#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/26/2232611.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232611_Fobs loop_ _publ_author_name 'Zhu, Guang-Zhou' 'Xu, Suo-Ping' 'Li, Cui-Yun' _publ_section_title ; 3,5-Dibromo-4-oxo-2,2,6,6-tetramethylpiperidin-1-yl oxide ; _journal_coeditor_code BX2376 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3262 _journal_volume 67 _journal_year 2011 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6745 _cell_length_b 16.0848 _cell_length_c 5.9301 _exptl_crystal_F_000 644.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file bx2376Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 110704d in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13482.56 13946.35 601.28 o 4 0 0 30970.83 30616.56 1314.38 o 6 0 0 20.04 95.98 29.37 o 8 0 0 6071.47 6206.11 286.45 o 10 0 0 2440.05 2613.08 147.71 o 12 0 0 4485.91 4399.06 229.21 o 2 1 0 10347.86 11321.74 411.85 o 4 1 0 20150.00 20738.46 725.85 o 6 1 0 10993.05 12290.69 498.22 o 8 1 0 927.64 929.91 64.19 o 10 1 0 971.72 1092.63 64.61 o 12 1 0 18.39 70.74 46.14 o 2 2 0 17693.75 17602.24 1058.30 o 4 2 0 3501.71 3768.25 191.31 o 6 2 0 1187.92 1291.29 43.98 o 8 2 0 16.58 56.58 27.19 o 10 2 0 1156.19 1178.76 97.83 o 12 2 0 1778.77 1883.85 132.67 o 2 3 0 9671.07 9797.11 1200.64 o 4 3 0 9724.17 10295.16 685.52 o 6 3 0 19133.06 18888.56 1044.58 o 8 3 0 14112.02 14454.96 1334.00 o 10 3 0 3848.52 3901.61 429.18 o 12 3 0 860.42 994.10 71.23 o 0 4 0 7287.18 7531.11 329.09 o 2 4 0 44.87 59.64 14.73 o 4 4 0 1973.53 2106.28 195.52 o 6 4 0 220.25 202.87 25.66 o 8 4 0 23.55 4.51 22.48 o 10 4 0 298.09 295.40 43.74 o 12 4 0 965.69 1047.13 144.05 o 2 5 0 4631.55 4513.29 554.81 o 4 5 0 16946.50 16023.90 2207.47 o 6 5 0 15679.12 15281.33 1616.38 o 8 5 0 6368.32 6370.63 609.86 o 10 5 0 2428.18 2600.06 320.56 o 12 5 0 3.09 10.15 46.86 o 0 6 0 45048.59 39335.16 1689.25 o 2 6 0 27135.88 23058.50 2039.89 o 4 6 0 12455.77 12081.92 2009.88 o 6 6 0 754.01 835.59 127.48 o 8 6 0 700.93 671.48 107.90 o 10 6 0 6153.76 5834.48 560.84 o 12 6 0 1793.40 1981.53 359.81 o 2 7 0 50.85 61.41 10.75 o 4 7 0 569.56 515.70 83.09 o 6 7 0 567.89 615.32 111.18 o 8 7 0 266.74 309.90 56.97 o 10 7 0 473.04 548.54 95.84 o 12 7 0 15.09 4.79 49.99 o 0 8 0 11814.88 11621.09 509.87 o 2 8 0 20379.65 19197.77 1234.00 o 4 8 0 3340.39 