#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/25/2232588.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232588_Fobs loop_ _publ_author_name 'Abbassi, Najat' 'Rakib, El Mostapha' 'Hannioui, Abdellah' 'Zouihri, Hafid' _publ_section_title ; N-[7-Ethoxy-2-(prop-2-en-1-yl)-2H-indazol-6-yl]-4-methylbenzenesulfonamide ; _journal_coeditor_code BT5700 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3211 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.097 _cell_angle_gamma 90.000 _cell_length_a 10.1459 _cell_length_b 9.9506 _cell_length_c 18.3720 _exptl_crystal_F_000 784.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file bt5700Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zouihri_Rakib_324_Froid_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 196.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1965.29 1657.56 72.41 o 2 0 0 1949.69 2068.00 36.47 o 3 0 0 121.66 106.05 3.53 o 4 0 0 8.36 2.86 0.36 o 5 0 0 1927.10 1977.75 32.42 o 6 0 0 16.16 38.94 1.24 o 7 0 0 1659.04 1748.23 33.34 o 8 0 0 294.16 265.82 8.06 o 9 0 0 11.01 8.63 2.10 o 10 0 0 634.92 575.55 15.47 o 11 0 0 214.31 227.38 8.28 o 12 0 0 85.12 71.70 8.61 o 1 1 0 6145.91 6176.95 75.31 o 2 1 0 12553.02 12532.15 150.07 o 3 1 0 1160.09 1161.32 12.22 o 4 1 0 70.54 70.66 1.46 o 5 1 0 7483.48 8221.64 107.06 o 6 1 0 11.41 10.91 0.59 o 7 1 0 301.25 311.31 4.44 o 8 1 0 22.27 9.19 0.66 o 9 1 0 582.67 542.57 9.18 o 10 1 0 5.26 7.26 1.67 o 11 1 0 0.00 0.47 1.48 o 12 1 0 13.03 18.02 2.23 o 0 2 0 269.98 301.02 5.12 o 1 2 0 560.69 448.01 3.50 o 2 2 0 1728.96 1824.20 15.72 o 3 2 0 2612.92 2766.66 26.97 o 4 2 0 157.98 99.65 1.49 o 5 2 0 47.01 20.89 0.85 o 6 2 0 590.82 646.45 8.86 o 7 2 0 38.17 33.33 1.21 o 8 2 0 584.50 640.60 8.53 o 9 2 0 839.58 789.88 13.98 o 10 2 0 142.28 151.96 4.38 o 11 2 0 3.49 1.24 1.50 o 12 2 0 116.55 141.95 4.76 o 1 3 0 6.41 0.81 0.19 o 2 3 0 606.32 701.14 6.26 o 3 3 0 56.50 59.64 1.01 o 4 3 0 793.06 926.15 9.34 o 5 3 0 153.60 213.53 3.13 o 6 3 0 1554.26 1542.41 20.06 o 7 3 0 839.35 817.45 12.13 o 8 3 0 26.82 38.66 1.53 o 9 3 0 1321.12 1348.31 17.04 o 10 3 0 4.97 4.05 1.58 o 11 3 0 1.47 0.00 1.45 o 12 3 0 37.94 47.83 2.89 o 0 4 0 96.48 63.96 