#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/25/2232586.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232586_Fobs loop_ _publ_author_name 'Rademeyer, M.' _publ_section_title ; Bis(3-methylanilinium) sulfate ; _journal_coeditor_code BT5698 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3172 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.819 _cell_angle_gamma 90.000 _cell_length_a 17.2168 _cell_length_b 15.0298 _cell_length_c 6.1283 _exptl_crystal_F_000 663.90 _reflns_d_resolution_high 0.6684 _[local]_cod_data_source_file bt5698Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' triclinic in P -1 C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 272.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 337.74 493.46 7.80 o 6 0 0 28.96 46.24 7.77 o 8 0 0 4635.60 4522.04 36.57 o 10 0 0 2944.81 3032.48 29.79 o 12 0 0 1461.88 1448.44 49.67 o 14 0 0 618.72 612.32 27.17 o 16 0 0 703.33 594.33 39.05 o 18 0 0 102.15 93.66 16.89 o 20 0 0 91.53 85.69 20.34 o 22 0 0 3.14 3.96 13.77 o 3 1 0 7026.51 7472.37 33.69 o 5 1 0 1250.19 1366.95 17.02 o 7 1 0 291.92 430.33 10.92 o 9 1 0 2429.95 2499.69 21.64 o 11 1 0 529.94 522.55 10.15 o 13 1 0 79.95 86.34 6.50 o 15 1 0 958.16 831.45 15.43 o 17 1 0 192.74 198.54 12.17 o 19 1 0 123.29 130.56 12.75 o 21 1 0 45.79 40.29 13.84 o 23 1 0 11.52 2.12 31.05 o 2 2 0 40.07 2.21 2.29 o 4 2 0 3067.60 3278.20 31.51 o 6 2 0 6690.22 7314.67 55.93 o 8 2 0 186.43 164.69 5.35 o 10 2 0 136.52 115.60 6.92 o 12 2 0 28.00 26.70 6.16 o 14 2 0 2.77 7.19 6.19 o 16 2 0 31.13 25.04 8.33 o 18 2 0 0.29 -2.54 8.67 o 20 2 0 9.36 19.71 11.49 o 22 2 0 47.22 31.74 17.94 o 1 3 0 2976.34 2733.71 516.50 o 3 3 0 14187.68 14302.38 71.29 o 5 3 0 7579.21 7728.48 25.92 o 7 3 0 169.63 152.45 5.02 o 9 3 0 5676.22 6078.17 30.38 o 11 3 0 486.13 512.54 10.45 o 13 3 0 537.79 517.66 11.66 o 15 3 0 51.13 40.23 7.90 o 17 3 0 126.01 114.76 10.04 o 19 3 0 285.37 299.87 13.17 o 21 3 0 22.06 20.07 15.05 o 23 3 0 6.23 -0.77 11.85 o 0 4 0 74224.92 66930.01 1488.12 o 2 4 0 98.63 159.44 3.91 o 4 4 0 11.37 12.60 2.76 o 6 4 0 8.26 8.36 3.06 o 8 4 0 3013.24 3146.49 21.09 o 10 4 0 1197.09 1166.24 14.66 o 12 4 0 452.44 407.71 10.07 o 14 4 0 526.12 569.31 12.84 o 16 4 0 203.52 182.48 9.64 o 18 4 0 157.50 147.86 11.91 o 20 4 0 193.31 205.91 15.44 o 22 4 0 0.56 5.47 22.06 o 1 5 0 872.75 722.00 6.02 o 3 5 0 1216.30 1383.83 9.35 o 5 5 0 408.97 