3021.53 575.65 o 6 8 0 86.01 110.54 22.79 o 8 8 0 543.44 627.20 229.76 o 10 8 0 1200.84 1130.11 166.92 o 12 8 0 1741.42 1725.14 425.48 o 2 9 0 4739.99 4610.72 196.31 o 4 9 0 3959.91 4018.45 679.59 o 6 9 0 9862.29 9008.17 1782.66 o 8 9 0 4892.60 4376.54 846.78 o 10 9 0 2039.49 1902.02 428.06 o 12 9 0 688.46 581.40 86.51 o 0 10 0 3707.84 3832.19 130.15 o 2 10 0 20.31 47.33 15.57 o 4 10 0 22.19 44.61 28.34 o 6 10 0 139.17 144.46 25.85 o 8 10 0 686.31 637.26 70.43 o 10 10 0 138.49 142.76 36.84 o 2 11 0 4284.04 4284.77 221.55 o 4 11 0 14171.38 14074.69 1947.58 o 6 11 0 10339.57 9426.06 1987.47 o 8 11 0 3998.22 3746.83 698.08 o 10 11 0 1286.21 1277.97 231.50 o 0 12 0 22689.04 22504.72 599.74 o 2 12 0 5719.35 5577.46 220.45 o 4 12 0 3609.13 3558.34 329.24 o 6 12 0 11.36 66.26 28.87 o 8 12 0 575.67 572.07 87.81 o 10 12 0 515.81 514.21 127.18 o 2 13 0 61.97 80.15 25.24 o 4 13 0 351.89 341.10 34.32 o 6 13 0 14.18 29.55 35.45 o 8 13 0 1375.86 1268.33 254.20 o 10 13 0 0.33 18.03 38.30 o 0 14 0 4132.10 4192.87 148.32 o 2 14 0 7697.15 7971.34 211.50 o 4 14 0 2238.82 2308.79 81.53 o 6 14 0 650.53 656.25 122.51 o 8 14 0 176.07 245.11 55.12 o 2 15 0 79.00 104.92 26.04 o 4 15 0 863.23 917.39 52.99 o 6 15 0 776.99 841.85 65.95 o 8 15 0 2167.26 2096.60 599.49 o 0 16 0 1769.87 1840.20 86.02 o 2 16 0 1751.92 1601.81 99.85 o 4 16 0 129.96 74.39 83.01 o 6 16 0 79.64 79.04 45.70 o 2 17 0 785.87 791.04 169.82 o 4 17 0 5001.98 5151.53 258.46 o 6 17 0 2672.90 2418.96 147.20 o 0 18 0 995.74 1048.04 106.85 o 2 18 0 1029.27 1142.69 108.46 o 4 18 0 499.98 578.21 83.11 o 1 0 1 9172.17 8229.21 195.41 o 2 0 1 1914.59 2053.72 79.87 o 3 0 1 18988.25 19974.05 942.86 o 4 0 1 21051.79 21379.60 694.95 o 5 0 1 26793.45 26751.94 676.43 o 6 0 1 3867.71 3852.48 200.23 o 7 0 1 10537.79 10693.48 1011.59 o 8 0 1 10489.12 11371.42 763.50 o 9 0 1 2660.26 2835.73 156.63 o 10 0 1 234.18 283.03 43.35 o 11 0 1 1573.35 1558.92 98.56 o 12 0 1 96.07 115.95 47.47 o 13 0 1 13.11 1.00 48.22 o 0 1 1 39.13 57.45 7.36 o 1 1 1 15854.67 14007.85 687.44 o 2 1 1 17632.18 17504.06 577.88 o 3 1 1 4699.38 5213.36 149.24 o 4 1 1 175.39 182.30 8.68 o 5 1 1 11.65 2.30 7.62 o 6 1 1 37.71 38.87 9.91 o 7 1 1 100.38 127.42 14.11 o 8 1 1 283.15 307.05 24.30 o 9 1 1 828.44 880.12 65.16 o 10 1 1 616.45 606.88 34.88 o 11 1 1 130.47 142.99 29.86 o 12 1 1 