#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:31:57 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181248 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/26/2232655.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232655_Fobs loop_ _publ_author_name 'Jin, Yu' _publ_section_title ; Tetraaquabis(2-methyl-1H-imidazole-\kN^3^)cobalt(II) naphthalene-1,5-disulfonate ; _journal_coeditor_code FJ2459 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1686 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.269 _cell_angle_gamma 90.000 _cell_length_a 8.0260 _cell_length_b 12.9234 _cell_length_c 11.6584 _exptl_crystal_F_000 602.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file fj2459Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 130.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6727.51 6803.82 87.77 o 4 0 0 1972.82 2040.26 265.93 o 6 0 0 42.90 59.67 7.28 o 8 0 0 36.85 31.75 3.20 o 10 0 0 290.67 294.56 15.88 o 1 1 0 6052.93 6005.66 78.39 o 2 1 0 183.25 222.57 2.15 o 3 1 0 4286.97 4270.05 48.83 o 4 1 0 1212.90 1253.70 15.65 o 5 1 0 629.64 634.13 8.21 o 6 1 0 630.31 614.42 30.66 o 7 1 0 142.29 156.83 11.14 o 8 1 0 251.10 259.02 7.90 o 9 1 0 1.41 2.51 1.50 o 10 1 0 96.46 99.12 6.08 o 1 2 0 5845.71 5801.72 71.41 o 2 2 0 119.47 126.44 2.73 o 3 2 0 286.59 295.40 4.99 o 4 2 0 6.63 23.76 1.38 o 5 2 0 270.55 244.78 5.68 o 6 2 0 2095.80 2087.45 44.17 o 7 2 0 349.32 341.62 8.73 o 8 2 0 18.03 27.80 6.44 o 9 2 0 4.74 5.10 1.60 o 10 2 0 150.71 155.51 8.90 o 1 3 0 693.34 779.33 10.23 o 2 3 0 9.96 5.72 0.66 o 3 3 0 57.51 71.03 1.71 o 4 3 0 2779.13 2980.03 45.30 o 5 3 0 1050.42 1007.39 16.54 o 6 3 0 811.22 790.91 14.79 o 7 3 0 7.94 10.30 1.22 o 8 3 0 150.14 150.35 10.02 o 9 3 0 993.69 1102.67 183.66 o 10 3 0 73.04 74.21 5.48 o 0 4 0 405.63 409.71 10.53 o 1 4 0 866.70 826.67 7.79 o 2 4 0 2016.07 1729.82 18.07 o 3 4 0 1066.28 997.58 25.06 o 4 4 0 542.18 519.60 7.73 o 5 4 0 936.78 908.45 15.28 o 6 4 0 1277.50 1256.89 24.02 o 7 4 0 208.80 203.44 5.39 o 8 4 0 186.85 192.13 5.55 o 9 4 0 59.92 71.87 9.69 o 1 5 0 1897.80 1885.39 17.54 o 2 5 0 26.04 24.58 1.16 o 3 5 0 2369.35 2397.80 21.96 o 4 5 0 166.23 178.06 3.75 o 5 5 0 1157.16 1051.21 17.35 o 6 5 0 