455.56 7.08 o 7 5 0 464.70 583.30 9.07 o 9 5 0 84.61 70.26 4.89 o 11 5 0 376.37 380.27 15.91 o 13 5 0 595.81 545.33 12.26 o 15 5 0 1475.83 1324.89 19.76 o 17 5 0 108.15 114.21 11.53 o 19 5 0 15.72 25.45 11.70 o 21 5 0 43.76 33.40 16.55 o 0 6 0 285.98 286.47 8.06 o 2 6 0 3.17 3.39 1.71 o 4 6 0 3307.37 3415.36 22.10 o 6 6 0 6414.11 6629.83 72.14 o 8 6 0 332.22 338.39 7.85 o 10 6 0 69.52 82.36 5.98 o 12 6 0 158.03 141.31 7.10 o 14 6 0 115.61 139.54 8.44 o 16 6 0 124.15 112.64 10.87 o 18 6 0 4.15 3.74 8.00 o 20 6 0 26.48 24.33 15.42 o 22 6 0 184.68 202.06 26.23 o 1 7 0 20.43 40.34 3.47 o 3 7 0 88.94 106.16 3.45 o 5 7 0 3087.84 3475.72 17.36 o 7 7 0 20.12 12.70 3.76 o 9 7 0 1668.50 1720.78 23.46 o 11 7 0 501.49 532.48 12.26 o 13 7 0 161.27 181.46 9.05 o 15 7 0 12.32 7.53 8.40 o 17 7 0 105.57 121.41 12.42 o 19 7 0 179.04 180.44 15.82 o 21 7 0 265.06 328.86 21.20 o 0 8 0 222.55 202.47 8.10 o 2 8 0 89.58 122.90 3.65 o 4 8 0 0.13 2.82 2.58 o 6 8 0 922.74 970.71 10.98 o 8 8 0 605.67 643.46 9.31 o 10 8 0 193.05 188.97 6.18 o 12 8 0 4.56 -1.29 6.32 o 14 8 0 309.56 346.70 11.24 o 16 8 0 0.35 -1.10 4.01 o 18 8 0 191.60 187.09 14.08 o 20 8 0 323.68 351.00 19.35 o 22 8 0 2.98 2.51 37.12 o 1 9 0 140.15 95.76 4.93 o 3 9 0 169.80 197.87 4.77 o 5 9 0 62.49 59.15 3.39 o 7 9 0 177.52 171.97 5.30 o 9 9 0 533.20 514.65 9.04 o 11 9 0 122.29 113.50 7.87 o 13 9 0 980.11 987.63 16.88 o 15 9 0 568.59 518.20 13.86 o 17 9 0 2.31 2.74 11.14 o 19 9 0 8.12 -0.80 7.13 o 21 9 0 3.08 13.54 23.03 o 0 10 0 1495.60 1600.47 37.87 o 2 10 0 97.50 115.64 5.69 o 4 10 0 87.05 99.03 4.43 o 6 10 0 26.22 21.55 4.45 o 8 10 0 4.99 6.73 4.98 o 10 10 0 33.94 17.55 6.97 o 12 10 0 36.67 25.16 8.52 o 14 10 0 315.31 334.02 11.39 o 16 10 0 57.78 56.37 13.40 o 18 10 0 16.03 26.52 17.68 o 20 10 0 8.86 -4.11 29.09 o 1 11 0 44.94 61.26 5.70 o 3 11 0 7.03 5.66 4.28 o 5 11 0 670.01 692.47 10.17 o 7 11 0 0.12 0.58 4.30 o 9 11 0 126.01 110.62 8.62 o 11 11 0 302.00 344.47 12.68 o 13 11 0 100.32 104.68 12.29 o 15 11 0 21.09 42.68 14.32 o 17 11 0 63.49 63.26 18.49 o 19 11 0 31.61 26.78 23.28 o 21 11 0 180.62 197.78 61.98 o 0 12 0 123.53 114.97 8.99 o 2 12 0 329.93 317.39 9.03 o 4 12 0 402.18 373.25 9.84 o 6 12 0 2111.88 2154.76 25.16 o 8 12 0 0.12 -2.36 8.92 o 10 12 0 244.17 249.10 14.21 o 12 12 0 7.63 4.97 13.14 o 14 12 0 203.66 190.43 17.15 o 16 12 0 0.07 -9.98 18.92 o 18 12 0 83.96 58.24 29.51 o 1 13 0 175.04 