367.12 450.65 39.87 o 13 1 1 87.72 128.85 36.61 o 1 2 1 5.30 13.85 5.04 o 2 2 1 224.78 218.86 12.86 o 3 2 1 3031.97 3171.04 95.36 o 4 2 1 1595.58 1553.09 45.60 o 5 2 1 3227.53 3285.90 123.96 o 6 2 1 2102.07 2228.43 72.43 o 7 2 1 5911.33 6095.23 189.39 o 8 2 1 334.96 339.31 22.05 o 9 2 1 3066.22 3136.19 121.85 o 10 2 1 820.85 891.48 42.63 o 11 2 1 347.10 401.20 33.56 o 12 2 1 18.45 58.61 31.60 o 13 2 1 69.42 80.81 36.77 o 0 3 1 11348.91 10511.29 367.02 o 1 3 1 22880.94 21304.82 1062.63 o 2 3 1 6912.92 6749.63 392.11 o 3 3 1 26335.68 23902.96 905.34 o 4 3 1 2847.00 2899.35 103.39 o 5 3 1 1399.00 1515.08 79.20 o 6 3 1 301.29 340.33 17.03 o 7 3 1 136.40 192.78 20.82 o 8 3 1 77.77 91.07 18.24 o 9 3 1 1369.24 1350.71 49.96 o 10 3 1 1387.75 1421.01 79.89 o 11 3 1 2542.13 2593.15 152.44 o 12 3 1 520.81 616.82 42.95 o 13 3 1 1783.04 1865.00 99.24 o 1 4 1 2139.23 2334.20 104.91 o 2 4 1 1195.63 1294.37 79.12 o 3 4 1 223.57 225.41 15.05 o 4 4 1 766.59 785.73 35.20 o 5 4 1 600.85 592.71 24.82 o 6 4 1 61.57 91.23 11.24 o 7 4 1 1434.13 1378.75 80.14 o 8 4 1 411.92 456.22 43.01 o 9 4 1 129.94 154.98 23.07 o 10 4 1 224.03 174.03 25.98 o 11 4 1 455.05 449.85 42.32 o 12 4 1 33.95 51.23 33.27 o 13 4 1 21.28 69.73 37.26 o 0 5 1 10919.68 11062.42 521.71 o 1 5 1 16154.47 15332.72 585.27 o 2 5 1 12864.67 12405.34 867.69 o 3 5 1 3845.83 3755.10 271.61 o 4 5 1 1361.88 1258.21 78.30 o 5 5 1 3232.09 3267.23 160.11 o 6 5 1 38.58 42.77 11.80 o 7 5 1 54.97 59.68 12.92 o 8 5 1 1113.38 1064.13 94.14 o 9 5 1 1343.72 1302.88 119.21 o 10 5 1 492.44 479.54 59.63 o 11 5 1 1413.23 1447.57 130.03 o 12 5 1 982.10 961.72 76.22 o 13 5 1 1025.09 1175.90 107.80 o 1 6 1 939.31 1158.99 69.82 o 2 6 1 6909.16 7108.91 472.49 o 3 6 1 9426.09 8708.55 668.26 o 4 6 1 6890.30 6433.84 485.47 o 5 6 1 10215.72 9667.31 703.49 o 6 6 1 7873.75 7515.60 514.68 o 7 6 1 7431.77 7050.80 528.21 o 8 6 1 3049.75 2860.77 232.76 o 9 6 1 6401.58 5955.11 541.31 o 10 6 1 363.49 435.98 34.66 o 11 6 1 377.00 444.51 46.21 o 12 6 1 89.71 142.99 38.32 o 13 6 1 53.42 106.72 42.21 o 0 7 1 276.40 321.58 16.06 o 1 7 1 3.88 41.27 17.23 o 2 7 1 3267.68 3479.95 224.35 o 3 7 1 178.66 224.45 12.02 o 4 7 1 0.83 -6.36 10.57 o 5 7 1 140.75 142.27 12.36 o 6 7 1 1.04 -7.45 14.44 o 7 7 1 475.77 447.21 60.02 o 8 7 1 160.65 144.78 22.10 o 9 7 1 92.17 78.00 21.55 o 10 7 1 6.14 