446.60 423.37 9.11 o 7 5 0 156.31 158.73 4.23 o 8 5 0 422.77 430.48 13.17 o 9 5 0 28.97 26.61 4.15 o 0 6 0 8189.61 7875.85 203.34 o 1 6 0 740.56 782.95 7.99 o 2 6 0 3274.88 3401.96 50.93 o 3 6 0 817.43 905.24 12.52 o 4 6 0 581.21 597.26 12.68 o 5 6 0 1008.44 990.92 22.53 o 6 6 0 85.20 84.34 3.56 o 7 6 0 7.46 9.39 1.72 o 8 6 0 48.96 45.45 3.42 o 9 6 0 73.78 64.44 5.10 o 1 7 0 1528.51 1567.30 24.52 o 2 7 0 1229.49 1319.72 20.47 o 3 7 0 2718.36 2716.76 43.95 o 4 7 0 0.96 5.17 1.97 o 5 7 0 3.86 8.10 1.76 o 6 7 0 75.21 88.66 3.97 o 7 7 0 1062.19 1076.89 30.45 o 8 7 0 17.56 18.11 2.51 o 9 7 0 181.27 170.47 8.86 o 0 8 0 2606.32 2695.65 52.88 o 1 8 0 287.91 246.40 3.53 o 2 8 0 331.86 348.90 6.39 o 3 8 0 198.32 202.43 3.98 o 4 8 0 765.41 775.34 18.25 o 5 8 0 13.46 18.06 1.92 o 6 8 0 2.30 2.23 1.40 o 7 8 0 21.05 23.82 2.97 o 8 8 0 270.12 265.68 10.18 o 9 8 0 4.96 4.18 2.44 o 1 9 0 904.01 864.10 12.82 o 2 9 0 55.09 52.25 2.00 o 3 9 0 209.91 209.57 4.36 o 4 9 0 117.56 133.93 4.66 o 5 9 0 3.06 11.89 1.85 o 6 9 0 14.08 16.92 2.30 o 7 9 0 230.04 235.14 8.92 o 8 9 0 158.13 165.72 7.72 o 0 10 0 431.78 419.23 9.47 o 1 10 0 550.59 579.80 13.59 o 2 10 0 3154.97 3089.25 63.15 o 3 10 0 88.41 92.13 2.91 o 4 10 0 25.67 24.91 2.23 o 5 10 0 55.58 58.06 3.34 o 6 10 0 180.60 179.04 7.08 o 7 10 0 25.72 27.83 3.27 o 8 10 0 212.53 211.88 9.64 o 1 11 0 803.87 814.99 19.98 o 2 11 0 1103.33 1072.12 22.90 o 3 11 0 178.61 181.56 4.91 o 4 11 0 368.65 357.39 10.93 o 5 11 0 326.64 327.64 10.83 o 6 11 0 128.92 120.28 6.13 o 7 11 0 21.82 24.68 2.86 o 0 12 0 607.75 612.22 23.24 o 1 12 0 22.88 29.07 3.26 o 2 12 0 816.94 813.35 18.34 o 3 12 0 221.61 219.73 5.97 o 4 12 0 311.15 301.89 10.01 o 5 12 0 243.52 239.65 8.91 o 6 12 0 6.56 7.60 2.04 o 7 12 0 2.82 3.27 1.90 o 1 13 0 359.01 342.61 8.71 o 2 13 0 207.91 202.47 6.10 o 3 13 0 362.12 360.20 11.43 o 4 13 0 377.88 355.14 11.95 o 5 13 0 92.66 92.50 5.27 o 6 13 0 233.72 234.00 9.99 o 0 14 0 429.00 453.62 19.68 o 1 14 0 197.47 196.45 7.50 o 2 14 0 1.51 0.09 1.24 o 3 14 0 5.15 12.53 2.20 o 4 14 0 665.69 649.83 21.77 o 5 14 0 66.02 68.28 4.67 o 1 15 0 56.72 63.40 3.88 o 2 15 0 0.50 0.91 2.29 o 3 15 0 176.45 193.24 10.45 o 4 15 0 87.27 97.02 6.90 o 0 16 0 17.79 29.38 4.05 