176.15 7.64 o 3 13 0 166.64 159.64 7.64 o 5 13 0 37.88 32.49 7.44 o 7 13 0 189.55 199.11 13.05 o 9 13 0 818.18 812.19 23.61 o 11 13 0 8.41 9.84 11.80 o 13 13 0 168.09 165.94 31.44 o 15 13 0 83.38 64.65 21.07 o 17 13 0 0.53 14.97 24.96 o 19 13 0 9.92 8.20 48.87 o 0 14 0 303.72 299.09 14.10 o 2 14 0 459.29 462.53 11.64 o 4 14 0 29.29 26.09 7.50 o 6 14 0 69.58 53.10 13.21 o 8 14 0 1.70 -1.56 9.07 o 10 14 0 3.23 0.08 6.15 o 12 14 0 38.29 40.56 16.18 o 14 14 0 116.28 119.32 23.97 o 16 14 0 17.57 4.54 26.34 o 18 14 0 0.62 10.17 44.03 o 1 15 0 573.85 605.66 15.56 o 3 15 0 271.35 297.09 10.32 o 5 15 0 259.35 222.85 12.12 o 7 15 0 157.73 173.79 15.59 o 9 15 0 27.47 29.87 14.30 o 11 15 0 104.44 105.50 18.88 o 13 15 0 214.21 240.34 22.12 o 15 15 0 131.55 141.17 28.28 o 17 15 0 14.67 18.47 43.12 o 0 16 0 94.98 88.68 13.61 o 2 16 0 366.18 367.00 11.72 o 4 16 0 346.70 355.26 14.83 o 6 16 0 962.03 996.85 44.08 o 8 16 0 75.83 85.27 14.92 o 10 16 0 247.10 269.28 18.81 o 12 16 0 47.14 46.82 20.31 o 14 16 0 159.11 167.24 32.86 o 16 16 0 12.36 9.31 43.72 o 1 17 0 11.76 18.22 10.02 o 3 17 0 32.19 18.98 11.96 o 5 17 0 32.70 31.18 11.91 o 7 17 0 63.59 80.99 18.43 o 9 17 0 175.12 159.04 19.68 o 11 17 0 0.28 -5.47 21.16 o 13 17 0 0.11 -11.32 36.65 o 0 18 0 2.22 9.00 15.97 o 2 18 0 324.92 321.69 14.82 o 4 18 0 152.27 149.91 16.53 o 6 18 0 0.51 -2.70 15.95 o 8 18 0 12.26 14.86 30.59 o 10 18 0 102.82 108.96 24.29 o 12 18 0 117.45 141.87 30.52 o 1 19 0 229.15 242.80 17.34 o 3 19 0 170.13 177.19 17.93 o 5 19 0 86.67 96.62 32.42 o 7 19 0 210.76 195.59 39.53 o 9 19 0 19.51 28.49 25.96 o 11 19 0 34.57 38.94 43.56 o 0 20 0 50.16 34.57 32.55 o 2 20 0 40.57 49.31 18.17 o 4 20 0 44.32 53.80 19.69 o 6 20 0 63.21 77.97 25.81 o 8 20 0 12.21 -4.76 35.81 o 1 21 0 8.14 1.71 25.33 o 3 21 0 5.80 -7.54 17.10 o 5 21 0 23.03 15.22 30.50 o -23 1 1 253.67 266.96 20.57 o -21 1 1 86.87 80.11 13.36 o -19 1 1 35.38 31.62 9.54 o -17 1 1 30.96 50.79 8.44 o -15 1 1 2266.53 2161.70 22.85 o -13 1 1 1063.39 1119.12 15.76 o -11 1 1 2805.70 3022.02 19.15 o -9 1 1 141.61 155.09 3.17 o -7 1 1 2887.19 2964.65 12.07 o -5 1 1 10129.23 9907.80 24.82 o -3 1 1 16349.25 16083.30 82.78 o -1 1 1 2302.83 0.61 1.92 o 1 1 1 11184.31 11202.79 71.83 o 3 1 1 2855.84 2665.75 10.07 o 5 1 1 26.45 16.83 2.06 o 7 1 1 3.61 3.70 1.97 o 9 1 1 33.61 36.84 3.97 o 11 1 1 1952.80 1876.47 23.10 o 13 1 1 113.24 110.01 9.07 o 15 1 1 117.95 