1.13 o 1 4 0 1789.36 2007.58 16.88 o 2 4 0 342.19 340.06 3.38 o 3 4 0 676.44 765.38 7.94 o 4 4 0 1947.80 1986.02 22.05 o 5 4 0 443.51 356.76 4.81 o 6 4 0 390.86 378.47 5.68 o 7 4 0 597.83 574.44 8.25 o 8 4 0 92.96 101.98 2.58 o 9 4 0 474.14 432.79 6.74 o 10 4 0 118.68 111.56 3.82 o 11 4 0 54.95 49.85 2.79 o 12 4 0 93.83 96.36 4.36 o 1 5 0 81.04 97.64 1.51 o 2 5 0 516.45 609.46 6.12 o 3 5 0 1177.09 1233.66 12.58 o 4 5 0 470.30 472.55 5.47 o 5 5 0 37.91 40.67 1.22 o 6 5 0 268.11 289.11 4.22 o 7 5 0 79.88 83.87 2.23 o 8 5 0 7.41 5.64 0.99 o 9 5 0 69.33 59.82 2.02 o 10 5 0 295.68 284.80 6.50 o 11 5 0 214.02 227.38 5.82 o 0 6 0 1.56 12.54 1.00 o 1 6 0 7.74 2.95 0.35 o 2 6 0 269.92 263.12 3.24 o 3 6 0 27.86 25.79 0.81 o 4 6 0 2.79 4.39 0.58 o 5 6 0 222.99 171.08 2.69 o 6 6 0 8.30 6.17 0.76 o 7 6 0 1727.82 1734.83 26.39 o 8 6 0 309.87 281.40 4.86 o 9 6 0 0.08 0.00 1.06 o 10 6 0 9.83 14.71 2.52 o 11 6 0 14.99 11.95 2.82 o 1 7 0 1268.95 1259.43 16.80 o 2 7 0 244.63 240.50 3.09 o 3 7 0 8.58 8.80 0.61 o 4 7 0 40.81 37.56 1.18 o 5 7 0 101.86 102.16 2.01 o 6 7 0 319.83 313.54 4.68 o 7 7 0 293.97 290.48 4.45 o 8 7 0 1.02 2.15 1.11 o 9 7 0 96.41 105.85 3.47 o 10 7 0 77.67 85.10 4.16 o 0 8 0 316.01 342.41 6.31 o 1 8 0 6.43 2.31 0.74 o 2 8 0 264.49 235.29 3.92 o 3 8 0 45.78 51.79 1.81 o 4 8 0 171.99 144.46 3.17 o 5 8 0 712.87 684.67 10.56 o 6 8 0 283.20 243.57 4.70 o 7 8 0 448.68 408.37 8.20 o 8 8 0 59.82 51.73 2.39 o 9 8 0 13.15 14.89 1.74 o 10 8 0 5.51 10.24 2.17 o 1 9 0 619.38 618.69 10.64 o 2 9 0 1185.29 1157.39 16.71 o 3 9 0 737.10 719.16 14.56 o 4 9 0 231.27 235.24 5.05 o 5 9 0 8.22 5.31 1.12 o 6 9 0 132.21 121.16 3.11 o 7 9 0 5.45 5.26 1.20 o 8 9 0 325.85 352.30 7.39 o 9 9 0 22.78 25.68 2.85 o 0 10 0 88.33 100.95 4.10 o 1 10 0 6.90 9.75 1.27 o 2 10 0 7.97 6.91 1.20 o 3 10 0 7.51 4.75 1.23 o 4 10 0 259.18 270.62 5.79 o 5 10 0 0.19 0.00 1.13 o 6 10 0 4.33 3.88 1.17 o 7 10 0 0.79 0.00 1.18 o 1 11 0 205.07 187.12 4.49 o 2 11 0 332.22 327.58 6.68 o 3 11 0 109.39 118.10 3.62 o 4 11 0 214.93 206.26 4.92 o 5 11 0 65.00 80.01 2.99 o 6 11 0 54.68 61.51 2.69 o 0 12 0 1.43 1.29 1.77 o 1 12 0 78.49 73.20 2.54 o 2 12 0 8.92 15.11 1.97 o 3 12 0 1.07 1.46 1.33 o 4 12 