o 1 16 0 16.50 21.15 2.75 o 2 16 0 130.19 130.20 7.99 o 3 16 0 6.05 8.94 5.18 o -9 0 1 108.51 101.22 6.32 o -7 0 1 109.69 103.38 4.66 o -5 0 1 5542.83 6251.80 884.44 o -3 0 1 670.32 781.49 108.22 o 1 0 1 1019.84 971.97 6.88 o 3 0 1 3403.46 3282.03 65.84 o 5 0 1 112.02 107.01 15.41 o 7 0 1 647.81 657.88 22.30 o 9 0 1 657.00 652.02 27.34 o -10 1 1 4.19 4.04 2.19 o -9 1 1 102.42 114.45 4.79 o -8 1 1 198.89 201.43 6.23 o -7 1 1 427.71 436.08 34.17 o -6 1 1 1928.94 1988.43 99.85 o -5 1 1 102.84 112.82 3.24 o -4 1 1 1770.49 1827.27 23.99 o -3 1 1 522.68 582.33 6.23 o -2 1 1 3037.66 2842.74 97.30 o -1 1 1 2036.87 2031.04 18.52 o 1 1 1 1788.26 1791.55 16.19 o 2 1 1 2079.06 2137.57 16.40 o 3 1 1 2315.17 2175.61 24.32 o 4 1 1 139.54 133.25 2.29 o 5 1 1 92.39 108.86 1.81 o 6 1 1 2122.46 2159.92 145.42 o 7 1 1 548.42 568.20 39.34 o 8 1 1 501.19 510.70 14.02 o 9 1 1 12.28 15.26 2.10 o 10 1 1 11.47 16.74 3.50 o -10 2 1 41.07 32.55 3.78 o -9 2 1 4.85 6.52 1.63 o -8 2 1 21.94 24.96 3.73 o -7 2 1 1895.49 2022.21 198.29 o -6 2 1 992.59 995.34 18.87 o -5 2 1 1636.48 1747.82 28.57 o -4 2 1 548.82 575.30 7.82 o -3 2 1 2064.88 2145.89 21.67 o -2 2 1 5420.81 5589.46 52.88 o -1 2 1 523.76 570.32 4.44 o 0 2 1 2878.62 2838.91 23.01 o 1 2 1 5269.66 5179.39 41.98 o 2 2 1 5734.99 5699.57 64.35 o 3 2 1 143.62 138.97 1.86 o 4 2 1 3.85 9.04 2.24 o 5 2 1 2166.30 2127.32 44.83 o 6 2 1 122.35 116.26 3.61 o 7 2 1 554.44 546.16 11.44 o 8 2 1 173.93 192.92 18.72 o 9 2 1 64.28 87.29 16.26 o 10 2 1 213.63 201.51 9.94 o -10 3 1 768.65 757.12 29.52 o -9 3 1 36.53 51.42 8.39 o -8 3 1 3.66 8.30 2.07 o -7 3 1 1.19 8.51 2.05 o -6 3 1 1515.67 1494.43 27.65 o -5 3 1 469.57 459.27 7.71 o -4 3 1 852.73 781.90 8.85 o -3 3 1 2762.55 3212.78 33.37 o -2 3 1 44.39 36.74 0.85 o -1 3 1 33.12 57.15 0.91 o 1 3 1 2272.22 2294.16 21.59 o 2 3 1 1128.51 1142.47 7.80 o 3 3 1 1084.88 1002.76 12.86 o 4 3 1 3548.94 3417.17 54.36 o 5 3 1 655.78 704.76 12.12 o 6 3 1 13.12 18.98 1.62 o 7 3 1 36.94 43.22 3.84 o 8 3 1 713.07 707.05 19.26 o 9 3 1 10.31 10.08 4.85 o -10 4 1 9.17 15.04 4.34 o -9 4 1 102.30 124.67 12.07 o -8 4 1 128.51 127.13 4.09 o -7 4 1 1069.99 1037.59 21.76 o -6 4 1 294.68 303.76 6.32 o -5 4 1 509.19 497.40 8.26 o -4 4 