5.56 24.12 o 11 7 1 1.41 12.54 28.70 o 12 7 1 61.33 110.87 33.43 o 1 8 1 2125.40 2461.95 109.38 o 2 8 1 138.95 152.53 15.56 o 3 8 1 5569.94 5347.75 371.96 o 4 8 1 1959.12 1870.87 166.55 o 5 8 1 7184.90 6704.39 655.21 o 6 8 1 2097.96 2050.58 208.16 o 7 8 1 5694.02 5324.61 572.73 o 8 8 1 1218.44 1087.76 134.55 o 9 8 1 1964.37 1834.95 186.50 o 10 8 1 854.92 833.91 109.63 o 11 8 1 406.92 425.81 51.03 o 12 8 1 8.44 31.33 33.04 o 0 9 1 4487.43 4714.60 160.33 o 1 9 1 11484.56 11545.05 402.80 o 2 9 1 1874.52 1744.26 99.10 o 3 9 1 5962.77 5786.26 340.24 o 4 9 1 1447.57 1452.33 121.16 o 5 9 1 1647.95 1538.22 167.21 o 6 9 1 220.29 217.70 19.29 o 7 9 1 27.35 43.96 17.84 o 8 9 1 6.57 21.36 19.67 o 9 9 1 229.48 221.18 30.81 o 10 9 1 631.95 670.93 79.25 o 11 9 1 969.70 928.13 107.32 o 12 9 1 248.75 237.35 38.55 o 1 10 1 632.20 650.33 23.29 o 2 10 1 267.26 304.84 27.15 o 3 10 1 4.50 0.89 13.55 o 4 10 1 209.85 236.57 30.47 o 5 10 1 467.58 499.11 56.23 o 6 10 1 107.04 99.38 18.71 o 7 10 1 40.02 54.58 20.11 o 8 10 1 61.03 39.79 20.70 o 9 10 1 90.45 59.94 22.63 o 10 10 1 60.52 62.76 29.47 o 11 10 1 12.77 22.93 26.73 o 0 11 1 4139.77 4233.73 114.96 o 1 11 1 12144.84 12233.92 361.01 o 2 11 1 5840.69 5940.46 278.30 o 3 11 1 4123.67 4171.02 264.89 o 4 11 1 1025.50 1038.32 73.42 o 5 11 1 881.66 902.49 67.22 o 6 11 1 6.28 26.27 18.33 o 7 11 1 248.86 233.88 22.73 o 8 11 1 475.97 484.89 65.28 o 9 11 1 902.36 862.12 83.30 o 10 11 1 775.02 721.02 74.46 o 11 11 1 902.65 916.95 80.70 o 1 12 1 656.66 747.01 23.29 o 2 12 1 530.94 577.97 25.73 o 3 12 1 2438.23 2486.60 131.24 o 4 12 1 2316.24 2212.51 153.03 o 5 12 1 3927.18 3701.27 278.93 o 6 12 1 1177.64 1129.50 98.82 o 7 12 1 1929.82 1799.39 183.66 o 8 12 1 2081.81 1858.91 219.87 o 9 12 1 688.69 694.45 118.94 o 10 12 1 128.11 120.43 30.09 o 0 13 1 1201.64 1096.00 116.53 o 1 13 1 72.48 99.73 16.22 o 2 13 1 222.30 238.63 18.66 o 3 13 1 549.07 569.01 29.67 o 4 13 1 136.74 140.34 23.10 o 5 13 1 7.73 -18.47 21.91 o 6 13 1 51.21 77.58 25.02 o 7 13 1 32.96 53.05 25.20 o 8 13 1 43.38 34.03 25.23 o 9 13 1 170.95 218.72 41.53 o 10 13 1 2.32 11.73 29.78 o 1 14 1 654.08 690.49 29.82 o 2 14 1 625.78 628.65 31.95 o 3 14 1 1014.22 1060.07 42.37 o 4 14 1 1002.44 1116.30 63.59 o 5 14 1 3012.89 2820.36 98.16 o 6 14 1 1941.31 1749.11 96.98 o 7 14 1 3863.42 3415.13 343.66 o 8 14 