102.07 10.27 o 17 1 1 109.08 103.57 10.79 o 19 1 1 5.56 -2.95 9.27 o 21 1 1 21.87 21.12 20.06 o -22 2 1 38.60 47.28 14.79 o -20 2 1 52.15 63.08 11.62 o -18 2 1 704.71 649.91 23.98 o -16 2 1 260.40 319.24 13.28 o -14 2 1 2372.85 2280.03 22.75 o -12 2 1 2442.80 2316.44 33.83 o -10 2 1 27.02 61.81 2.94 o -8 2 1 8120.31 8699.03 45.62 o -6 2 1 1323.96 1167.45 7.15 o -4 2 1 685.97 620.37 6.33 o -2 2 1 8301.56 9068.40 34.58 o 0 2 1 5733.63 6224.94 12.66 o 2 2 1 14087.84 13644.87 128.50 o 4 2 1 2039.92 1898.22 10.24 o 6 2 1 251.92 293.58 6.61 o 8 2 1 299.82 376.17 8.28 o 10 2 1 90.59 86.73 5.63 o 12 2 1 4389.69 4248.53 35.21 o 14 2 1 469.96 499.66 14.70 o 16 2 1 32.76 39.19 14.87 o 18 2 1 97.01 118.54 15.16 o 20 2 1 359.98 395.56 20.84 o 22 2 1 16.93 21.84 33.27 o -23 3 1 360.70 394.52 20.35 o -21 3 1 30.98 35.13 14.47 o -19 3 1 12.56 12.16 10.40 o -17 3 1 2.08 -0.16 8.36 o -15 3 1 1281.50 1253.36 18.13 o -13 3 1 1066.93 1050.37 15.38 o -11 3 1 32.41 23.87 3.55 o -9 3 1 1776.09 1917.91 11.94 o -7 3 1 168.37 212.06 4.21 o -5 3 1 76.14 48.24 2.43 o -3 3 1 23899.11 23098.68 137.19 o -1 3 1 2028.85 1997.73 11.35 o 1 3 1 2264.00 2512.38 11.29 o 3 3 1 2677.26 2580.83 23.40 o 5 3 1 2.24 3.63 2.24 o 7 3 1 102.16 125.33 3.27 o 9 3 1 303.81 292.69 7.91 o 11 3 1 1152.40 1108.30 15.77 o 13 3 1 202.83 214.69 8.71 o 15 3 1 342.38 303.96 10.83 o 17 3 1 77.99 75.53 13.34 o 19 3 1 13.78 14.44 15.08 o 21 3 1 69.83 65.50 18.99 o -22 4 1 4.43 7.41 13.91 o -20 4 1 34.49 37.89 13.39 o -18 4 1 129.97 130.37 11.54 o -16 4 1 78.59 77.89 8.91 o -14 4 1 20.04 13.84 6.70 o -12 4 1 32.06 48.10 5.97 o -10 4 1 1894.47 1989.30 19.73 o -8 4 1 2821.86 3018.85 15.50 o -6 4 1 1253.02 1364.13 9.94 o -4 4 1 104.47 85.07 2.28 o -2 4 1 20848.28 20147.91 154.05 o 0 4 1 8469.09 9390.15 39.22 o 2 4 1 264.72 249.92 3.77 o 4 4 1 790.38 879.76 7.85 o 6 4 1 2850.47 2963.03 14.77 o 8 4 1 888.10 901.90 12.40 o 10 4 1 5.45 0.69 3.80 o 12 4 1 1853.56 1805.45 21.03 o 14 4 1 18.52 18.64 7.50 o 16 4 1 19.21 8.56 9.46 o 18 4 1 9.72 12.47 13.55 o 20 4 1 3.12 0.47 4.71 o 22 4 1 0.10 -5.27 19.07 o -23 5 1 104.97 120.44 25.32 o -21 5 1 230.23 244.21 18.67 o -19 5 1 210.76 208.63 12.91 o -17 5 1 70.32 84.46 10.03 o -15 5 1 186.88 177.37 8.42 o -13 5 1 146.50 160.63 10.83 o -11 5 1 1075.98 1146.29 14.51 o -9 5 1 954.51 1003.89 13.78 o -7 5 1 4358.14 4434.47 21.47 o -5 5 1 3616.61 3698.49 37.21 o -3 5 1 946.91 