1 16.25 31.99 1.69 o -3 4 1 531.41 443.37 5.62 o -2 4 1 3456.36 3537.62 21.15 o -1 4 1 491.38 574.81 6.11 o 0 4 1 3968.39 3939.72 40.21 o 1 4 1 1164.12 1106.88 10.02 o 2 4 1 153.34 165.89 1.59 o 3 4 1 1543.82 1508.80 19.93 o 4 4 1 1237.85 1340.29 20.39 o 5 4 1 347.48 332.20 6.23 o 6 4 1 10.73 14.58 1.24 o 7 4 1 1561.25 1525.23 33.26 o 8 4 1 44.96 50.73 2.63 o 9 4 1 11.45 20.63 7.45 o -9 5 1 229.03 219.84 12.26 o -8 5 1 164.24 158.59 6.92 o -7 5 1 83.16 67.47 2.80 o -6 5 1 597.15 591.44 11.37 o -5 5 1 0.24 2.12 1.26 o -4 5 1 621.47 597.47 5.98 o -3 5 1 236.93 272.65 4.61 o -2 5 1 885.48 787.03 10.21 o -1 5 1 718.43 735.59 6.92 o 0 5 1 858.37 861.24 8.91 o 1 5 1 19.57 10.53 0.68 o 2 5 1 110.73 79.46 2.96 o 3 5 1 122.37 100.87 2.34 o 4 5 1 2102.06 2218.15 34.46 o 5 5 1 22.48 20.53 1.59 o 6 5 1 723.88 706.50 14.04 o 7 5 1 536.94 514.78 12.11 o 8 5 1 88.30 89.46 4.35 o 9 5 1 222.94 232.40 11.17 o -9 6 1 575.84 564.97 19.04 o -8 6 1 33.15 40.30 3.08 o -7 6 1 1.69 4.26 1.43 o -6 6 1 139.77 130.82 4.53 o -5 6 1 795.75 733.39 16.77 o -4 6 1 11.11 4.03 0.81 o -3 6 1 713.40 675.89 9.80 o -2 6 1 133.63 116.56 2.20 o -1 6 1 1048.42 900.27 9.55 o 0 6 1 180.27 184.44 2.60 o 1 6 1 4990.12 5130.61 63.04 o 2 6 1 58.01 80.40 1.25 o 3 6 1 817.62 719.05 17.75 o 4 6 1 60.14 58.39 1.26 o 5 6 1 47.39 49.02 1.50 o 6 6 1 68.22 78.42 4.22 o 7 6 1 232.92 214.12 7.34 o 8 6 1 118.37 131.11 5.70 o 9 6 1 444.92 444.59 18.91 o -9 7 1 34.29 40.98 3.48 o -8 7 1 949.28 967.15 29.73 o -7 7 1 22.44 22.17 2.28 o -6 7 1 113.99 104.13 4.27 o -5 7 1 282.63 276.39 7.94 o -4 7 1 1000.31 1003.99 15.47 o -3 7 1 38.12 25.16 1.96 o -2 7 1 2447.93 2481.40 40.06 o -1 7 1 8.85 18.22 1.09 o 0 7 1 313.74 300.23 3.95 o 1 7 1 99.39 107.64 1.81 o 2 7 1 2055.78 1987.03 31.58 o 3 7 1 281.39 301.21 4.80 o 4 7 1 6.10 6.19 1.32 o 5 7 1 53.84 62.07 2.96 o 6 7 1 2018.54 1925.32 51.30 o 7 7 1 274.09 255.49 8.84 o 8 7 1 1.25 2.12 1.64 o 9 7 1 7.58 9.84 3.84 o -9 8 1 86.25 87.20 5.30 o -8 8 1 32.48 30.26 3.19 o -7 8 1 49.97 55.49 3.52 o -6 8 1 499.09 479.91 13.78 o -5 8 1 3105.27 3024.63 78.90 o -4 8 1 492.52 492.57 8.51 o -3 8 1 640.16 644.36 11.35 o -2 8 1 2001.59 2048.83 35.76 o -1 8 1 18.26 8.36 0.49 o 0 8 1 327.77 343.38 4.81 o 