0 37.49 57.56 2.72 o -12 1 1 65.98 57.79 3.13 o -11 1 1 11.73 11.27 1.92 o -10 1 1 48.93 57.98 3.30 o -9 1 1 374.18 381.75 6.17 o -8 1 1 793.80 801.55 10.34 o -7 1 1 1292.63 1259.22 14.49 o -6 1 1 433.40 523.63 6.33 o -5 1 1 2396.98 2695.65 29.67 o -4 1 1 1413.29 1624.62 19.33 o -3 1 1 3315.16 3217.32 37.86 o -2 1 1 11749.65 11502.49 132.46 o -1 1 1 8832.54 8734.49 110.01 o 0 1 1 349.15 367.53 9.57 o 1 1 1 705.31 694.48 5.67 o 2 1 1 1876.92 1782.69 18.55 o 3 1 1 28.58 18.87 0.66 o 4 1 1 741.87 891.51 11.61 o 5 1 1 622.17 593.01 7.37 o 6 1 1 41.06 57.38 1.74 o 7 1 1 2043.89 2206.64 30.97 o 8 1 1 115.04 128.86 3.83 o 9 1 1 386.19 361.31 6.69 o 10 1 1 140.50 157.94 4.55 o 11 1 1 39.36 41.98 2.58 o 12 1 1 251.72 273.13 6.85 o -12 2 1 0.18 1.95 1.74 o -11 2 1 3.99 3.48 1.66 o -10 2 1 58.38 57.92 2.78 o -9 2 1 245.81 203.92 3.47 o -8 2 1 1019.97 971.60 12.43 o -7 2 1 0.77 1.26 0.60 o -6 2 1 124.59 143.23 2.10 o -5 2 1 679.85 849.66 8.76 o -4 2 1 3777.05 4223.95 43.48 o -3 2 1 633.74 796.33 8.73 o -2 2 1 556.89 535.17 5.40 o -1 2 1 2771.22 2676.04 23.76 o 0 2 1 162.03 190.48 1.85 o 1 2 1 2890.09 2753.20 24.85 o 2 2 1 347.41 335.45 3.36 o 3 2 1 2558.20 2685.84 25.16 o 4 2 1 747.09 783.63 8.83 o 5 2 1 9.51 15.96 0.77 o 6 2 1 1090.61 1295.61 15.62 o 7 2 1 182.60 183.93 2.88 o 8 2 1 247.41 256.13 5.23 o 9 2 1 110.04 101.05 3.08 o 10 2 1 212.66 198.27 5.13 o 11 2 1 0.02 0.00 1.44 o 12 2 1 0.54 4.32 2.29 o -12 3 1 85.02 96.26 4.00 o -11 3 1 30.78 28.09 2.31 o -10 3 1 478.19 448.11 9.01 o -9 3 1 755.12 726.28 9.75 o -8 3 1 507.99 470.09 6.61 o -7 3 1 3493.88 3307.36 42.08 o -6 3 1 2.46 1.91 0.59 o -5 3 1 45.48 54.02 1.26 o -4 3 1 364.92 304.67 3.59 o -3 3 1 378.32 292.40 3.40 o -2 3 1 1158.31 1182.98 11.22 o -1 3 1 560.53 607.79 5.65 o 0 3 1 645.49 705.66 6.02 o 1 3 1 30.16 38.02 0.66 o 2 3 1 458.30 303.03 3.14 o 3 3 1 1181.69 1170.25 11.78 o 4 3 1 116.40 150.17 2.11 o 5 3 1 380.10 420.23 5.07 o 6 3 1 2.20 4.49 0.86 o 7 3 1 2955.58 2983.05 38.07 o 8 3 1 1.85 2.15 0.80 o 9 3 1 1008.98 1002.44 15.02 o 10 3 1 34.46 39.63 2.41 o 11 3 1 159.69 143.19 4.47 o 12 3 1 151.37 169.43 5.15 o -12 4 1 77.50 88.79 4.41 o -11 4 1 156.67 141.63 4.43 o -10 4 1 357.65 356.23 