(pyrimidinyl-\kC^5^)bis(triphenylphosphane-\kP)palladium(II) ; _journal_coeditor_code BG2434 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1820 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.748 _cell_angle_gamma 90.000 _cell_length_a 15.0953 _cell_length_b 12.0379 _cell_length_c 19.8066 _exptl_crystal_F_000 1592.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file bg2434Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ic15222 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 352.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7130.07 1.45 8.53 o 2 0 0 111594.76 125165.54 6868.13 o 3 0 0 1716.45 2566.05 323.88 o 4 0 0 3043.68 4021.63 417.82 o 5 0 0 4104.59 4236.54 287.90 o 6 0 0 29117.67 30137.73 1042.95 o 7 0 0 14564.92 15461.01 982.24 o 8 0 0 18856.39 18140.12 888.00 o 9 0 0 22912.21 21176.59 1761.18 o 10 0 0 13.40 115.06 97.52 o 11 0 0 27193.47 25194.49 1802.54 o 12 0 0 6550.57 6160.16 625.33 o 13 0 0 1041.35 1441.96 254.17 o 14 0 0 269.56 44.85 136.26 o 15 0 0 1748.27 1234.44 300.36 o 16 0 0 42.79 -11.62 157.65 o 17 0 0 4550.64 4231.16 1325.52 o 18 0 0 155.00 342.08 204.52 o 1 1 0 18294.38 19374.36 542.33 o 2 1 0 3280.59 2913.47 89.22 o 3 1 0 3357.32 3285.76 130.35 o 4 1 0 1.59 10.64 23.00 o 5 1 0 265.36 355.43 51.20 o 6 1 0 6004.43 6211.77 256.32 o 7 1 0 15711.32 14653.09 436.80 o 8 1 0 2826.60 2839.59 140.48 o 9 1 0 5887.50 5831.26 235.29 o 10 1 0 9539.80 8531.54 376.35 o 11 1 0 59.60 287.43 102.20 o 12 1 0 4140.49 3689.54 269.90 o 13 1 0 4.78 -52.40 77.83 o 14 1 0 1048.99 930.00 155.62 o 15 1 0 670.69 351.03 130.93 o 16 1 0 2364.05 2122.34 239.95 o 17 1 0 3.14 -97.81 102.65 o 18 1 0 1372.32 1119.38 277.12 o 0 2 0 528.51 633.28 50.94 o 1 2 0 600.55 769.43 43.39 o 2 2 0 9601.66 10546.27 313.36 o 3 2 0 3143.02 2956.97 103.07 o 4 2 0 1489.15 1665.15 72.12 o 5 2 0 159.54 199.17 34.34 o 6 2 0 117.27 233.44 46.77 o 7 2 0 530.11 474.77 59.55 o 8 2 0 632.19 517.28 81.26 o 9 2 0 2312.27 2468.75 200.12 o 10 2 0 121.41 151.63 57.15 o 11 2 0 1088.38 965.09 141.05 o 12 2 0 123.25 -22.49 84.72 o 13 2 0 276.70 125.11 90.22 o 14 2 0 66.56 110.01 101.60 o 15 2 0 20.64 36.75 102.56 o 16 2 0 195.56 225.64 130.19 o 17 2 0 175.24 270.47 129.14 o 18 2 0 271.99 338.71 154.52 o 1 3 0 60501.34 63676.34 1769.79 o 2 3 0 7261.33 6507.58 211.24 o 3 3 0 90.92 58.34 24.91 o 4 3 0 4747.34 4564.14 152.84 o 5 3 0 913.20 1005.36 63.96 o 6 3 0 2717.04 2908.81 247.85 o 7 3 0 16510.62 16134.97 486.55 o 8 3 0 9831.36 10058.96 374.39 o 9 3 0 4929.90 4853.07 384.03 o 10 3 0 15399.35 14608.54 472.51 o 11 3 0 354.72 124.89 92.99 o 12 3 0 3480.26 3374.94 258.27 o 13 3 0 536.58 451.66 134.45 o 