1 8 1 806.93 781.45 18.19 o 2 8 1 495.39 526.05 9.24 o 3 8 1 1494.62 1503.63 25.60 o 4 8 1 74.69 77.94 3.26 o 5 8 1 238.49 232.82 7.09 o 6 8 1 140.81 141.35 5.78 o 7 8 1 214.00 186.29 7.38 o 8 8 1 144.23 150.91 6.90 o -8 9 1 109.47 114.92 6.00 o -7 9 1 22.88 26.85 3.79 o -6 9 1 624.73 571.72 16.89 o -5 9 1 0.73 4.57 4.06 o -4 9 1 326.29 320.09 8.88 o -3 9 1 69.20 79.26 2.43 o -2 9 1 562.70 565.98 10.55 o -1 9 1 193.39 184.20 4.74 o 0 9 1 1608.05 1639.61 24.29 o 1 9 1 219.69 212.05 3.62 o 2 9 1 6.16 8.50 1.18 o 3 9 1 613.62 589.78 11.14 o 4 9 1 409.14 384.99 10.16 o 5 9 1 551.39 561.45 15.49 o 6 9 1 257.36 250.99 8.68 o 7 9 1 226.83 204.97 8.29 o 8 9 1 369.93 353.72 13.28 o -8 10 1 18.49 20.38 3.06 o -7 10 1 771.57 751.54 24.57 o -6 10 1 74.27 61.96 3.84 o -5 10 1 150.88 148.40 5.71 o -4 10 1 944.14 926.65 23.99 o -3 10 1 1795.66 1799.09 36.36 o -2 10 1 33.54 29.27 2.85 o -1 10 1 1132.15 1125.80 25.27 o 0 10 1 9.54 14.40 0.95 o 1 10 1 1334.71 1332.50 30.21 o 2 10 1 178.74 174.71 4.59 o 3 10 1 26.67 31.06 1.69 o 4 10 1 31.62 31.96 2.89 o 5 10 1 737.79 708.34 19.98 o 6 10 1 34.08 35.42 4.15 o 7 10 1 466.43 475.56 16.57 o 8 10 1 0.03 4.03 3.20 o -7 11 1 1.60 2.21 1.89 o -6 11 1 382.50 360.81 12.35 o -5 11 1 62.22 70.14 3.91 o -4 11 1 409.24 414.82 12.29 o -3 11 1 75.34 70.42 2.86 o -2 11 1 15.18 17.77 3.31 o -1 11 1 22.93 22.15 3.24 o 0 11 1 364.64 373.15 6.59 o 1 11 1 8.34 11.74 1.93 o 2 11 1 41.67 42.67 2.14 o 3 11 1 297.37 291.83 7.01 o 4 11 1 1371.81 1383.35 38.66 o 5 11 1 12.92 19.61 3.74 o 6 11 1 71.83 74.71 4.36 o 7 11 1 73.82 60.91 4.35 o -7 12 1 58.57 61.62 4.45 o -6 12 1 129.43 130.93 6.42 o -5 12 1 27.58 24.11 2.59 o -4 12 1 41.29 45.32 3.19 o -3 12 1 274.45 273.89 7.26 o -2 12 1 923.44 904.18 20.37 o -1 12 1 619.49 590.55 12.96 o 0 12 1 787.73 780.06 20.47 o 1 12 1 150.91 156.03 4.32 o 2 12 1 113.43 107.02 3.68 o 3 12 1 339.94 333.80 10.32 o 4 12 1 35.66 32.18 2.76 o 5 12 1 43.46 38.87 3.17 o 6 12 1 120.27 111.72 5.66 o 7 12 1 209.04 211.31 9.32 o -6 13 1 37.56 40.14 3.64 o -5 13 1 68.65 72.51 4.33 o -4 13 1 236.11 228.79 9.01 o -3 13 1 0.69 0.74 1.58 o -2 13 1 885.28 880.02 21.15 o -1 13 1 7.91 9.08 1.37 o 0 13 1 1.20 2.08 1.42 o 1 13 1 153.85 161.78 4.72 o 2 