1 368.14 400.58 49.44 o 9 14 1 1588.55 1450.69 147.58 o 0 15 1 1484.31 1506.26 164.87 o 1 15 1 1107.91 1154.57 65.40 o 2 15 1 271.09 288.35 27.57 o 3 15 1 1607.10 1571.59 64.46 o 4 15 1 470.29 442.02 31.68 o 5 15 1 351.33 341.75 31.75 o 6 15 1 40.20 -9.18 31.44 o 7 15 1 215.90 196.66 35.46 o 8 15 1 0.85 -6.17 33.76 o 1 16 1 16.79 14.50 31.55 o 2 16 1 339.56 396.82 36.18 o 3 16 1 730.15 773.20 38.94 o 4 16 1 173.84 219.76 29.83 o 5 16 1 866.72 836.38 44.65 o 6 16 1 530.07 449.67 37.67 o 7 16 1 296.78 246.49 33.92 o 0 17 1 2794.79 2414.89 399.71 o 1 17 1 3407.71 3006.10 304.35 o 2 17 1 1204.13 1260.04 64.96 o 3 17 1 1857.06 1836.40 67.42 o 4 17 1 560.97 522.75 37.14 o 5 17 1 384.87 432.69 37.34 o 6 17 1 0.52 30.74 53.49 o 1 18 1 6.52 -5.55 41.09 o 2 18 1 258.89 237.30 61.73 o 3 18 1 69.05 66.26 35.17 o 4 18 1 129.02 196.85 36.76 o 0 0 2 4539.89 4765.32 166.11 o 1 0 2 22234.47 18632.75 438.98 o 2 0 2 5299.11 5280.52 174.45 o 3 0 2 24750.77 23149.24 690.62 o 4 0 2 61.74 39.51 10.34 o 5 0 2 1206.18 1078.08 44.73 o 6 0 2 293.32 277.26 24.56 o 7 0 2 12.58 52.57 15.91 o 8 0 2 301.41 273.24 24.21 o 9 0 2 2261.66 2193.23 233.29 o 10 0 2 6.64 -2.47 30.28 o 11 0 2 3659.91 3708.15 518.27 o 12 0 2 187.30 169.25 54.33 o 13 0 2 1596.62 1666.99 295.13 o 1 1 2 1671.11 1513.00 30.40 o 2 1 2 3.16 22.14 9.93 o 3 1 2 735.09 719.00 16.08 o 4 1 2 2187.51 2452.80 65.48 o 5 1 2 1994.50 1923.86 58.96 o 6 1 2 171.93 201.31 12.00 o 7 1 2 3749.68 3775.04 152.97 o 8 1 2 426.66 457.43 24.98 o 9 1 2 1152.02 1061.18 49.39 o 10 1 2 31.93 24.26 24.26 o 11 1 2 85.44 143.38 28.88 o 12 1 2 37.25 -11.92 35.15 o 13 1 2 2.41 47.74 52.19 o 0 2 2 3425.39 3148.28 149.15 o 1 2 2 16987.23 15620.43 262.02 o 2 2 2 1195.29 1191.92 35.36 o 3 2 2 1946.10 1831.30 47.31 o 4 2 2 2170.33 2315.02 79.80 o 5 2 2 2417.15 2449.80 71.19 o 6 2 2 31.91 35.11 10.22 o 7 2 2 317.47 305.65 20.57 o 8 2 2 34.03 44.00 13.12 o 9 2 2 750.78 818.47 30.10 o 10 2 2 462.84 453.92 34.74 o 11 2 2 828.86 882.17 48.09 o 12 2 2 168.89 178.93 33.75 o 13 2 2 696.90 766.39 51.51 o 1 3 2 3082.85 3065.94 60.83 o 2 3 2 482.87 465.06 21.16 o 3 3 2 7127.82 6638.71 263.52 o 4 3 2 3331.29 3355.47 128.03 o 5 3 2 19435.88 18536.75 738.65 o 6 3 2 2079.75 2032.85 76.70 o 7 3 2 9814.82 9443.88 429.95 o 8 3 2 2094.54 2028.21 111.00 o 9 3 2 4667.71 4693.72 248.33 o 10 3 2 