14 3 0 186.45 218.54 119.75 o 15 3 0 302.44 294.47 130.94 o 16 3 0 2051.50 1648.22 217.04 o 17 3 0 283.56 308.79 148.84 o 18 3 0 1384.83 1367.51 252.86 o 0 4 0 35092.29 35170.18 1412.37 o 1 4 0 38112.60 38804.42 1270.84 o 2 4 0 3543.23 3413.79 134.47 o 3 4 0 6557.97 6332.24 258.45 o 4 4 0 5112.29 4827.42 165.24 o 5 4 0 2863.53 2938.53 127.25 o 6 4 0 355.94 400.61 48.45 o 7 4 0 306.31 472.69 53.23 o 8 4 0 1834.65 1852.19 98.68 o 9 4 0 4666.53 4839.04 246.92 o 10 4 0 206.47 202.90 71.70 o 11 4 0 452.52 502.89 103.03 o 12 4 0 3497.03 3695.31 326.65 o 13 4 0 745.63 697.31 187.17 o 14 4 0 1153.55 1499.39 197.80 o 15 4 0 573.25 302.67 135.40 o 16 4 0 353.57 404.98 198.35 o 17 4 0 62.30 47.97 198.33 o 1 5 0 14492.02 14738.90 450.20 o 2 5 0 189.41 225.96 81.64 o 3 5 0 14439.83 14822.44 459.34 o 4 5 0 2395.38 2387.71 188.13 o 5 5 0 15587.83 15529.60 448.18 o 6 5 0 9291.65 9078.21 288.48 o 7 5 0 318.72 359.96 69.97 o 8 5 0 4678.29 4464.42 184.23 o 9 5 0 1239.72 1477.72 138.54 o 10 5 0 4344.13 3898.25 230.67 o 11 5 0 518.80 500.99 100.15 o 12 5 0 3910.67 3696.73 307.32 o 13 5 0 563.98 525.14 149.18 o 14 5 0 2447.30 2479.75 273.80 o 15 5 0 336.18 401.73 246.91 o 16 5 0 1026.37 1203.93 213.14 o 17 5 0 335.66 336.95 173.68 o 0 6 0 9901.88 7712.74 372.80 o 1 6 0 11710.86 11498.76 365.78 o 2 6 0 12201.04 10986.03 357.23 o 3 6 0 17692.33 17550.21 542.23 o 4 6 0 5490.19 5893.74 283.52 o 5 6 0 1667.49 1680.25 127.84 o 6 6 0 6990.95 7067.40 246.07 o 7 6 0 4860.10 4901.85 284.65 o 8 6 0 3374.87 3265.16 162.81 o 9 6 0 9297.70 9333.17 377.89 o 10 6 0 1163.03 1567.37 287.44 o 11 6 0 8098.42 8325.16 367.30 o 12 6 0 224.91 286.14 119.95 o 13 6 0 610.51 766.69 159.38 o 14 6 0 304.38 116.83 134.32 o 15 6 0 751.07 597.13 175.91 o 16 6 0 65.63 -204.93 136.62 o 17 6 0 1851.32 2007.32 311.94 o 1 7 0 602.75 416.55 55.12 o 2 7 0 15054.66 14484.69 463.62 o 3 7 0 322.79 264.22 54.44 o 4 7 0 0.37 55.26 44.45 o 5 7 0 53.20 45.83 46.73 o 6 7 0 946.57 910.85 86.50 o 7 7 0 8134.91 7958.70 302.27 o 8 7 0 383.62 518.86 74.26 o 9 7 0 8026.10 7981.52 350.03 o 10 7 0 4275.46 4688.42 269.94 o 11 7 0 302.92 373.81 100.85 o 12 7 0 906.44 788.38 125.47 o 13 7 0 174.91 120.11 129.32 o 14 7 0 71.04 -170.77 116.55 o 15 7 0 684.48 886.69 180.31 o 16 7 0 618.36 458.48 262.59 o 0 8 0 416.99 419.85 86.15 o 1 8 0 3616.48 3479.08 163.46 o 2 8 0 3985.12 4323.21 191.70 o 3 8 0 6.66 58.22 46.50 o 4 8 0 6908.54 6524.18 258.44 o 5 8 0 2188.00 2465.92 155.55 o 6 8 0 1174.25 1337.05 169.81 o 7 8 0 1722.22 2080.22 140.76 o 8 8 0 37.93 57.26 75.73 o 9 8 0 1040.25 1048.28 131.42 o 10 8 0 323.35 406.01 102.65 o 11 8 0 3640.11 3583.80 376.69 o 12 8 0 1095.47 