13 1 1074.10 1046.96 24.87 o 3 13 1 230.20 219.27 7.96 o 4 13 1 18.70 15.85 2.27 o 5 13 1 15.84 20.61 3.21 o 6 13 1 273.78 272.49 11.01 o -5 14 1 303.55 310.42 12.56 o -4 14 1 128.54 134.26 6.28 o -3 14 1 33.11 31.31 2.73 o -2 14 1 82.44 89.09 4.52 o -1 14 1 1510.95 1474.91 44.20 o 0 14 1 55.53 69.63 4.65 o 1 14 1 1.02 2.44 1.66 o 2 14 1 1.06 3.05 3.61 o 3 14 1 451.65 431.82 14.31 o 4 14 1 72.01 75.15 4.74 o 5 14 1 156.24 144.40 7.17 o -4 15 1 107.45 95.93 7.32 o -3 15 1 49.93 54.61 4.84 o -2 15 1 264.84 258.56 12.01 o -1 15 1 25.29 31.30 2.90 o 0 15 1 86.38 87.32 4.59 o 1 15 1 1.36 5.64 2.08 o 2 15 1 401.55 396.11 17.58 o 3 15 1 54.15 54.96 5.06 o 4 15 1 7.81 9.08 2.82 o -3 16 1 58.48 62.32 5.34 o -2 16 1 92.90 92.75 6.98 o -1 16 1 65.36 58.50 3.97 o 0 16 1 31.31 33.53 3.17 o 1 16 1 4.40 11.72 6.91 o 2 16 1 72.18 67.25 5.61 o -10 0 2 1635.06 1548.03 66.63 o -8 0 2 296.94 303.45 12.60 o -6 0 2 2541.64 2606.53 59.29 o -4 0 2 103.39 40.04 19.08 o 0 0 2 4477.10 4429.34 33.02 o 2 0 2 1818.40 1939.35 82.12 o 4 0 2 2852.59 2860.20 388.53 o 6 0 2 1150.14 1209.68 26.92 o 8 0 2 239.51 240.03 12.01 o -10 1 2 2.62 5.91 2.30 o -9 1 2 165.64 173.32 6.51 o -8 1 2 11.42 13.94 1.38 o -7 1 2 206.70 185.38 4.44 o -6 1 2 85.54 76.42 6.27 o -5 1 2 3729.20 3794.25 61.29 o -4 1 2 1118.80 1109.74 16.47 o -3 1 2 72.93 47.59 1.49 o -2 1 2 5122.43 4978.29 64.37 o -1 1 2 571.79 550.45 4.32 o 0 1 2 9750.71 9556.08 89.21 o 2 1 2 1995.33 1948.17 20.93 o 3 1 2 311.05 281.34 3.51 o 4 1 2 289.89 240.23 3.55 o 5 1 2 545.50 557.77 7.66 o 6 1 2 87.05 94.21 4.54 o 7 1 2 1.87 2.94 2.02 o 8 1 2 31.86 32.55 2.63 o 9 1 2 71.13 72.70 3.99 o -10 2 2 163.89 150.69 9.67 o -9 2 2 306.59 311.64 9.99 o -8 2 2 109.58 126.32 14.04 o -7 2 2 51.30 53.60 2.63 o -6 2 2 51.87 54.06 3.48 o -5 2 2 2.49 3.91 1.38 o -4 2 2 1441.07 1373.22 16.68 o -3 2 2 1331.59 1328.25 16.30 o -2 2 2 482.84 520.68 13.84 o -1 2 2 1422.23 1356.20 36.25 o 0 2 2 764.66 778.53 6.82 o 1 2 2 6562.69 6687.81 73.88 o 2 2 2 1412.43 1428.25 13.86 o 3 2 2 2653.45 2867.44 31.79 o 4 2 2 5898.90 5786.90 82.65 o 5 2 2 478.42 426.55 22.67 o 6 2 2 27.20 31.57 1.87 o 7 2 2 431.03 410.25 9.25 o 8 2 2 169.61 181.40 14.98 o 9 2 2 38.54 35.82 3.02 o -10 3 2 8.01 10.09 