14.32 o -9 4 1 280.29 286.88 4.91 o -8 4 1 886.05 838.49 11.66 o -7 4 1 15.37 7.32 0.92 o -6 4 1 567.49 580.73 7.60 o -5 4 1 113.37 83.62 1.56 o -4 4 1 599.81 583.20 6.90 o -3 4 1 1244.24 1336.51 14.14 o -2 4 1 1268.03 1389.15 13.96 o -1 4 1 60.80 62.37 0.91 o 0 4 1 215.93 246.91 2.63 o 1 4 1 1034.63 929.97 8.61 o 2 4 1 1343.51 1375.95 12.57 o 3 4 1 470.81 545.06 6.07 o 4 4 1 1574.93 1815.14 20.21 o 5 4 1 256.63 277.49 3.91 o 6 4 1 1121.14 1132.61 13.80 o 7 4 1 708.51 698.09 9.79 o 8 4 1 1234.05 1303.67 17.46 o 9 4 1 293.80 231.04 6.56 o 10 4 1 6.06 6.49 2.47 o 11 4 1 64.31 62.36 3.05 o 12 4 1 101.46 113.29 4.29 o -11 5 1 17.04 12.54 2.39 o -10 5 1 20.55 25.01 2.07 o -9 5 1 0.34 4.71 1.08 o -8 5 1 34.17 28.29 1.43 o -7 5 1 387.58 376.00 5.86 o -6 5 1 11.67 16.51 0.93 o -5 5 1 1119.79 1170.40 13.41 o -4 5 1 20.38 18.83 0.72 o -3 5 1 673.83 822.46 8.97 o -2 5 1 296.62 302.53 3.26 o -1 5 1 969.70 1204.98 12.23 o 0 5 1 2865.12 3044.07 27.59 o 1 5 1 900.51 902.86 9.78 o 2 5 1 2430.46 2454.36 22.19 o 3 5 1 2361.18 2657.99 27.72 o 4 5 1 2.50 4.61 0.52 o 5 5 1 548.17 464.82 5.78 o 6 5 1 553.31 540.46 6.69 o 7 5 1 318.81 286.31 5.31 o 8 5 1 111.58 101.03 2.52 o 9 5 1 5.50 3.89 1.14 o 10 5 1 92.45 100.88 3.64 o 11 5 1 3.87 6.29 2.51 o -11 6 1 41.71 52.24 3.44 o -10 6 1 25.77 28.05 2.54 o -9 6 1 37.02 34.43 1.81 o -8 6 1 95.04 92.82 3.52 o -7 6 1 26.49 24.45 1.40 o -6 6 1 110.98 121.80 2.25 o -5 6 1 262.88 289.03 3.75 o -4 6 1 147.77 143.30 2.17 o -3 6 1 929.26 965.88 10.52 o -2 6 1 392.45 382.78 4.29 o -1 6 1 251.24 292.93 3.49 o 0 6 1 11.06 13.67 0.50 o 1 6 1 0.77 5.60 0.39 o 2 6 1 309.50 289.71 3.19 o 3 6 1 171.54 168.91 2.37 o 4 6 1 62.09 70.34 1.40 o 5 6 1 2356.40 2367.62 26.31 o 6 6 1 87.05 78.09 1.75 o 7 6 1 359.02 380.10 5.16 o 8 6 1 169.49 181.49 3.62 o 9 6 1 163.75 164.63 3.82 o 10 6 1 146.93 137.78 4.21 o 11 6 1 0.11 0.00 4.13 o -10 7 1 22.70 29.99 2.80 o -9 7 1 54.18 52.63 4.07 o -8 7 1 49.38 44.76 1.94 o -7 7 1 6.00 2.68 1.05 o -6 7 1 1640.32 1507.23 21.47 o -5 7 1 4.95 5.63 0.97 o -4 7 1 590.35 561.39 9.09 o -3 7 1 0.29 0.91 0.60 o -2 7 1 46.73 54.11 1.80 o -1 7 1 68.08 79.56 1.39 o 0 7 1 270.11 238.70 3.13 o 1 7 1 1077.59 1111.32 11.94 o 