1005.02 165.84 o 13 8 0 2173.68 2340.29 352.80 o 14 8 0 33.67 83.31 417.59 o 15 8 0 1594.28 1766.96 404.66 o 1 9 0 3450.64 3513.26 174.77 o 2 9 0 981.25 1281.09 118.87 o 3 9 0 3378.24 3409.90 177.87 o 4 9 0 1518.87 1628.00 126.32 o 5 9 0 893.06 999.12 125.17 o 6 9 0 794.45 833.58 107.54 o 7 9 0 1372.93 1469.33 145.11 o 8 9 0 1015.97 1292.15 352.39 o 9 9 0 125.28 -14.25 101.70 o 10 9 0 2592.34 2622.04 261.45 o 11 9 0 31.13 -77.62 115.05 o 12 9 0 1377.58 1497.32 211.00 o 13 9 0 538.49 740.68 254.18 o 14 9 0 1150.56 805.90 281.84 o 15 9 0 502.36 720.50 444.31 o 0 10 0 3653.36 3240.07 446.02 o 1 10 0 1721.63 1512.33 220.90 o 2 10 0 0.55 -27.82 74.93 o 3 10 0 2152.06 2247.31 189.91 o 4 10 0 2173.51 2343.16 198.50 o 5 10 0 23.70 81.04 77.61 o 6 10 0 9.62 23.10 75.34 o 7 10 0 665.24 472.25 126.42 o 8 10 0 67.49 79.72 106.07 o 9 10 0 17.04 93.27 114.11 o 10 10 0 415.65 283.01 141.94 o 11 10 0 194.14 112.90 270.91 o 12 10 0 3089.42 2694.47 292.39 o 13 10 0 440.10 189.60 220.74 o 14 10 0 100.73 -143.39 231.13 o 1 11 0 5466.12 4966.34 412.98 o 2 11 0 153.70 66.44 135.23 o 3 11 0 13040.95 12151.08 661.55 o 4 11 0 3057.29 3228.27 325.80 o 5 11 0 7060.28 7003.67 487.20 o 6 11 0 11432.04 10008.60 809.63 o 7 11 0 226.85 352.62 126.11 o 8 11 0 3284.36 3133.83 286.79 o 9 11 0 37.43 209.07 129.18 o 10 11 0 737.61 726.42 156.65 o 11 11 0 528.26 664.05 171.92 o 12 11 0 824.46 850.13 220.52 o 13 11 0 15.56 19.10 204.16 o 0 12 0 206.08 224.49 224.80 o 1 12 0 4.23 -48.45 214.75 o 2 12 0 2914.10 2373.37 345.30 o 3 12 0 457.75 313.38 186.09 o 4 12 0 4869.18 4320.07 436.36 o 5 12 0 2432.24 2457.15 295.13 o 6 12 0 1802.31 1524.47 240.81 o 7 12 0 989.18 1354.87 502.49 o 8 12 0 655.53 1119.56 393.68 o 9 12 0 1742.76 2016.05 316.65 o 10 12 0 827.73 960.21 264.92 o 11 12 0 3682.87 4855.28 904.82 o 1 13 0 472.76 412.17 199.45 o 2 13 0 531.23 863.74 224.39 o 3 13 0 184.18 146.98 186.24 o 4 13 0 20.12 -39.30 134.40 o 5 13 0 11.04 -72.46 191.39 o 6 13 0 594.93 626.60 176.86 o 7 13 0 122.65 177.25 167.39 o 8 13 0 284.08 486.79 200.51 o 9 13 0 182.02 262.58 196.23 o 10 13 0 80.31 -46.47 222.39 o 0 14 0 302.09 522.04 286.65 o 1 14 0 816.65 734.78 263.83 o 2 14 0 1830.01 1720.37 483.41 o 3 14 0 825.86 697.34 212.40 o 4 14 0 3781.67 3784.49 399.49 o 5 14 0 2057.23 2489.30 322.78 o 6 14 0 1259.35 1172.54 194.49 o 7 14 0 2121.43 1917.65 897.34 o 8 14 0 250.32 -14.94 183.20 o 1 15 0 503.38 792.84 280.18 o 2 15 0 31.07 -230.35 323.34 o 3 15 0 3710.39 3168.57 400.37 o 4 15 0 567.64 707.98 235.09 o 5 15 0 2009.38 2252.52 319.73 o -18 1 1 36.08 -138.69 118.58 o -17 1 1 524.59 594.14 150.30 o -16 1 1 13.82 6.14 105.53 o -15 1 1 828.51 