729.86 732.53 31.44 o 11 3 2 1529.89 1655.76 110.19 o 12 3 2 123.40 142.37 33.00 o 13 3 2 6.16 -1.75 35.25 o 0 4 2 3865.05 3925.56 120.81 o 1 4 2 2097.47 2000.21 48.15 o 2 4 2 30.18 19.11 7.70 o 3 4 2 595.36 575.45 36.89 o 4 4 2 463.65 493.55 22.20 o 5 4 2 661.92 645.49 28.11 o 6 4 2 3.61 11.64 10.49 o 7 4 2 193.10 203.76 15.53 o 8 4 2 1.18 5.64 15.40 o 9 4 2 230.77 252.83 26.36 o 10 4 2 21.58 2.32 23.77 o 11 4 2 155.25 155.62 28.07 o 12 4 2 18.09 -13.84 32.61 o 13 4 2 173.66 135.34 42.85 o 1 5 2 3476.75 3771.52 105.41 o 2 5 2 253.12 274.74 12.43 o 3 5 2 6438.65 6368.42 354.31 o 4 5 2 54.08 54.46 9.85 o 5 5 2 7302.38 7136.49 415.32 o 6 5 2 1226.69 1252.65 83.94 o 7 5 2 6046.58 5886.63 472.30 o 8 5 2 497.48 508.72 36.24 o 9 5 2 1117.00 1109.72 97.10 o 10 5 2 365.56 369.07 40.22 o 11 5 2 183.92 240.41 35.32 o 12 5 2 91.00 75.28 29.95 o 0 6 2 91.69 118.20 18.85 o 1 6 2 24533.90 24767.89 696.29 o 2 6 2 2931.24 3245.87 106.50 o 3 6 2 8400.81 8156.13 353.32 o 4 6 2 505.17 515.31 37.28 o 5 6 2 2543.88 2620.74 185.79 o 6 6 2 820.30 866.30 85.36 o 7 6 2 1494.11 1473.76 141.22 o 8 6 2 3.21 21.78 19.62 o 9 6 2 417.41 412.51 55.50 o 10 6 2 94.49 62.78 26.64 o 11 6 2 2040.02 1914.98 162.89 o 12 6 2 230.09 219.91 33.37 o 1 7 2 2643.43 3004.71 89.95 o 2 7 2 163.95 176.65 9.47 o 3 7 2 0.44 9.03 8.22 o 4 7 2 153.97 179.57 12.77 o 5 7 2 262.74 299.73 17.72 o 6 7 2 83.81 82.55 14.57 o 7 7 2 212.30 253.40 24.87 o 8 7 2 71.11 95.39 21.23 o 9 7 2 49.83 48.10 23.59 o 10 7 2 1.49 -39.41 26.27 o 11 7 2 83.43 98.90 29.41 o 12 7 2 21.68 19.42 30.69 o 0 8 2 3717.66 3914.42 100.28 o 1 8 2 10241.49 10452.96 325.38 o 2 8 2 2402.78 2436.66 82.00 o 3 8 2 5508.83 5655.13 287.76 o 4 8 2 936.59 990.19 62.26 o 5 8 2 1224.77 1215.25 83.57 o 6 8 2 24.54 43.31 16.62 o 7 8 2 23.61 51.62 18.24 o 8 8 2 1.03 -2.19 22.34 o 9 8 2 1756.65 1714.35 203.61 o 10 8 2 395.52 382.73 34.73 o 11 8 2 1402.63 1411.40 147.94 o 1 9 2 241.22 269.44 15.00 o 2 9 2 720.63 737.78 49.12 o 3 9 2 3260.86 3195.37 178.48 o 4 9 2 503.83 513.33 40.80 o 5 9 2 6903.94 6919.48 630.34 o 6 9 2 1648.69 1722.96 152.62 o 7 9 2 4462.52 4738.70 477.17 o 8 9 2 323.85 387.06 31.46 o 9 9 2 3052.20 3155.00 396.41 o 10 9 2 393.77 401.08 46.01 o 11 9 2 758.62 794.92 54.23 o 0 10 2 68.58 58.06 17.76 o 1 10 2 1.15 -8.01 15.36 o 2 10 2 1.43 -7.10 15.11 o 3 10 2 493.67 