929.51 6.91 o -1 5 1 1850.07 2218.39 12.31 o 1 5 1 2429.05 2331.10 10.40 o 3 5 1 4760.52 4851.02 25.94 o 5 5 1 265.36 235.08 5.87 o 7 5 1 1210.59 1225.91 18.39 o 9 5 1 203.64 218.28 7.31 o 11 5 1 1362.87 1426.51 18.17 o 13 5 1 114.03 104.61 7.82 o 15 5 1 98.83 106.14 9.83 o 17 5 1 151.45 158.25 12.14 o 19 5 1 38.42 55.23 21.58 o 21 5 1 53.28 55.30 24.71 o -22 6 1 114.61 112.33 21.77 o -20 6 1 60.46 59.59 14.24 o -18 6 1 115.96 105.88 12.55 o -16 6 1 1.27 3.40 5.37 o -14 6 1 352.37 325.08 10.08 o -12 6 1 266.85 258.24 8.46 o -10 6 1 0.24 1.29 2.47 o -8 6 1 1372.93 1444.16 17.59 o -6 6 1 1082.51 1048.71 12.89 o -4 6 1 583.66 556.48 5.85 o -2 6 1 284.62 362.53 5.74 o 0 6 1 1153.15 1095.40 9.05 o 2 6 1 1079.57 992.24 7.29 o 4 6 1 409.40 378.09 7.11 o 6 6 1 5547.73 5996.45 64.32 o 8 6 1 192.68 181.72 6.57 o 10 6 1 176.04 165.84 7.32 o 12 6 1 2293.10 2235.56 34.71 o 14 6 1 60.74 74.23 9.31 o 16 6 1 205.62 235.36 20.10 o 18 6 1 46.90 41.96 13.76 o 20 6 1 243.14 240.21 24.68 o 22 6 1 66.36 70.16 63.16 o -23 7 1 306.29 277.17 50.57 o -21 7 1 70.09 86.51 17.73 o -19 7 1 25.45 25.18 12.57 o -17 7 1 21.33 21.26 10.01 o -15 7 1 43.83 30.65 8.50 o -13 7 1 214.52 192.57 8.00 o -11 7 1 190.16 204.23 10.65 o -9 7 1 0.10 3.31 3.42 o -7 7 1 120.17 117.92 3.98 o -5 7 1 317.16 331.13 5.53 o -3 7 1 4449.18 4744.51 27.94 o -1 7 1 1296.49 1500.14 13.32 o 1 7 1 25.18 19.73 2.27 o 3 7 1 1145.28 1190.99 9.51 o 5 7 1 291.13 243.09 6.27 o 7 7 1 24.71 15.78 4.91 o 9 7 1 587.49 571.17 11.98 o 11 7 1 175.31 177.02 8.21 o 13 7 1 273.67 288.65 10.30 o 15 7 1 122.75 106.80 11.32 o 17 7 1 17.97 16.45 11.97 o 19 7 1 1.87 1.89 14.37 o 21 7 1 186.11 184.26 37.48 o -22 8 1 15.07 4.06 17.65 o -20 8 1 20.73 22.39 15.45 o -18 8 1 41.49 58.66 12.67 o -16 8 1 287.04 288.72 10.93 o -14 8 1 133.48 112.76 8.97 o -12 8 1 60.78 44.14 6.89 o -10 8 1 1028.69 1066.16 14.65 o -8 8 1 23.39 39.36 4.59 o -6 8 1 35.04 48.03 3.85 o -4 8 1 193.08 197.01 3.73 o -2 8 1 4940.68 5308.26 26.31 o 0 8 1 962.23 1038.64 12.13 o 2 8 1 14.84 22.74 2.93 o 4 8 1 356.34 426.37 6.49 o 6 8 1 2989.14 3118.58 19.73 o 8 8 1 454.17 411.34 9.44 o 10 8 1 89.99 80.06 7.52 o 12 8 1 745.75 679.18 14.17 o 14 8 1 163.82 139.35 11.14 o 16 8 1 49.80 53.33 12.05 o 18 8 1 52.41 62.07 16.42 o 20 8 1 0.78 4.08 20.52 o -21 9 1 76.48 87.39 22.92 o -19 9 1 208.49 227.38 16.75 o -17 9 1 228.79 217.75 12.99 o -15 9 1 182.11 168.32 10.59 