616.71 138.10 o -14 1 1 843.65 775.61 164.37 o -13 1 1 7028.07 6458.05 570.09 o -12 1 1 193.87 303.97 112.42 o -11 1 1 7216.45 6987.96 356.54 o -10 1 1 6244.61 6578.57 588.91 o -9 1 1 2265.33 2411.31 222.72 o -8 1 1 1429.46 1166.83 98.06 o -7 1 1 897.34 1043.34 76.65 o -6 1 1 2687.60 3109.76 209.55 o -5 1 1 37.29 151.94 33.30 o -4 1 1 21156.59 24101.05 806.10 o -3 1 1 572.52 476.93 55.02 o -2 1 1 64920.80 69246.36 1963.13 o -1 1 1 8353.85 8737.14 292.66 o 0 1 1 28633.91 22791.75 1283.38 o 1 1 1 24612.08 25007.25 718.29 o 2 1 1 2737.64 2533.69 158.64 o 3 1 1 39845.59 41925.45 1101.43 o 4 1 1 10653.62 11470.72 333.08 o 5 1 1 2837.86 2919.87 160.30 o 6 1 1 2730.87 2630.02 178.99 o 7 1 1 18758.83 18038.10 526.84 o 8 1 1 425.67 493.48 71.96 o 9 1 1 14514.19 13748.66 431.54 o 10 1 1 6079.51 5866.01 317.89 o 11 1 1 2679.87 2690.75 220.88 o 12 1 1 1481.58 1609.81 179.33 o 13 1 1 83.79 166.46 105.93 o 14 1 1 221.09 315.90 116.06 o 15 1 1 689.90 681.67 142.05 o 16 1 1 315.42 211.63 183.24 o 17 1 1 310.59 407.93 147.60 o 18 1 1 813.33 701.02 189.82 o -18 2 1 1591.46 1699.68 378.69 o -17 2 1 4.68 94.48 122.27 o -16 2 1 1411.42 1019.73 277.13 o -15 2 1 2.11 41.67 103.88 o -14 2 1 1047.55 1001.36 163.37 o -13 2 1 11.01 78.83 96.02 o -12 2 1 8125.99 7146.86 612.89 o -11 2 1 7106.69 6959.22 358.24 o -10 2 1 1443.01 1264.07 121.38 o -9 2 1 13065.51 12220.10 393.00 o -8 2 1 4456.77 4575.94 197.73 o -7 2 1 346.94 317.63 52.37 o -6 2 1 1298.87 1147.08 87.99 o -5 2 1 7732.59 9096.59 248.06 o -4 2 1 5646.06 5213.13 175.01 o -3 2 1 30812.06 32863.16 956.21 o -2 2 1 1619.35 1770.25 90.67 o -1 2 1 1789.01 1417.87 69.81 o 0 2 1 716.62 909.04 53.05 o 1 2 1 1032.99 1293.55 87.29 o 2 2 1 22039.72 24036.73 703.09 o 3 2 1 17878.13 18305.98 504.81 o 4 2 1 358.39 590.08 78.50 o 5 2 1 3547.60 3194.39 130.68 o 6 2 1 4595.99 4835.37 203.71 o 7 2 1 10281.05 9485.86 310.61 o 8 2 1 24710.63 22812.62 658.11 o 9 2 1 643.77 569.02 107.42 o 10 2 1 8535.49 7923.32 299.47 o 11 2 1 1246.14 1396.25 158.68 o 12 2 1 1668.08 1637.06 178.34 o 13 2 1 51.14 38.12 90.16 o 14 2 1 455.53 508.59 128.77 o 15 2 1 210.35 68.27 102.46 o 16 2 1 1408.64 1140.91 191.50 o 17 2 1 2195.99 2114.29 422.23 o 18 2 1 8.51 179.42 167.69 o -18 3 1 46.96 -42.15 143.24 o -17 3 1 162.70 177.71 139.99 o -16 3 1 129.11 110.52 126.94 o -15 3 1 575.80 442.88 140.15 o -14 3 1 421.39 270.48 121.58 o -13 3 1 479.51 325.94 114.92 o -12 3 1 161.15 247.27 102.04 o -11 3 1 12.39 -0.24 54.10 o -10 3 1 29.23 11.00 55.71 o -9 3 1 951.30 1146.09 106.30 o -8 3 1 977.00 1102.35 101.34 o -7 3 1 193.20 163.66 30.50 o -6 3 1 104.72 115.03 48.37 o -5 3 1 181.88 194.42 33.79 o -4 3 1 