515.49 35.70 o 4 10 2 2.64 -14.27 17.88 o 5 10 2 592.52 635.92 31.63 o 6 10 2 4.21 -22.78 21.69 o 7 10 2 2.42 9.44 21.27 o 8 10 2 121.54 160.42 25.54 o 9 10 2 243.05 227.82 31.65 o 10 10 2 35.23 31.61 32.24 o 11 10 2 29.78 -0.59 34.27 o 1 11 2 212.09 246.34 21.23 o 2 11 2 144.36 128.35 18.96 o 3 11 2 4629.48 4618.68 171.89 o 4 11 2 1191.25 1226.94 99.05 o 5 11 2 4554.18 4533.96 407.97 o 6 11 2 320.18 351.07 29.37 o 7 11 2 5003.86 4942.30 588.87 o 8 11 2 580.47 601.01 48.48 o 9 11 2 2049.41 2019.78 262.00 o 10 11 2 84.12 106.23 38.79 o 0 12 2 292.35 325.38 44.83 o 1 12 2 3811.79 3533.72 158.17 o 2 12 2 987.13 960.99 53.18 o 3 12 2 4597.99 4565.18 220.56 o 4 12 2 17.91 24.02 22.14 o 5 12 2 333.69 362.08 36.97 o 6 12 2 50.25 62.16 24.96 o 7 12 2 88.81 113.20 28.05 o 8 12 2 8.06 26.59 29.46 o 9 12 2 433.40 448.20 37.45 o 10 12 2 1.82 -22.39 40.53 o 1 13 2 61.26 21.08 24.85 o 2 13 2 11.67 -6.47 23.13 o 3 13 2 447.62 453.04 28.74 o 4 13 2 35.42 32.68 23.84 o 5 13 2 585.09 607.52 51.71 o 6 13 2 280.75 290.32 30.72 o 7 13 2 105.03 92.45 29.52 o 8 13 2 136.50 136.76 31.07 o 9 13 2 0.83 52.43 33.40 o 0 14 2 2053.51 1957.88 224.38 o 1 14 2 6716.84 6033.87 462.41 o 2 14 2 222.51 222.84 32.80 o 3 14 2 2962.13 2887.40 109.50 o 4 14 2 1039.93 1084.51 48.56 o 5 14 2 359.22 386.45 72.53 o 6 14 2 84.74 7.97 31.78 o 7 14 2 30.83 35.47 29.73 o 8 14 2 0.83 6.14 32.64 o 1 15 2 72.09 83.08 30.14 o 2 15 2 0.48 11.76 32.59 o 3 15 2 746.04 760.11 47.98 o 4 15 2 104.71 99.65 27.97 o 5 15 2 1356.16 1367.84 73.83 o 6 15 2 81.28 15.94 29.41 o 7 15 2 913.40 858.72 46.08 o 0 16 2 115.21 19.95 81.20 o 1 16 2 672.30 734.97 107.38 o 2 16 2 189.82 218.72 37.53 o 3 16 2 294.40 370.38 41.33 o 4 16 2 11.27 26.25 37.19 o 5 16 2 7.37 -24.46 38.50 o 6 16 2 1.51 -6.49 32.97 o 1 17 2 347.98 282.76 68.47 o 2 17 2 71.17 57.58 45.15 o 3 17 2 1536.67 1538.01 135.51 o 4 17 2 128.44 157.95 42.64 o 5 17 2 2107.21 2138.84 153.16 o 0 18 2 25.95 -15.20 168.22 o 1 18 2 839.90 676.85 133.80 o 2 18 2 1.09 -13.67 41.89 o 1 0 3 313.50 315.20 19.91 o 2 0 3 2436.42 2354.74 91.69 o 3 0 3 399.06 358.82 18.66 o 4 0 3 7877.63 7577.29 208.60 o 5 0 3 625.27 585.25 26.46 o 6 0 3 8796.92 8207.57 252.68 o 7 0 3 278.12 277.56 21.78 o 8 0 3 8135.98 7543.20 310.22 o 9 0 3 230.42 209.63 28.39 o 10 0 3 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