2 7 1 153.37 148.10 2.33 o 3 7 1 202.84 198.00 2.74 o 4 7 1 955.62 968.93 10.72 o 5 7 1 508.12 496.28 6.84 o 6 7 1 99.23 84.94 2.05 o 7 7 1 123.74 115.06 2.61 o 8 7 1 1.10 0.57 1.03 o 9 7 1 46.85 47.14 2.37 o 10 7 1 14.91 16.67 2.28 o -10 8 1 2.27 4.50 1.64 o -9 8 1 15.61 19.01 2.11 o -8 8 1 72.07 81.26 3.00 o -7 8 1 13.73 3.81 1.28 o -6 8 1 423.90 436.37 7.31 o -5 8 1 12.31 9.42 1.14 o -4 8 1 1463.66 1449.97 18.89 o -3 8 1 4.04 1.77 0.87 o -2 8 1 138.75 132.72 2.49 o -1 8 1 349.49 358.15 5.37 o 0 8 1 437.23 456.53 6.22 o 1 8 1 913.86 938.73 12.60 o 2 8 1 286.58 279.76 4.07 o 3 8 1 4.61 8.03 0.84 o 4 8 1 130.88 112.47 2.90 o 5 8 1 29.44 38.69 1.67 o 6 8 1 18.23 23.66 1.47 o 7 8 1 1.80 2.98 1.16 o 8 8 1 348.09 344.91 7.19 o 9 8 1 23.96 21.80 1.96 o -9 9 1 5.81 5.09 1.58 o -8 9 1 215.52 220.69 5.36 o -7 9 1 41.74 42.44 2.15 o -6 9 1 3.46 3.60 1.08 o -5 9 1 73.52 78.91 2.42 o -4 9 1 4.62 6.85 1.21 o -3 9 1 7.54 4.35 1.36 o -2 9 1 458.25 432.39 7.92 o -1 9 1 75.28 77.75 2.50 o 0 9 1 1020.42 976.14 15.98 o 1 9 1 224.36 231.80 4.83 o 2 9 1 196.68 187.41 3.73 o 3 9 1 0.92 0.08 0.99 o 4 9 1 159.87 131.88 3.46 o 5 9 1 246.34 233.55 4.60 o 6 9 1 0.59 0.24 1.04 o 7 9 1 85.75 74.14 2.97 o 8 9 1 9.46 9.96 1.66 o 9 9 1 10.83 14.38 1.83 o -8 10 1 170.68 183.08 4.85 o -7 10 1 103.81 104.11 3.07 o -6 10 1 204.35 208.86 4.46 o -5 10 1 5.26 3.89 1.25 o -4 10 1 182.35 176.46 4.35 o -3 10 1 27.49 30.67 1.74 o -2 10 1 805.36 758.32 12.98 o -1 10 1 653.27 660.14 11.46 o 0 10 1 1.68 0.00 0.93 o 1 10 1 508.90 503.24 9.07 o 2 10 1 61.06 60.02 2.01 o 3 10 1 612.16 584.67 10.43 o 4 10 1 725.07 675.69 11.87 o 5 10 1 24.63 22.27 2.68 o 6 10 1 88.47 93.98 2.82 o 7 10 1 28.12 23.61 1.68 o -6 11 1 66.09 71.05 2.90 o -5 11 1 4.08 1.40 1.29 o -4 11 1 7.19 10.39 1.49 o -3 11 1 39.95 44.27 2.18 o -2 11 1 39.79 41.42 2.46 o -1 11 1 4.12 0.00 0.96 o 0 11 1 176.98 193.63 5.91 o 1 11 1 10.85 16.22 1.52 o 2 11 1 265.50 298.70 5.49 o 3 11 1 96.65 101.06 3.23 o 4 11 1 59.26 55.21 2.53 o 5 11 1 94.49 86.40 3.11 o 6 11 1 0.94 4.00 1.46 o -4 12 1 419.78 429.78 8.55 o -3 12 1 0.41 0.00 1.29 o -2 12 1 182.89 178.92 4.54 o -1 12 1 266.47 290.87 5.46 o 0 12 1 1.30 0.36 2.04 o 1 12 1 499.75 