1019.70 1160.23 69.50 o -3 3 1 10921.77 11231.10 344.57 o -2 3 1 20116.61 22864.06 932.33 o -1 3 1 58.81 143.09 44.94 o 0 3 1 16262.56 18488.54 614.31 o 1 3 1 50956.26 55815.21 1796.54 o 2 3 1 1327.53 1352.85 80.47 o 3 3 1 3860.02 3557.47 144.65 o 4 3 1 2989.25 2856.25 164.72 o 5 3 1 288.63 524.27 52.95 o 6 3 1 107.00 185.28 45.62 o 7 3 1 296.50 391.64 52.10 o 8 3 1 314.26 237.59 59.28 o 9 3 1 353.00 396.69 121.92 o 10 3 1 495.47 480.95 81.10 o 11 3 1 3357.20 3166.54 294.66 o 12 3 1 127.92 17.81 88.87 o 13 3 1 997.49 880.68 157.22 o 14 3 1 329.42 350.49 132.12 o 15 3 1 682.90 557.89 142.06 o 16 3 1 13.49 111.19 125.11 o 17 3 1 77.13 26.32 126.47 o -18 4 1 1306.21 1761.95 265.06 o -17 4 1 61.63 -124.13 208.30 o -16 4 1 1762.24 1597.50 218.97 o -15 4 1 210.70 285.46 137.31 o -14 4 1 2774.20 2807.04 255.55 o -13 4 1 984.82 1321.62 177.80 o -12 4 1 8445.10 7725.03 494.85 o -11 4 1 6151.84 6137.49 279.66 o -10 4 1 3203.10 3185.83 197.76 o -9 4 1 13289.53 13262.79 468.32 o -8 4 1 243.51 295.04 46.19 o -7 4 1 6598.32 6231.50 211.02 o -6 4 1 105.42 56.26 31.94 o -5 4 1 9586.91 10055.48 300.28 o -4 4 1 226.33 230.78 48.19 o -3 4 1 17640.13 18507.51 552.38 o -2 4 1 6802.87 7325.40 241.79 o -1 4 1 83206.04 90581.75 2514.81 o 0 4 1 2580.21 2440.71 117.26 o 1 4 1 21687.66 24449.95 813.49 o 2 4 1 1950.66 1799.95 91.79 o 3 4 1 7560.37 8458.91 275.95 o 4 4 1 2118.96 2128.58 104.17 o 5 4 1 12718.58 12781.48 374.29 o 6 4 1 2323.53 2387.08 136.51 o 7 4 1 3740.33 3713.15 165.34 o 8 4 1 11275.08 10944.73 373.28 o 9 4 1 592.54 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10718.33 10153.36 318.02 o 7 5 1 8037.74 7984.59 264.81 o 8 5 1 79.09 180.24 99.07 o 9 5 1 9311.71 8965.94 364.47 o 10 5 1 8343.90 8108.06 345.62 o 11 5 1 1779.64 1576.27 152.93 o 12 5 1 2553.45 2554.07 255.77 o 13 5 1 26.95 64.50 119.28 o 14 5 1 21.59 -24.36 120.68 o 15 5 1 510.70 588.08 168.99 o 16 5 1 263.39 270.36 162.21 o 17 5 1 639.41 864.86 203.12 o -17 6 1 164.18 387.89 180.44 o -16 6 1 32.59 164.27 159.57 o -15 6 1 29.96 64.44 130.42 o -14 6 1 849.49 601.64 162.30 o -13 6 1 532.78 570.07 145.18 o -12 6 1 289.72 168.54 85.69 o -11 6 1 3418.13 3321.80 226.06 o -10 6 1 1296.91 1360.26 141.54 o -9 6 1 5556.96 5938.54 286.03 o -8 6 1 5405.05 5837.41 226.99 o -7 6 1 10.54 31.78 41.24 o -6 6 1 1456.62 1611.73 111.21 o -5 6 1 11262.70 10799.87 364.21 o -4 6 1 257.16 146.04 76.95 o -3 6 1 40.38 60.39 41.58 o -2 6 1 427.14 482.71 67.12 o -1 6 1 26.97 19.84 31.05 o 0 6 1 168.17 117.01 41.60 o 1 6 1 188.73 142.96 36.09 o 2 6 1 1551.70 1774.30 105.03 o 3 6 1 4451.29 4167.91 172.68 o 4 6 1 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