2.64 o -9 3 2 238.60 251.39 39.64 o -8 3 2 41.90 48.64 4.80 o -7 3 2 2.35 5.72 1.30 o -6 3 2 25.55 30.49 1.44 o -5 3 2 372.85 406.14 13.62 o -4 3 2 50.05 49.97 3.25 o -3 3 2 761.85 856.67 9.38 o -2 3 2 15.13 6.28 0.82 o -1 3 2 8001.43 7794.11 89.80 o 0 3 2 2391.35 2422.00 29.25 o 1 3 2 4087.35 4192.76 43.65 o 2 3 2 2496.85 2615.69 29.24 o 3 3 2 1611.67 1614.45 16.06 o 4 3 2 118.47 144.50 2.85 o 5 3 2 4.43 12.42 1.03 o 6 3 2 75.54 74.48 2.44 o 7 3 2 1624.19 1596.12 34.39 o 8 3 2 48.73 51.26 3.21 o 9 3 2 226.45 247.55 37.81 o -10 4 2 5.42 3.12 2.20 o -9 4 2 114.83 129.58 19.23 o -8 4 2 571.54 586.93 13.53 o -7 4 2 260.56 267.04 6.42 o -6 4 2 1.77 6.86 0.99 o -5 4 2 630.01 657.00 8.45 o -4 4 2 2753.88 2785.98 35.14 o -3 4 2 1616.99 1790.78 20.11 o -2 4 2 133.14 125.12 1.37 o -1 4 2 273.96 333.31 3.34 o 0 4 2 5.80 6.47 0.61 o 1 4 2 2859.48 2994.99 33.01 o 2 4 2 4246.46 4152.36 48.04 o 3 4 2 111.30 134.77 1.52 o 4 4 2 316.38 367.63 6.23 o 5 4 2 1.17 3.27 1.99 o 6 4 2 1793.30 1805.70 36.29 o 7 4 2 300.58 286.47 7.36 o 8 4 2 5.82 7.87 1.49 o 9 4 2 104.61 118.78 17.39 o -9 5 2 39.54 43.37 3.22 o -8 5 2 49.60 48.53 3.19 o -7 5 2 498.42 505.61 10.81 o -6 5 2 0.04 0.76 0.73 o -5 5 2 510.46 448.28 8.57 o -4 5 2 620.95 597.57 7.06 o -3 5 2 3027.04 3209.84 37.13 o -2 5 2 1737.71 1794.17 19.60 o -1 5 2 2583.15 2502.39 28.44 o 1 5 2 3268.73 3360.89 40.31 o 2 5 2 124.04 156.66 6.05 o 3 5 2 210.34 176.89 2.92 o 4 5 2 397.18 389.50 6.65 o 5 5 2 218.03 210.38 4.62 o 6 5 2 634.24 629.99 13.24 o 7 5 2 488.24 485.73 11.43 o 8 5 2 31.88 28.66 2.71 o 9 5 2 14.66 16.76 3.01 o -9 6 2 47.58 41.51 3.39 o -8 6 2 11.60 12.45 2.00 o -7 6 2 545.60 537.42 15.21 o -6 6 2 937.88 1003.93 25.14 o -5 6 2 1028.98 1032.53 23.33 o -4 6 2 898.45 909.78 14.28 o -3 6 2 147.69 134.71 2.66 o -2 6 2 3039.50 2998.11 32.40 o -1 6 2 35.65 57.23 1.22 o 0 6 2 6864.23 7037.40 97.32 o 1 6 2 161.03 147.41 2.09 o 2 6 2 158.33 156.67 3.42 o 3 6 2 72.17 75.51 1.59 o 4 6 2 363.37 343.43 5.87 o 5 6 2 788.52 737.12 13.41 o 6 6 2 53.49 53.76 3.01 o 7 6 2 285.99 292.81 9.72 o 8 6 2 405.82 398.02 13.57 o 9 6 2 38.27 42.37 4.13 o -9 7 2 131.43 127.79 6.32 o -8 7 2 109.55 112.94 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