543.23 8.94 o 2 12 1 89.57 85.94 3.08 o 3 12 1 0.23 3.78 1.39 o 4 12 1 4.96 3.92 1.50 o -12 0 2 1.08 0.43 2.45 o -11 0 2 29.51 22.57 3.03 o -10 0 2 3361.94 3236.90 80.83 o -9 0 2 41.27 34.99 1.28 o -8 0 2 888.57 844.56 16.34 o -7 0 2 59.23 85.73 3.88 o -6 0 2 30.89 52.27 3.11 o -5 0 2 521.72 601.95 12.06 o -4 0 2 6.23 17.27 1.24 o -3 0 2 16093.20 16135.91 562.08 o -2 0 2 6741.33 6797.19 125.68 o -1 0 2 818.51 847.34 13.05 o 0 0 2 22015.17 20650.72 755.07 o 1 0 2 0.50 0.00 1.09 o 2 0 2 24665.41 24940.78 702.15 o 3 0 2 1540.86 1546.05 24.33 o 4 0 2 652.83 662.09 15.25 o 5 0 2 3062.29 3584.15 77.78 o 6 0 2 183.38 198.90 6.86 o 7 0 2 1349.79 1400.99 27.11 o 8 0 2 166.38 208.40 5.36 o 9 0 2 6.34 11.32 2.21 o 10 0 2 9.95 8.46 2.29 o 11 0 2 18.30 16.45 2.94 o 12 0 2 214.55 213.91 8.32 o -12 1 2 40.53 43.10 2.76 o -11 1 2 49.65 47.73 2.84 o -10 1 2 2.04 0.30 1.49 o -9 1 2 9.80 5.36 1.03 o -8 1 2 383.13 413.62 5.34 o -7 1 2 383.41 437.25 5.40 o -6 1 2 149.08 147.46 2.82 o -5 1 2 1471.03 1441.10 19.34 o -4 1 2 280.99 263.88 4.59 o -3 1 2 1851.66 1794.29 25.47 o -2 1 2 1798.29 1756.43 22.49 o -1 1 2 1468.61 1429.64 17.24 o 0 1 2 837.82 766.61 8.19 o 1 1 2 672.54 647.79 5.13 o 2 1 2 3997.14 4354.80 40.64 o 3 1 2 3694.96 3748.89 38.98 o 4 1 2 271.71 328.16 3.91 o 5 1 2 624.34 747.02 10.88 o 6 1 2 860.34 899.78 14.81 o 7 1 2 23.90 16.08 1.44 o 8 1 2 102.67 91.96 3.15 o 9 1 2 644.77 636.31 11.62 o 10 1 2 466.40 430.51 8.79 o 11 1 2 75.15 84.33 4.05 o 12 1 2 47.76 57.23 3.22 o -12 2 2 223.68 236.62 6.24 o -11 2 2 161.27 164.69 4.82 o -10 2 2 104.16 96.28 4.46 o -9 2 2 415.89 356.04 5.30 o -8 2 2 752.84 789.83 10.32 o -7 2 2 1026.77 1038.68 10.79 o -6 2 2 2224.04 2374.42 25.12 o -5 2 2 178.22 259.78 3.40 o -4 2 2 732.27 730.98 10.56 o -3 2 2 287.77 315.41 4.35 o -2 2 2 5638.14 5899.21 59.55 o -1 2 2 4946.22 4686.43 43.22 o 0 2 2 17248.74 13470.60 352.58 o 1 2 2 776.19 767.76 6.71 o 2 2 2 1650.15 1621.57 15.45 o 3 2 2 7.90 4.83 0.33 o 4 2 2 475.26 469.05 4.71 o 5 2 2 3697.21 4068.76 44.21 o 6 2 2 205.29 194.04 3.17 o 7 2 2 105.94 99.11 2.67 o 8 2 2 1004.06 1000.22 16.84 o 9 2 2 1353.34 1335.65 22.17 o 10 2 2 32.29 38.72 2.33 o 11 2 2 17.95 9.94 1.80 o 12 2 2 52.49 