o -13 9 1 56.47 77.25 8.84 o -11 9 1 25.26 22.28 7.12 o -9 9 1 1328.44 1276.24 25.65 o -7 9 1 890.58 852.53 10.21 o -5 9 1 129.85 124.08 3.66 o -3 9 1 15.54 13.14 4.47 o -1 9 1 0.20 0.88 3.90 o 1 9 1 53.90 54.87 3.90 o 3 9 1 2196.83 2292.10 13.83 o 5 9 1 311.88 286.60 6.50 o 7 9 1 1269.07 1291.63 13.86 o 9 9 1 688.77 709.05 12.89 o 11 9 1 361.19 376.73 10.78 o 13 9 1 117.18 125.41 10.10 o 15 9 1 214.35 247.36 12.92 o 17 9 1 196.10 212.75 16.27 o 19 9 1 51.67 42.49 23.06 o -22 10 1 111.10 124.37 36.30 o -20 10 1 64.40 62.30 21.86 o -18 10 1 59.70 71.32 18.23 o -16 10 1 10.70 5.87 12.18 o -14 10 1 209.27 218.55 11.58 o -12 10 1 128.62 113.25 10.07 o -10 10 1 0.30 -0.68 7.24 o -8 10 1 591.18 618.83 24.25 o -6 10 1 969.90 934.57 14.29 o -4 10 1 1154.04 1199.64 14.42 o -2 10 1 272.52 319.58 8.03 o 0 10 1 141.27 148.78 6.05 o 2 10 1 194.65 189.83 4.68 o 4 10 1 203.71 202.84 5.97 o 6 10 1 3369.31 3385.21 23.28 o 8 10 1 440.50 457.50 9.25 o 10 10 1 229.74 219.41 8.02 o 12 10 1 270.59 245.31 10.51 o 14 10 1 0.70 -1.15 10.46 o 16 10 1 157.57 150.71 16.36 o 18 10 1 253.48 279.65 20.51 o 20 10 1 62.60 34.70 39.98 o -21 11 1 0.01 -7.59 11.64 o -19 11 1 2.81 3.93 20.50 o -17 11 1 188.66 180.11 18.50 o -15 11 1 2.43 -2.50 11.73 o -13 11 1 0.29 -4.58 8.66 o -11 11 1 1.44 1.26 9.85 o -9 11 1 1440.63 1331.10 36.36 o -7 11 1 74.07 48.38 9.48 o -5 11 1 234.24 214.20 7.17 o -3 11 1 517.15 587.26 11.04 o -1 11 1 477.21 473.52 10.11 o 1 11 1 7.13 5.05 4.75 o 3 11 1 159.03 151.65 5.71 o 5 11 1 322.45 321.86 7.91 o 7 11 1 48.10 37.58 7.01 o 9 11 1 6.52 2.23 7.73 o 11 11 1 4.48 -0.60 4.49 o 13 11 1 2.82 -1.64 10.91 o 15 11 1 0.01 -10.64 13.11 o 17 11 1 1.41 -6.92 14.19 o 19 11 1 34.28 27.98 53.87 o -20 12 1 1.43 6.55 26.19 o -18 12 1 0.33 1.88 13.40 o -16 12 1 283.16 287.09 17.59 o -14 12 1 60.64 52.18 13.29 o -12 12 1 53.63 43.01 11.51 o -10 12 1 464.07 479.08 15.05 o -8 12 1 240.50 211.45 13.07 o -6 12 1 96.74 96.44 8.03 o -4 12 1 0.07 -3.33 4.49 o -2 12 1 499.33 523.55 11.03 o 0 12 1 227.17 208.40 7.80 o 2 12 1 49.36 37.74 6.63 o 4 12 1 24.58 24.50 6.20 o 6 12 1 308.62 342.92 11.65 o 8 12 1 83.78 87.90 10.44 o 10 12 1 254.76 284.28 15.99 o 12 12 1 7.36 2.11 14.13 o 14 12 1 169.27 161.37 20.65 o 16 12 1 150.47 174.06 24.71 o 18 12 1 35.03 55.90 31.74 o -19 13 1 77.72 80.79 32.62 o -17 13 1 420.15 451.26 26.38 o -15 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