51.42 3.00 o -12 3 2 0.49 0.00 1.58 o -11 3 2 45.64 46.24 2.67 o -10 3 2 134.82 116.71 3.87 o -9 3 2 47.83 53.88 1.81 o -8 3 2 62.21 40.97 1.47 o -7 3 2 1572.73 1607.06 17.36 o -6 3 2 738.66 821.12 9.16 o -5 3 2 286.25 299.58 3.87 o -4 3 2 4526.78 4806.03 55.87 o -3 3 2 6.12 1.72 0.36 o -2 3 2 3208.93 3304.22 35.89 o -1 3 2 5249.09 5094.68 52.27 o 0 3 2 2396.00 2443.97 25.44 o 1 3 2 3416.08 3341.56 38.61 o 2 3 2 612.00 644.68 6.05 o 3 3 2 4564.79 4671.79 46.49 o 4 3 2 30.44 39.45 0.76 o 5 3 2 129.59 160.69 2.64 o 6 3 2 230.95 259.42 3.69 o 7 3 2 34.54 29.53 2.05 o 8 3 2 21.27 30.01 2.15 o 9 3 2 1241.52 1207.16 22.31 o 10 3 2 61.72 67.97 2.95 o 11 3 2 16.86 20.16 2.12 o 12 3 2 15.06 17.52 2.21 o -12 4 2 2.52 4.30 1.91 o -11 4 2 0.98 0.00 1.45 o -10 4 2 131.88 139.58 4.20 o -9 4 2 171.65 167.14 3.76 o -8 4 2 731.02 701.64 9.21 o -7 4 2 71.25 73.61 1.58 o -6 4 2 2108.27 2110.34 25.37 o -5 4 2 162.68 140.92 2.55 o -4 4 2 380.53 461.45 5.60 o -3 4 2 26.04 41.08 0.87 o -2 4 2 559.96 556.59 6.13 o -1 4 2 4.06 1.60 0.52 o 0 4 2 242.25 285.88 3.01 o 1 4 2 2885.62 2853.58 33.13 o 2 4 2 12.35 4.23 0.35 o 3 4 2 41.32 55.94 1.03 o 4 4 2 333.15 295.85 3.45 o 5 4 2 67.17 86.09 1.60 o 6 4 2 685.52 693.96 8.18 o 7 4 2 144.04 131.76 2.78 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0.00 1.81 o -2 1 22 8.97 13.13 3.37 o -1 1 22 190.32 179.60 5.25 o 0 1 22 0.00 0.00 1.56 o 1 1 22 0.10 0.00 1.54 o 2 1 22 95.81 101.57 4.32 o 3 1 22 7.75 4.43 2.01 o -5 2 22 56.76 57.02 3.04 o -4 2 22 28.19 25.67 2.26 o -3 2 22 190.31 188.35 5.43 o -2 2 22 42.29 42.53 2.69 o -1 2 22 152.29 152.09 4.16 o 0 2 22 0.67 0.76 1.31 o 1 2 22 238.96 231.26 5.76 o 2 2 22 0.03 0.31 1.36 o -4 3 22 29.66 33.27 2.46 o -3 3 22 1.46 1.75 1.62 o -2 3 22 28.31 28.80 2.34 o -1 3 22 84.02 90.76 3.69 o 0 3 22 54.20 57.89 2.44 o 1 3 22 326.58 310.31 6.87 o 2 3 22 0.02 0.00 1.62 o -3 4 22 221.44 217.79 5.42 o -2 4 22 0.85 0.00 1.35 o -1 4 22 525.28 581.73 11.02 o 0 4 22 5.16 2.46 1.42 o -3 1 23 113.98 122.53 14.08 o -2 1 23 93.33 94.09 4.80 o -1 1 23 138.87 152.15 9.23 o 0 1 23 10.77 11.25 2.36 o 1 1 23 69.28 81.33 5.18 o -2 2 23 23.76 23.03 2.79 o -1 2 23 9.71 4.61 2.09 o 0 2 23 2.05 1.53 1.97 o